Changeset 1741
- Timestamp:
- Mar 18, 2015 3:32:56 PM (9 years ago)
- Location:
- Tutorials/SAimages
- Files:
-
- 40 edited
Legend:
- Unmodified
- Added
- Removed
-
Tutorials/SAimages/Small Angle Image Processing.htm
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Name="List Continue 4"/> 232 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 233 Name="List Continue 5"/> 234 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 235 Name="Message Header"/> 236 <w:LsdException Locked="false" Priority="11" QFormat="true" Name="Subtitle"/> 237 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 238 Name="Salutation"/> 239 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 240 Name="Date"/> 241 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 242 Name="Body Text First Indent"/> 243 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 244 Name="Body Text First Indent 2"/> 245 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 246 Name="Note Heading"/> 247 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 248 Name="Body Text 2"/> 249 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 250 Name="Body Text 3"/> 251 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 252 Name="Body Text Indent 2"/> 253 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 254 Name="Body Text Indent 3"/> 255 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 256 Name="Block Text"/> 257 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 258 Name="Hyperlink"/> 259 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 260 Name="FollowedHyperlink"/> 261 <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/> 262 <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/> 263 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 264 Name="Document Map"/> 265 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 266 Name="Plain Text"/> 267 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 268 Name="E-mail Signature"/> 269 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 270 Name="HTML Top of Form"/> 271 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 272 Name="HTML Bottom of Form"/> 273 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 274 Name="Normal (Web)"/> 275 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 276 Name="HTML Acronym"/> 277 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 278 Name="HTML Address"/> 279 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 280 Name="HTML Cite"/> 281 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 282 Name="HTML Code"/> 283 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 284 Name="HTML Definition"/> 285 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 286 Name="HTML Keyboard"/> 287 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 288 Name="HTML Preformatted"/> 289 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 290 Name="HTML Sample"/> 291 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 292 Name="HTML Typewriter"/> 293 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 294 Name="HTML Variable"/> 295 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 296 Name="Normal Table"/> 297 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 298 Name="annotation subject"/> 299 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 300 Name="No List"/> 301 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 302 Name="Outline List 1"/> 303 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 304 Name="Outline List 2"/> 305 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 306 Name="Outline List 3"/> 307 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 308 Name="Table Simple 1"/> 309 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 310 Name="Table Simple 2"/> 311 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 312 Name="Table Simple 3"/> 313 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 314 Name="Table Classic 1"/> 315 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 316 Name="Table Classic 2"/> 317 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 318 Name="Table Classic 3"/> 319 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 320 Name="Table Classic 4"/> 321 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 322 Name="Table Colorful 1"/> 323 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 324 Name="Table Colorful 2"/> 325 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 326 Name="Table Colorful 3"/> 327 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 328 Name="Table Columns 1"/> 329 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 330 Name="Table Columns 2"/> 331 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 332 Name="Table Columns 3"/> 333 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 334 Name="Table Columns 4"/> 335 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 336 Name="Table Columns 5"/> 337 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 338 Name="Table Grid 1"/> 339 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 340 Name="Table Grid 2"/> 341 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 342 Name="Table Grid 3"/> 343 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 344 Name="Table Grid 4"/> 345 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 346 Name="Table Grid 5"/> 347 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 348 Name="Table Grid 6"/> 349 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 350 Name="Table Grid 7"/> 351 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 352 Name="Table Grid 8"/> 353 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 354 Name="Table List 1"/> 355 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 356 Name="Table List 2"/> 357 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 358 Name="Table List 3"/> 359 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 360 Name="Table List 4"/> 361 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 362 Name="Table List 5"/> 363 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 364 Name="Table List 6"/> 365 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 366 Name="Table List 7"/> 367 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 368 Name="Table List 8"/> 369 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 370 Name="Table 3D effects 1"/> 371 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 372 Name="Table 3D effects 2"/> 373 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 374 Name="Table 3D effects 3"/> 375 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 376 Name="Table Contemporary"/> 377 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 378 Name="Table Elegant"/> 379 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 380 Name="Table Professional"/> 381 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 382 Name="Table Subtle 1"/> 383 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 384 Name="Table Subtle 2"/> 385 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 386 Name="Table Web 1"/> 387 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 388 Name="Table Web 2"/> 389 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 390 Name="Table Web 3"/> 391 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 392 Name="Balloon Text"/> 393 <w:LsdException Locked="false" Priority="59" Name="Table Grid"/> 394 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 395 Name="Table Theme"/> 396 <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/> 397 <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/> 398 <w:LsdException Locked="false" Priority="60" Name="Light Shading"/> 399 <w:LsdException Locked="false" Priority="61" Name="Light List"/> 400 <w:LsdException Locked="false" Priority="62" Name="Light Grid"/> 401 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/> 402 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/> 403 <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/> 404 <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/> 405 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/> 406 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/> 407 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/> 408 <w:LsdException Locked="false" Priority="70" Name="Dark List"/> 409 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/> 410 <w:LsdException Locked="false" Priority="72" Name="Colorful List"/> 411 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/> 412 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/> 413 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/> 414 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/> 415 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/> 416 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/> 417 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/> 418 <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/> 419 <w:LsdException Locked="false" Priority="34" QFormat="true" 420 Name="List Paragraph"/> 421 <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/> 422 <w:LsdException Locked="false" Priority="30" QFormat="true" 423 Name="Intense Quote"/> 424 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/> 425 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/> 426 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/> 427 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/> 428 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/> 429 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/> 430 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/> 431 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/> 432 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/> 433 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/> 434 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/> 435 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/> 436 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/> 437 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/> 438 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/> 439 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/> 440 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/> 441 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/> 442 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/> 443 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/> 444 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/> 445 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/> 446 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/> 447 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/> 448 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/> 449 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/> 450 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/> 451 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/> 452 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/> 453 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/> 454 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/> 455 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/> 456 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/> 457 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/> 458 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/> 459 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/> 460 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/> 461 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/> 462 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/> 463 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/> 464 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/> 465 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/> 466 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/> 467 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/> 468 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/> 469 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/> 470 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/> 471 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/> 472 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/> 473 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/> 474 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/> 475 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/> 476 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/> 477 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/> 478 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/> 479 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/> 480 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/> 481 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/> 482 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/> 483 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/> 484 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/> 485 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/> 486 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/> 487 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/> 488 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/> 489 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/> 490 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/> 491 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/> 492 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/> 493 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/> 494 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/> 495 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/> 496 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/> 497 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/> 498 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/> 499 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/> 500 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/> 501 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/> 502 <w:LsdException Locked="false" Priority="19" QFormat="true" 503 Name="Subtle Emphasis"/> 504 <w:LsdException Locked="false" Priority="21" QFormat="true" 505 Name="Intense Emphasis"/> 506 <w:LsdException Locked="false" Priority="31" QFormat="true" 507 Name="Subtle Reference"/> 508 <w:LsdException Locked="false" Priority="32" QFormat="true" 509 Name="Intense Reference"/> 510 <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/> 511 <w:LsdException Locked="false" Priority="37" SemiHidden="true" 512 UnhideWhenUsed="true" Name="Bibliography"/> 513 <w:LsdException Locked="false" Priority="39" SemiHidden="true" 514 UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/> 515 <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/> 516 <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/> 517 <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/> 518 <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/> 519 <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/> 520 <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/> 521 <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/> 522 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/> 523 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/> 524 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/> 525 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/> 526 <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/> 527 <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/> 528 <w:LsdException Locked="false" Priority="46" 529 Name="Grid Table 1 Light Accent 1"/> 530 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/> 531 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/> 532 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/> 533 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/> 534 <w:LsdException Locked="false" Priority="51" 535 Name="Grid Table 6 Colorful Accent 1"/> 536 <w:LsdException Locked="false" Priority="52" 537 Name="Grid Table 7 Colorful Accent 1"/> 538 <w:LsdException Locked="false" Priority="46" 539 Name="Grid Table 1 Light Accent 2"/> 540 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/> 541 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/> 542 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/> 543 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/> 544 <w:LsdException Locked="false" Priority="51" 545 Name="Grid Table 6 Colorful Accent 2"/> 546 <w:LsdException Locked="false" Priority="52" 547 Name="Grid Table 7 Colorful Accent 2"/> 548 <w:LsdException Locked="false" Priority="46" 549 Name="Grid Table 1 Light Accent 3"/> 550 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/> 551 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/> 552 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/> 553 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/> 554 <w:LsdException Locked="false" Priority="51" 555 Name="Grid Table 6 Colorful Accent 3"/> 556 <w:LsdException Locked="false" Priority="52" 557 Name="Grid Table 7 Colorful Accent 3"/> 558 <w:LsdException Locked="false" Priority="46" 559 Name="Grid Table 1 Light Accent 4"/> 560 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/> 561 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/> 562 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/> 563 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/> 564 <w:LsdException Locked="false" Priority="51" 565 Name="Grid Table 6 Colorful Accent 4"/> 566 <w:LsdException Locked="false" Priority="52" 567 Name="Grid Table 7 Colorful Accent 4"/> 568 <w:LsdException Locked="false" Priority="46" 569 Name="Grid Table 1 Light Accent 5"/> 570 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/> 571 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/> 572 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/> 573 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/> 574 <w:LsdException Locked="false" Priority="51" 575 Name="Grid Table 6 Colorful Accent 5"/> 576 <w:LsdException Locked="false" Priority="52" 577 Name="Grid Table 7 Colorful Accent 5"/> 578 <w:LsdException Locked="false" Priority="46" 579 Name="Grid Table 1 Light Accent 6"/> 580 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/> 581 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/> 582 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/> 583 <w:LsdException Locked="false" Priority="50" 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763 1079 mso-bidi-font-size:10.0pt; 764 font-family:"Calibri", "sans-serif";1080 font-family:"Calibri",sans-serif; 765 1081 mso-ascii-font-family:Calibri; 766 1082 mso-ascii-theme-font:minor-latin; … … 796 1112 mso-pagination:widow-orphan; 797 1113 font-size:10.0pt; 798 font-family:"Calibri", "sans-serif";1114 font-family:"Calibri",sans-serif; 799 1115 mso-ascii-font-family:Calibri; 800 1116 mso-ascii-theme-font:minor-latin; … … 816 1132 mso-pagination:widow-orphan; 817 1133 font-size:10.0pt; 818 font-family:"Calibri", "sans-serif";1134 font-family:"Calibri",sans-serif; 819 1135 mso-ascii-font-family:Calibri; 820 1136 mso-ascii-theme-font:minor-latin; … … 848 1164 detector placed ~570mm from the sample. Note that menu entries are listed in 849 1165 bold face below as <b style='mso-bidi-font-weight:normal'><span 850 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1166 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 851 1167 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 852 1168 minor-latin'>Help/About GSAS-II</span></b>, which lists first the name of the 853 1169 menu (here <b style='mso-bidi-font-weight:normal'><span style='font-family: 854 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1170 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 855 1171 minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Help</span></b>) 856 1172 and second the name of the entry in the menu (here <b style='mso-bidi-font-weight: 857 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1173 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 858 1174 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 859 1175 mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).<span … … 862 1178 italic'><o:p></o:p></span></p> 863 1179 864 <p class=MsoNormal>If you have not done so already, <a 865 href="Starting%20GSAS.htm">start GSAS-II</a>.</p> 1180 <p class=MsoNormal>If you have not done so already, start GSAS-II.</p> 866 1181 867 1182 <h2>Step 1: Detector calibration</h2> … … 869 1184 <p class=MsoNormal>The detector position is determined by using an image 870 1185 collected from silver <span class=SpellE>behenate</span>; do <b 871 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1186 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 872 1187 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Data/Read 873 1188 Image data 874 </span></b> and a file selection dialog box will appear</p> 1189 </span></b> and a file selection dialog box will appear. Go to <b 1190 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1191 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>exercises/<span 1192 class=SpellE>SAimages</span></span></b> and select <b style='mso-bidi-font-weight: 1193 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1194 minor-latin;mso-hansi-theme-font:minor-latin'>AgBehenate_003.tif</span></b> 1195 with either a mouse button double click or <b style='mso-bidi-font-weight:normal'><span 1196 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1197 mso-hansi-theme-font:minor-latin'>Open</span></b>; the image will appear</p> 875 1198 876 1199 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype … … 894 1217 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> 895 1218 <o:lock v:ext="edit" aspectratio="t"/> 896 </v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i106 5" type="#_x0000_t75"897 style='width:5 37pt;height:397.5pt;visibility:visible;mso-wrap-style:square'>1219 </v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1062" type="#_x0000_t75" 1220 style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'> 898 1221 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image001.png" 899 1222 o:title=""/> 900 </v:shape><![endif]--><![if !vml]><img border=0 width=716 height=5301223 </v:shape><![endif]--><![if !vml]><img width=700 height=600 901 1224 src="Small%20Angle%20Image%20Processing_files/image001.png" v:shapes="Picture_x0020_1"><![endif]></span></p> 902 1225 903 1226 <p class=MsoNormal><o:p> </o:p></p> 904 1227 905 <p class=MsoNormal>Go to <b style='mso-bidi-font-weight:normal'><span 906 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 907 mso-hansi-theme-font:minor-latin'>Exercises/Small angle/Image reduction</span></b> 908 and select <b style='mso-bidi-font-weight:normal'><span style='font-family: 909 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 910 minor-latin'>AgBehenate_003.tif</span></b> with either a mouse button double 911 click or <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 912 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Open</span></b>; 913 the image will appear</p> 914 915 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 916 id="Picture_x0020_16" o:spid="_x0000_i1064" type="#_x0000_t75" style='width:525pt; 917 height:450pt;visibility:visible;mso-wrap-style:square'> 1228 <p class=MsoNormal>And the <b style='mso-bidi-font-weight:normal'><span 1229 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1230 mso-hansi-theme-font:minor-latin'>Image controls</span></b> window will show</p> 1231 1232 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1233 id="Picture_x0020_2" o:spid="_x0000_i1061" type="#_x0000_t75" style='width:472.5pt; 1234 height:388.5pt;visibility:visible;mso-wrap-style:square'> 918 1235 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image002.png" 919 1236 o:title=""/> 920 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 921 src="Small%20Angle%20Image%20Processing_files/image002.png" v:shapes="Picture_x0020_16"><![endif]></span></p> 922 923 <p class=MsoNormal><o:p> </o:p></p> 924 925 <p class=MsoNormal>And the <b style='mso-bidi-font-weight:normal'><span 926 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 927 mso-hansi-theme-font:minor-latin'>Image controls</span></b> window will show</p> 928 929 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 930 id="Picture_x0020_3" o:spid="_x0000_i1063" type="#_x0000_t75" style='width:472.5pt; 931 height:388.5pt;visibility:visible;mso-wrap-style:square'> 932 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image003.png" 933 o:title=""/> 934 </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 935 src="Small%20Angle%20Image%20Processing_files/image003.png" v:shapes="Picture_x0020_3"><![endif]></span></p> 1237 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1238 src="Small%20Angle%20Image%20Processing_files/image002.png" v:shapes="Picture_x0020_2"><![endif]></span></p> 936 1239 937 1240 <p class=MsoNormal><o:p> </o:p></p> 938 1241 939 1242 <p class=MsoNormal>Note the default <b style='mso-bidi-font-weight:normal'><span 940 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1243 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 941 1244 mso-hansi-theme-font:minor-latin'>Type of image data</span></b> is <b 942 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1245 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 943 1246 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>PWDR - 944 1247 powder diffraction data</span></b>; you will change that <span 945 1248 style='mso-no-proof:yes'>now.</span> Select <b style='mso-bidi-font-weight: 946 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1249 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 947 1250 minor-latin;mso-hansi-theme-font:minor-latin'>SASD small angle scattering 948 1251 data</span></b> (the window will change). Enter the <b style='mso-bidi-font-weight: 949 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1252 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 950 1253 minor-latin;mso-hansi-theme-font:minor-latin'>wavelength</span></b> (<b 951 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1254 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 952 1255 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1.0332</span></b>), 953 1256 and select the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 954 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1257 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 955 1258 mso-hansi-theme-font:minor-latin'>Calibrant</span></b></span> (near bottom of 956 1259 window) as <b style='mso-bidi-font-weight:normal'><span style='font-family: 957 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1260 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 958 1261 minor-latin'>Ag <span class=SpellE>behenate</span></span></b>. Note that the 959 1262 calibration info for Ag <span class=SpellE>behenate</span> was read from a 960 1263 python file <b style='mso-bidi-font-weight:normal'><span style='font-family: 961 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1264 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 962 1265 minor-latin'>GSASII/ImageCalibrants.py</span></b>. If you have a <span 963 1266 class=SpellE>calibrant</span> that isnt in this file you should enter it in 964 the file <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1267 the file <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 965 1268 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>UserCalibrants.py</span></b>; 966 1269 just follow the format of the examples within <b style='mso-bidi-font-weight: 967 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1270 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 968 1271 minor-latin;mso-hansi-theme-font:minor-latin'>ImageCalibrants.py</span></b>. 969 1272 You should move the <b style='mso-bidi-font-weight:normal'><span 970 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1273 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 971 1274 mso-hansi-theme-font:minor-latin'>Max intensity</span></b> slider to near the 972 1275 middle of the range that will improve the image. When done the <b 973 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1276 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 974 1277 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 975 1278 controls</span></b> window should look like</p> 976 1279 977 1280 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 978 id="Picture_x0020_ 4" o:spid="_x0000_i1062" type="#_x0000_t75" style='width:472.5pt;1281 id="Picture_x0020_3" o:spid="_x0000_i1060" type="#_x0000_t75" style='width:472.5pt; 979 1282 height:388.5pt;visibility:visible;mso-wrap-style:square'> 980 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image00 4.png"981 o:title=""/> 982 </v:shape><![endif]--><![if !vml]><img border=0width=630 height=518983 src="Small%20Angle%20Image%20Processing_files/image00 4.png" v:shapes="Picture_x0020_4"><![endif]></span></p>1283 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image003.png" 1284 o:title=""/> 1285 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1286 src="Small%20Angle%20Image%20Processing_files/image003.png" v:shapes="Picture_x0020_3"><![endif]></span></p> 984 1287 985 1288 <p class=MsoNormal><o:p> </o:p></p> … … 1036 1339 absolute;z-index:251659264;margin-left:234px;margin-top:274px;width:73px; 1037 1340 height:38px'><img width=73 height=38 1038 src="Small%20Angle%20Image%20Processing_files/image00 5.png" v:shapes="Straight_x0020_Arrow_x0020_Connector_x0020_21"></span><![endif]><span1039 style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_ 5"1040 o:spid="_x0000_i10 61" type="#_x0000_t75" style='width:525pt;height:450pt;1341 src="Small%20Angle%20Image%20Processing_files/image004.png" v:shapes="Straight_x0020_Arrow_x0020_Connector_x0020_21"></span><![endif]><span 1342 style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_4" 1343 o:spid="_x0000_i1059" type="#_x0000_t75" style='width:525pt;height:450pt; 1041 1344 visibility:visible;mso-wrap-style:square'> 1042 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image00 6.png"1043 o:title=""/> 1044 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001045 src="Small%20Angle%20Image%20Processing_files/image00 6.png" v:shapes="Picture_x0020_5"><![endif]></span></p>1345 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image005.png" 1346 o:title=""/> 1347 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1348 src="Small%20Angle%20Image%20Processing_files/image005.png" v:shapes="Picture_x0020_4"><![endif]></span></p> 1046 1349 1047 1350 <p class=MsoNormal><o:p> </o:p></p> 1048 1351 1049 1352 <p class=MsoNormal>Next select <b style='mso-bidi-font-weight:normal'><span 1050 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1353 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1051 1354 mso-hansi-theme-font:minor-latin'>Operations/Calibrate</span></b> from the <b 1052 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1355 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1053 1356 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 1054 1357 Controls</span></b> menu; a bit of instruction will appear on the status line … … 1057 1360 finish; calibration will proceed. A sequence of concentric red rings will 1058 1361 appear; they will switch to blue when calibration is finished. Select <b 1059 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1362 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1060 1363 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Show ring 1061 1364 picks</span></b> (near bottom right of <b style='mso-bidi-font-weight:normal'><span 1062 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1365 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1063 1366 mso-hansi-theme-font:minor-latin'>Image Controls</span></b> window). The <b 1064 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1367 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1065 1368 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 1066 1369 Controls</span></b> window will show the results of the calibration</p> 1067 1370 1068 1371 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1069 id="Picture_x0020_ 6" o:spid="_x0000_i1060" type="#_x0000_t75" style='width:472.5pt;1372 id="Picture_x0020_5" o:spid="_x0000_i1058" type="#_x0000_t75" style='width:472.5pt; 1070 1373 height:388.5pt;visibility:visible;mso-wrap-style:square'> 1071 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image00 7.png"1072 o:title=""/> 1073 </v:shape><![endif]--><![if !vml]><img border=0width=630 height=5181074 src="Small%20Angle%20Image%20Processing_files/image00 7.png" v:shapes="Picture_x0020_6"><![endif]></span></p>1374 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image006.png" 1375 o:title=""/> 1376 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1377 src="Small%20Angle%20Image%20Processing_files/image006.png" v:shapes="Picture_x0020_5"><![endif]></span></p> 1075 1378 1076 1379 <p class=MsoNormal><o:p> </o:p></p> … … 1080 1383 1081 1384 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1082 id="Picture_x0020_ 23" o:spid="_x0000_i1059" type="#_x0000_t75" style='width:525pt;1385 id="Picture_x0020_6" o:spid="_x0000_i1057" type="#_x0000_t75" style='width:525pt; 1083 1386 height:450pt;visibility:visible;mso-wrap-style:square'> 1084 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image00 8.png"1085 o:title=""/> 1086 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001087 src="Small%20Angle%20Image%20Processing_files/image00 8.png" v:shapes="Picture_x0020_23"><![endif]></span></p>1387 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image007.png" 1388 o:title=""/> 1389 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1390 src="Small%20Angle%20Image%20Processing_files/image007.png" v:shapes="Picture_x0020_6"><![endif]></span></p> 1088 1391 1089 1392 <p class=MsoNormal><o:p> </o:p></p> … … 1091 1394 <p class=MsoNormal>You would like to use more points from just the visible 1092 1395 rings. I suggest you change <b style='mso-bidi-font-weight:normal'><span 1093 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1396 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1094 1397 mso-hansi-theme-font:minor-latin'>Min ring I/<span class=SpellE><span 1095 1398 class=GramE>Ib</span></span></span></b> to <b style='mso-bidi-font-weight:normal'><span 1096 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1399 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1097 1400 mso-hansi-theme-font:minor-latin'>0.5</span></b> and <b style='mso-bidi-font-weight: 1098 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1401 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1099 1402 minor-latin;mso-hansi-theme-font:minor-latin'>Min <span class=SpellE>calib</span> 1100 1403 d-spacing</span></b> to <b style='mso-bidi-font-weight:normal'><span 1101 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1404 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1102 1405 mso-hansi-theme-font:minor-latin'>10.0</span></b>. Do <b style='mso-bidi-font-weight: 1103 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1406 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1104 1407 minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Recalibrate</span></b>; 1105 1408 more points will be used and they will be limited to the 5 visible rings in the … … 1107 1410 1108 1411 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1109 id="Picture_x0020_ 8" o:spid="_x0000_i1058" type="#_x0000_t75" style='width:525pt;1412 id="Picture_x0020_7" o:spid="_x0000_i1056" type="#_x0000_t75" style='width:525pt; 1110 1413 height:450pt;visibility:visible;mso-wrap-style:square'> 1414 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image008.png" 1415 o:title=""/> 1416 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1417 src="Small%20Angle%20Image%20Processing_files/image008.png" v:shapes="Picture_x0020_7"><![endif]></span></p> 1418 1419 <p class=MsoNormal><o:p> </o:p></p> 1420 1421 <p class=MsoNormal>And give the calibration result as</p> 1422 1423 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1424 id="Picture_x0020_8" o:spid="_x0000_i1055" type="#_x0000_t75" style='width:472.5pt; 1425 height:388.5pt;visibility:visible;mso-wrap-style:square'> 1111 1426 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image009.png" 1112 1427 o:title=""/> 1113 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=6001428 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1114 1429 src="Small%20Angle%20Image%20Processing_files/image009.png" v:shapes="Picture_x0020_8"><![endif]></span></p> 1115 1116 <p class=MsoNormal><o:p> </o:p></p>1117 1118 <p class=MsoNormal>And give the calibration result as</p>1119 1120 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape1121 id="Picture_x0020_25" o:spid="_x0000_i1057" type="#_x0000_t75" style='width:472.5pt;1122 height:388.5pt;visibility:visible;mso-wrap-style:square'>1123 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image010.png"1124 o:title=""/>1125 </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=5181126 src="Small%20Angle%20Image%20Processing_files/image010.png" v:shapes="Picture_x0020_25"><![endif]></span></p>1127 1430 1128 1431 <p class=MsoNormal><o:p> </o:p></p> … … 1130 1433 <p class=MsoNormal>You will need this calibration information to process the 1131 1434 other images in this tutorial. To save it for future use do <b 1132 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1435 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1133 1436 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Save 1134 controls</span></b>; a file dialog will appear</p> 1135 1136 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1137 id="Picture_x0020_26" o:spid="_x0000_i1056" type="#_x0000_t75" style='width:537pt; 1138 height:397.5pt;visibility:visible;mso-wrap-style:square'> 1139 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image011.png" 1140 o:title=""/> 1141 </v:shape><![endif]--><![if !vml]><img border=0 width=716 height=530 1142 src="Small%20Angle%20Image%20Processing_files/image011.png" v:shapes="Picture_x0020_26"><![endif]></span></p> 1143 1144 <p class=MsoNormal><o:p> </o:p></p> 1145 1146 <p class=MsoNormal>Makeup a file name (no extension needed) for this; I chose <b 1147 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1148 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD</span></b>. 1149 Press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1150 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Save</span></b> 1151 and the file <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1152 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1153 mso-hansi-theme-font:minor-latin'>SASD.imctrl</span></b></span> will be written 1154 to the local directory.</p> 1155 1156 <p class=MsoNormal>If you are continuing on to the next step do <b 1157 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1158 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/New 1159 Project</span></b> (dont bother saving the project file unless you want it; we 1160 will not need it here); otherwise you can exit GSAS-II.</p> 1437 controls</span></b>; a file dialog will appear. Makeup a file name (no 1438 extension needed) for this; I chose <b style='mso-bidi-font-weight:normal'><span 1439 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1440 mso-hansi-theme-font:minor-latin'>SASD</span></b>. Press <b style='mso-bidi-font-weight: 1441 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1442 minor-latin;mso-hansi-theme-font:minor-latin'>Save</span></b> and the file <span 1443 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1444 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1445 minor-latin'>SASD.imctrl</span></b></span> will be written to the local 1446 directory. If you are continuing on to the next step do <b style='mso-bidi-font-weight: 1447 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1448 minor-latin;mso-hansi-theme-font:minor-latin'>File/New Project</span></b> 1449 (dont bother saving the project file unless you want it; we will not need it 1450 here); otherwise you can exit GSAS-II.</p> 1161 1451 1162 1452 <h2>Step 2: Data image integration</h2> … … 1165 1455 images, a glassy carbon image, an empty container image and a dark image. The 1166 1456 images will be integrated after creating masks to remove the beam stop and 1167 other objectionable parts of the images. If you have not done so already, <a1168 href="Starting%20GSAS.htm">start GSAS-II</a>. </p>1457 other objectionable parts of the images. If you have not done so already, start 1458 GSAS-II. </p> 1169 1459 1170 1460 <p class=MsoNormal><o:p> </o:p></p> 1171 1461 1172 1462 <p class=MsoNormal>First do <b style='mso-bidi-font-weight:normal'><span 1173 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1463 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1174 1464 mso-hansi-theme-font:minor-latin'>Data/Read image data 1175 1465 </span></b>, go to <b 1176 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1177 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Exercises/Small1178 angle/Image reduction</span></b> and select all images except <b1179 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1466 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1467 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>exercises/<span 1468 class=SpellE>SAimages</span></span></b> and select all images except <b 1469 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1180 1470 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>AgBehenate_003.tif</span></b>; 1181 1471 then press <b style='mso-bidi-font-weight:normal'><span style='font-family: 1182 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1472 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1183 1473 minor-latin'>Open</span></b> to read all of them. The GSAS-II data tree window 1184 1474 will show entries for 7 images and will expand the last one</p> 1185 1475 1186 1476 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1187 id=" Picture_x0020_11" o:spid="_x0000_i1055" type="#_x0000_t75" style='width:300pt;1188 height:308.25pt;visibility:visible;mso-wrap-style:square'>1189 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image01 3.png"1190 o:title=""/> 1191 </v:shape><![endif]--><![if !vml]><img border=0 width=400 height=4111192 src="Small%20Angle%20Image%20Processing_files/image01 3.png" v:shapes="Picture_x0020_11"><![endif]></span></p>1477 id="_x0000_i1054" type="#_x0000_t75" style='width:300pt;height:310.5pt; 1478 visibility:visible;mso-wrap-style:square'> 1479 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image010.png" 1480 o:title=""/> 1481 </v:shape><![endif]--><![if !vml]><img width=400 height=414 1482 src="Small%20Angle%20Image%20Processing_files/image010.png" v:shapes="_x0000_i1054"><![endif]></span></p> 1193 1483 1194 1484 <p class=MsoNormal><o:p> </o:p></p> … … 1197 1487 5s images and the Sa1-4 ones are 40s images; this time information is needed 1198 1488 later to obtain correct scaling. First select the <b style='mso-bidi-font-weight: 1199 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1489 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1200 1490 minor-latin;mso-hansi-theme-font:minor-latin'>IMG GC_5s_200.tif</span></b> 1201 1491 entry from the tree and expand it (press the <b style='mso-bidi-font-weight: 1202 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1492 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1203 1493 minor-latin;mso-hansi-theme-font:minor-latin'>+</span></b> box); then select <b 1204 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1494 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1205 1495 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 1206 1496 controls</span></b>. The data window (<b style='mso-bidi-font-weight:normal'><span 1207 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1497 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1208 1498 mso-hansi-theme-font:minor-latin'>Image Controls</span></b>) will show the 1209 1499 default settings.</p> 1210 1500 1211 1501 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1212 id=" Picture_x0020_12" o:spid="_x0000_i1054" type="#_x0000_t75" style='width:472.5pt;1213 height:388.5pt;visibility:visible;mso-wrap-style:square'>1214 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image01 4.png"1215 o:title=""/> 1216 </v:shape><![endif]--><![if !vml]><img border=0width=630 height=5181217 src="Small%20Angle%20Image%20Processing_files/image01 4.png" v:shapes="Picture_x0020_12"><![endif]></span></p>1502 id="_x0000_i1053" type="#_x0000_t75" style='width:472.5pt;height:388.5pt; 1503 visibility:visible;mso-wrap-style:square'> 1504 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image011.png" 1505 o:title=""/> 1506 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1507 src="Small%20Angle%20Image%20Processing_files/image011.png" v:shapes="_x0000_i1053"><![endif]></span></p> 1218 1508 1219 1509 <p class=MsoNormal><o:p> </o:p></p> 1220 1510 1221 1511 <p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span 1222 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1512 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1223 1513 mso-hansi-theme-font:minor-latin'>Operations/Load controls</span></b> from the 1224 1514 menu; a file selection dialog will appear showing the available *.<span 1225 class=SpellE>imctrl</span> files (the one you made in Step 1 should be seen).</p> 1226 1227 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1228 id="Picture_x0020_13" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:537pt; 1229 height:397.5pt;visibility:visible;mso-wrap-style:square'> 1230 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image015.png" 1231 o:title=""/> 1232 </v:shape><![endif]--><![if !vml]><img border=0 width=716 height=530 1233 src="Small%20Angle%20Image%20Processing_files/image015.png" v:shapes="Picture_x0020_13"><![endif]></span></p> 1234 1235 <p class=MsoNormal><o:p> </o:p></p> 1236 1237 <p class=MsoNormal>Select it and press <b style='mso-bidi-font-weight:normal'><span 1238 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1515 class=SpellE>imctrl</span> files (the one you made in Step 1 should be seen). 1516 Select it and press <b style='mso-bidi-font-weight:normal'><span 1517 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1239 1518 mso-hansi-theme-font:minor-latin'>Open</span></b>; the <b style='mso-bidi-font-weight: 1240 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1519 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1241 1520 minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> window 1242 1521 will be redrawn with the settings obtained in <b style='mso-bidi-font-weight: 1243 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1522 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1244 1523 minor-latin;mso-hansi-theme-font:minor-latin'>Step 1: Detector calibration</span></b></p> 1245 1524 1246 1525 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1247 id=" Picture_x0020_14" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:472.5pt;1248 height:388.5pt;visibility:visible;mso-wrap-style:square'>1249 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image01 6.png"1250 o:title=""/> 1251 </v:shape><![endif]--><![if !vml]><img border=0width=630 height=5181252 src="Small%20Angle%20Image%20Processing_files/image01 6.png" v:shapes="Picture_x0020_14"><![endif]></span></p>1526 id="_x0000_i1052" type="#_x0000_t75" style='width:472.5pt;height:388.5pt; 1527 visibility:visible;mso-wrap-style:square'> 1528 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image012.png" 1529 o:title=""/> 1530 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1531 src="Small%20Angle%20Image%20Processing_files/image012.png" v:shapes="_x0000_i1052"><![endif]></span></p> 1253 1532 1254 1533 <p class=MsoNormal><o:p> </o:p></p> … … 1256 1535 <p class=MsoNormal><span class=GramE>and</span> the image will be that of 1257 1536 glassy carbon. Changing the <b style='mso-bidi-font-weight:normal'><span 1258 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1537 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1259 1538 mso-hansi-theme-font:minor-latin'>Max intensity</span></b> slider on the <b 1260 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1539 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1261 1540 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 1262 1541 Controls</span></b> window will show that the image from the <span … … 1266 1545 1267 1546 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1268 id="Picture_x0020_ 15" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:525pt;1547 id="Picture_x0020_55" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:525pt; 1269 1548 height:450pt;visibility:visible;mso-wrap-style:square'> 1270 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image01 7.png"1271 o:title=""/> 1272 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001273 src="Small%20Angle%20Image%20Processing_files/image01 7.png" v:shapes="Picture_x0020_15"><![endif]></span></p>1549 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image013.png" 1550 o:title=""/> 1551 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1552 src="Small%20Angle%20Image%20Processing_files/image013.png" v:shapes="Picture_x0020_55"><![endif]></span></p> 1274 1553 1275 1554 <p class=MsoNormal><o:p> </o:p></p> … … 1277 1556 <p class=MsoNormal>The next step we will be doing is to set up the integration 1278 1557 controls. The <b style='mso-bidi-font-weight:normal'><span style='font-family: 1279 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1558 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1280 1559 minor-latin'>Dark image</span></b> is <b style='mso-bidi-font-weight:normal'><span 1281 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1560 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1282 1561 mso-hansi-theme-font:minor-latin'>IMG Dark_5s_003.tif</span></b>, the <b 1283 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1562 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1284 1563 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background 1285 1564 image</span></b> is <b style='mso-bidi-font-weight:normal'><span 1286 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1565 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1287 1566 mso-hansi-theme-font:minor-latin'>IMG Empty_5s_014.tif</span></b>; select these 1288 two. The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1567 two. The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1289 1568 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> 1290 1569 for each are <b style='mso-bidi-font-weight:normal'><span style='font-family: 1291 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1570 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1292 1571 minor-latin'>-1.0</span></b> because their exposures were the same as this 1293 1572 glassy carbon image (5s). Next check the boxes for <b style='mso-bidi-font-weight: 1294 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1573 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1295 1574 minor-latin;mso-hansi-theme-font:minor-latin'>Show integration limits?</span></b> 1296 1575 <span class=GramE>and</span> <b style='mso-bidi-font-weight:normal'><span 1297 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1576 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1298 1577 mso-hansi-theme-font:minor-latin'>Do full integration?</span></b> A pair of 1299 1578 circles with a connecting diagonal line will appear on the plot. Set the <b 1300 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1579 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1301 1580 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Inner/Outer 1302 2-theta</span></b> values to <b style='mso-bidi-font-weight:normal'><span1303 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1304 mso-hansi-theme-font:minor-latin'>0. 5</span></b> and <b style='mso-bidi-font-weight:1305 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1306 minor-latin;mso-hansi-theme-font:minor-latin'> 9.0</span></b>, respectively, and1307 set the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1581 q</span></b> values to <b style='mso-bidi-font-weight:normal'><span 1582 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1583 mso-hansi-theme-font:minor-latin'>0.05</span></b> and <b style='mso-bidi-font-weight: 1584 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1585 minor-latin;mso-hansi-theme-font:minor-latin'>0.9</span></b>, respectively, and 1586 set the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1308 1587 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Start 1309 1588 azimuth</span></b> to <b style='mso-bidi-font-weight:normal'><span 1310 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1589 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1311 1590 mso-hansi-theme-font:minor-latin'>0</span></b>. Set the <b style='mso-bidi-font-weight: 1312 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1591 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1313 1592 minor-latin;mso-hansi-theme-font:minor-latin'>No. 2-theta bins</span></b> to <b 1314 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1593 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1315 1594 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>250</span></b>, 1316 1595 which is more appropriate for small angle scattering, and set the <b 1317 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1596 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1318 1597 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Bin style: 1319 1598 Constant step bins in</span></b> to <span class=GramE><b style='mso-bidi-font-weight: 1320 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1599 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1321 1600 minor-latin;mso-hansi-theme-font:minor-latin'>log(</span></b></span><b 1322 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1601 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1323 1602 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>q)</span></b>. 1324 1603 You should also check the <b style='mso-bidi-font-weight:normal'><span 1325 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1604 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1326 1605 mso-hansi-theme-font:minor-latin'>Apply sample absorption?</span></b> <span 1327 1606 class=GramE>and</span> <b style='mso-bidi-font-weight:normal'><span 1328 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1607 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1329 1608 mso-hansi-theme-font:minor-latin'>Apply polarization?</span></b> <span 1330 1609 class=GramE>boxes</span>; enter the measured <b style='mso-bidi-font-weight: 1331 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1610 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1332 1611 minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> (<b 1333 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1612 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1334 1613 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.818</span></b>) 1335 1614 for the glassy carbon sample. When done the <b style='mso-bidi-font-weight: 1336 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1615 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1337 1616 minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> data 1338 1617 window should look like</p> 1339 1618 1340 1619 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1341 id="Picture_x0020_ 29" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:472.5pt;1620 id="Picture_x0020_40" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:472.5pt; 1342 1621 height:388.5pt;visibility:visible;mso-wrap-style:square'> 1343 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image01 8.png"1344 o:title=""/> 1345 </v:shape><![endif]--><![if !vml]><img border=0width=630 height=5181346 src="Small%20Angle%20Image%20Processing_files/image01 8.png" v:shapes="Picture_x0020_29"><![endif]></span></p>1622 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image014.png" 1623 o:title=""/> 1624 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1625 src="Small%20Angle%20Image%20Processing_files/image014.png" v:shapes="Picture_x0020_40"><![endif]></span></p> 1347 1626 1348 1627 <p class=MsoNormal><o:p> </o:p></p> … … 1351 1630 1352 1631 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1353 id="Picture_x0020_ 28" o:spid="_x0000_i1049" type="#_x0000_t75" style='width:525pt;1632 id="Picture_x0020_41" o:spid="_x0000_i1049" type="#_x0000_t75" style='width:525pt; 1354 1633 height:450pt;visibility:visible;mso-wrap-style:square'> 1355 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image01 9.png"1356 o:title=""/> 1357 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001358 src="Small%20Angle%20Image%20Processing_files/image01 9.png" v:shapes="Picture_x0020_28"><![endif]></span></p>1634 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image015.png" 1635 o:title=""/> 1636 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1637 src="Small%20Angle%20Image%20Processing_files/image015.png" v:shapes="Picture_x0020_41"><![endif]></span></p> 1359 1638 1360 1639 <p class=MsoNormal><o:p> </o:p></p> 1361 1640 1362 1641 <p class=MsoNormal>Now copy these controls to the other images. Do <b 1363 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1642 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1364 1643 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Copy 1365 1644 controls</span></b> and select just the <b style='mso-bidi-font-weight:normal'><span 1366 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1645 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1367 1646 mso-hansi-theme-font:minor-latin'>Sa1-4</span></b> data names. </p> 1368 1647 1369 1648 <p class=MsoNormal>We now need to go to the <b style='mso-bidi-font-weight: 1370 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1649 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1371 1650 minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> for 1372 each of <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1651 each of <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1373 1652 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sa1-Sa4</span></b> 1374 1653 to enter the correct transmission for each and change the Dark & Background 1375 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1654 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1376 1655 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> 1377 1656 to account for the different exposure times. Start with <b style='mso-bidi-font-weight: 1378 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1657 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1379 1658 minor-latin;mso-hansi-theme-font:minor-latin'>IMG Sa1_40s_067.tif</span></b> 1380 1659 and change <b style='mso-bidi-font-weight:normal'><span style='font-family: 1381 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1660 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1382 1661 minor-latin'>transmission</span></b> to <b style='mso-bidi-font-weight:normal'><span 1383 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1662 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1384 1663 mso-hansi-theme-font:minor-latin'>0.943</span></b> and the two <b 1385 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1664 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1386 1665 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> 1387 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1666 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1388 1667 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. 1389 1668 Then go to <b style='mso-bidi-font-weight:normal'><span style='font-family: 1390 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1669 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1391 1670 minor-latin'>IMG Sa2_40s_069.tif</span></b> and change <b style='mso-bidi-font-weight: 1392 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1671 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1393 1672 minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> to <b 1394 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1673 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1395 1674 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.979</span></b>; 1396 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1675 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1397 1676 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> 1398 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1677 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1399 1678 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. 1400 Next go <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1679 Next go <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1401 1680 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>to IMG 1402 1681 Sa3_40s_059.tif</span></b> and change <b style='mso-bidi-font-weight:normal'><span 1403 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1682 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1404 1683 mso-hansi-theme-font:minor-latin'>transmission</span></b> to <b 1405 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1684 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1406 1685 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.960</span></b>; 1407 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1686 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1408 1687 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> 1409 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1688 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1410 1689 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. 1411 1690 Finally, go to <b style='mso-bidi-font-weight:normal'><span style='font-family: 1412 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1691 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1413 1692 minor-latin'>IMG Sa4_40s_061.tif</span></b> and change <b style='mso-bidi-font-weight: 1414 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1693 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1415 1694 minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> to <b 1416 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1695 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1417 1696 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.968</span></b>; 1418 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1697 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1419 1698 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> 1420 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1699 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1421 1700 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. 1422 The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1701 The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1423 1702 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 1424 1703 Controls</span></b> data window for this should look like</p> 1425 1704 1426 1705 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1427 id="Picture_x0020_ 38" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:472.5pt;1706 id="Picture_x0020_43" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:472.5pt; 1428 1707 height:388.5pt;visibility:visible;mso-wrap-style:square'> 1429 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 20.png"1430 o:title=""/> 1431 </v:shape><![endif]--><![if !vml]><img border=0width=630 height=5181432 src="Small%20Angle%20Image%20Processing_files/image0 20.png" v:shapes="Picture_x0020_38"><![endif]></span></p>1708 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image016.png" 1709 o:title=""/> 1710 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1711 src="Small%20Angle%20Image%20Processing_files/image016.png" v:shapes="Picture_x0020_43"><![endif]></span></p> 1433 1712 1434 1713 <p class=MsoNormal><o:p> </o:p></p> 1435 1714 1436 1715 <p class=MsoNormal>This is a reasonable time to save the project; do <b 1437 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1716 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1438 1717 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/Save 1439 1718 project as 1440 1719 </span></b> from the main GSAS-II data tree menu. Choose a file name 1441 1720 (I assumed <b style='mso-bidi-font-weight:normal'><span style='font-family: 1442 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1721 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1443 1722 minor-latin'>image</span></b>) and it will be written on the local file 1444 1723 directory. </p> … … 1446 1725 <p class=MsoNormal>As noted earlier, the images contain some unwanted features; 1447 1726 so lets create masks to remove them. Select <b style='mso-bidi-font-weight: 1448 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1727 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1449 1728 minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> from the GSAS-II 1450 1729 data tree under <b style='mso-bidi-font-weight:normal'><span style='font-family: 1451 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1730 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1452 1731 minor-latin'>IMG GC_5s_200.tif</span></b>; the data window will show</p> 1453 1732 … … 1455 1734 id="Picture_x0020_17" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:337.5pt; 1456 1735 height:99.75pt;visibility:visible;mso-wrap-style:square'> 1457 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 21.png"1458 o:title=""/> 1459 </v:shape><![endif]--><![if !vml]><img border=0width=450 height=1331460 src="Small%20Angle%20Image%20Processing_files/image0 21.png" v:shapes="Picture_x0020_17"><![endif]></span></p>1736 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image017.png" 1737 o:title=""/> 1738 </v:shape><![endif]--><![if !vml]><img width=450 height=133 1739 src="Small%20Angle%20Image%20Processing_files/image017.png" v:shapes="Picture_x0020_17"><![endif]></span></p> 1461 1740 1462 1741 <p class=MsoNormal><o:p> </o:p></p> … … 1464 1743 <p class=MsoNormal>To mask out the regions beyond the circular <span 1465 1744 class=SpellE>MarCCD</span> image change the <span class=GramE><b 1466 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1745 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1467 1746 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Lower<span 1468 1747 style='mso-spacerun:yes'> </span><span class=SpellE>threshhold</span></span></b></span> 1469 from <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1748 from <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1470 1749 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0</span></b> 1471 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1750 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1472 1751 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1</span></b>; 1473 1752 the image will be redrawn with these regions in red</p> 1474 1753 1475 1754 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1476 id="Picture_x0020_ 30" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:525pt;1755 id="Picture_x0020_45" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:525pt; 1477 1756 height:450pt;visibility:visible;mso-wrap-style:square'> 1478 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 22.png"1479 o:title=""/> 1480 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001481 src="Small%20Angle%20Image%20Processing_files/image0 22.png" v:shapes="Picture_x0020_30"><![endif]></span></p>1757 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image018.png" 1758 o:title=""/> 1759 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1760 src="Small%20Angle%20Image%20Processing_files/image018.png" v:shapes="Picture_x0020_45"><![endif]></span></p> 1482 1761 1483 1762 <p class=MsoNormal><o:p> </o:p></p> 1484 1763 1485 1764 <p class=MsoNormal>These are now excluded. The status line for the <b 1486 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1765 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1487 1766 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> 1488 1767 data window gives the directions for adding additional masks. You can make arcs … … 1494 1773 1495 1774 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1496 id="Picture_x0020_ 19" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:525pt;1775 id="Picture_x0020_62" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:525pt; 1497 1776 height:450pt;visibility:visible;mso-wrap-style:square'> 1498 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 23.png"1499 o:title=""/> 1500 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001501 src="Small%20Angle%20Image%20Processing_files/image0 23.png" v:shapes="Picture_x0020_19"><![endif]></span></p>1777 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image019.png" 1778 o:title=""/> 1779 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1780 src="Small%20Angle%20Image%20Processing_files/image019.png" v:shapes="Picture_x0020_62"><![endif]></span></p> 1502 1781 1503 1782 <p class=MsoNormal><o:p> </o:p></p> … … 1505 1784 <p class=MsoNormal>To add the mask 1: be sure the focus is on the image and the 1506 1785 zoom buttons are off, 2: type <span class=GramE><b style='mso-bidi-font-weight: 1507 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1786 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1508 1787 minor-latin;mso-hansi-theme-font:minor-latin'>a</span></b> to</span> activate 1509 1788 the arc mask entry 3: press the left mouse button (<b style='mso-bidi-font-weight: 1510 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1789 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1511 1790 minor-latin;mso-hansi-theme-font:minor-latin'>LB</span></b>) with the cursor 1512 1791 centered on the bad arc. The <b style='mso-bidi-font-weight:normal'><span 1513 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1792 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1514 1793 mso-hansi-theme-font:minor-latin'>Masks</span></b> window will show a new entry 1515 1794 </p> 1516 1795 1517 1796 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1518 id="Picture_x0020_ 20" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:337.5pt;1519 height:13 5pt;visibility:visible;mso-wrap-style:square'>1520 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image02 4.png"1521 o:title=""/> 1522 </v:shape><![endif]--><![if !vml]><img border=0 width=450 height=1801523 src="Small%20Angle%20Image%20Processing_files/image02 4.png" v:shapes="Picture_x0020_20"><![endif]></span><span1797 id="Picture_x0020_63" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:342pt; 1798 height:136.5pt;visibility:visible;mso-wrap-style:square'> 1799 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image020.png" 1800 o:title=""/> 1801 </v:shape><![endif]--><![if !vml]><img width=456 height=182 1802 src="Small%20Angle%20Image%20Processing_files/image020.png" v:shapes="Picture_x0020_63"><![endif]></span><span 1524 1803 style='mso-spacerun:yes'> </span></p> 1525 1804 … … 1530 1809 1531 1810 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1532 id="Picture_x0020_ 22" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:525pt;1811 id="Picture_x0020_64" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:525pt; 1533 1812 height:450pt;visibility:visible;mso-wrap-style:square'> 1534 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image02 5.png"1535 o:title=""/> 1536 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001537 src="Small%20Angle%20Image%20Processing_files/image02 5.png" v:shapes="Picture_x0020_22"><![endif]></span></p>1813 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image021.png" 1814 o:title=""/> 1815 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1816 src="Small%20Angle%20Image%20Processing_files/image021.png" v:shapes="Picture_x0020_64"><![endif]></span></p> 1538 1817 1539 1818 <p class=MsoNormal><o:p> </o:p></p> 1540 1819 1541 1820 <p class=MsoNormal>You can change the angular width of the arc by changing <b 1542 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1821 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1543 1822 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>thickness</span></b> 1544 in the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1823 in the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1545 1824 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> 1546 1825 data window, you can change the angular range of the arc by dragging either end 1547 of the arc , and you can move the arc<span style='mso-spacerun:yes'>1548 </span>along a constant 2Θ angle by dragging on any point inside the mask. 1549 The curvature is centered on the beam center position and follows a constant 1550 2Θ curve established by the detector calibration.<span style='mso-no-proof: 1551 yes'> <!--[if gte vml 1]><v:shape id="Picture_x0020_34" o:spid="_x0000_i1042" 1552 type="#_x0000_t75" style='width:525pt;height:450pt;visibility:visible; 1553 mso-wrap-style:square'> 1554 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image026.png"1555 o:title=""/>1556 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 1557 src="Small%20Angle%20Image%20Processing_files/image026.png" v:shapes="Picture_x0020_34"><![endif]></span></p>1558 1559 <p class=MsoNormal><o:p> </o:p></p>1826 of the arc (NB: increments only in whole degrees), and you can move the 1827 arc<span style='mso-spacerun:yes'> </span>along a constant 2Θ angle by 1828 dragging on any point inside the mask. The curvature is centered on the beam 1829 center position and follows a constant 2Θ curve established by the 1830 detector calibration.<span style='mso-no-proof:yes'> </span></p> 1831 1832 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1833 id="Picture_x0020_65" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:525pt; 1834 height:450pt;visibility:visible;mso-wrap-style:square'> 1835 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image022.png" 1836 o:title=""/> 1837 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1838 src="Small%20Angle%20Image%20Processing_files/image022.png" v:shapes="Picture_x0020_65"><![endif]></span></p> 1560 1839 1561 1840 <p class=MsoNormal>Next lets deal with the beam stop. Im going to use both a 1562 polygon and a spot to cover it. Move the zoom area to be around the center, 1563 makesure the zoom buttons are off, enter <b style='mso-bidi-font-weight:normal'><span1564 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1841 polygon and a spot to cover it. Move the zoom area to be around the center, make 1842 sure the zoom buttons are off, enter <b style='mso-bidi-font-weight:normal'><span 1843 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1565 1844 mso-hansi-theme-font:minor-latin'>s</span></b> on the plot and press mouse <b 1566 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1845 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1567 1846 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>LB</span></b> 1568 1847 with the cursor positioned where you want the spot. A 1mm diameter red circle … … 1570 1849 1571 1850 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1572 id="Picture_x0020_ 35" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:525pt;1851 id="Picture_x0020_66" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:525pt; 1573 1852 height:450pt;visibility:visible;mso-wrap-style:square'> 1574 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image02 7.png"1575 o:title=""/> 1576 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001577 src="Small%20Angle%20Image%20Processing_files/image02 7.png" v:shapes="Picture_x0020_35"><![endif]></span></p>1853 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image023.png" 1854 o:title=""/> 1855 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1856 src="Small%20Angle%20Image%20Processing_files/image023.png" v:shapes="Picture_x0020_66"><![endif]></span></p> 1578 1857 1579 1858 <p class=MsoNormal><o:p> </o:p></p> 1580 1859 1581 1860 <p class=MsoNormal>And the <b style='mso-bidi-font-weight:normal'><span 1582 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1861 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1583 1862 mso-hansi-theme-font:minor-latin'>Masks</span></b> window will have new 1584 1863 information</p> … … 1587 1866 id="Picture_x0020_24" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:337.5pt; 1588 1867 height:170.25pt;visibility:visible;mso-wrap-style:square'> 1589 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image02 8.png"1590 o:title=""/> 1591 </v:shape><![endif]--><![if !vml]><img border=0width=450 height=2271592 src="Small%20Angle%20Image%20Processing_files/image02 8.png" v:shapes="Picture_x0020_24"><![endif]></span></p>1868 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image024.png" 1869 o:title=""/> 1870 </v:shape><![endif]--><![if !vml]><img width=450 height=227 1871 src="Small%20Angle%20Image%20Processing_files/image024.png" v:shapes="Picture_x0020_24"><![endif]></span></p> 1593 1872 1594 1873 <p class=MsoNormal><o:p> </o:p></p> 1595 1874 1596 1875 <p class=MsoNormal>You can change the diameter of the spot, I used <b 1597 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1876 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1598 1877 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>7.0</span></b>; 1599 1878 the plot now shows a ring that just covers the beam stop. You may have to drag … … 1601 1880 1602 1881 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1603 id="Picture_x0020_ 36" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:525pt;1882 id="Picture_x0020_67" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:525pt; 1604 1883 height:450pt;visibility:visible;mso-wrap-style:square'> 1605 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image02 9.png"1606 o:title=""/> 1607 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001608 src="Small%20Angle%20Image%20Processing_files/image02 9.png" v:shapes="Picture_x0020_36"><![endif]></span></p>1884 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image025.png" 1885 o:title=""/> 1886 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1887 src="Small%20Angle%20Image%20Processing_files/image025.png" v:shapes="Picture_x0020_67"><![endif]></span></p> 1609 1888 1610 1889 <p class=MsoNormal><o:p> </o:p></p> … … 1613 1892 use a 4 sided polygon for this. Adjust the zoom & position so you can see 1614 1893 the entire beam stop stick. Make sure all zoom buttons are off, press <b 1615 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1894 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1616 1895 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>p</span></b> 1617 1896 on the plot, then press the mouse <b style='mso-bidi-font-weight:normal'><span 1618 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1897 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1619 1898 mso-hansi-theme-font:minor-latin'>LB</span></b> at four points in succession 1620 1899 around the beam stop stick. A line segment for the polygon will be drawn 1621 1900 following your mouse clicks. Finally press the mouse <b style='mso-bidi-font-weight: 1622 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1901 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1623 1902 minor-latin;mso-hansi-theme-font:minor-latin'>RB</span></b> to close the 1624 1903 polygon. You should see something like</p> 1625 1904 1626 1905 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1627 id="Picture_x0020_ 37" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:525pt;1906 id="Picture_x0020_68" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:525pt; 1628 1907 height:450pt;visibility:visible;mso-wrap-style:square'> 1629 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 30.png"1630 o:title=""/> 1631 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001632 src="Small%20Angle%20Image%20Processing_files/image0 30.png" v:shapes="Picture_x0020_37"><![endif]></span></p>1908 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image026.png" 1909 o:title=""/> 1910 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1911 src="Small%20Angle%20Image%20Processing_files/image026.png" v:shapes="Picture_x0020_68"><![endif]></span></p> 1633 1912 1634 1913 <p class=MsoNormal><o:p> </o:p></p> … … 1636 1915 <p class=MsoNormal>You can adjust the position of the polygon vertices by 1637 1916 closely dragging it with mouse <b style='mso-bidi-font-weight:normal'><span 1638 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1639 mso-hansi-theme-font:minor-latin'>LB</span></b> pressed; a new vertex can be 1640 addedby dragging an existing vertex with the mouse <b style='mso-bidi-font-weight:1641 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1917 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1918 mso-hansi-theme-font:minor-latin'>LB</span></b> pressed; a new vertex can be added 1919 by dragging an existing vertex with the mouse <b style='mso-bidi-font-weight: 1920 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1642 1921 minor-latin;mso-hansi-theme-font:minor-latin'>RB</span></b> pressed. If you 1643 1922 drag one vertex onto another, they are merged and cannot be separated.</p> 1644 1923 1645 <p class=MsoNormal>We want to use these masks for all the Sa1-4 images. <span1646 class=GramE>Do</span> <b style='mso-bidi-font-weight:normal'><span 1647 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1648 m so-hansi-theme-font:minor-latin'>Operations/Copy mask</span></b>; a <b1649 style=' mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";1650 mso- ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Copy mask1651 information</span></b> dialog box will appear. Select the <b style='mso-bidi-font-weight: 1652 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1653 m inor-latin;mso-hansi-theme-font:minor-latin'>Sa1-4</span></b> items and press <b1654 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1924 <p class=MsoNormal>We want to use these masks for all the Sa1-4 images. Do <b 1925 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1926 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Copy 1927 mask</span></b>; a <b style='mso-bidi-font-weight:normal'><span 1928 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1929 mso-hansi-theme-font:minor-latin'>Copy mask information</span></b> dialog box will 1930 appear. Select the <b style='mso-bidi-font-weight:normal'><span 1931 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1932 mso-hansi-theme-font:minor-latin'>Sa1-4</span></b> items and press <b 1933 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1655 1934 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ok</span></b>. 1656 1935 Here is a useful place to save your project; do <b style='mso-bidi-font-weight: 1657 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1936 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1658 1937 minor-latin;mso-hansi-theme-font:minor-latin'>File/Save project</span></b> from 1659 1938 the main GSAS-II data tree menu.</p> … … 1663 1942 <p class=MsoNormal>We are now ready to integrate the glassy carbon and the four 1664 1943 <span class=GramE>Sa</span> images. Select any <b style='mso-bidi-font-weight: 1665 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1944 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1666 1945 minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> and 1667 then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1946 then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1668 1947 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Integrate 1669 all</span></b>. A selection dialog will appear; select only the GC and Sa1-Sa4 1670 data sets and press Ok. The image integration will proceed; a progress bar 1671 shows as each one is done. Five SASD data items will appear on the GSAS-II data 1672 tree; the last one (<b style='mso-bidi-font-weight:normal'><span 1673 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1948 all</span></b>. A selection dialog will appear; select only the <b 1949 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1950 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>GC</span></b> 1951 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1952 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sa1-Sa4</span></b> 1953 data sets and press <b style='mso-bidi-font-weight:normal'><span 1954 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1955 mso-hansi-theme-font:minor-latin'>Ok</span></b>. The image integration will 1956 proceed; a progress bar shows as each one is done. Five SASD data items will appear 1957 on the GSAS-II data tree; the last one (<b style='mso-bidi-font-weight:normal'><span 1958 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1674 1959 mso-hansi-theme-font:minor-latin'>SASD Sa4_40s_061.tif <span class=SpellE>Azm</span>=45.00</span></b>) 1675 1960 will be expanded and plotted (you may have to select the <b style='mso-bidi-font-weight: 1676 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1961 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1677 1962 minor-latin;mso-hansi-theme-font:minor-latin'>Powder Patterns</span></b> tab to 1678 1963 see it).</p> 1679 1964 1680 1965 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1681 id=" Picture_x0020_39" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:525pt;1682 height:450pt;visibility:visible;mso-wrap-style:square'>1683 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 31.png"1684 o:title=""/> 1685 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001686 src="Small%20Angle%20Image%20Processing_files/image0 31.png" v:shapes="Picture_x0020_39"><![endif]></span></p>1966 id="_x0000_i1037" type="#_x0000_t75" style='width:525pt;height:450pt; 1967 visibility:visible;mso-wrap-style:square'> 1968 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image027.png" 1969 o:title=""/> 1970 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1971 src="Small%20Angle%20Image%20Processing_files/image027.png" v:shapes="_x0000_i1037"><![endif]></span></p> 1687 1972 1688 1973 <p class=MsoNormal><o:p> </o:p></p> … … 1693 1978 1694 1979 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1695 id="Picture_x0020_4 0" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt;1980 id="Picture_x0020_48" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt; 1696 1981 height:450pt;visibility:visible;mso-wrap-style:square'> 1697 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 32.png"1698 o:title=""/> 1699 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001700 src="Small%20Angle%20Image%20Processing_files/image0 32.png" v:shapes="Picture_x0020_40"><![endif]></span></p>1982 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image028.png" 1983 o:title=""/> 1984 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1985 src="Small%20Angle%20Image%20Processing_files/image028.png" v:shapes="Picture_x0020_48"><![endif]></span></p> 1701 1986 1702 1987 <p class=MsoNormal><o:p> </o:p></p> … … 1707 1992 absolute scaled glassy carbon scan. One of these is in the same directory as 1708 1993 the image data; do <b style='mso-bidi-font-weight:normal'><span 1709 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1994 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1710 1995 mso-hansi-theme-font:minor-latin'>Import/Small Angle Data/ from <span 1711 1996 class=GramE>q(</span>A-1) step X-ray QIE data file</span></b> and select <b 1712 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1997 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1713 1998 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>GC 1714 1999 calibrated data.txt</span></b> from the file selection dialog. You will need to 1715 select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2000 select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1716 2001 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>any <span 1717 2002 class=GramE>file(</span>*.*)</span></b> to see it. A <b style='mso-bidi-font-weight: 1718 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1719 minor-latin;mso-hansi-theme-font:minor-latin'>Is <span class=GramE>this the</span>1720 file you want</span></b> dialog will appear respond <b style='mso-bidi-font-weight: 1721 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1722 m inor-latin;mso-hansi-theme-font:minor-latin'>Yes</span></b> to read the file;1723 it will beplotted.</p>1724 1725 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1726 id="Picture_x0020_4 1" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:525pt;2003 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2004 minor-latin;mso-hansi-theme-font:minor-latin'>Is this the file you want</span></b> 2005 dialog will appear respond <b style='mso-bidi-font-weight:normal'><span 2006 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2007 mso-hansi-theme-font:minor-latin'>Yes</span></b> to read the file; it will be 2008 plotted.</p> 2009 2010 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 2011 id="Picture_x0020_49" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:525pt; 1727 2012 height:450pt;visibility:visible;mso-wrap-style:square'> 1728 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 33.png"1729 o:title=""/> 1730 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001731 src="Small%20Angle%20Image%20Processing_files/image0 33.png" v:shapes="Picture_x0020_41"><![endif]></span></p>2013 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image029.png" 2014 o:title=""/> 2015 </v:shape><![endif]--><![if !vml]><img width=700 height=600 2016 src="Small%20Angle%20Image%20Processing_files/image029.png" v:shapes="Picture_x0020_49"><![endif]></span></p> 1732 2017 1733 2018 <p class=MsoNormal><o:p> </o:p></p> 1734 2019 1735 2020 <p class=MsoNormal>If you enter <b style='mso-bidi-font-weight:normal'><span 1736 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2021 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1737 2022 mso-hansi-theme-font:minor-latin'>m</span></b> on the plot window, all of the 1738 2023 SASD patterns will be plotted together (Ive adjusted the zoom to see them … … 1740 2025 1741 2026 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1742 id="Picture_x0020_ 42" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt;2027 id="Picture_x0020_50" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt; 1743 2028 height:450pt;visibility:visible;mso-wrap-style:square'> 1744 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image03 4.png"1745 o:title=""/> 1746 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001747 src="Small%20Angle%20Image%20Processing_files/image03 4.png" v:shapes="Picture_x0020_42"><![endif]></span></p>2029 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image030.png" 2030 o:title=""/> 2031 </v:shape><![endif]--><![if !vml]><img width=700 height=600 2032 src="Small%20Angle%20Image%20Processing_files/image030.png" v:shapes="Picture_x0020_50"><![endif]></span></p> 1748 2033 1749 2034 <p class=MsoNormal><o:p> </o:p></p> … … 1752 2037 have them on absolute scale. First is to discover the scaling between the two 1753 2038 glassy carbon patterns. Go to the measured one (<b style='mso-bidi-font-weight: 1754 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:2039 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1755 2040 minor-latin;mso-hansi-theme-font:minor-latin'>SASD GC_5s_200.tif</span></b>) 1756 2041 and select <b style='mso-bidi-font-weight:normal'><span style='font-family: 1757 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:2042 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1758 2043 minor-latin'>Sample Parameters</span></b>.</p> 1759 2044 1760 2045 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1761 id="Picture_x0020_ 43" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:291.75pt;1762 height: 388.5pt;visibility:visible;mso-wrap-style:square'>1763 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image03 5.png"1764 o:title=""/> 1765 </v:shape><![endif]--><![if !vml]><img border=0 width=389 height=5181766 src="Small%20Angle%20Image%20Processing_files/image03 5.png" v:shapes="Picture_x0020_43"><![endif]></span></p>2046 id="Picture_x0020_51" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:291.75pt; 2047 height:408pt;visibility:visible;mso-wrap-style:square'> 2048 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image031.png" 2049 o:title=""/> 2050 </v:shape><![endif]--><![if !vml]><img width=389 height=544 2051 src="Small%20Angle%20Image%20Processing_files/image031.png" v:shapes="Picture_x0020_51"><![endif]></span></p> 1767 2052 1768 2053 <p class=MsoNormal><o:p> </o:p></p> 1769 2054 1770 2055 <p class=MsoNormal>We will change <b style='mso-bidi-font-weight:normal'><span 1771 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2056 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1772 2057 mso-hansi-theme-font:minor-latin'>Histogram scale factor</span></b> by 1773 2058 comparison with the absolute glassy carbon scan. Do <b style='mso-bidi-font-weight: 1774 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:2059 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1775 2060 minor-latin;mso-hansi-theme-font:minor-latin'>Command/Set scale</span></b> from 1776 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2061 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1777 2062 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sample 1778 2063 Parameters</span></b> menu; a <b style='mso-bidi-font-weight:normal'><span 1779 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2064 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1780 2065 mso-hansi-theme-font:minor-latin'>Reference histogram</span></b> dialog will 1781 2066 appear.</p> … … 1784 2069 id="Picture_x0020_44" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:259.5pt; 1785 2070 height:252pt;visibility:visible;mso-wrap-style:square'> 1786 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image03 6.png"1787 o:title=""/> 1788 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=3361789 src="Small%20Angle%20Image%20Processing_files/image03 6.png" v:shapes="Picture_x0020_44"><![endif]></span></p>2071 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image032.png" 2072 o:title=""/> 2073 </v:shape><![endif]--><![if !vml]><img width=346 height=336 2074 src="Small%20Angle%20Image%20Processing_files/image032.png" v:shapes="Picture_x0020_44"><![endif]></span></p> 1790 2075 1791 2076 <p class=MsoNormal><o:p> </o:p></p> 1792 2077 1793 2078 <p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span 1794 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2079 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1795 2080 mso-hansi-theme-font:minor-latin'>SASD GC calibrated data.txt</span></b> (shown 1796 2081 in blue above) and press <b style='mso-bidi-font-weight:normal'><span 1797 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2082 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1798 2083 mso-hansi-theme-font:minor-latin'>Ok</span></b>; the <b style='mso-bidi-font-weight: 1799 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:2084 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1800 2085 minor-latin;mso-hansi-theme-font:minor-latin'>GC_5s_200.tif</span></b> data 1801 2086 will be rescaled to the <b style='mso-bidi-font-weight:normal'><span 1802 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2087 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1803 2088 mso-hansi-theme-font:minor-latin'>GC calibrated data</span></b> and the <b 1804 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2089 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1805 2090 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Histogram 1806 2091 scale factor</span></b> will be changed to the new scaling factor (<b 1807 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2092 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1808 2093 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.0008536</span></b>). 1809 2094 The plot will be redrawn with the scaled data.</p> 1810 2095 1811 2096 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1812 id="Picture_x0020_ 45" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt;2097 id="Picture_x0020_52" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt; 1813 2098 height:450pt;visibility:visible;mso-wrap-style:square'> 1814 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image03 7.png"1815 o:title=""/> 1816 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001817 src="Small%20Angle%20Image%20Processing_files/image03 7.png" v:shapes="Picture_x0020_45"><![endif]></span></p>2099 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image033.png" 2100 o:title=""/> 2101 </v:shape><![endif]--><![if !vml]><img width=700 height=600 2102 src="Small%20Angle%20Image%20Processing_files/image033.png" v:shapes="Picture_x0020_52"><![endif]></span></p> 1818 2103 1819 2104 <p class=MsoNormal><o:p> </o:p></p> … … 1822 2107 contribution to the standard that is not present in our measured one. Next we 1823 2108 have to apply this scale factor to the Sa1-Sa4 data sets. Do <b 1824 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2109 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1825 2110 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Command/Copy 1826 2111 selected 1827 2112 </span></b> from the <b style='mso-bidi-font-weight:normal'><span 1828 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2113 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1829 2114 mso-hansi-theme-font:minor-latin'>Sample Parameters</span></b> menu; a <b 1830 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2115 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1831 2116 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Select 1832 2117 sample parameters</span></b> dialog will appear</p> … … 1835 2120 id="Picture_x0020_46" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:240pt; 1836 2121 height:232.5pt;visibility:visible;mso-wrap-style:square'> 1837 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image03 8.png"1838 o:title=""/> 1839 </v:shape><![endif]--><![if !vml]><img border=0width=320 height=3101840 src="Small%20Angle%20Image%20Processing_files/image03 8.png" v:shapes="Picture_x0020_46"><![endif]></span></p>2122 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image034.png" 2123 o:title=""/> 2124 </v:shape><![endif]--><![if !vml]><img width=320 height=310 2125 src="Small%20Angle%20Image%20Processing_files/image034.png" v:shapes="Picture_x0020_46"><![endif]></span></p> 1841 2126 1842 2127 <p class=MsoNormal><o:p> </o:p></p> 1843 2128 1844 2129 <p class=MsoNormal>Select only <b style='mso-bidi-font-weight:normal'><span 1845 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2130 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1846 2131 mso-hansi-theme-font:minor-latin'>Histogram scale factor</span></b> and press <b 1847 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2132 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1848 2133 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ok</span></b>; 1849 a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2134 a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1850 2135 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Copy sample 1851 2136 parameters</span></b> dialog will appear</p> … … 1854 2139 id="Picture_x0020_47" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:240pt; 1855 2140 height:232.5pt;visibility:visible;mso-wrap-style:square'> 1856 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image03 9.png"1857 o:title=""/> 1858 </v:shape><![endif]--><![if !vml]><img border=0width=320 height=3101859 src="Small%20Angle%20Image%20Processing_files/image03 9.png" v:shapes="Picture_x0020_47"><![endif]></span></p>2141 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image035.png" 2142 o:title=""/> 2143 </v:shape><![endif]--><![if !vml]><img width=320 height=310 2144 src="Small%20Angle%20Image%20Processing_files/image035.png" v:shapes="Picture_x0020_47"><![endif]></span></p> 1860 2145 1861 2146 <p class=MsoNormal><o:p> </o:p></p> 1862 2147 1863 2148 <p class=MsoNormal>Select only the <b style='mso-bidi-font-weight:normal'><span 1864 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2149 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1865 2150 mso-hansi-theme-font:minor-latin'>Sa1-Sa4</span></b> data sets and press <b 1866 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2151 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1867 2152 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ok</span></b>. 1868 2153 The copy will occur and the plot redrawn</p> 1869 2154 1870 2155 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1871 id="Picture_x0020_ 48" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:525pt;2156 id="Picture_x0020_53" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:525pt; 1872 2157 height:450pt;visibility:visible;mso-wrap-style:square'> 1873 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 40.png"1874 o:title=""/> 1875 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001876 src="Small%20Angle%20Image%20Processing_files/image0 40.png" v:shapes="Picture_x0020_48"><![endif]></span></p>2158 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image036.png" 2159 o:title=""/> 2160 </v:shape><![endif]--><![if !vml]><img width=700 height=600 2161 src="Small%20Angle%20Image%20Processing_files/image036.png" v:shapes="Picture_x0020_53"><![endif]></span></p> 1877 2162 1878 2163 <p class=MsoNormal><o:p> </o:p></p> … … 1881 2166 done; the scales for the Sa1-Sa4 data sets have to be further reduced by a 1882 2167 factor of 8 to account for the longer exposure time. Select <b 1883 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2168 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1884 2169 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD 1885 2170 Sa1_40s_067.tif</span></b> from the GSAS-II data tree, expand it and choose <b 1886 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2171 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1887 2172 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sample 1888 2173 Parameters</span></b></p> 1889 2174 1890 2175 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1891 id="Picture_x0020_ 49" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:291.75pt;1892 height: 388.5pt;visibility:visible;mso-wrap-style:square'>1893 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 41.png"1894 o:title=""/> 1895 </v:shape><![endif]--><![if !vml]><img border=0 width=389 height=5181896 src="Small%20Angle%20Image%20Processing_files/image0 41.png" v:shapes="Picture_x0020_49"><![endif]></span></p>2176 id="Picture_x0020_54" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:291.75pt; 2177 height:408pt;visibility:visible;mso-wrap-style:square'> 2178 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image037.png" 2179 o:title=""/> 2180 </v:shape><![endif]--><![if !vml]><img width=389 height=544 2181 src="Small%20Angle%20Image%20Processing_files/image037.png" v:shapes="Picture_x0020_54"><![endif]></span></p> 1897 2182 1898 2183 <p class=MsoNormal><o:p> </o:p></p> 1899 2184 1900 2185 <p class=MsoNormal>The data items here can take simple mathematical expressions 1901 so change <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2186 so change <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1902 2187 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Histogram 1903 2188 scale factor</span></b> to <b style='mso-bidi-font-weight:normal'><span 1904 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2189 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1905 2190 mso-hansi-theme-font:minor-latin'>0.0008536/8</span></b> and press <b 1906 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";2191 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1907 2192 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Enter</span></b>. 1908 2193 The value will change to <b style='mso-bidi-font-weight:normal'><span 1909 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2194 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1910 2195 mso-hansi-theme-font:minor-latin'>0.0001067</span></b> and the plot redrawn.</p> 1911 2196 1912 2197 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1913 id="Picture_x0020_5 0" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:525pt;2198 id="Picture_x0020_56" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:525pt; 1914 2199 height:450pt;visibility:visible;mso-wrap-style:square'> 1915 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 42.png"1916 o:title=""/> 1917 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001918 src="Small%20Angle%20Image%20Processing_files/image0 42.png" v:shapes="Picture_x0020_50"><![endif]></span></p>2200 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image038.png" 2201 o:title=""/> 2202 </v:shape><![endif]--><![if !vml]><img width=700 height=600 2203 src="Small%20Angle%20Image%20Processing_files/image038.png" v:shapes="Picture_x0020_56"><![endif]></span></p> 1919 2204 1920 2205 <p class=MsoNormal><o:p> </o:p></p> 1921 2206 1922 2207 <p class=MsoNormal>Next do <b style='mso-bidi-font-weight:normal'><span 1923 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2208 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1924 2209 mso-hansi-theme-font:minor-latin'>Command/Copy selected</span></b> as before to 1925 2210 copy this new scale factor to the other <span class=GramE>Sa</span> data sets. … … 1927 2212 1928 2213 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1929 id="Picture_x0020_5 1" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;2214 id="Picture_x0020_57" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt; 1930 2215 height:450pt;visibility:visible;mso-wrap-style:square'> 1931 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image0 43.png"1932 o:title=""/> 1933 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001934 src="Small%20Angle%20Image%20Processing_files/image0 43.png" v:shapes="Picture_x0020_51"><![endif]></span></p>2216 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image039.png" 2217 o:title=""/> 2218 </v:shape><![endif]--><![if !vml]><img width=700 height=600 2219 src="Small%20Angle%20Image%20Processing_files/image039.png" v:shapes="Picture_x0020_57"><![endif]></span></p> 1935 2220 1936 2221 <p class=MsoNormal><o:p> </o:p></p> … … 1939 2224 samples are quite weak small angle <span class=SpellE>scatterers</span>. This 1940 2225 is a good point to do a <b style='mso-bidi-font-weight:normal'><span 1941 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;2226 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1942 2227 mso-hansi-theme-font:minor-latin'>File/Save project</span></b> from the main 1943 2228 GSAS-II data tree menu. You can try to fit unified & <span class=SpellE>Porod</span> 1944 2229 models to them following the procedures demonstrated in the <strong><span 1945 style='font-weight:normal ;mso-bidi-font-weight:bold'><a1946 href="Fitting%20Small%20Angle%20Scattering%20Data.htm"><span style='mso-bidi-font-weight: 1947 normal'>Fitting Small Angle X-Ray Data</span></a> tutorial. Id set the high Q 1948 limit to about 0.25Å<sup>-1</sup> as above that is only noisybackground.</span></strong></p>2230 style='font-weight:normal'>Fitting Small Angle X-Ray Data</span></strong><strong><span 2231 style='font-weight:normal;mso-bidi-font-weight:bold'> tutorial. Id set the 2232 high Q limit to about 0.25Å<sup>-1</sup> as above that is only noisy 2233 background.</span></strong></p> 1949 2234 1950 2235 </div> -
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