Changeset 676


Ignore:
Timestamp:
Jul 3, 2012 2:42:57 PM (9 years ago)
Author:
vondreele
Message:
 
Location:
trunk/help
Files:
17 edited

Legend:

Unmodified
Added
Removed
  • trunk/help/Calibration of an area detector in GSAS.htm

    r639 r676  
    2525  <o:Author>Von Dreele</o:Author>
    2626  <o:LastAuthor>Von Dreele</o:LastAuthor>
    27   <o:Revision>12</o:Revision>
    28   <o:TotalTime>122</o:TotalTime>
     27  <o:Revision>13</o:Revision>
     28  <o:TotalTime>124</o:TotalTime>
    2929  <o:Created>2012-05-04T19:00:00Z</o:Created>
    30   <o:LastSaved>2012-05-07T21:40:00Z</o:LastSaved>
     30  <o:LastSaved>2012-07-03T19:08:00Z</o:LastSaved>
    3131  <o:Pages>4</o:Pages>
    3232  <o:Words>706</o:Words>
    33   <o:Characters>4029</o:Characters>
     33  <o:Characters>4028</o:Characters>
    3434  <o:Company>Argonne National Laboratory</o:Company>
    3535  <o:Lines>33</o:Lines>
    3636  <o:Paragraphs>9</o:Paragraphs>
    37   <o:CharactersWithSpaces>4726</o:CharactersWithSpaces>
     37  <o:CharactersWithSpaces>4725</o:CharactersWithSpaces>
    3838  <o:Version>14.00</o:Version>
    3939 </o:DocumentProperties>
     
    842842the data file into the current GSAS-II project. </p>
    843843
    844 <p class=MsoNormal><span style='mso-no-proof:yes'>
    845  <img border=0 width=300 height=273
    846 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.jpg"
    847 v:shapes="Picture_x0020_1"></span><span
    848 style='mso-spacerun:yes'> </span></p>
     844<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
    849845
    850846<p class=MsoNormal>A file selection dialog will be shown; its appearance will
     
    861857minor-latin'>Open</span></b>.<span style='mso-no-proof:yes'> <o:p></o:p></span></p>
    862858
    863 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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    871886
     
    877892
    878893<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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    884 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
    885 v:shapes="Picture_x0020_5"><![endif]></span></p>
     898</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=414
     899src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png"
     900v:shapes="_x0000_i1031"><![endif]></span></p>
    886901
    887902<p class=MsoNormal><span style='mso-spacerun:yes'> </span>The plot window shows
     
    891906minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span></b> marks the
    892907default beam location (image center); your calibration will correctly place it.
    893 Also notice that the values shown in the plot window status bar (at bottom of plot
    894 window) change as you move the cursor over the plot; these values are at
     908Also notice that the values shown in the plot window status bar (at bottom of
     909plot window) change as you move the cursor over the plot; these values are at
    895910present in error as they are computed from the default calibration values. They
    896911will be correct after you finish the calibration.</p>
     
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     920src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
    906921v:shapes="Picture_x0020_4"><![endif]></span></p>
    907922
     
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     994src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
    980995v:shapes="Picture_x0020_8"><![endif]></span></p>
    981996
     
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    1013 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
     1028src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
    10141029v:shapes="Picture_x0020_9"><![endif]></span><span
    10151030style='mso-spacerun:yes'> </span></p>
     
    10211036
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    1028 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
    1029 v:shapes="Picture_x0020_12"><![endif]></span><span
     1042</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=414
     1043src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png"
     1044v:shapes="Picture_x0020_10"><![endif]></span><span
    10301045style='mso-spacerun:yes'> </span></p>
    10311046
     
    10371052 id="Picture_x0020_14" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:396.75pt;
    10381053 height:134.25pt;visibility:visible;mso-wrap-style:square'>
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    10401055  o:title=""/>
    10411056</v:shape><![endif]--><![if !vml]><img border=0 width=529 height=179
    1042 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image009.png"
     1057src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
    10431058v:shapes="Picture_x0020_14"><![endif]></span></p>
    10441059
    1045 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>To see the actual points
    1046 selected by the program, click on the <b style='mso-bidi-font-weight:normal'><span
    1047 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
    1048 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>show ring
    1049 picks?</span></b> <span class=GramE>check</span> box </p>
     1060<p class=MsoNormal><span style='mso-spacerun:yes'> </span>To see the actual
     1061points selected by the program, click on the <b style='mso-bidi-font-weight:
     1062normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1063minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>show
     1064ring picks?</span></b> <span class=GramE>check</span> box </p>
    10501065
    10511066<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    10521067 id="Picture_x0020_15" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;
    10531068 height:450pt;visibility:visible;mso-wrap-style:square'>
    1054  <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image010.png"
     1069 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
    10551070  o:title=""/>
    10561071</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
    1057 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image010.png"
     1072src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
    10581073v:shapes="Picture_x0020_15"><![endif]></span><span
    10591074style='mso-spacerun:yes'> </span><span style='color:#1F497D;mso-themecolor:
  • trunk/help/Calibration of an area detector in GSAS_files/filelist.xml

    r588 r676  
    44 <o:File HRef="colorschememapping.xml"/>
    55 <o:File HRef="image001.png"/>
    6  <o:File HRef="image002.jpg"/>
     6 <o:File HRef="image002.png"/>
    77 <o:File HRef="image003.png"/>
    88 <o:File HRef="image004.png"/>
     
    1111 <o:File HRef="image007.png"/>
    1212 <o:File HRef="image008.png"/>
    13  <o:File HRef="image009.png"/>
    14  <o:File HRef="image010.png"/>
    1513 <o:File HRef="filelist.xml"/>
    1614</xml>
  • trunk/help/Fit Peaks.htm

    r624 r676  
    2323  <o:Author>Von Dreele</o:Author>
    2424  <o:LastAuthor>Von Dreele</o:LastAuthor>
    25   <o:Revision>15</o:Revision>
    26   <o:TotalTime>256</o:TotalTime>
     25  <o:Revision>16</o:Revision>
     26  <o:TotalTime>275</o:TotalTime>
    2727  <o:Created>2012-05-05T16:28:00Z</o:Created>
    28   <o:LastSaved>2012-05-18T18:04:00Z</o:LastSaved>
     28  <o:LastSaved>2012-07-03T19:35:00Z</o:LastSaved>
    2929  <o:Pages>9</o:Pages>
    30   <o:Words>1787</o:Words>
    31   <o:Characters>10190</o:Characters>
     30  <o:Words>1831</o:Words>
     31  <o:Characters>10439</o:Characters>
    3232  <o:Company>Argonne National Laboratory</o:Company>
    33   <o:Lines>84</o:Lines>
    34   <o:Paragraphs>23</o:Paragraphs>
    35   <o:CharactersWithSpaces>11954</o:CharactersWithSpaces>
     33  <o:Lines>86</o:Lines>
     34  <o:Paragraphs>24</o:Paragraphs>
     35  <o:CharactersWithSpaces>12246</o:CharactersWithSpaces>
    3636  <o:Version>14.00</o:Version>
    3737 </o:DocumentProperties>
     
    599599        mso-font-kerning:14.0pt;}
    600600a:link, span.MsoHyperlink
    601         {mso-style-noshow:yes;
    602         mso-style-priority:99;
     601        {mso-style-priority:99;
    603602        color:blue;
    604603        text-decoration:underline;
     
    11471146data file into the current GSAS-II project. This read option is set to read any
    11481147of the powder data formats (except neutron TOF time map files) defined for GSAS
    1149 (angles in <span class=SpellE>centidegrees</span>). Other submenu items will read
    1150 the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
     1148(angles in <span class=SpellE>centidegrees</span>). Other submenu items will
     1149read the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
    11511150style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
    11521151mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>cif</span></b></span>
     
    11871186<p class=MsoListParagraphCxSpLast style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span
    11881187style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>3.<span
    1189 style='font:7.0pt "Times New Roman"'>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp; </span></span></span><![endif]>Select
    1190 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    1191 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
    1192 minor-latin'>11bmb_3844.prm</span></b> instrument parameter file in the second
    1193 dialog and press <b style='mso-bidi-font-weight:normal'><span style='font-family:
    1194 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1195 minor-latin;mso-bidi-theme-font:minor-latin'>Open</span></b>. The 11BM-B
    1196 instrument processing software automatically produced this file when the
    1197 corresponding <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
    1198 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
    1199 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>fxye</span></b></span>
    1200 file was created from the 12 detector raw data.</p>
     1188style='font:7.0pt "Times New Roman"'>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp; </span></span></span><![endif]>The
     1189file <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1190mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
     1191minor-latin'>11bmb_3844.prm</span></b> instrument parameter file is
     1192automatically selected; it was produced by 11BM-B instrument processing
     1193software when the corresponding <span class=SpellE><b style='mso-bidi-font-weight:
     1194normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1195minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>fxye</span></b></span>
     1196file was created from the 12 detector raw data. If absent or the name doesn’t
     1197match the data file name, a file dialog will appear for you to select the
     1198correct instrument parameter file.</p>
    12011199
    12021200<p class=MsoNormal>At this point the <b style='mso-bidi-font-weight:normal'><span
     
    14161414style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span
    14171415style='font:7.0pt "Times New Roman"'>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp; </span></span></span><![endif]>Now
    1418 add refinement of the peak positions. This can be done by clicking on all the refinement
    1419 flags for the individual peaks or it is possible to set them all at the same
    1420 time using this recipe: </p>
     1416add refinement of the peak positions. This can be done by clicking on all the
     1417refinement flags for the individual peaks or it is possible to set them all at
     1418the same time using this recipe: </p>
    14211419
    14221420<p class=MsoListParagraphCxSpMiddle style='margin-left:1.0in;mso-add-space:
     
    15181516normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
    15191517minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Index
    1520 Peak List</span></b> item in the data tree. In the initially empty window
    1521 created by this action, use menu item <b style='mso-bidi-font-weight:normal'><span
     1518Peak List</span></b> item in the data tree. In the initially empty window created
     1519by this action, use menu item <b style='mso-bidi-font-weight:normal'><span
    15221520style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
    15231521mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Index Peaks
     
    16051603<h2><span class=GramE>Step 8.</span> Select/Refine Cell</h2>
    16061604
    1607 <p class=MsoNormal>Select the cell with M20 ~ 2900 with a = 4.1568 Å. This
    1608 indexes all peaks with almost a perfect fit to the peak positions (compare
    1609 dashed red lines to solid blue ones). Import the cell information using the <b
     1605<p class=MsoNormal>Select the cell with M20 ~ 2900 with a = 4.1568 Å. This indexes
     1606all peaks with almost a perfect fit to the peak positions (compare dashed red
     1607lines to solid blue ones). Import the cell information using the <b
    16101608style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    16111609mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
     
    16631661class=GramE>do the menu item</span> <b style='mso-bidi-font-weight:normal'><span
    16641662style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
    1665 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>File/Close
    1666 project</span></b> in the <b style='mso-bidi-font-weight:normal'><span
    1667 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
    1668 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data
    1669 tree </span></b>window. You will be asked if you want it saved; if <span
    1670 class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family:
    1671 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1672 minor-latin;mso-bidi-theme-font:minor-latin'>Yes</span></b></span> then all the
    1673 peak fitting/indexing &amp; cell refinement results will be saved to the <b
    1674 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1663mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>File/Close project</span></b>
     1664in the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1665mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
     1666minor-latin'>GSAS-II data tree </span></b>window. You will be asked if you want
     1667it saved; if <span class=GramE><b style='mso-bidi-font-weight:normal'><span
     1668style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1669mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Yes</span></b></span>
     1670then all the peak fitting/indexing &amp; cell refinement results will be saved
     1671to the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    16751672mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
    16761673minor-latin'>LaB6.gpx</span></b> file. If <b style='mso-bidi-font-weight:normal'><span
     
    16821679
    16831680<p class=MsoNormal>In this exercise we will fit peaks and index them for the
    1684 new mineral <span class=SpellE>jadarite</span> (aka “kryptonite”). The data was
    1685 also collected on 11BM-B at APS. The unit cell is monoclinic so is a more
    1686 substantial test of the indexing capability of GSAS-II.</p>
     1681new mineral <a href="http://en.wikipedia.org/wiki/Jadarite"><span class=SpellE>jadarite</span></a>
     1682(aka “<a href="http://en.wikipedia.org/wiki/Kryptonite">kryptonite</a>”). The
     1683data was also collected on 11BM-B at APS. The unit cell is monoclinic so is a
     1684more substantial test of the indexing capability of GSAS-II.</p>
    16871685
    16881686<h2><span class=GramE>Step 1.</span> Read in the data. </h2>
     
    18231821<p class=MsoNormal>Although the weak peak at 2<span style='font-family:Symbol;
    18241822mso-char-type:symbol;mso-symbol-font-family:Symbol'><span style='mso-char-type:
    1825 symbol;mso-symbol-font-family:Symbol'>Q</span></span>~7.3 has a shoulder that
    1826 wasn’t indexed. I presume that is a contaminant. By sliding the cursor over the
    1827 index lines without any visible peak you can see that the missing ones are
    1828 (010, 100, 001, 110, 030, 111, 20-1, 10-2, 041, 050, 21-2, 23-1, 22-2, 141,
    1829 201,102, 15-1, 112, &amp; 24-1). Many of these are accidental but the 0k0; k&#8800;2n
    1830 and h0l; h+l&#8800;2n ones characterize the space group P2<sub>1</sub>/n. Armed
    1831 with this information you can <b style='mso-bidi-font-weight:normal'><span
     1823symbol;mso-symbol-font-family:Symbol'>Q</span></span>~7.3 has a shoulder that wasn’t
     1824indexed. I presume that is a contaminant. By sliding the cursor over the index
     1825lines without any visible peak you can see that the missing ones are (010, 100,
     1826001, 110, 030, 111, 20-1, 10-2, 041, 050, 21-2, 23-1, 22-2, 141, 201,102, 15-1,
     1827112, &amp; 24-1). Many of these are accidental but the 0k0; k&#8800;2n and h0l;
     1828h+l&#8800;2n ones characterize the space group P2<sub>1</sub>/n. Armed with
     1829this information you can <b style='mso-bidi-font-weight:normal'><span
    18321830style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
    18331831mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Make new
     
    18601858src="Fit%20Peaks_files/image024.png" v:shapes="Picture_x0020_23"><![endif]></span></p>
    18611859
    1862 <p class=MsoNormal>This concludes this exercise. The features of the <b
     1860<p class=MsoNormal>This concludes this exercise; <span class=GramE><b
     1861style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1862mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
     1863minor-latin'>Save</span></b></span> the project file as it is needed for the <b
     1864style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1865mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
     1866minor-latin'>Charge Flipping</span></b> exercise. The features of the <b
    18631867style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    18641868mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
  • trunk/help/Integration of area detector data in GSAS.htm

    r602 r676  
    2525  <o:Author>Von Dreele</o:Author>
    2626  <o:LastAuthor>Von Dreele</o:LastAuthor>
    27   <o:Revision>10</o:Revision>
    28   <o:TotalTime>103</o:TotalTime>
     27  <o:Revision>11</o:Revision>
     28  <o:TotalTime>109</o:TotalTime>
    2929  <o:Created>2012-05-04T20:46:00Z</o:Created>
    30   <o:LastSaved>2012-05-07T21:41:00Z</o:LastSaved>
     30  <o:LastSaved>2012-07-03T19:15:00Z</o:LastSaved>
    3131  <o:Pages>3</o:Pages>
    32   <o:Words>741</o:Words>
    33   <o:Characters>4229</o:Characters>
     32  <o:Words>800</o:Words>
     33  <o:Characters>4563</o:Characters>
    3434  <o:Company>Argonne National Laboratory</o:Company>
    35   <o:Lines>35</o:Lines>
    36   <o:Paragraphs>9</o:Paragraphs>
    37   <o:CharactersWithSpaces>4961</o:CharactersWithSpaces>
     35  <o:Lines>38</o:Lines>
     36  <o:Paragraphs>10</o:Paragraphs>
     37  <o:CharactersWithSpaces>5353</o:CharactersWithSpaces>
    3838  <o:Version>14.00</o:Version>
    3939 </o:DocumentProperties>
     
    10581058 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
    10591059 <o:lock v:ext="edit" aspectratio="t"/>
    1060 </v:shapetype><v:shape id="Picture_x0020_2" o:spid="_x0000_i1029" type="#_x0000_t75"
    1061  style='width:468pt;height:277.5pt;visibility:visible;mso-wrap-style:square'>
     1060</v:shapetype><v:shape id="Picture_x0020_6" o:spid="_x0000_i1029" type="#_x0000_t75"
     1061 style='width:472.5pt;height:310.5pt;visibility:visible;mso-wrap-style:square'>
    10621062 <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image001.png"
    10631063  o:title=""/>
    1064 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=370
    1065 src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image002.png"
    1066 v:shapes="Picture_x0020_2"><![endif]></span></p>
     1064</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=414
     1065src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image001.png"
     1066v:shapes="Picture_x0020_6"><![endif]></span></p>
    10671067
    10681068<h3>Other useful controls:</h3>
     
    11161116<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
    11171117style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1118mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Appl. det.
     1119absorption</span></b> and <b style='mso-bidi-font-weight:normal'><span
     1120style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1121mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>value</span></b>:
     1122The scattered ray beams are partially absorbed by the detector depending on the
     1123scattering angle. This reduces the intensity of higher angle data more than low
     1124angle data. The value is dependent on the wavelength and the materials used for
     1125the front surface of the detector, so some experimentation with a standard is
     1126needed to establish an appropriate value.</p>
     1127
     1128<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
     1129style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
    11181130mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Background
    11191131Image</span> </b>and<b style='mso-bidi-font-weight:normal'> </b><b
     
    11311143 id="Picture_x0020_1" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:468pt;
    11321144 height:401.25pt;visibility:visible;mso-wrap-style:square'>
    1133  <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image003.png"
     1145 <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image002.png"
    11341146  o:title=""/>
    11351147</v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535
    1136 src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image004.png"
     1148src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image003.png"
    11371149v:shapes="Picture_x0020_1"><![endif]></span></p>
    11381150
     
    11591171 id="Picture_x0020_3" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:225pt;
    11601172 height:203.25pt;visibility:visible;mso-wrap-style:square'>
    1161  <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image005.png"
     1173 <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image004.png"
    11621174  o:title=""/>
    11631175</v:shape><![endif]--><![if !vml]><img border=0 width=300 height=271
    1164 src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image005.png"
     1176src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image004.png"
    11651177v:shapes="Picture_x0020_3"><![endif]></span><span
    11661178style='mso-spacerun:yes'> </span></p>
     
    11691181style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    11701182mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
    1171 minor-latin'>2D Integration</span></b>) shows the diffraction intensity as a
    1172 function of both 2-theta and (when there is more than one azimuthal integration
    1173 region) azimuthal angle.</p>
     1183minor-latin'>2D Integration</span></b>) shows the diffraction intensity as a function
     1184of both 2-theta and (when there is more than one azimuthal integration region)
     1185azimuthal angle.</p>
    11741186
    11751187<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    11761188 id="Picture_x0020_4" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:525pt;
     1189 height:450pt;visibility:visible;mso-wrap-style:square'>
     1190 <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image005.png"
     1191  o:title=""/>
     1192</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
     1193src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image005.png"
     1194v:shapes="Picture_x0020_4"><![endif]></span><span
     1195style='mso-spacerun:yes'> </span></p>
     1196
     1197<p class=MsoNormal><span class=GramE>and</span> a conventional 1-D powder
     1198pattern(s) for each &quot;slice&quot;</p>
     1199
     1200<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
     1201 id="Picture_x0020_5" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;
    11771202 height:450pt;visibility:visible;mso-wrap-style:square'>
    11781203 <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image006.png"
     
    11801205</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
    11811206src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image006.png"
    1182 v:shapes="Picture_x0020_4"><![endif]></span><span
    1183 style='mso-spacerun:yes'> </span></p>
    1184 
    1185 <p class=MsoNormal><span class=GramE>and</span> a conventional 1-D powder
    1186 pattern(s) for each &quot;slice&quot;</p>
    1187 
    1188 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1189  id="Picture_x0020_5" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;
    1190  height:450pt;visibility:visible;mso-wrap-style:square'>
    1191  <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image007.png"
    1192   o:title=""/>
    1193 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
    1194 src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image007.png"
    11951207v:shapes="Picture_x0020_5"><![endif]></span></p>
    11961208
  • trunk/help/Integration of area detector data in GSAS_files/filelist.xml

    r588 r676  
    99 <o:File HRef="image005.png"/>
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    1211 <o:File HRef="filelist.xml"/>
    1312</xml>
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