Changeset 898
- Timestamp:
- May 8, 2013 1:02:28 PM (11 years ago)
- Location:
- trunk/help
- Files:
-
- 2 edited
Legend:
- Unmodified
- Added
- Removed
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trunk/help/Calibration of an area detector in GSAS.htm
r895 r898 904 904 905 905 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>The plot window shows 906 the image; notice the elliptical shape of the powder diffraction rings. The 906 the image; notice the elliptical shape of the powder diffraction rings 907 due to the 45 degree detector tilt. The 907 908 blue <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 908 909 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 909 910 Calibri;mso-bidi-theme-font:minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span></b> 910 marks the default beam location (image center); your calibration will correctly 911 place it. Also notice that the values shown in the plot window status bar (at 912 bottom of plot window) change as you move the cursor over the plot; these 913 values are at present in error as they are computed from the default 914 calibration values. They will be correct after you finish the calibration.</p> 911 marks the beam location (which defaults to the image center); the 912 calibration you will perform here will find the correct 913 placement for it. Also note that as the mouse is moved across the plot 914 the plot window status bar (at bottom of plot window) shows the 915 cursor position, as computed from the default (incorrect) 916 calibration values. These constants will be correctly determined after you finish the calibration.</p> 915 917 916 918 <p class=MsoNormal><span style='mso-spacerun:yes'> </span><span … … 1004 1006 1005 1007 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>To remove a point 1006 added in error click on that point with the right mouse button [on the Mac, if1007 you have a single-button mouse, hold the Command (<span style='font-family: 1008 "Cambria Math","serif";mso-bidi-font-family:"Cambria Math"'>⌘</span>) key 1009 down and click].</p>1008 added in error click on that point with the right mouse button 1009 (on the Mac, if you have a single-button mouse, hold the shift and control keys 1010 down and click). 1011 </p> 1010 1012 1011 1013 <h3><span style='mso-spacerun:yes'> </span>Fourth:</h3> 1012 1014 1013 1015 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>When done, press the 1014 right mouse button well away from any points that have been added [on the Mac,1015 if you have a single-button mouse, hold the Command (<span style='font-family: 1016 "Cambria Math","serif";mso-bidi-font-family:"Cambria Math"'>⌘</span>) key 1017 down and click].</p>1016 right mouse button well away from any points that have been added 1017 (on the Mac, if you have a single-button mouse, hold the shift and control keys 1018 down and click). 1019 </p> 1018 1020 1019 1021 <p class=MsoNormal>The calibration is then performed. First the rings are -
trunk/help/Fit Peaks.htm
r895 r898 1731 1731 new mineral <a href="http://en.wikipedia.org/wiki/Jadarite"><span class=SpellE>jadarite</span></a> 1732 1732 (aka <a href="http://en.wikipedia.org/wiki/Kryptonite">kryptonite</a>). The 1733 data w asalso collected on 11BM-B at APS. The unit cell is monoclinic so it is1733 data were also collected on 11BM-B at APS. The unit cell is monoclinic so it is 1734 1734 a more substantial test of the indexing capability of GSAS-II.</p> 1735 1735 … … 1770 1770 small ones); use <b style='mso-bidi-font-weight:normal'><span style='font-family: 1771 1771 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1772 minor-latin'>Auto search</span></b> to start and then fill in by hand. Note 1772 minor-latin'>Auto search</span></b> to start and then fill in by hand: 1773 Add peaks by left-clicking on a data point near the top of the 1774 peak. Peak positions can be moved by dragging the peak line and peaks 1775 can be deleted by right-clicking on them. This only works when the 1776 zoom and reposition modes (below) are not selected. Also note 1773 1777 some peaks have shoulders most notably at 5.07, 6.04, 7.81deg. I found 28 peaks 1774 1778 (there was one very weak shoulder at ~7.3 deg. I skipped it might be from a … … 1939 1943 1940 1944 <p class=MsoNormal>In this exercise we will fit peaks and index them for 1941 sucrose in preparation for a charge flipping exercise. The data w asalso1945 sucrose in preparation for a charge flipping exercise. The data were also 1942 1946 collected on 11BM-B at APS. The unit cell is monoclinic so is a more 1943 1947 substantial test of the indexing capability of GSAS-II.</p> … … 1988 1992 small ones); use <b style='mso-bidi-font-weight:normal'><span style='font-family: 1989 1993 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1990 minor-latin'>Auto search</span></b> to start and then fill in by hand. Note the 1994 minor-latin'>Auto search</span></b> to start and then fill in by hand: 1995 Add peaks by left-clicking on a data point near the top of the 1996 peak. Peak positions can be moved by dragging the peak line and peaks 1997 can be deleted by right-clicking on them. This only works when the 1998 zoom and reposition modes (below) are not selected. Also note the 1991 1999 shoulder at ~6.3 <span class=SpellE>deg</span> that should be added to the 1992 2000 list. I skipped a couple of very weak peaks; the total list has 28 peaks.</p>
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