Changeset 1742
- Timestamp:
- Mar 19, 2015 11:41:56 AM (10 years ago)
- Location:
- Tutorials/SAseqref
- Files:
-
- 17 edited
Legend:
- Unmodified
- Added
- Removed
-
TabularUnified Tutorials/SAseqref/Sequential Refinement of Small Angle Scattering Data.htm ¶
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SemiHidden="true" UnhideWhenUsed="true" 239 Name="Salutation"/> 240 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 241 Name="Date"/> 242 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 243 Name="Body Text First Indent"/> 244 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 245 Name="Body Text First Indent 2"/> 246 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 247 Name="Note Heading"/> 248 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 249 Name="Body Text 2"/> 250 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 251 Name="Body Text 3"/> 252 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 253 Name="Body Text Indent 2"/> 254 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 255 Name="Body Text Indent 3"/> 256 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 257 Name="Block Text"/> 258 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 259 Name="Hyperlink"/> 260 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 261 Name="FollowedHyperlink"/> 262 <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/> 263 <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/> 264 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 265 Name="Document Map"/> 266 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 267 Name="Plain Text"/> 268 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 269 Name="E-mail Signature"/> 270 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 271 Name="HTML Top of Form"/> 272 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 273 Name="HTML Bottom of Form"/> 274 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 275 Name="Normal (Web)"/> 276 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 277 Name="HTML Acronym"/> 278 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 279 Name="HTML Address"/> 280 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 281 Name="HTML Cite"/> 282 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 283 Name="HTML Code"/> 284 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 285 Name="HTML Definition"/> 286 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 287 Name="HTML Keyboard"/> 288 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 289 Name="HTML Preformatted"/> 290 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 291 Name="HTML Sample"/> 292 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 293 Name="HTML Typewriter"/> 294 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 295 Name="HTML Variable"/> 296 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 297 Name="Normal Table"/> 298 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 299 Name="annotation subject"/> 300 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 301 Name="No List"/> 302 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 303 Name="Outline List 1"/> 304 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 305 Name="Outline List 2"/> 306 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 307 Name="Outline List 3"/> 308 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 309 Name="Table Simple 1"/> 310 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 311 Name="Table Simple 2"/> 312 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 313 Name="Table Simple 3"/> 314 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 315 Name="Table Classic 1"/> 316 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 317 Name="Table Classic 2"/> 318 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 319 Name="Table Classic 3"/> 320 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 321 Name="Table Classic 4"/> 322 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 323 Name="Table Colorful 1"/> 324 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 325 Name="Table Colorful 2"/> 326 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 327 Name="Table Colorful 3"/> 328 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 329 Name="Table Columns 1"/> 330 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 331 Name="Table Columns 2"/> 332 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 333 Name="Table Columns 3"/> 334 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 335 Name="Table Columns 4"/> 336 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 337 Name="Table Columns 5"/> 338 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 339 Name="Table Grid 1"/> 340 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 341 Name="Table Grid 2"/> 342 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 343 Name="Table Grid 3"/> 344 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 345 Name="Table Grid 4"/> 346 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 347 Name="Table Grid 5"/> 348 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 349 Name="Table Grid 6"/> 350 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 351 Name="Table Grid 7"/> 352 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 353 Name="Table Grid 8"/> 354 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 355 Name="Table List 1"/> 356 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 357 Name="Table List 2"/> 358 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 359 Name="Table List 3"/> 360 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 361 Name="Table List 4"/> 362 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 363 Name="Table List 5"/> 364 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 365 Name="Table List 6"/> 366 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 367 Name="Table List 7"/> 368 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 369 Name="Table List 8"/> 370 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 371 Name="Table 3D effects 1"/> 372 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 373 Name="Table 3D effects 2"/> 374 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 375 Name="Table 3D effects 3"/> 376 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 377 Name="Table Contemporary"/> 378 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 379 Name="Table Elegant"/> 380 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 381 Name="Table Professional"/> 382 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 383 Name="Table Subtle 1"/> 384 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 385 Name="Table Subtle 2"/> 386 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 387 Name="Table Web 1"/> 388 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 389 Name="Table Web 2"/> 390 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 391 Name="Table Web 3"/> 392 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 393 Name="Balloon Text"/> 394 <w:LsdException Locked="false" Priority="59" Name="Table Grid"/> 395 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 396 Name="Table Theme"/> 397 <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/> 398 <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/> 399 <w:LsdException Locked="false" Priority="60" Name="Light Shading"/> 400 <w:LsdException Locked="false" Priority="61" Name="Light List"/> 401 <w:LsdException Locked="false" Priority="62" Name="Light Grid"/> 402 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/> 403 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/> 404 <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/> 405 <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/> 406 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/> 407 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/> 408 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/> 409 <w:LsdException Locked="false" Priority="70" Name="Dark List"/> 410 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/> 411 <w:LsdException Locked="false" Priority="72" Name="Colorful List"/> 412 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/> 413 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/> 414 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/> 415 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/> 416 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/> 417 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/> 418 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/> 419 <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/> 420 <w:LsdException Locked="false" Priority="34" QFormat="true" 421 Name="List Paragraph"/> 422 <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/> 423 <w:LsdException Locked="false" Priority="30" QFormat="true" 424 Name="Intense Quote"/> 425 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/> 426 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/> 427 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/> 428 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/> 429 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/> 430 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/> 431 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/> 432 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/> 433 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/> 434 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/> 435 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/> 436 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/> 437 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/> 438 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/> 439 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/> 440 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/> 441 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/> 442 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/> 443 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/> 444 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/> 445 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/> 446 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/> 447 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/> 448 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/> 449 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/> 450 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/> 451 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/> 452 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/> 453 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/> 454 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/> 455 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/> 456 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/> 457 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/> 458 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/> 459 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/> 460 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/> 461 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/> 462 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/> 463 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/> 464 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/> 465 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/> 466 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/> 467 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/> 468 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/> 469 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/> 470 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/> 471 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/> 472 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/> 473 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/> 474 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/> 475 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/> 476 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/> 477 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/> 478 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/> 479 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/> 480 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/> 481 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/> 482 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/> 483 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/> 484 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/> 485 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/> 486 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/> 487 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/> 488 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/> 489 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/> 490 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/> 491 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/> 492 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/> 493 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/> 494 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/> 495 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/> 496 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/> 497 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/> 498 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/> 499 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/> 500 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/> 501 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/> 502 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/> 503 <w:LsdException Locked="false" Priority="19" QFormat="true" 504 Name="Subtle Emphasis"/> 505 <w:LsdException Locked="false" Priority="21" QFormat="true" 506 Name="Intense Emphasis"/> 507 <w:LsdException Locked="false" Priority="31" QFormat="true" 508 Name="Subtle Reference"/> 509 <w:LsdException Locked="false" Priority="32" QFormat="true" 510 Name="Intense Reference"/> 511 <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/> 512 <w:LsdException Locked="false" Priority="37" SemiHidden="true" 513 UnhideWhenUsed="true" Name="Bibliography"/> 514 <w:LsdException Locked="false" Priority="39" SemiHidden="true" 515 UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/> 516 <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/> 517 <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/> 518 <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/> 519 <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/> 520 <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/> 521 <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/> 522 <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/> 523 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/> 524 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/> 525 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/> 526 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/> 527 <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/> 528 <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/> 529 <w:LsdException Locked="false" Priority="46" 530 Name="Grid Table 1 Light Accent 1"/> 531 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/> 532 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/> 533 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/> 534 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/> 535 <w:LsdException Locked="false" Priority="51" 536 Name="Grid Table 6 Colorful Accent 1"/> 537 <w:LsdException Locked="false" Priority="52" 538 Name="Grid Table 7 Colorful Accent 1"/> 539 <w:LsdException Locked="false" Priority="46" 540 Name="Grid Table 1 Light Accent 2"/> 541 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/> 542 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/> 543 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/> 544 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/> 545 <w:LsdException Locked="false" Priority="51" 546 Name="Grid Table 6 Colorful Accent 2"/> 547 <w:LsdException Locked="false" Priority="52" 548 Name="Grid Table 7 Colorful Accent 2"/> 549 <w:LsdException Locked="false" Priority="46" 550 Name="Grid Table 1 Light Accent 3"/> 551 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/> 552 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/> 553 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/> 554 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/> 555 <w:LsdException Locked="false" Priority="51" 556 Name="Grid Table 6 Colorful Accent 3"/> 557 <w:LsdException Locked="false" Priority="52" 558 Name="Grid Table 7 Colorful Accent 3"/> 559 <w:LsdException Locked="false" Priority="46" 560 Name="Grid Table 1 Light Accent 4"/> 561 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/> 562 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/> 563 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/> 564 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/> 565 <w:LsdException Locked="false" Priority="51" 566 Name="Grid Table 6 Colorful Accent 4"/> 567 <w:LsdException Locked="false" Priority="52" 568 Name="Grid Table 7 Colorful Accent 4"/> 569 <w:LsdException Locked="false" Priority="46" 570 Name="Grid Table 1 Light Accent 5"/> 571 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/> 572 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/> 573 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/> 574 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/> 575 <w:LsdException Locked="false" Priority="51" 576 Name="Grid Table 6 Colorful Accent 5"/> 577 <w:LsdException Locked="false" Priority="52" 578 Name="Grid Table 7 Colorful Accent 5"/> 579 <w:LsdException Locked="false" Priority="46" 580 Name="Grid Table 1 Light Accent 6"/> 581 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/> 582 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/> 583 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/> 584 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/> 585 <w:LsdException Locked="false" Priority="51" 586 Name="Grid Table 6 Colorful Accent 6"/> 587 <w:LsdException Locked="false" Priority="52" 588 Name="Grid Table 7 Colorful Accent 6"/> 589 <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/> 590 <w:LsdException Locked="false" Priority="47" Name="List Table 2"/> 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1020 mso-ascii-font-family:"Times New Roman"; 702 1021 mso-fareast-font-family:"Times New Roman"; … … 727 1046 mso-ansi-font-size:8.0pt; 728 1047 mso-bidi-font-size:8.0pt; 729 font-family:"Tahoma", "sans-serif";1048 font-family:"Tahoma",sans-serif; 730 1049 mso-ascii-font-family:Tahoma; 731 1050 mso-fareast-font-family:"Times New Roman"; … … 742 1061 mso-ansi-font-size:8.0pt; 743 1062 mso-bidi-font-size:8.0pt; 744 font-family:"Tahoma", "sans-serif";1063 font-family:"Tahoma",sans-serif; 745 1064 mso-ascii-font-family:Tahoma; 746 1065 mso-fareast-font-family:"Times New Roman"; … … 760 1079 mso-ansi-font-size:10.0pt; 761 1080 mso-bidi-font-size:10.0pt; 762 font-family:"Calibri", "sans-serif";1081 font-family:"Calibri",sans-serif; 763 1082 mso-ascii-font-family:Calibri; 764 1083 mso-ascii-theme-font:minor-latin; … … 845 1164 mso-pagination:widow-orphan; 846 1165 font-size:10.0pt; 847 font-family:"Calibri", "sans-serif";1166 font-family:"Calibri",sans-serif; 848 1167 mso-ascii-font-family:Calibri; 849 1168 mso-ascii-theme-font:minor-latin; … … 865 1184 mso-pagination:widow-orphan; 866 1185 font-size:10.0pt; 867 font-family:"Calibri", "sans-serif";1186 font-family:"Calibri",sans-serif; 868 1187 mso-ascii-font-family:Calibri; 869 1188 mso-ascii-theme-font:minor-latin; … … 894 1213 minor-latin;mso-bidi-font-weight:bold;mso-bidi-font-style:italic'><o:p></o:p></span></p> 895 1214 896 <p class=MsoNormal>If you have not done so already, <a 897 href="Starting%20GSAS.htm">start GSAS-II</a>.</p> 1215 <p class=MsoNormal>If you have not done so already, start GSAS-II.</p> 898 1216 899 1217 <h2>Step 1: read in the data files</h2> … … 902 1220 style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span 903 1221 style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Use 904 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1222 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 905 1223 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 906 Calibri;mso-bidi-theme-font:minor-latin'>Import/Small Angle Data/from a q step 907 QIE data file</span></b> menu item to read the data files into GSAS-II. This 908 read option is set to read three column small angle scattering data (SASD) as Q 909 in Å<sup>-1</sup>, intensity and estimated standard deviation in intensity; 910 there may be a header with metadata information in the front of this file.<span 911 style='mso-spacerun:yes'> </span>It will read multiple files from a single 912 directory. Change the file directory to <b style='mso-bidi-font-weight:normal'><span 913 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1224 Calibri;mso-bidi-theme-font:minor-latin'>Import/Small Angle Data/from q (A-1) 1225 step X-ray QIE data file</span></b> menu item to read the data files into 1226 GSAS-II. This read option is set to read three column small angle scattering 1227 data (SASD) as Q in Å<sup>-1</sup>, intensity and estimated standard deviation 1228 in intensity; there may be a header with metadata information in the front of 1229 this file.<span style='mso-spacerun:yes'> </span>It will read multiple files 1230 from a single directory. Change the file directory to <b style='mso-bidi-font-weight: 1231 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1232 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 1233 mso-bidi-theme-font:minor-latin'>exercises/<span class=SpellE>SAseqref</span></span></b><span 1234 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 914 1235 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 915 minor-latin'>Exercises/Small angle</span></b><span style='font-family:"Calibri","sans-serif"; 916 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 917 Calibri;mso-bidi-theme-font:minor-latin'> to find the files.</span></p> 1236 minor-latin'> to find the files.</span></p> 918 1237 919 1238 <p class=MsoListParagraphCxSpMiddle style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span 920 1239 style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span 921 1240 style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Select 922 the six<span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 923 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 924 mso-bidi-theme-font:minor-latin'> data</span> files with <span class=SpellE><b 925 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 926 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ludox</span></b></span> 927 in their name in the first dialog and press <b style='mso-bidi-font-weight: 928 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 929 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 930 mso-bidi-theme-font:minor-latin'>Open</span></b>. All six will immediately be 931 read into GSAS-II; you will have to select the <b style='mso-bidi-font-weight: 932 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 933 minor-latin;mso-hansi-theme-font:minor-latin'>any file (*.*)</span></b> filter 934 to see them.</p> 1241 the six<span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1242 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 1243 minor-latin'> data</span> files with <span class=SpellE><b style='mso-bidi-font-weight: 1244 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1245 minor-latin;mso-hansi-theme-font:minor-latin'>Ludox</span></b></span> in their 1246 name in the first dialog and press <b style='mso-bidi-font-weight:normal'><span 1247 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1248 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 1249 minor-latin'>Open</span></b>. All six will immediately be read into GSAS-II; 1250 you will have to select the <b style='mso-bidi-font-weight:normal'><span 1251 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1252 mso-hansi-theme-font:minor-latin'>any file (*.*)</span></b> filter to see them.</p> 935 1253 936 1254 <p class=MsoListParagraphCxSpLast><o:p> </o:p></p> 937 1255 938 1256 <p class=MsoNormal>At this point the <b style='mso-bidi-font-weight:normal'><span 939 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1257 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 940 1258 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 941 1259 minor-latin'>GSAS-II data tree</span></b> window will have several entries and 942 the plot window will show the SASD pattern for all six as a log-log plot of intensity 943 vs. Q; one shows error bars (<b style='mso-bidi-font-weight:normal'><span 944 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1260 the plot window will show the SASD pattern for one as a log-log plot of 1261 intensity vs. Q; enter <b style='mso-bidi-font-weight:normal'><span 1262 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1263 mso-hansi-theme-font:minor-latin'>m</span></b> on the plot. Now all are shown; 1264 one shows error bars (<b style='mso-bidi-font-weight:normal'><span 1265 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 945 1266 mso-hansi-theme-font:minor-latin'>SASD S49_Ludox6_1pct.dat</span></b>) as it is 946 1267 the selected tree entry and the others as lines.</p> … … 966 1287 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> 967 1288 <o:lock v:ext="edit" aspectratio="t"/> 968 </v:shapetype><v:shape id="Picture_x0020_ 25" o:spid="_x0000_i1056" type="#_x0000_t75"1289 </v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1056" type="#_x0000_t75" 969 1290 style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'> 970 1291 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image001.png" 971 1292 o:title=""/> 972 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001293 </v:shape><![endif]--><![if !vml]><img width=700 height=600 973 1294 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image001.png" 974 v:shapes="Picture_x0020_ 25"><![endif]></span></p>1295 v:shapes="Picture_x0020_1"><![endif]></span></p> 975 1296 976 1297 <h2><a name="_Ref386704789">Step 2: Set Limits</a></h2> … … 979 1300 low-Q (<10<sup>-3</sup>) part of the patterns which do not seem to follow 980 1301 the sequence evident in the 10<sup>-2</sup> 10<sup>-1</sup> part. Select <b 981 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1302 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 982 1303 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Limits</span></b> 983 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";984 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina985 data.dat</span></b> from the GSAS-II tree. Set the lower limit using the cursor 986 on the plot by picking a point somewhere in the flat region at Q~3x10<sup>-3</sup> 987 with the left or right mouse button. The limits window should look something 988 like</p>1304 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1305 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD 1306 S35_Ludox_40pct.dat</span></b> from the GSAS-II tree. Set the lower limit using 1307 the cursor on the plot by picking a point somewhere in the flat region at 1308 Q~3x10<sup>-3</sup> with the left mouse button. The limits window should look 1309 something like</p> 989 1310 990 1311 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 993 1314 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image002.png" 994 1315 o:title=""/> 995 </v:shape><![endif]--><![if !vml]><img border=0width=300 height=2601316 </v:shape><![endif]--><![if !vml]><img width=300 height=260 996 1317 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image002.png" 997 1318 v:shapes="Picture_x0020_26"><![endif]></span><span … … 1001 1322 1002 1323 <p class=MsoNormal>To copy these limits to the other data sets use the <b 1003 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1324 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1004 1325 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Copy</span></b> 1005 1326 command from the data window menu; a popup window will give the selection of … … 1010 1331 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image003.png" 1011 1332 o:title=""/> 1012 </v:shape><![endif]--><![if !vml]><img border=0width=320 height=3101333 </v:shape><![endif]--><![if !vml]><img width=320 height=310 1013 1334 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image003.png" 1014 1335 v:shapes="Picture_x0020_27"><![endif]></span></p> … … 1017 1338 1018 1339 <p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span 1019 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1340 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1020 1341 mso-hansi-theme-font:minor-latin'>Set All</span></b> (all boxes will be 1021 1342 checked) and then press <b style='mso-bidi-font-weight:normal'><span 1022 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1343 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1023 1344 mso-hansi-theme-font:minor-latin'>Enter</span></b> to do the copy.</p> 1024 1345 … … 1029 1350 case one is silica and the other is water. Parameters for a number of 1030 1351 substances are defined in the file </span><b style='mso-bidi-font-weight:normal'><span 1031 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1352 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1032 1353 mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span 1033 1354 style='mso-no-proof:yes'>. You can add your own substances to this or better 1034 1355 put them in </span><b style='mso-bidi-font-weight:normal'><span 1035 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1356 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1036 1357 mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span 1037 1358 style='mso-no-proof:yes'>; this is read after Substances.py when you load 1038 1359 substances for your selection. </span>Select <b style='mso-bidi-font-weight: 1039 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1360 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1040 1361 minor-latin;mso-hansi-theme-font:minor-latin'>Substances</span></b> from the 1041 1362 GSAS-II tree. Then do <b style='mso-bidi-font-weight:normal'><span 1042 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1363 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1043 1364 mso-hansi-theme-font:minor-latin'>Edit/Load</span></b> substance from the menu; 1044 1365 a popup window will appear with possible selections</p> … … 1049 1370 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image004.png" 1050 1371 o:title=""/> 1051 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=3361372 </v:shape><![endif]--><![if !vml]><img width=346 height=336 1052 1373 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image004.png" 1053 1374 v:shapes="Picture_x0020_3"><![endif]><o:p></o:p></span></p> … … 1057 1378 <p class=MsoNormal>Notice that silica is not one of the choices; we will add it 1058 1379 in a moment. Select <b style='mso-bidi-font-weight:normal'><span 1059 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1380 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1060 1381 mso-hansi-theme-font:minor-latin'>Water</span></b> and press <b 1061 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1382 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1062 1383 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>; 1063 1384 the relevant data for water (and vacuum) are displayed next</p> … … 1068 1389 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image005.png" 1069 1390 o:title=""/> 1070 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=2601391 </v:shape><![endif]--><![if !vml]><img width=346 height=260 1071 1392 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image005.png" 1072 1393 v:shapes="Picture_x0020_28"><![endif]></span><span … … 1080 1401 each substance. These can each be edited; the other values will change 1081 1402 accordingly. Since silica wasnt in the list of known substances, do <b 1082 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1403 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1083 1404 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Add 1084 1405 substance</span></b> to create it; you will be asked for a name enter <b 1085 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1406 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1086 1407 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>silica</span></b> 1087 1408 and then a periodic table of the elements will be shown. Select <b 1088 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1409 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1089 1410 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Si</span></b> 1090 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1411 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1091 1412 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>O</span></b></p> 1092 1413 … … 1096 1417 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image006.png" 1097 1418 o:title=""/> 1098 </v:shape><![endif]--><![if !vml]><img border=0width=580 height=3601419 </v:shape><![endif]--><![if !vml]><img width=580 height=360 1099 1420 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image006.png" 1100 1421 v:shapes="Picture_x0020_29"><![endif]></span><span … … 1104 1425 1105 1426 <p class=MsoNormal>They appear in red. Press <b style='mso-bidi-font-weight: 1106 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1427 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1107 1428 minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b> and silica will be 1108 1429 added to your substance list</p> … … 1113 1434 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image007.png" 1114 1435 o:title=""/> 1115 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=3771436 </v:shape><![endif]--><![if !vml]><img width=346 height=377 1116 1437 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image007.png" 1117 1438 v:shapes="Picture_x0020_30"><![endif]></span></p> … … 1120 1441 1121 1442 <p class=MsoNormal>Change the O-atom entry to <b style='mso-bidi-font-weight: 1122 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1443 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1123 1444 minor-latin;mso-hansi-theme-font:minor-latin'>2.0</span></b> and the density to 1124 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1445 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1125 1446 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>2.65</span></b>; 1126 1447 the window will change each time giving new values and should finally show</p> … … 1131 1452 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image008.png" 1132 1453 o:title=""/> 1133 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=3771454 </v:shape><![endif]--><![if !vml]><img width=346 height=377 1134 1455 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image008.png" 1135 1456 v:shapes="Picture_x0020_8"><![endif]></span><span … … 1139 1460 affected by resonant scattering for the listed wavelength is displayed (the 1140 1461 wavelength can be changed in the <b style='mso-bidi-font-weight:normal'><span 1141 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1462 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1142 1463 mso-hansi-theme-font:minor-latin'>Instrument Parameters</span></b> GSAS-II tree 1143 1464 item if needed). The resonant scattering value is used for contrast … … 1146 1467 <p class=MsoNormal>Just as for Limits, this information needs to be copied to 1147 1468 the other SASD entries in the GSAS-II tree. Do <b style='mso-bidi-font-weight: 1148 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1469 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1149 1470 minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Copy substances</span></b> 1150 1471 from the data window menu and follow the same selection procedure as you used … … 1157 1478 their preparation, it would be useful to have this information available to 1158 1479 GSAS-II for subsequent analysis. Select Sample parameters from the data tree. 1159 I sshows (for </span><b style='mso-bidi-font-weight:normal'><span1160 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1161 mso-hansi-theme-font:minor-latin'>SASD <span class=GramE>S49_Ludox6_1pct.dat</span>)<o:p></o:p></span></b></p>1480 It shows (for </span><b style='mso-bidi-font-weight:normal'><span 1481 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1482 mso-hansi-theme-font:minor-latin'>SASD S49_Ludox6_1pct.dat)<o:p></o:p></span></b></p> 1162 1483 1163 1484 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1166 1487 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image009.png" 1167 1488 o:title=""/> 1168 </v:shape><![endif]--><![if !vml]><img border=0width=389 height=5181489 </v:shape><![endif]--><![if !vml]><img width=389 height=518 1169 1490 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image009.png" 1170 1491 v:shapes="Picture_x0020_9"><![endif]><o:p></o:p></span></p> … … 1174 1495 <p class=MsoNormal><span style='mso-no-proof:yes'>NB: we will not be needing to 1175 1496 select the </span><b style='mso-bidi-font-weight:normal'><span 1176 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1497 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1177 1498 mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Material</span></b><span 1178 1499 style='mso-no-proof:yes'> for this analysis; material selection is only 1179 1500 required for </span><b style='mso-bidi-font-weight:normal'><span 1180 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1501 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1181 1502 mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Size distribution</span></b><span 1182 1503 style='mso-no-proof:yes'> analysis. Notice that the last three column names can 1183 1504 be changed; pick the first one and change it to </span><b style='mso-bidi-font-weight: 1184 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1505 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1185 1506 minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>fraction</span></b><span 1186 1507 style='mso-no-proof:yes'>. Then enter </span><b style='mso-bidi-font-weight: 1187 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1508 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1188 1509 minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>0.01</span></b><span 1189 1510 style='mso-no-proof:yes'> which corresponds to the </span><b style='mso-bidi-font-weight: 1190 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1511 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1191 1512 minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>1pct</span></b><span 1192 1513 style='mso-no-proof:yes'> in the file name. The data window should look like<o:p></o:p></span></p> … … 1197 1518 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image010.png" 1198 1519 o:title=""/> 1199 </v:shape><![endif]--><![if !vml]><img border=0width=389 height=5181520 </v:shape><![endif]--><![if !vml]><img width=389 height=518 1200 1521 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image010.png" 1201 1522 v:shapes="Picture_x0020_10"><![endif]><o:p></o:p></span></p> … … 1204 1525 1205 1526 <p class=MsoNormal><span style='mso-no-proof:yes'>Now do the same for the </span><b 1206 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1527 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1207 1528 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof: 1208 1529 yes'>Sample Parameters</span></b><span style='mso-no-proof:yes'> for the other 1209 1530 data sets putting in the correct fraction from the respective file names. If 1210 1531 you first </span><b style='mso-bidi-font-weight:normal'><span style='font-family: 1211 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1532 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1212 1533 minor-latin;mso-no-proof:yes'>Copy</span></b><span style='mso-no-proof:yes'> 1213 1534 this one to the others, that will save you the step of changing the names. You 1214 1535 will end up on the </span><b style='mso-bidi-font-weight:normal'><span 1215 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1536 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1216 1537 mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Sample parameters</span></b><span 1217 1538 style='mso-no-proof:yes'> page for </span><b style='mso-bidi-font-weight:normal'><span 1218 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1539 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1219 1540 mso-hansi-theme-font:minor-latin'>SASD S53_Ludox6_40pct.dat </span></b>GSAS-II 1220 1541 data tree.</p> … … 1225 1546 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image011.png" 1226 1547 o:title=""/> 1227 </v:shape><![endif]--><![if !vml]><img border=0width=389 height=5181548 </v:shape><![endif]--><![if !vml]><img width=389 height=518 1228 1549 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image011.png" 1229 1550 v:shapes="Picture_x0020_11"><![endif]></span><span … … 1232 1553 <h2>Step 5: Set Model parameters </h2> 1233 1554 1234 <p class=MsoNormal>Looking at the data plot ( <span class=GramE>key <b1235 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1236 m so-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>s</span></b></span>1237 to select a single data set) for <b style='mso-bidi-font-weight:normal'><span 1238 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1239 m so-hansi-theme-font:minor-latin'>SASD S53_Ludox6_40pct.dat</span></b>, one1240 sees just one feature with oscillations at higher Q. This is the signal for a 1241 non-dilute <spanclass=SpellE>scatterer</span>. </p>1242 1243 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1244 id="Picture_x0020_ 21" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:525pt;1555 <p class=MsoNormal>Looking at the data plot (key <b style='mso-bidi-font-weight: 1556 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1557 minor-latin;mso-hansi-theme-font:minor-latin'>m</span></b> to select a single 1558 data set) for <b style='mso-bidi-font-weight:normal'><span style='font-family: 1559 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1560 minor-latin'>SASD S53_Ludox6_40pct.dat</span></b>, one sees just one feature 1561 with oscillations at higher Q. This is the signal for a non-dilute <span 1562 class=SpellE>scatterer</span>. </p> 1563 1564 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1565 id="Picture_x0020_12" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:525pt; 1245 1566 height:450pt;visibility:visible;mso-wrap-style:square'> 1246 1567 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image012.png" 1247 1568 o:title=""/> 1248 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001569 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1249 1570 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image012.png" 1250 v:shapes="Picture_x0020_21"><![endif]></span></p> 1251 1252 <p class=MsoNormal><o:p> </o:p></p> 1253 1254 <p class=MsoNormal>In the data window switch <b style='mso-bidi-font-weight: 1255 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1256 minor-latin;mso-hansi-theme-font:minor-latin'>Size dist.</span></b> to <b 1257 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1258 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Particle fit</span></b>, 1259 and add a reasonable value (<b style='mso-bidi-font-weight:normal'><span 1260 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1571 v:shapes="Picture_x0020_12"><![endif]></span></p> 1572 1573 <p class=MsoNormal><o:p> </o:p></p> 1574 1575 <p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span 1576 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1577 mso-hansi-theme-font:minor-latin'>Models</span></b> from the GSASII data tree 1578 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1579 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD 1580 S35_Ludox1_40pct.dat</span></b>, switch <b style='mso-bidi-font-weight:normal'><span 1581 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1582 mso-hansi-theme-font:minor-latin'>Size dist.</span></b> to <b style='mso-bidi-font-weight: 1583 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1584 minor-latin;mso-hansi-theme-font:minor-latin'>Particle fit</span></b>, and add 1585 a reasonable value (<b style='mso-bidi-font-weight:normal'><span 1586 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1261 1587 mso-hansi-theme-font:minor-latin'>0.25</span></b>) for the <b style='mso-bidi-font-weight: 1262 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1588 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1263 1589 minor-latin;mso-hansi-theme-font:minor-latin'>Background</span></b>; a 1264 1590 horizontal red line will appear. Next do <b style='mso-bidi-font-weight:normal'><span 1265 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1266 mso-hansi-theme-font:minor-latin'>Models/Add</span></b>; the window will display1267 a default component; change the <b style='mso-bidi-font-weight:normal'><span1268 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1591 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1592 mso-hansi-theme-font:minor-latin'>Models/Add</span></b>; the window will 1593 display a default component; change the <b style='mso-bidi-font-weight:normal'><span 1594 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1269 1595 mso-hansi-theme-font:minor-latin'>Material</span></b> to <b style='mso-bidi-font-weight: 1270 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1596 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1271 1597 minor-latin;mso-hansi-theme-font:minor-latin'>silica</span></b>. Also change 1272 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1598 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1273 1599 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Matrix</span></b> 1274 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1600 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1275 1601 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Water</span></b>; 1276 1602 the calculated contrast should be 175.60 10<sup>20</sup>cm<sup>-4</sup>. The … … 1278 1604 1279 1605 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1280 id=" Picture_x0020_37" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:525pt;1281 height:450pt;visibility:visible;mso-wrap-style:square'>1606 id="_x0000_i1044" type="#_x0000_t75" style='width:525pt;height:450pt; 1607 visibility:visible;mso-wrap-style:square'> 1282 1608 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image013.png" 1283 1609 o:title=""/> 1284 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001610 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1285 1611 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image013.png" 1286 v:shapes=" Picture_x0020_37"><![endif]></span></p>1612 v:shapes="_x0000_i1044"><![endif]></span></p> 1287 1613 1288 1614 <p class=MsoNormal><span style='mso-no-proof:yes'><o:p> </o:p></span></p> 1289 1615 1290 1616 <p class=MsoNormal>The default <span class=SpellE><b style='mso-bidi-font-weight: 1291 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1617 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1292 1618 minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1293 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1619 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1294 1620 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b> 1295 of <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1621 of <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1296 1622 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1e+03</span></b> 1297 1623 is too large, try something smaller and increase the <span class=SpellE><b 1298 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1624 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1299 1625 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1300 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1626 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1301 1627 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b> 1302 1628 (the sliders work well for this). Since this is a non-dilute system, change the 1303 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1629 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1304 1630 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Structure 1305 1631 factor</span></b> to <span class=GramE><b style='mso-bidi-font-weight:normal'><span 1306 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1632 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1307 1633 mso-hansi-theme-font:minor-latin'>Hard</span></b></span><b style='mso-bidi-font-weight: 1308 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1634 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1309 1635 minor-latin;mso-hansi-theme-font:minor-latin'> sphere</span></b> and set the <b 1310 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1636 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1311 1637 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SF <span 1312 1638 class=SpellE>VolFr</span></span></b> to <b style='mso-bidi-font-weight:normal'><span 1313 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1639 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1314 1640 mso-hansi-theme-font:minor-latin'>0.4</span></b>. Your data window should look 1315 1641 something like</p> 1316 1642 1317 1643 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1318 id=" Picture_x0020_38" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:384.75pt;1319 height:358.5pt;visibility:visible;mso-wrap-style:square'>1644 id="_x0000_i1043" type="#_x0000_t75" style='width:384.75pt;height:358.5pt; 1645 visibility:visible;mso-wrap-style:square'> 1320 1646 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image014.png" 1321 1647 o:title=""/> 1322 </v:shape><![endif]--><![if !vml]><img border=0width=513 height=4781648 </v:shape><![endif]--><![if !vml]><img width=513 height=478 1323 1649 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image014.png" 1324 v:shapes=" Picture_x0020_38"><![endif]></span></p>1650 v:shapes="_x0000_i1043"><![endif]></span></p> 1325 1651 1326 1652 <p class=MsoNormal><o:p> </o:p></p> … … 1329 1655 1330 1656 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1331 id="Picture_x0020_3 9" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:525pt;1657 id="Picture_x0020_34" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:525pt; 1332 1658 height:450pt;visibility:visible;mso-wrap-style:square'> 1333 1659 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image015.png" 1334 1660 o:title=""/> 1335 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001661 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1336 1662 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image015.png" 1337 v:shapes="Picture_x0020_3 9"><![endif]></span><br clear=all style='mso-special-character:1663 v:shapes="Picture_x0020_34"><![endif]></span><br clear=all style='mso-special-character: 1338 1664 line-break'> 1339 1665 </p> … … 1341 1667 <p class=MsoNormal>The calculated curve shows oscillations but they are not in 1342 1668 the right place and are too broad. Try the <span class=SpellE><b 1343 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1669 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1344 1670 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1345 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1671 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1346 1672 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> <span 1347 1673 class=SpellE>StdDev</span></span></b> slider and make it smaller; somewhere 1348 about <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1674 about <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1349 1675 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.132</span></b> 1350 1676 gives a curve with the right shape but too high. Reduce the <span class=SpellE><b 1351 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1677 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1352 1678 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1353 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1679 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1354 1680 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b> 1355 1681 to improve the match. Shift the <b style='mso-bidi-font-weight:normal'><span 1356 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1682 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1357 1683 mso-hansi-theme-font:minor-latin'>SF <span class=SpellE>Dist</span></span></b> 1358 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1684 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1359 1685 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SF <span 1360 1686 class=SpellE>VolFr</span></span></b> as well to get the curves to match. … … 1363 1689 1364 1690 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1365 id="Picture_x0020_ 40" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:384.75pt;1691 id="Picture_x0020_36" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:384.75pt; 1366 1692 height:358.5pt;visibility:visible;mso-wrap-style:square'> 1367 1693 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image016.png" 1368 1694 o:title=""/> 1369 </v:shape><![endif]--><![if !vml]><img border=0width=513 height=4781695 </v:shape><![endif]--><![if !vml]><img width=513 height=478 1370 1696 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image016.png" 1371 v:shapes="Picture_x0020_ 40"><![endif]></span></p>1697 v:shapes="Picture_x0020_36"><![endif]></span></p> 1372 1698 1373 1699 <p class=MsoNormal><o:p> </o:p></p> … … 1376 1702 1377 1703 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1378 id="Picture_x0020_ 41" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:525pt;1704 id="Picture_x0020_37" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:525pt; 1379 1705 height:450pt;visibility:visible;mso-wrap-style:square'> 1380 1706 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image017.png" 1381 1707 o:title=""/> 1382 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001708 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1383 1709 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image017.png" 1384 v:shapes="Picture_x0020_ 41"><![endif]></span></p>1710 v:shapes="Picture_x0020_37"><![endif]></span></p> 1385 1711 1386 1712 <h2>Step 6: Initial refinement</h2> 1387 1713 1388 1714 <p class=MsoNormal>We can be brave and set all six <b style='mso-bidi-font-weight: 1389 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1715 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1390 1716 minor-latin;mso-hansi-theme-font:minor-latin'>Refine?</span></b> <span 1391 1717 class=GramE>boxes</span> (NB: the one for <b style='mso-bidi-font-weight:normal'><span 1392 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1718 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1393 1719 mso-hansi-theme-font:minor-latin'>Matrix Volume fraction</span></b> currently 1394 1720 does not operate ignore it). Then do <b style='mso-bidi-font-weight:normal'><span 1395 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1721 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1396 1722 mso-hansi-theme-font:minor-latin'>Models/Fit</span></b>; the least squares very 1397 1723 quickly minimizes to give</p> 1398 1724 1399 1725 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1400 id="Picture_x0020_ 42" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:384.75pt;1726 id="Picture_x0020_38" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:384.75pt; 1401 1727 height:358.5pt;visibility:visible;mso-wrap-style:square'> 1402 1728 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image018.png" 1403 1729 o:title=""/> 1404 </v:shape><![endif]--><![if !vml]><img border=0width=513 height=4781730 </v:shape><![endif]--><![if !vml]><img width=513 height=478 1405 1731 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image018.png" 1406 v:shapes="Picture_x0020_ 42"><![endif]></span></p>1732 v:shapes="Picture_x0020_38"><![endif]></span></p> 1407 1733 1408 1734 <p class=MsoNormal><o:p> </o:p></p> … … 1411 1737 1412 1738 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1413 id="Picture_x0020_ 43" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:549.75pt;1739 id="Picture_x0020_39" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:609.75pt; 1414 1740 height:152.25pt;visibility:visible;mso-wrap-style:square'> 1415 1741 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image019.png" 1416 1742 o:title=""/> 1417 </v:shape><![endif]--><![if !vml]><img border=0 width=733 height=2031743 </v:shape><![endif]--><![if !vml]><img width=813 height=203 1418 1744 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image019.png" 1419 v:shapes="Picture_x0020_ 43"><![endif]></span></p>1745 v:shapes="Picture_x0020_39"><![endif]></span></p> 1420 1746 1421 1747 <p class=MsoNormal><o:p> </o:p></p> … … 1424 1750 1425 1751 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1426 id="Picture_x0020_4 4" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:525pt;1752 id="Picture_x0020_40" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:525pt; 1427 1753 height:450pt;visibility:visible;mso-wrap-style:square'> 1428 1754 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image020.png" 1429 1755 o:title=""/> 1430 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001756 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1431 1757 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image020.png" 1432 v:shapes="Picture_x0020_4 4"><![endif]></span></p>1758 v:shapes="Picture_x0020_40"><![endif]></span></p> 1433 1759 1434 1760 <p class=MsoNormal><o:p> </o:p></p> … … 1441 1767 1442 1768 <p class=MsoNormal>We are now ready to try a sequential refinement starting 1443 with this fit for the 1<sup>st</sup> data set. <span class=GramE>Do</span> <b1444 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1445 m so-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Sequential1446 fit</span></b>;a dialog box will appear for selection of the data sets.</p>1447 1448 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1449 id=" _x0000_i1036" type="#_x0000_t75" style='width:240pt;height:232.5pt;1450 visibility:visible;mso-wrap-style:square'>1769 with this fit for the 1<sup>st</sup> data set. Do <b style='mso-bidi-font-weight: 1770 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1771 minor-latin;mso-hansi-theme-font:minor-latin'>Models/Sequential fit</span></b>; 1772 a dialog box will appear for selection of the data sets.</p> 1773 1774 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1775 id="Picture_x0020_21" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:240pt; 1776 height:232.5pt;visibility:visible;mso-wrap-style:square'> 1451 1777 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image021.png" 1452 1778 o:title=""/> 1453 </v:shape><![endif]--><![if !vml]><img border=0width=320 height=3101779 </v:shape><![endif]--><![if !vml]><img width=320 height=310 1454 1780 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image021.png" 1455 v:shapes=" _x0000_i1036"><![endif]></span></p>1781 v:shapes="Picture_x0020_21"><![endif]></span></p> 1456 1782 1457 1783 <p class=MsoNormal><o:p> </o:p></p> 1458 1784 1459 1785 <p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span 1460 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1786 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1461 1787 mso-hansi-theme-font:minor-latin'>Set <span class=GramE>All</span></span></b>, 1462 1788 all boxes will be checked showing selection of the data sets. Then press <b 1463 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1789 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1464 1790 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>; 1465 1791 a new dialog box will appear</p> … … 1470 1796 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image022.png" 1471 1797 o:title=""/> 1472 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=3361798 </v:shape><![endif]--><![if !vml]><img width=346 height=336 1473 1799 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image022.png" 1474 1800 v:shapes="Picture_x0020_33"><![endif]></span></p> … … 1478 1804 <p class=MsoNormal>This allows you to instruct the sequential refinement to 1479 1805 start at the last data set and proceed backwards through them (<b 1480 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1806 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1481 1807 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Reverse 1482 1808 sequence</span></b>). It also allows you to instruct the sequential refinement … … 1488 1814 great for the least squares to handle; going in the forward direction works 1489 1815 just fine (as you will see next). Select <b style='mso-bidi-font-weight:normal'><span 1490 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1816 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1491 1817 mso-hansi-theme-font:minor-latin'>Copy from prev.</span></b> and press <b 1492 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1818 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1493 1819 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>; 1494 the sequential refinement will <span class=GramE>proceed</span> very rapidly1495 d isplaying results for each data set on the console and finally ending by1496 displaying the <b style='mso-bidi-font-weight:normal'><span style='font-family: 1497 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1498 minor-latin'>Sequentialresults.<o:p></o:p></span></b></p>1499 1500 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1501 id="Picture_x0020_4 5" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt;1820 the sequential refinement will proceed very rapidly displaying results for each 1821 data set on the console and finally ending by displaying the <b 1822 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1823 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sequential 1824 results.<o:p></o:p></span></b></p> 1825 1826 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1827 id="Picture_x0020_42" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:564pt; 1502 1828 height:262.5pt;visibility:visible;mso-wrap-style:square'> 1503 1829 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image023.png" 1504 1830 o:title=""/> 1505 </v:shape><![endif]--><![if !vml]><img border=0 width=700height=3501831 </v:shape><![endif]--><![if !vml]><img width=752 height=350 1506 1832 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image023.png" 1507 v:shapes="Picture_x0020_4 5"><![endif]></span></p>1833 v:shapes="Picture_x0020_42"><![endif]></span></p> 1508 1834 1509 1835 <p class=MsoNormal><o:p> </o:p></p> 1510 1836 1511 1837 <p class=MsoNormal>Note the comment in the plot status bar: double click on the 1512 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1838 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1513 1839 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0<span 1514 class=GramE> :Volume</span></span></b> and a new plot will appear.</p>1515 1516 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1517 id="Picture_x0020_ 35" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:525pt;1840 class=GramE>;Volume</span></span></b> and a new plot will appear.</p> 1841 1842 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1843 id="Picture_x0020_43" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:525pt; 1518 1844 height:450pt;visibility:visible;mso-wrap-style:square'> 1519 1845 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image024.png" 1520 1846 o:title=""/> 1521 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001847 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1522 1848 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image024.png" 1523 v:shapes="Picture_x0020_ 35"><![endif]></span></p>1849 v:shapes="Picture_x0020_43"><![endif]></span></p> 1524 1850 1525 1851 <p class=MsoNormal><o:p> </o:p></p> … … 1527 1853 <p class=MsoNormal>Each point has an error bar extracted from the least squares 1528 1854 it represents a 1 σ variation in the value. Now press the <b 1529 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1855 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1530 1856 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>s</span></b> 1531 1857 key (or select <b style='mso-bidi-font-weight:normal'><span style='font-family: 1532 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1858 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1533 1859 minor-latin'>s</span></b> from the <b style='mso-bidi-font-weight:normal'><span 1534 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1860 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1535 1861 mso-hansi-theme-font:minor-latin'>K</span></b> box); a dialog box will appear 1536 1862 with a selection of parameters to plot along the x-axis. Select <b 1537 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1863 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1538 1864 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>fraction</span></b> 1539 1865 and the plot will be redrawn (it may require selection of another column & 1540 then <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1866 then <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1541 1867 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0<span 1542 class=GramE> :Volume</span></span></b> to make it appear).</p>1543 1544 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1545 id="Picture_x0020_4 6" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt;1868 class=GramE>;Volume</span></span></b> to make it appear).</p> 1869 1870 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1871 id="Picture_x0020_44" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt; 1546 1872 height:450pt;visibility:visible;mso-wrap-style:square'> 1547 1873 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image025.png" 1548 1874 o:title=""/> 1549 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001875 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1550 1876 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image025.png" 1551 v:shapes="Picture_x0020_4 6"><![endif]></span></p>1877 v:shapes="Picture_x0020_44"><![endif]></span></p> 1552 1878 1553 1879 <p class=MsoNormal><o:p> </o:p></p> … … 1556 1882 composition is linear. You can now determine the slope & intercept (or fit 1557 1883 to some other function!) directly with GSAS-II; do <b style='mso-bidi-font-weight: 1558 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1884 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1559 1885 minor-latin;mso-hansi-theme-font:minor-latin'>Parametric Fit/Add function</span></b> 1560 and the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1886 and the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1561 1887 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Expression 1562 1888 Editor</span></b> dialog box will appear.</p> 1563 1889 1564 1890 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1565 id=" Picture_x0020_47" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:465pt;1566 height:225pt;visibility:visible;mso-wrap-style:square'>1891 id="_x0000_i1031" type="#_x0000_t75" style='width:465pt;height:225pt; 1892 visibility:visible;mso-wrap-style:square'> 1567 1893 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image026.png" 1568 1894 o:title=""/> 1569 </v:shape><![endif]--><![if !vml]><img border=0width=620 height=3001895 </v:shape><![endif]--><![if !vml]><img width=620 height=300 1570 1896 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image026.png" 1571 v:shapes=" Picture_x0020_47"><![endif]></span></p>1897 v:shapes="_x0000_i1031"><![endif]></span></p> 1572 1898 1573 1899 <p class=MsoNormal><o:p> </o:p></p> 1574 1900 1575 1901 <p class=MsoNormal>The pull down in the upper left corner has two choices; 1576 select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1577 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Hist<span 1578 class=GramE>./</span>Phase</span></b> and a new dialog box will appear giving 1579 you choices from the <b style='mso-bidi-font-weight:normal'><span 1580 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1581 mso-hansi-theme-font:minor-latin'>Sequential results</span></b> table. Select <b 1582 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1583 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0<span 1584 class=GramE>:Volume</span></span></b> and the <b style='mso-bidi-font-weight: 1585 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1586 minor-latin;mso-hansi-theme-font:minor-latin'>Expression Editor</span></b> will 1587 reappear.</p> 1588 1589 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1590 id="Picture_x0020_48" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:465pt; 1591 height:225pt;visibility:visible;mso-wrap-style:square'> 1902 select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1903 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Global</span></b> 1904 and a new dialog box will appear giving you choices from the <b 1905 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1906 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sequential 1907 results</span></b> table. Select <b style='mso-bidi-font-weight:normal'><span 1908 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1909 mso-hansi-theme-font:minor-latin'>0<span class=GramE>;Volume</span></span></b> 1910 and the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1911 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Expression 1912 Editor</span></b> will reappear.</p> 1913 1914 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1915 id="Picture_x0020_45" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:465pt; 1916 height:255pt;visibility:visible;mso-wrap-style:square'> 1592 1917 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image027.png" 1593 1918 o:title=""/> 1594 </v:shape><![endif]--><![if !vml]><img border=0 width=620 height=3001919 </v:shape><![endif]--><![if !vml]><img width=620 height=340 1595 1920 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image027.png" 1596 v:shapes="Picture_x0020_4 8"><![endif]></span></p>1921 v:shapes="Picture_x0020_45"><![endif]></span></p> 1597 1922 1598 1923 <p class=MsoNormal><o:p> </o:p></p> 1599 1924 1600 1925 <p class=MsoNormal>Next enter the function you wish to use in fitting <b 1601 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1926 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1602 1927 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0<span 1603 1928 class=GramE>:Volume</span></span></b>; enter <b style='mso-bidi-font-weight: 1604 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1929 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1605 1930 minor-latin;mso-hansi-theme-font:minor-latin'>m*<span class=SpellE>x+b</span></span></b> 1606 1931 (equation for a straight line). After a pause, the <b style='mso-bidi-font-weight: 1607 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1932 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1608 1933 minor-latin;mso-hansi-theme-font:minor-latin'>Expression Editor</span></b> will 1609 1934 be redrawn allowing you to assign <b style='mso-bidi-font-weight:normal'><span 1610 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1935 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1611 1936 mso-hansi-theme-font:minor-latin'>b</span></b>, <b style='mso-bidi-font-weight: 1612 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1937 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1613 1938 minor-latin;mso-hansi-theme-font:minor-latin'>m</span></b> & <b 1614 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1939 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1615 1940 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>x</span></b>.</p> 1616 1941 1617 1942 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1618 id="Picture_x0020_4 9" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;1619 height:2 25pt;visibility:visible;mso-wrap-style:square'>1943 id="Picture_x0020_46" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt; 1944 height:255pt;visibility:visible;mso-wrap-style:square'> 1620 1945 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image028.png" 1621 1946 o:title=""/> 1622 </v:shape><![endif]--><![if !vml]><img border=0 width=620 height=3001947 </v:shape><![endif]--><![if !vml]><img width=620 height=340 1623 1948 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image028.png" 1624 v:shapes="Picture_x0020_4 9"><![endif]></span></p>1949 v:shapes="Picture_x0020_46"><![endif]></span></p> 1625 1950 1626 1951 <p class=MsoNormal><o:p> </o:p></p> 1627 1952 1628 1953 <p class=MsoNormal>For <b style='mso-bidi-font-weight:normal'><span 1629 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1954 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1630 1955 mso-hansi-theme-font:minor-latin'>b</span></b> & <b style='mso-bidi-font-weight: 1631 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1956 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1632 1957 minor-latin;mso-hansi-theme-font:minor-latin'>m</span></b> select <span 1633 1958 class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1634 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1959 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1635 1960 minor-latin'>Free</span></b></span>; these will be the parameters for your fit. 1636 For <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1961 For <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1637 1962 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>x</span></b> 1638 select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1963 select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1639 1964 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Global</span></b>; 1640 1965 a new dialog box will appear giving you two choices.</p> 1641 1966 1642 1967 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1643 id=" Picture_x0020_50" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:468.75pt;1644 height:187.5pt;visibility:visible;mso-wrap-style:square'>1968 id="_x0000_i1028" type="#_x0000_t75" style='width:468.75pt;height:187.5pt; 1969 visibility:visible;mso-wrap-style:square'> 1645 1970 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image029.png" 1646 1971 o:title=""/> 1647 </v:shape><![endif]--><![if !vml]><img border=0width=625 height=2501972 </v:shape><![endif]--><![if !vml]><img width=625 height=250 1648 1973 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image029.png" 1649 v:shapes=" Picture_x0020_50"><![endif]></span></p>1974 v:shapes="_x0000_i1028"><![endif]></span></p> 1650 1975 1651 1976 <p class=MsoNormal><o:p> </o:p></p> 1652 1977 1653 1978 <p class=MsoNormal>Select the 2<sup>nd</sup> line (<b style='mso-bidi-font-weight: 1654 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1979 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1655 1980 minor-latin;mso-hansi-theme-font:minor-latin'>fraction 1656 1981 </span></b>); it will 1657 1982 appear in blue. Then press <b style='mso-bidi-font-weight:normal'><span 1658 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1983 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1659 1984 mso-hansi-theme-font:minor-latin'>OK</span></b>; the <b style='mso-bidi-font-weight: 1660 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1985 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1661 1986 minor-latin;mso-hansi-theme-font:minor-latin'>Expression Editor</span></b> will 1662 1987 reappear with more information.</p> 1663 1988 1664 1989 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1665 id="Picture_x0020_ 51" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt;1666 height:2 25pt;visibility:visible;mso-wrap-style:square'>1990 id="Picture_x0020_47" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt; 1991 height:255pt;visibility:visible;mso-wrap-style:square'> 1667 1992 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image030.png" 1668 1993 o:title=""/> 1669 </v:shape><![endif]--><![if !vml]><img border=0 width=620 height=3001994 </v:shape><![endif]--><![if !vml]><img width=620 height=340 1670 1995 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image030.png" 1671 v:shapes="Picture_x0020_ 51"><![endif]></span></p>1672 1673 <p class=MsoNormal><o:p> </o:p></p> 1674 1675 <p class=MsoNormal>Next <span class=GramE>press</span> <b style='mso-bidi-font-weight:1676 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1677 m inor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>; the equation will1678 be fitted tothe data and the results displayed on the console</p>1679 1680 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1681 id="Picture_x0020_ 31" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:387.75pt;1682 height: 107.25pt;visibility:visible;mso-wrap-style:square'>1996 v:shapes="Picture_x0020_47"><![endif]></span></p> 1997 1998 <p class=MsoNormal><o:p> </o:p></p> 1999 2000 <p class=MsoNormal>Next press <b style='mso-bidi-font-weight:normal'><span 2001 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2002 mso-hansi-theme-font:minor-latin'>OK</span></b>; the equation will be fitted to 2003 the data and the results displayed on the console</p> 2004 2005 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 2006 id="Picture_x0020_49" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:303.75pt; 2007 height:98.25pt;visibility:visible;mso-wrap-style:square'> 1683 2008 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image031.png" 1684 2009 o:title=""/> 1685 </v:shape><![endif]--><![if !vml]><img border=0 width=517 height=1432010 </v:shape><![endif]--><![if !vml]><img width=405 height=131 1686 2011 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image031.png" 1687 v:shapes="Picture_x0020_ 31"><![endif]></span></p>2012 v:shapes="Picture_x0020_49"><![endif]></span></p> 1688 2013 1689 2014 <p class=MsoNormal><o:p> </o:p></p> … … 1694 2019 1695 2020 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1696 id="Picture_x0020_ 32" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;2021 id="Picture_x0020_50" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt; 1697 2022 height:450pt;visibility:visible;mso-wrap-style:square'> 1698 2023 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image032.png" 1699 2024 o:title=""/> 1700 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6002025 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1701 2026 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image032.png" 1702 v:shapes="Picture_x0020_ 32"><![endif]></span></p>2027 v:shapes="Picture_x0020_50"><![endif]></span></p> 1703 2028 1704 2029 <p class=MsoNormal><o:p> </o:p></p> 1705 2030 1706 2031 <p class=MsoNormal>For this particular experiment there was an expectation that 1707 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2032 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1708 2033 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Volume</span></b>s 1709 2034 obtained from the SASD model fits would match the makeup concentrations for
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