Changeset 4923
- Timestamp:
- Jun 8, 2021 9:13:19 AM (2 years ago)
- Location:
- Tutorials/2DTexture
- Files:
-
- 69 edited
Legend:
- Unmodified
- Added
- Removed
-
Tutorials/2DTexture/Texture analysis of 2D data in GSAS-II.htm
r4457 r4923 24 24 <o:DocumentProperties> 25 25 <o:Author>Von Dreele</o:Author> 26 <o:LastAuthor> vondreele</o:LastAuthor>27 <o:Revision>1 2</o:Revision>28 <o:TotalTime>227 4</o:TotalTime>26 <o:LastAuthor>Von Dreele, Robert B.</o:LastAuthor> 27 <o:Revision>14</o:Revision> 28 <o:TotalTime>2275</o:TotalTime> 29 29 <o:Created>2015-05-14T17:06:00Z</o:Created> 30 <o:LastSaved>20 17-09-08T18:45:00Z</o:LastSaved>31 <o:Pages> 47</o:Pages>32 <o:Words>43 56</o:Words>33 <o:Characters>2 4830</o:Characters>30 <o:LastSaved>2021-06-08T14:08:00Z</o:LastSaved> 31 <o:Pages>1</o:Pages> 32 <o:Words>4394</o:Words> 33 <o:Characters>25049</o:Characters> 34 34 <o:Company>Argonne National Laboratory</o:Company> 35 <o:Lines>20 6</o:Lines>35 <o:Lines>208</o:Lines> 36 36 <o:Paragraphs>58</o:Paragraphs> 37 <o:CharactersWithSpaces>29 128</o:CharactersWithSpaces>37 <o:CharactersWithSpaces>29385</o:CharactersWithSpaces> 38 38 <o:Version>16.00</o:Version> 39 39 </o:DocumentProperties> … … 49 49 <w:WordDocument> 50 50 <w:View>Print</w:View> 51 <w:Zoom>124</w:Zoom>52 51 <w:SpellingState>Clean</w:SpellingState> 53 52 <w:GrammarState>Clean</w:GrammarState> … … 96 95 <w:LatentStyles DefLockedState="false" DefUnhideWhenUsed="false" 97 96 DefSemiHidden="false" DefQFormat="false" DefPriority="99" 98 LatentStyleCount="37 1">97 LatentStyleCount="376"> 99 98 <w:LsdException Locked="false" Priority="0" QFormat="true" Name="Normal"/> 100 99 <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 1"/> … … 302 301 Name="HTML Variable"/> 303 302 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 304 Name="Normal Table"/>305 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"306 303 Name="annotation subject"/> 307 304 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" … … 388 385 Name="Table Professional"/> 389 386 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 390 Name="Table Subtle 1"/>391 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"392 387 Name="Table Subtle 2"/> 393 388 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 394 389 Name="Table Web 1"/> 395 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"396 Name="Table Web 2"/>397 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"398 Name="Table Web 3"/>399 390 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 400 391 Name="Balloon Text"/> … … 661 652 <w:LsdException Locked="false" Priority="52" 662 653 Name="List Table 7 Colorful Accent 6"/> 654 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 655 Name="Mention"/> 656 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 657 Name="Smart Hyperlink"/> 658 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 659 Name="Hashtag"/> 660 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 661 Name="Unresolved Mention"/> 662 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 663 Name="Smart Link"/> 663 664 </w:LatentStyles> 664 665 </xml><![endif]--> … … 672 673 mso-generic-font-family:roman; 673 674 mso-font-pitch:variable; 674 mso-font-signature:-5368 70145 1107305727 00 415 0;}675 mso-font-signature:-536869121 1107305727 33554432 0 415 0;} 675 676 @font-face 676 677 {font-family:Calibri; … … 679 680 mso-generic-font-family:swiss; 680 681 mso-font-pitch:variable; 681 mso-font-signature:- 536859905-1073732485 9 0 511 0;}682 mso-font-signature:-469750017 -1073732485 9 0 511 0;} 682 683 @font-face 683 684 {font-family:Tahoma; … … 835 836 mso-style-type:export-only; 836 837 margin:0in; 837 margin-bottom:.0001pt;838 838 mso-add-space:auto; 839 839 mso-pagination:widow-orphan; … … 867 867 mso-style-type:export-only; 868 868 margin:0in; 869 margin-bottom:.0001pt;870 869 mso-add-space:auto; 871 870 mso-pagination:widow-orphan; … … 1032 1031 margin-bottom:0in; 1033 1032 margin-left:.5in; 1034 margin-bottom:.0001pt;1035 1033 mso-add-space:auto; 1036 1034 mso-pagination:widow-orphan; … … 1049 1047 margin-bottom:0in; 1050 1048 margin-left:.5in; 1051 margin-bottom:.0001pt;1052 1049 mso-add-space:auto; 1053 1050 mso-pagination:widow-orphan; … … 1407 1404 mso-padding-alt:0in 5.4pt 0in 5.4pt; 1408 1405 mso-para-margin:0in; 1409 mso-para-margin-bottom:.0001pt;1410 1406 mso-pagination:widow-orphan; 1411 1407 font-size:10.0pt; … … 1426 1422 </head> 1427 1423 1428 <body lang=EN-US link=blue vlink=purple style='tab-interval:.5in'> 1424 <body lang=EN-US link=blue vlink=purple style='tab-interval:.5in;word-wrap: 1425 break-word'> 1429 1426 1430 1427 <div class=WordSection1> 1431 1428 1432 1429 <h1 style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt;margin-left: 1433 0in;line-height:115%'>Texture analysis of 2D data in GSAS-II</h1> 1434 1435 <P><BL> 1436 <LI><B>A video version of this tutorial is available at 1437 <A href="https://anl.box.com/v/Textureanalysisof2DdatainGSAS-" target="_blank"> 1438 https://anl.box.com/v/Textureanalysisof2DdatainGSAS-</A></B> 1439 <LI>Exercise files are found <A href="./data/" target="_blank">here</a> 1440 </BL></P><P></P> 1430 0in;line-height:115%'>Texture analysis of 2D data in GSAS-II<o:p></o:p></h1> 1431 1432 <p class=MsoNormal style='margin-bottom:0in'><BL><span style='font-family:Symbol; 1433 mso-ascii-font-family:"Times New Roman";mso-fareast-font-family:Calibri; 1434 mso-fareast-theme-font:minor-latin'>·</span><span style='mso-fareast-font-family: 1435 Calibri;mso-fareast-theme-font:minor-latin'><span style='mso-spacerun:yes'> 1436 </span><b>A video version of this tutorial is available at <a 1437 href="https://anl.box.com/v/Textureanalysisof2DdatainGSAS-" target="_blank">https://anl.box.com/v/Textureanalysisof2DdatainGSAS-</a></b> 1438 <o:p></o:p></span></p> 1439 1440 <p class=MsoNormal style='margin-bottom:0in'><span style='font-family:Symbol; 1441 mso-ascii-font-family:"Times New Roman";mso-fareast-font-family:Calibri; 1442 mso-fareast-theme-font:minor-latin'>·</span><span style='mso-fareast-font-family: 1443 Calibri;mso-fareast-theme-font:minor-latin'><span style='mso-spacerun:yes'> 1444 </span>Exercise files are found <a href="data/" target="_blank">here</a> <o:p></o:p></span></p> 1445 1446 </BL> 1441 1447 1442 1448 <h2 style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt;margin-left: … … 1533 1539 o:title="" chromakey="white"/> 1534 1540 </v:shape><![endif]--><![if !vml]><img width=357 height=56 1535 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 51.png"1541 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image002.png" 1536 1542 v:shapes="_x0000_i1025"><![endif]></span><![endif]></p> 1537 1543 … … 1557 1563 o:title="" chromakey="white"/> 1558 1564 </v:shape><![endif]--><![if !vml]><img width=43 height=35 1559 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 52.png"1565 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image004.png" 1560 1566 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 1561 1567 style='mso-spacerun:yes'> </span>and <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span … … 1575 1581 o:title="" chromakey="white"/> 1576 1582 </v:shape><![endif]--><![if !vml]><img width=40 height=35 1577 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 53.png"1583 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image006.png" 1578 1584 v:shapes="_x0000_i1025"><![endif]></span><![endif]>, take on values according 1579 1585 to the crystal and sample symmetries, respectively, and thus the two inner … … 1600 1606 o:title="" chromakey="white"/> 1601 1607 </v:shape><![endif]--><![if !vml]><img width=39 height=35 1602 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 54.png"1608 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image008.png" 1603 1609 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 1604 1610 style='mso-spacerun:yes'> </span>terms are nonzero so the rest are excluded … … 1618 1624 o:title="" chromakey="white"/> 1619 1625 </v:shape><![endif]--><![if !vml]><img width=28 height=35 1620 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 55.png"1626 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image010.png" 1621 1627 v:shapes="_x0000_i1025"><![endif]></span><![endif]>coefficients is sufficient 1622 1628 to describe the effect on the diffraction patterns due to texture. The crystal … … 1637 1643 o:title="" chromakey="white"/> 1638 1644 </v:shape><![endif]--><![if !vml]><img width=43 height=35 1639 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 56.png"1645 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image012.png" 1640 1646 v:shapes="_x0000_i1025"><![endif]></span><![endif]>, is defined for each 1641 1647 reflection, h, <i>via</i> polar and azimuthal coordinates (<span … … 1663 1669 o:title="" chromakey="white"/> 1664 1670 </v:shape><![endif]--><![if !vml]><img width=40 height=35 1665 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 53.png"1671 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image006.png" 1666 1672 v:shapes="_x0000_i1025"><![endif]></span><![endif]>, is defined according to 1667 1673 polar and azimuthal coordinates (<span style='font-family:Symbol'>y</span>, <span … … 1738 1744 o:title="" chromakey="white"/> 1739 1745 </v:shape><![endif]--><![if !vml]><img width=428 height=72 1740 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 57.png"1746 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image014.png" 1741 1747 v:shapes="_x0000_i1025"><![endif]></span><![endif]><br style='mso-special-character: 1742 1748 line-break'> … … 1766 1772 style='mso-spacerun:yes'> </span></span>= 0.<span style='mso-spacerun:yes'> 1767 1773 </span>Finally, as the sample may be mounted so that the sample coordinate 1768 system (I<sub>s</sub>, <span class=SpellE>J<sub>s</sub></span>, K<sub>s</sub>) 1769 does not coincide with the instrument coordinate system (I, J, K), we define 1770 three <span class=SpellE>eulerian</span> sample rotation offset angles (<span 1771 style='font-family:Symbol'>W</span><sub>s</sub>, <span style='font-family:Symbol'>C</span><sub>s</sub>, 1772 <span style='font-family:Symbol'>F</span><sub>s</sub>) that describe the 1773 rotation from (I<sub>s</sub>, <span class=SpellE>J<sub>s</sub></span>, K<sub>s</sub>) 1774 to (I, J, K).<span style='mso-spacerun:yes'> </span>The sample rotation angles 1775 are defined so that with the goniometer angles at zero <span style='font-family: 1776 Symbol'>W</span><sub>s</sub> and <span style='font-family:Symbol'>F</span><sub>s</sub> 1777 are rotations about I and <span style='font-family:Symbol'>C</span><sub>s</sub> 1778 is a rotation about J.<span style='mso-spacerun:yes'> </span>The zeros of 1779 these three sample rotation angles can be refined as part of the Rietveld 1780 analysis to accommodate any angular offset in sample mounting. After including 1781 the diffraction angle, <span style='font-family:Symbol'>Q</span>, and a 1782 detector azimuthal angle, A, the full rotation matrix, <b style='mso-bidi-font-weight: 1783 normal'>M</b>, is </p> 1774 system (I<sub>s</sub>, J<sub>s</sub>, K<sub>s</sub>) does not coincide with the 1775 instrument coordinate system (I, J, K), we define three <span class=SpellE>eulerian</span> 1776 sample rotation offset angles (<span style='font-family:Symbol'>W</span><sub>s</sub>, 1777 <span style='font-family:Symbol'>C</span><sub>s</sub>, <span style='font-family: 1778 Symbol'>F</span><sub>s</sub>) that describe the rotation from (I<sub>s</sub>, J<sub>s</sub>, 1779 K<sub>s</sub>) to (I, J, K).<span style='mso-spacerun:yes'> </span>The sample 1780 rotation angles are defined so that with the goniometer angles at zero <span 1781 style='font-family:Symbol'>W</span><sub>s</sub> and <span style='font-family: 1782 Symbol'>F</span><sub>s</sub> are rotations about K and <span style='font-family: 1783 Symbol'>C</span><sub>s</sub> is a rotation about J.<span 1784 style='mso-spacerun:yes'> </span>The zeros of these three sample rotation 1785 angles can be refined as part of the Rietveld analysis to accommodate any 1786 angular offset in sample mounting. After including the diffraction angle, <span 1787 style='font-family:Symbol'>Q</span>, and a detector azimuthal angle, A, the 1788 full rotation matrix, <b style='mso-bidi-font-weight:normal'>M</b>, is </p> 1784 1789 1785 1790 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; … … 1794 1799 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 1795 1800 margin-left:0in;line-height:115%'>By transformation of unit Cartesian vectors 1796 (100, 010 and 001) with this rotation matrix, the sample orientation coordinates1797 (<span style='font-family:Symbol'>y</span>, <span style='font-family:Symbol'>g</span>) 1798 are given by</p>1801 (100, 010 and 001) with this rotation matrix, the sample orientation 1802 coordinates (<span style='font-family:Symbol'>y</span>, <span style='font-family: 1803 Symbol'>g</span>) are given by</p> 1799 1804 1800 1805 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; … … 1820 1825 o:title="" chromakey="white"/> 1821 1826 </v:shape><![endif]--><![if !vml]><img width=45 height=67 1822 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 58.png"1827 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image016.png" 1823 1828 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 1824 1829 style='mso-spacerun:yes'> </span>and<span style='mso-spacerun:yes'> </span><i>tan</i>(<span … … 1857 1862 o:title="" chromakey="white"/> 1858 1863 </v:shape><![endif]--><![if !vml]><img width=107 height=67 1859 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 59.png"1864 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image018.png" 1860 1865 v:shapes="_x0000_i1025"><![endif]></span><![endif]></p> 1861 1866 … … 1877 1882 o:title="" chromakey="white"/> 1878 1883 </v:shape><![endif]--><![if !vml]><img width=62 height=35 1879 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 60.png"1884 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image020.png" 1880 1885 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 1881 1886 style='mso-spacerun:yes'> </span>and <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span … … 1895 1900 o:title="" chromakey="white"/> 1896 1901 </v:shape><![endif]--><![if !vml]><img width=57 height=35 1897 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 61.png"1902 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image022.png" 1898 1903 v:shapes="_x0000_i1025"><![endif]></span><![endif]>, are developed from</p> 1899 1904 … … 1950 1955 o:title="" chromakey="white"/> 1951 1956 </v:shape><![endif]--><![if !vml]><img width=220 height=56 1952 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 62.png"1957 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image024.png" 1953 1958 v:shapes="_x0000_i1025"><![endif]></span><![endif]></p> 1954 1959 … … 1974 1979 o:title="" chromakey="white"/> 1975 1980 </v:shape><![endif]--><![if !vml]><img width=44 height=35 1976 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 63.png"1981 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image026.png" 1977 1982 v:shapes="_x0000_i1025"><![endif]></span><![endif]>, are defined via a Fourier 1978 1983 expansion as</p> … … 2026 2031 o:title="" chromakey="white"/> 2027 2032 </v:shape><![endif]--><![if !vml]><img width=206 height=70 2028 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 64.png"2033 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image028.png" 2029 2034 v:shapes="_x0000_i1025"><![endif]></span><![endif]></p> 2030 2035 … … 2080 2085 o:title="" chromakey="white"/> 2081 2086 </v:shape><![endif]--><![if !vml]><img width=211 height=70 2082 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 67.png"2087 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image030.png" 2083 2088 v:shapes="_x0000_i1025"><![endif]></span><![endif]></p> 2084 2089 … … 2102 2107 o:title="" chromakey="white"/> 2103 2108 </v:shape><![endif]--><![if !vml]><img width=33 height=35 2104 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 68.png"2109 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image032.png" 2105 2110 v:shapes="_x0000_i1025"><![endif]></span><![endif]>.<span 2106 2111 style='mso-spacerun:yes'> </span>These Fourier coefficients are determined so … … 2225 2230 "Times New Roman";mso-fareast-theme-font:minor-fareast;mso-ansi-language:EN-US; 2226 2231 mso-fareast-language:EN-US;mso-bidi-language:AR-SA'><!--[if gte vml 1]><v:shape 2227 id="_x0000_i1025" type="#_x0000_t75" style='width:423.7 pt;height:55.5pt'>2232 id="_x0000_i1025" type="#_x0000_t75" style='width:423.75pt;height:55.5pt'> 2228 2233 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image033.png" 2229 2234 o:title="" chromakey="white"/> 2230 2235 </v:shape><![endif]--><![if !vml]><img width=565 height=74 2231 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 69.png"2236 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image034.png" 2232 2237 v:shapes="_x0000_i1025"><![endif]></span><![endif]></p> 2233 2238 … … 2267 2272 o:title="" chromakey="white"/> 2268 2273 </v:shape><![endif]--><![if !vml]><img width=148 height=35 2269 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 70.png"2274 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image036.png" 2270 2275 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 2271 2276 style='mso-spacerun:yes'> </span>and <!--[if gte msEquation 12]><m:oMath><m:func><m:funcPr><span … … 2302 2307 o:title="" chromakey="white"/> 2303 2308 </v:shape><![endif]--><![if !vml]><img width=134 height=35 2304 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 71.png"2309 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image038.png" 2305 2310 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 2306 2311 style='mso-spacerun:yes'> </span>are combined depending on the symmetry and the … … 2323 2328 o:title="" chromakey="white"/> 2324 2329 </v:shape><![endif]--><![if !vml]><img width=64 height=35 2325 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 72.png"2330 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image040.png" 2326 2331 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 2327 2332 style='mso-spacerun:yes'> </span>and <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span … … 2342 2347 o:title="" chromakey="white"/> 2343 2348 </v:shape><![endif]--><![if !vml]><img width=60 height=35 2344 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 73.png"2349 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image042.png" 2345 2350 v:shapes="_x0000_i1025"><![endif]></span><![endif]>.<span 2346 2351 style='mso-spacerun:yes'> </span>For cubic crystal symmetry, the term <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span … … 2361 2366 o:title="" chromakey="white"/> 2362 2367 </v:shape><![endif]--><![if !vml]><img width=64 height=35 2363 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 72.png"2368 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image040.png" 2364 2369 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 2365 2370 style='mso-spacerun:yes'> </span>is obtained directly from the Fourier … … 2422 2427 o:title="" chromakey="white"/> 2423 2428 </v:shape><![endif]--><![if !vml]><img width=258 height=70 2424 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 74.png"2429 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image044.png" 2425 2430 v:shapes="_x0000_i1025"><![endif]></span><![endif]></p> 2426 2431 … … 2441 2446 o:title="" chromakey="white"/> 2442 2447 </v:shape><![endif]--><![if !vml]><img width=30 height=35 2443 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 75.png"2448 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image046.png" 2444 2449 v:shapes="_x0000_i1025"><![endif]></span><![endif]>, as tabulated by Bunge 2445 2450 (1982). </p> … … 2463 2468 o:title="" chromakey="white"/> 2464 2469 </v:shape><![endif]--><![if !vml]><img width=29 height=35 2465 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 76.png"2466 v:shapes="_x0000_i1025"><![endif]></span><![endif]>, and the three sample 2467 orientationangles, <span style='font-family:Symbol'>W</span><sub>s</sub>, <span2470 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image048.png" 2471 v:shapes="_x0000_i1025"><![endif]></span><![endif]>, and the three sample orientation 2472 angles, <span style='font-family:Symbol'>W</span><sub>s</sub>, <span 2468 2473 style='font-family:Symbol'>C</span><sub>s</sub>, <span style='font-family:Symbol'>F</span><sub>s</sub>, 2469 2474 all of which can be adjustable parameters of the refinement. Once the … … 2484 2489 o:title="" chromakey="white"/> 2485 2490 </v:shape><![endif]--><![if !vml]><img width=29 height=35 2486 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 76.png"2491 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image048.png" 2487 2492 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 2488 2493 style='mso-spacerun:yes'> </span>and the sample orientation angles <span … … 2542 2547 o:title="" chromakey="white"/> 2543 2548 </v:shape><![endif]--><![if !vml]><img width=241 height=72 2544 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 77.png"2549 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image050.png" 2545 2550 v:shapes="_x0000_i1025"><![endif]></span><![endif]></p> 2546 2551 … … 2554 2559 to accommodate the two possible uses of this correction. In one, a suite of 2555 2560 spherical harmonics coefficients is defined for the texture of a phase in the 2556 sample; this can have any of the possible sample symmetries and is the usual 2557 result desired for texture analysis. The other is the suite of spherical 2558 harmonicsterms for cylindrical sample symmetry for each phase in each powder pattern2561 sample; this can have any of the possible sample symmetries and is the usual result 2562 desired for texture analysis. The other is the suite of spherical harmonics 2563 terms for cylindrical sample symmetry for each phase in each powder pattern 2559 2564 (histogram) and is usually used to accommodate preferred orientation effects 2560 2565 in a Rietveld refinement. The former description allows refinement of the 2561 2566 sample orientation zeros, <span style='font-family:Symbol'>W</span><sub>s</sub>, 2562 2567 <span style='font-family:Symbol'>C</span><sub>s</sub>, <span style='font-family: 2563 Symbol'>F</span><sub>s</sub>, but the latter description does not (they are 2564 assumedto be zero and not refinable). The sample orientation angles, (<span2568 Symbol'>F</span><sub>s</sub>, but the latter description does not (they are assumed 2569 to be zero and not refinable). The sample orientation angles, (<span 2565 2570 style='font-family:Symbol'>W</span>, <span style='font-family:Symbol'>C</span>, 2566 2571 <span style='font-family:Symbol'>F) </span>are specified in the Sample … … 2617 2622 o:spid="_x0000_i1081" type="#_x0000_t75" style='width:468pt;height:401.25pt; 2618 2623 visibility:visible;mso-wrap-style:square'> 2619 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 105.png"2624 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image051.png" 2620 2625 o:title=""/> 2621 2626 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 2622 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image0 78.png"2627 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image052.png" 2623 2628 v:shapes="Picture_x0020_58"><![endif]></span></p> 2624 2629 2625 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span2626 class=GramE>and</span> the <b style='mso-bidi-font-weight:normal'><span 2627 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2628 mso-hansi-theme-font:minor-latin'>ImageControls</span></b> data page will show</p>2630 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and the <b 2631 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2632 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 2633 Controls</span></b> data page will show</p> 2629 2634 2630 2635 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 2632 2637 o:spid="_x0000_i1080" type="#_x0000_t75" style='width:468pt;height:291.75pt; 2633 2638 visibility:visible;mso-wrap-style:square'> 2634 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 107.png"2639 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image053.png" 2635 2640 o:title=""/> 2636 2641 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=389 2637 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 163.png"2642 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image054.png" 2638 2643 v:shapes="Picture_x0020_59"><![endif]></span></p> 2639 2644 … … 2661 2666 o:spid="_x0000_i1079" type="#_x0000_t75" style='width:468pt;height:291.75pt; 2662 2667 visibility:visible;mso-wrap-style:square'> 2663 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 109.png"2668 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image055.png" 2664 2669 o:title=""/> 2665 2670 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=389 2666 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 164.png"2671 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image056.png" 2667 2672 v:shapes="Picture_x0020_60"><![endif]></span></p> 2668 2673 … … 2687 2692 o:spid="_x0000_i1078" type="#_x0000_t75" style='width:468pt;height:391.5pt; 2688 2693 visibility:visible;mso-wrap-style:square'> 2689 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 111.png"2694 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image057.png" 2690 2695 o:title=""/> 2691 2696 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=522 2692 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 165.png"2697 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image058.png" 2693 2698 v:shapes="Picture_x0020_61"><![endif]></span></p> 2694 2699 2695 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>For texture analysis 2696 we will need to integrate the image into a number of slices sampling the 2697 changing ring intensity with azimuthal angle. Also note that the image seems to 2698 have <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2699 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>mm</span></b> 2700 symmetry so that the unique part of this intensity variation covers 0-90° of 2701 azimuth. In addition the ring intensity variation is such that using 10° slices 2702 will capture it reasonably well. However, we want to include both 0° and 90° as 2703 slice centers. Thus there will be 10 slices beginning at -5° and ending at 95°. 2704 Check the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2705 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Show 2706 integration limits?</span></b> box and uncheck the <b style='mso-bidi-font-weight: 2700 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>For texture 2701 analysis we will need to integrate the image into a number of slices sampling 2702 the changing ring intensity with azimuthal angle. Also note that the image 2703 seems to have <b style='mso-bidi-font-weight:normal'><span style='font-family: 2704 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 2705 minor-latin'>mm</span></b> symmetry so that the unique part of this intensity 2706 variation covers 0-90° of azimuth. In addition the ring intensity variation is 2707 such that using 10° slices will capture it reasonably well. However, we want to 2708 include both 0° and 90° as slice centers. Thus there will be 10 slices 2709 beginning at -5° and ending at 95°. Check the <b style='mso-bidi-font-weight: 2707 2710 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2708 minor-latin;mso-hansi-theme-font:minor-latin'>Do full integration? </span></b>box, 2709 enter <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2711 minor-latin;mso-hansi-theme-font:minor-latin'>Show integration limits?</span></b> 2712 box and uncheck the <b style='mso-bidi-font-weight:normal'><span 2713 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2714 mso-hansi-theme-font:minor-latin'>Do full integration? </span></b>box, enter <b 2715 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2710 2716 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>10</span></b> 2711 2717 in the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; … … 2735 2741 o:spid="_x0000_i1077" type="#_x0000_t75" style='width:468pt;height:391.5pt; 2736 2742 visibility:visible;mso-wrap-style:square'> 2737 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 113.png"2743 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image059.png" 2738 2744 o:title=""/> 2739 2745 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=522 2740 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 166.png"2746 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image060.png" 2741 2747 v:shapes="Picture_x0020_62"><![endif]></span></p> 2742 2748 … … 2750 2756 o:spid="_x0000_i1076" type="#_x0000_t75" style='width:468pt;height:291.75pt; 2751 2757 visibility:visible;mso-wrap-style:square'> 2752 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 115.png"2758 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image061.png" 2753 2759 o:title=""/> 2754 2760 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=389 2755 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 167.png"2761 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image062.png" 2756 2762 v:shapes="Picture_x0020_63"><![endif]></span></p> 2757 2763 … … 2767 2773 o:spid="_x0000_i1075" type="#_x0000_t75" style='width:468pt;height:143.25pt; 2768 2774 visibility:visible;mso-wrap-style:square'> 2769 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 117.png"2775 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image063.png" 2770 2776 o:title=""/> 2771 2777 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=191 2772 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 168.png"2778 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image064.png" 2773 2779 v:shapes="Picture_x0020_64"><![endif]></span></p> 2774 2780 … … 2778 2784 threshold</span></b> to <b style='mso-bidi-font-weight:normal'><span 2779 2785 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2780 mso-hansi-theme-font:minor-latin'>2500</span></b>; the image will be redrawn 2781 reflecting this mask. By zooming in you may see isolated red pixels; these are 2782 excluded points. Make sure the diffraction rings do not have any excluded 2783 points. Forexample with the level set to 2200 the plot shows</p>2786 mso-hansi-theme-font:minor-latin'>2500</span></b>; the image will be redrawn reflecting 2787 this mask. By zooming in you may see isolated red pixels; these are excluded 2788 points. Make sure the diffraction rings do not have any excluded points. For 2789 example with the level set to 2200 the plot shows</p> 2784 2790 2785 2791 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 2787 2793 o:spid="_x0000_i1074" type="#_x0000_t75" style='width:468pt;height:391.5pt; 2788 2794 visibility:visible;mso-wrap-style:square'> 2789 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 119.png"2795 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image065.png" 2790 2796 o:title=""/> 2791 2797 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=522 2792 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 169.png"2798 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image066.png" 2793 2799 v:shapes="Picture_x0020_65"><![endif]></span></p> 2794 2800 2795 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span2796 class=GramE>for</span> one ring. This level is too low. Return to the <b 2797 style=' mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;2798 mso- ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image2799 Controls</span></b> item in the datatree.</p>2801 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>for one ring. 2802 This level is too low. Return to the <b style='mso-bidi-font-weight:normal'><span 2803 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2804 mso-hansi-theme-font:minor-latin'>Image Controls</span></b> item in the data 2805 tree.</p> 2800 2806 2801 2807 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>We are now … … 2812 2818 o:spid="_x0000_i1073" type="#_x0000_t75" style='width:468pt;height:391.5pt; 2813 2819 visibility:visible;mso-wrap-style:square'> 2814 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 121.png"2820 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image067.png" 2815 2821 o:title=""/> 2816 2822 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=522 2817 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 170.png"2823 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image068.png" 2818 2824 v:shapes="Picture_x0020_66"><![endif]></span></p> 2819 2825 … … 2888 2894 o:spid="_x0000_i1072" type="#_x0000_t75" style='width:468pt;height:132pt; 2889 2895 visibility:visible;mso-wrap-style:square'> 2890 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 123.png"2896 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image069.png" 2891 2897 o:title=""/> 2892 2898 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=176 2893 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 171.png"2899 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image070.png" 2894 2900 v:shapes="Picture_x0020_68"><![endif]></span></p> 2895 2901 2896 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span2897 class=GramE>and</span> the B19Atoms table should be</p>2902 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and the B19 2903 Atoms table should be</p> 2898 2904 2899 2905 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 2901 2907 o:spid="_x0000_i1071" type="#_x0000_t75" style='width:468pt;height:132pt; 2902 2908 visibility:visible;mso-wrap-style:square'> 2903 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 125.png"2909 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image071.png" 2904 2910 o:title=""/> 2905 2911 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=176 2906 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 172.png"2912 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image072.png" 2907 2913 v:shapes="Picture_x0020_69"><![endif]></span></p> 2908 2914 … … 2912 2918 tab for each phase; there will be a message indicating the lack of data for 2913 2919 each. Do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2914 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Phase/Add2915 powder histograms</span></b>, do <b style='mso-bidi-font-weight:normal'><span2920 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit 2921 Phase/Add powder histograms</span></b>, do <b style='mso-bidi-font-weight:normal'><span 2916 2922 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2917 2923 mso-hansi-theme-font:minor-latin'>Set All</span></b> on the popup selection … … 2924 2930 o:spid="_x0000_i1070" type="#_x0000_t75" style='width:468pt;height:325.5pt; 2925 2931 visibility:visible;mso-wrap-style:square'> 2926 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 127.png"2932 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image073.png" 2927 2933 o:title=""/> 2928 2934 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=434 2929 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 173.png"2935 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image074.png" 2930 2936 v:shapes="Picture_x0020_70"><![endif]></span></p> 2931 2937 2932 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span2933 class=GramE>and</span> that forB19 will be</p>2938 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and that for 2939 B19 will be</p> 2934 2940 2935 2941 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 2937 2943 o:spid="_x0000_i1069" type="#_x0000_t75" style='width:468pt;height:341.25pt; 2938 2944 visibility:visible;mso-wrap-style:square'> 2939 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 129.png"2945 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image075.png" 2940 2946 o:title=""/> 2941 2947 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=455 2942 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 174.png"2948 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image076.png" 2943 2949 v:shapes="Picture_x0020_71"><![endif]></span></p> 2944 2950 … … 2970 2976 case because of the relatively small number of histograms (10 in this case) 2971 2977 needed for the texture determination; do recall that each phase in each 2972 histogram has a set of parameters (e.g. phase fraction, size, <span 2973 class=SpellE>mustrain</span> & hydrostatic strain) in addition to the ones 2974 for each histogram (e.g. background & scale factor). Consequently the total 2975 number of parameters can build up very quickly in this method of analysis. The 2976 other two methods seek to reduce this problem by splitting the fitting into a 2977 sequential refinement (histogram by histogram) step followed by a texture 2978 fitting step.</p> 2978 histogram has a set of parameters (e.g. phase fraction, size, mustrain & 2979 hydrostatic strain) in addition to the ones for each histogram (e.g. background 2980 & scale factor). Consequently the total number of parameters can build up 2981 very quickly in this method of analysis. The other two methods seek to reduce 2982 this problem by splitting the fitting into a sequential refinement (histogram 2983 by histogram) step followed by a texture fitting step.</p> 2979 2984 2980 2985 <h3 style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt;margin-left: … … 3008 3013 varying the phase fractions instead.</p> 3009 3014 3010 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Next select the3011 B2 phase and pick the Data tab; you will see</p>3015 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Next select 3016 the B2 phase and pick the Data tab; you will see</p> 3012 3017 3013 3018 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3015 3020 o:spid="_x0000_i1068" type="#_x0000_t75" style='width:468pt;height:353.25pt; 3016 3021 visibility:visible;mso-wrap-style:square'> 3017 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 131.png"3022 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image077.png" 3018 3023 o:title=""/> 3019 3024 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=471 3020 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 175.png"3025 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image078.png" 3021 3026 v:shapes="Picture_x0020_72"><![endif]></span></p> 3022 3027 … … 3028 3033 mso-hansi-theme-font:minor-latin'>Edit Phase/Copy data</span></b>, select <b 3029 3034 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3030 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Set <span 3031 class=GramE>All</span></span></b> & press <b style='mso-bidi-font-weight: 3032 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3033 minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b> to copy these to 3034 the other histograms. Next select the <b style='mso-bidi-font-weight:normal'><span 3035 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3036 mso-hansi-theme-font:minor-latin'>B19</span></b> phase and repeat this 3037 process. We are now ready for the first refinement; do <b style='mso-bidi-font-weight: 3038 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3039 minor-latin;mso-hansi-theme-font:minor-latin'>Calculate/Refine</span></b> from 3040 the main GSAS-II data tree window. A progress bar popup will appear and when 3041 done a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3042 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Refinement 3043 results</span></b> popup will show with Rw~32%. Press <b style='mso-bidi-font-weight: 3044 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3045 minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b> to load this 3046 result; GSAS-II will return you to the last window you were using and display 3047 (NB: pick the 1<sup>st</sup> PWDR entry) the 1<sup>st</sup> powder pattern 3048 showing you the fit</p> 3035 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Set All</span></b> 3036 & press <b style='mso-bidi-font-weight:normal'><span style='font-family: 3037 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3038 minor-latin'>OK</span></b> to copy these to the other histograms. Next select 3039 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3040 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>B19</span></b> 3041 phase and repeat this process. We are now ready for the first refinement; do <b 3042 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3043 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Calculate/Refine</span></b> 3044 from the main GSAS-II data tree window. A progress bar popup will appear and 3045 when done a <b style='mso-bidi-font-weight:normal'><span style='font-family: 3046 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3047 minor-latin'>Refinement results</span></b> popup will show with Rw~32%. Press <b 3048 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3049 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b> 3050 to load this result; GSAS-II will return you to the last window you were using 3051 and display (NB: pick the 1<sup>st</sup> PWDR entry) the 1<sup>st</sup> powder 3052 pattern showing you the fit</p> 3049 3053 3050 3054 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3052 3056 o:spid="_x0000_i1067" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3053 3057 visibility:visible;mso-wrap-style:square'> 3054 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 133.png"3058 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image079.png" 3055 3059 o:title=""/> 3056 3060 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3057 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 176.png"3061 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image080.png" 3058 3062 v:shapes="Picture_x0020_73"><![endif]></span></p> 3059 3063 … … 3076 3080 o:spid="_x0000_i1066" type="#_x0000_t75" style='width:468pt;height:164.25pt; 3077 3081 visibility:visible;mso-wrap-style:square'> 3078 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 135.png"3082 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image081.png" 3079 3083 o:title=""/> 3080 3084 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=219 3081 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 177.png"3085 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image082.png" 3082 3086 v:shapes="Picture_x0020_74"><![endif]></span></p> 3083 3087 … … 3101 3105 o:spid="_x0000_i1065" type="#_x0000_t75" style='width:468pt;height:174pt; 3102 3106 visibility:visible;mso-wrap-style:square'> 3103 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 137.png"3107 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image083.png" 3104 3108 o:title=""/> 3105 3109 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=232 3106 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 178.png"3110 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image084.png" 3107 3111 v:shapes="Picture_x0020_75"><![endif]></span></p> 3108 3112 … … 3121 3125 o:spid="_x0000_i1064" type="#_x0000_t75" style='width:468pt;height:240.75pt; 3122 3126 visibility:visible;mso-wrap-style:square'> 3123 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 139.png"3127 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image085.png" 3124 3128 o:title=""/> 3125 3129 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=321 3126 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 179.png"3130 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image086.png" 3127 3131 v:shapes="Picture_x0020_76"><![endif]></span></p> 3128 3132 3129 3133 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Then do <b 3130 3134 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3131 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Phase/Copy3132 flags</span></b> to have <b style='mso-bidi-font-weight:normal'><span3135 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit 3136 Phase/Copy flags</span></b> to have <b style='mso-bidi-font-weight:normal'><span 3133 3137 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3134 3138 mso-hansi-theme-font:minor-latin'>D11</span></b> refined for all PWDR data … … 3151 3155 o:spid="_x0000_i1063" type="#_x0000_t75" style='width:468pt;height:227.25pt; 3152 3156 visibility:visible;mso-wrap-style:square'> 3153 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 141.png"3157 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image087.png" 3154 3158 o:title=""/> 3155 3159 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=303 3156 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 180.png"3160 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image088.png" 3157 3161 v:shapes="Picture_x0020_77"><![endif]></span></p> 3158 3162 … … 3173 3177 o:spid="_x0000_i1062" type="#_x0000_t75" style='width:468pt;height:270pt; 3174 3178 visibility:visible;mso-wrap-style:square'> 3175 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 143.png"3179 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image089.png" 3176 3180 o:title=""/> 3177 3181 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=360 3178 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 181.png"3182 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image090.png" 3179 3183 v:shapes="Picture_x0020_78"><![endif]></span></p> 3180 3184 … … 3189 3193 o:spid="_x0000_i1061" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3190 3194 visibility:visible;mso-wrap-style:square'> 3191 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 145.png"3195 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image091.png" 3192 3196 o:title=""/> 3193 3197 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3194 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 182.png"3198 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image092.png" 3195 3199 v:shapes="Picture_x0020_79"><![endif]></span></p> 3196 3200 … … 3206 3210 mso-hansi-theme-font:minor-latin'>microstrain</span></b></span> box. Then do <b 3207 3211 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3208 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Phase/Copy3209 flags</span></b> to set it for the other PWDR data sets. Do the same for the <b 3210 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;3212 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit 3213 Phase/Copy flags</span></b> to set it for the other PWDR data sets. Do the same 3214 for the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3211 3215 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>B19</span></b> 3212 3216 phase. Then do <b style='mso-bidi-font-weight:normal'><span style='font-family: … … 3225 3229 o:spid="_x0000_i1060" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3226 3230 visibility:visible;mso-wrap-style:square'> 3227 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 147.png"3231 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image093.png" 3228 3232 o:title=""/> 3229 3233 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3230 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 183.png"3234 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image094.png" 3231 3235 v:shapes="Picture_x0020_80"><![endif]></span></p> 3232 3236 … … 3240 3244 o:spid="_x0000_i1059" type="#_x0000_t75" style='width:468pt;height:192.75pt; 3241 3245 visibility:visible;mso-wrap-style:square'> 3242 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 149.png"3246 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image095.png" 3243 3247 o:title=""/> 3244 3248 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=257 3245 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 184.png"3249 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image096.png" 3246 3250 v:shapes="Picture_x0020_81"><![endif]></span></p> 3247 3251 … … 3255 3259 o:spid="_x0000_i1058" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3256 3260 visibility:visible;mso-wrap-style:square'> 3257 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 151.png"3261 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image097.png" 3258 3262 o:title=""/> 3259 3263 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3260 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 185.png"3264 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image098.png" 3261 3265 v:shapes="Picture_x0020_82"><![endif]></span></p> 3262 3266 … … 3274 3278 o:spid="_x0000_i1057" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3275 3279 visibility:visible;mso-wrap-style:square'> 3276 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 153.png"3280 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image099.png" 3277 3281 o:title=""/> 3278 3282 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3279 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 86.png"3283 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image100.png" 3280 3284 v:shapes="Picture_x0020_83"><![endif]></span></p> 3281 3285 3282 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>This phase is 3283 verystrongly textured (the cursor shows 12-13 MRD at the peaks) along the -1403286 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>This phase is very 3287 strongly textured (the cursor shows 12-13 MRD at the peaks) along the -140 3284 3288 direction. Again we want to increment the Harmonic order to the next higher 3285 3289 level (8). Again do Calculate/Refine from the main menu; the <span … … 3301 3305 o:spid="_x0000_i1056" type="#_x0000_t75" style='width:468pt;height:237.75pt; 3302 3306 visibility:visible;mso-wrap-style:square'> 3303 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 55.png"3307 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image101.png" 3304 3308 o:title=""/> 3305 3309 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=317 3306 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 87.png"3310 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image102.png" 3307 3311 v:shapes="Picture_x0020_84"><![endif]></span></p> 3308 3312 3309 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span3310 class=GramE>and</span> inversepole figure</p>3313 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and inverse 3314 pole figure</p> 3311 3315 3312 3316 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3314 3318 o:spid="_x0000_i1055" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3315 3319 visibility:visible;mso-wrap-style:square'> 3316 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 57.png"3320 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image103.png" 3317 3321 o:title=""/> 3318 3322 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3319 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 88.png"3323 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image104.png" 3320 3324 v:shapes="Picture_x0020_85"><![endif]></span></p> 3321 3325 … … 3327 3331 o:spid="_x0000_i1054" type="#_x0000_t75" style='width:468pt;height:168pt; 3328 3332 visibility:visible;mso-wrap-style:square'> 3329 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 59.png"3333 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image105.png" 3330 3334 o:title=""/> 3331 3335 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=224 3332 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 89.png"3336 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image106.png" 3333 3337 v:shapes="Picture_x0020_86"><![endif]></span></p> 3334 3338 3335 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span3336 class=GramE>and</span> inversepole figure</p>3339 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and inverse 3340 pole figure</p> 3337 3341 3338 3342 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3340 3344 o:spid="_x0000_i1053" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3341 3345 visibility:visible;mso-wrap-style:square'> 3342 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 61.png"3346 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image107.png" 3343 3347 o:title=""/> 3344 3348 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3345 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 90.png"3349 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image108.png" 3346 3350 v:shapes="Picture_x0020_87"><![endif]></span></p> 3347 3351 3348 3352 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>This completes 3349 the tutorial on Method A for doing texture analysis. It is useful for a case 3350 likethis one where there are very few data sets required for the texture analysis.3353 the tutorial on Method A for doing texture analysis. It is useful for a case like 3354 this one where there are very few data sets required for the texture analysis. 3351 3355 However, for the case of lower sample symmetry one must several dozen or even a 3352 3356 few hundred histograms and then the suite of parameters can easily be > 1000 … … 3423 3427 mso-hansi-theme-font:minor-latin'>Spherical harmonics</span></b>. Then do <b 3424 3428 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3425 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Phase/Copy 3426 data</span></b> to copy both the flag and the model to the other PWDR entries.</p> 3429 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit 3430 Phase/Copy data</span></b> to copy both the flag and the model to the other 3431 PWDR entries.</p> 3427 3432 3428 3433 <p class=MsoListParagraphCxSpLast style='margin-bottom:12.0pt;mso-add-space: … … 3443 3448 mso-hansi-theme-font:minor-latin'>Spherical harmonics</span></b>. Then do <b 3444 3449 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3445 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Phase/Copy 3446 data</span></b> to copy both the flag and the model to the other PWDR entries.</p> 3450 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit 3451 Phase/Copy data</span></b> to copy both the flag and the model to the other 3452 PWDR entries.</p> 3447 3453 3448 3454 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Now select <b … … 3455 3461 o:spid="_x0000_i1052" type="#_x0000_t75" style='width:468pt;height:143.25pt; 3456 3462 visibility:visible;mso-wrap-style:square'> 3457 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 91.png"3463 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image109.png" 3458 3464 o:title=""/> 3459 3465 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=191 3460 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 92.png"3466 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image110.png" 3461 3467 v:shapes="Picture_x0020_88"><![endif]></span></p> 3462 3468 … … 3480 3486 o:spid="_x0000_i1051" type="#_x0000_t75" style='width:468pt;height:149.25pt; 3481 3487 visibility:visible;mso-wrap-style:square'> 3482 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 93.png"3488 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image111.png" 3483 3489 o:title=""/> 3484 3490 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=199 3485 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 94.png"3491 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image112.png" 3486 3492 v:shapes="Picture_x0020_89"><![endif]></span></p> 3487 3493 … … 3510 3516 o:spid="_x0000_i1050" type="#_x0000_t75" style='width:468pt;height:132pt; 3511 3517 visibility:visible;mso-wrap-style:square'> 3512 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 95.png"3518 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image113.png" 3513 3519 o:title=""/> 3514 3520 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=176 3515 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 96.png"3521 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image114.png" 3516 3522 v:shapes="Picture_x0020_90"><![endif]></span></p> 3517 3523 3518 3524 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>There is a row 3519 for each data set and columns for all refined parameters and some derived ones 3520 along with residual and convergence indicators. The residuals are not very good 3521 (we havent really refined much) but the Δχ<sup>2</sup> column shows 3522 that convergence was achieved (NB: poor convergence will be highlighted in 3523 yellow orred depending on how bad it is).</p>3525 for each data set and columns for all refined parameters and some derived ones along 3526 with residual and convergence indicators. The residuals are not very good (we 3527 havent really refined much) but the Δχ<sup>2</sup> column shows that 3528 convergence was achieved (NB: poor convergence will be highlighted in yellow or 3529 red depending on how bad it is).</p> 3524 3530 3525 3531 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>If you examine … … 3531 3537 o:spid="_x0000_i1049" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3532 3538 visibility:visible;mso-wrap-style:square'> 3533 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 97.png"3539 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image115.png" 3534 3540 o:title=""/> 3535 3541 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3536 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 98.png"3542 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image116.png" 3537 3543 v:shapes="Picture_x0020_91"><![endif]></span></p> 3538 3544 … … 3544 3550 o:spid="_x0000_i1048" type="#_x0000_t75" style='width:381pt;height:375pt; 3545 3551 visibility:visible;mso-wrap-style:square'> 3546 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 083.png"3552 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image117.png" 3547 3553 o:title=""/> 3548 3554 </v:shape><![endif]--><![if !vml]><img border=0 width=508 height=500 3549 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 083.png"3555 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image117.png" 3550 3556 v:shapes="Picture_x0020_5"><![endif]></span></p> 3551 3557 … … 3570 3576 for the file selection. Then do <b style='mso-bidi-font-weight:normal'><span 3571 3577 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3572 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Edit Phase/Copy3573 selected data</span></b>; that will bring up a new popup</p>3578 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Edit 3579 Phase/Copy selected data</span></b>; that will bring up a new popup</p> 3574 3580 3575 3581 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3577 3583 o:spid="_x0000_i1047" type="#_x0000_t75" style='width:241.5pt;height:292.5pt; 3578 3584 visibility:visible;mso-wrap-style:square'> 3579 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 99.png"3585 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image118.png" 3580 3586 o:title=""/> 3581 3587 </v:shape><![endif]--><![if !vml]><img border=0 width=322 height=390 3582 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image1 99.png"3588 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image118.png" 3583 3589 v:shapes="Picture_x0020_92"><![endif]></span></p> 3584 3590 … … 3592 3598 the file selection is next. Do <b style='mso-bidi-font-weight:normal'><span 3593 3599 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3594 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set <span 3595 class=GramE>All</span></span></b> and <b style='mso-bidi-font-weight:normal'><span 3596 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3597 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b> 3598 to do this copy. That copies the full spherical harmonics model to the other 3599 data sets. Select one to check if youd like.</p> 3600 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set All</span></b> 3601 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3602 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: 3603 minor-latin'>OK</span></b> to do this copy. That copies the full spherical 3604 harmonics model to the other data sets. Select one to check if youd like.</p> 3600 3605 3601 3606 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Next do the … … 3615 3620 o:spid="_x0000_i1046" type="#_x0000_t75" style='width:468pt;height:315.75pt; 3616 3621 visibility:visible;mso-wrap-style:square'> 3617 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 200.png"3622 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image119.png" 3618 3623 o:title=""/> 3619 3624 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=421 3620 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 201.png"3625 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image120.png" 3621 3626 v:shapes="Picture_x0020_93"><![endif]></span></p> 3622 3627 … … 3633 3638 o:spid="_x0000_i1045" type="#_x0000_t75" style='width:468pt;height:153pt; 3634 3639 visibility:visible;mso-wrap-style:square'> 3635 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 202.png"3640 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image121.png" 3636 3641 o:title=""/> 3637 3642 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=204 3638 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 203.png"3643 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image122.png" 3639 3644 v:shapes="Picture_x0020_95"><![endif]></span></p> 3640 3645 … … 3647 3652 o:spid="_x0000_i1044" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3648 3653 visibility:visible;mso-wrap-style:square'> 3649 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 204.png"3654 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image123.png" 3650 3655 o:title=""/> 3651 3656 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3652 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 205.png"3657 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image124.png" 3653 3658 v:shapes="Picture_x0020_96"><![endif]></span></p> 3654 3659 3655 3660 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>As our 3656 3661 experience in Method A, the calculated peaks are too sharp. We need to vary the 3657 <span class=SpellE>mustrain</span> parameters for both phases. Go to the Data 3658 t ab for each phase, check the <span class=SpellE><b style='mso-bidi-font-weight:3659 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3660 m inor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>microstrain</span></b></span>3662 mustrain parameters for both phases. Go to the Data tab for each phase, check 3663 the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 3664 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3665 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>microstrain</span></b></span> 3661 3666 box and do <b style='mso-bidi-font-weight:normal'><span style='font-family: 3662 3667 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: … … 3672 3677 o:spid="_x0000_i1043" type="#_x0000_t75" style='width:468pt;height:153pt; 3673 3678 visibility:visible;mso-wrap-style:square'> 3674 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 206.png"3679 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image125.png" 3675 3680 o:title=""/> 3676 3681 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=204 3677 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 207.png"3682 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image126.png" 3678 3683 v:shapes="Picture_x0020_97"><![endif]></span></p> 3679 3684 … … 3685 3690 o:spid="_x0000_i1042" type="#_x0000_t75" style='width:468pt;height:153pt; 3686 3691 visibility:visible;mso-wrap-style:square'> 3687 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 208.png"3692 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image127.png" 3688 3693 o:title=""/> 3689 3694 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=204 3690 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 209.png"3695 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image128.png" 3691 3696 v:shapes="Picture_x0020_98"><![endif]></span></p> 3692 3697 … … 3699 3704 o:spid="_x0000_i1041" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3700 3705 visibility:visible;mso-wrap-style:square'> 3701 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 210.png"3706 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image129.png" 3702 3707 o:title=""/> 3703 3708 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3704 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 211.png"3709 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image130.png" 3705 3710 v:shapes="Picture_x0020_99"><![endif]></span></p> 3706 3711 … … 3728 3733 o:spid="_x0000_i1040" type="#_x0000_t75" style='width:468pt;height:153pt; 3729 3734 visibility:visible;mso-wrap-style:square'> 3730 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 212.png"3735 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image131.png" 3731 3736 o:title=""/> 3732 3737 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=204 3733 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 213.png"3738 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image132.png" 3734 3739 v:shapes="Picture_x0020_100"><![endif]></span></p> 3735 3740 … … 3757 3762 o:spid="_x0000_i1039" type="#_x0000_t75" style='width:468pt;height:153pt; 3758 3763 visibility:visible;mso-wrap-style:square'> 3759 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 214.png"3764 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image133.png" 3760 3765 o:title=""/> 3761 3766 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=204 3762 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 215.png"3767 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image134.png" 3763 3768 v:shapes="Picture_x0020_101"><![endif]></span></p> 3764 3769 3765 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span3766 class=GramE>and</span> for theB19 phase we see</p>3770 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and for the 3771 B19 phase we see</p> 3767 3772 3768 3773 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3770 3775 o:spid="_x0000_i1038" type="#_x0000_t75" style='width:468pt;height:153pt; 3771 3776 visibility:visible;mso-wrap-style:square'> 3772 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 216.png"3777 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image135.png" 3773 3778 o:title=""/> 3774 3779 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=204 3775 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 217.png"3780 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image136.png" 3776 3781 v:shapes="Picture_x0020_102"><![endif]></span></p> 3777 3782 … … 3787 3792 o:spid="_x0000_i1037" type="#_x0000_t75" style='width:456pt;height:217.5pt; 3788 3793 visibility:visible;mso-wrap-style:square'> 3789 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 065.png"3794 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image137.png" 3790 3795 o:title=""/> 3791 3796 </v:shape><![endif]--><![if !vml]><img border=0 width=608 height=290 3792 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 065.png"3797 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image137.png" 3793 3798 v:shapes="Picture_x0020_16"><![endif]></span></p> 3794 3799 … … 3815 3820 o:spid="_x0000_i1036" type="#_x0000_t75" style='width:468pt;height:168.75pt; 3816 3821 visibility:visible;mso-wrap-style:square'> 3817 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 218.png"3822 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image138.png" 3818 3823 o:title=""/> 3819 3824 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=225 3820 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 219.png"3825 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image139.png" 3821 3826 v:shapes="Picture_x0020_103"><![endif]></span></p> 3822 3827 … … 3831 3836 o:spid="_x0000_i1035" type="#_x0000_t75" style='width:468pt;height:168.75pt; 3832 3837 visibility:visible;mso-wrap-style:square'> 3833 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 220.png"3838 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image140.png" 3834 3839 o:title=""/> 3835 3840 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=225 3836 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 221.png"3841 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image141.png" 3837 3842 v:shapes="Picture_x0020_104"><![endif]></span></p> 3838 3843 … … 3849 3854 o:spid="_x0000_i1034" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3850 3855 visibility:visible;mso-wrap-style:square'> 3851 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 222.png"3856 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image142.png" 3852 3857 o:title=""/> 3853 3858 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3854 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 223.png"3859 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image143.png" 3855 3860 v:shapes="Picture_x0020_105"><![endif]></span></p> 3856 3861 3857 3862 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>This is 3858 essentially the same as we obtained earlier in Method <span class=GramE>A</span>3859 (maybe not quite asstrong here).</p>3863 essentially the same as we obtained earlier in Method A (maybe not quite as 3864 strong here).</p> 3860 3865 3861 3866 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Now select the … … 3872 3877 o:spid="_x0000_i1033" type="#_x0000_t75" style='width:468pt;height:243pt; 3873 3878 visibility:visible;mso-wrap-style:square'> 3874 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 224.png"3879 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image144.png" 3875 3880 o:title=""/> 3876 3881 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=324 3877 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 225.png"3882 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image145.png" 3878 3883 v:shapes="Picture_x0020_106"><![endif]></span></p> 3879 3884 … … 3885 3890 o:spid="_x0000_i1032" type="#_x0000_t75" style='width:468pt;height:401.25pt; 3886 3891 visibility:visible;mso-wrap-style:square'> 3887 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 226.png"3892 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image146.png" 3888 3893 o:title=""/> 3889 3894 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 3890 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 227.png"3895 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image147.png" 3891 3896 v:shapes="Picture_x0020_107"><![endif]></span></p> 3892 3897 … … 3971 3976 phase and its <b style='mso-bidi-font-weight:normal'><span style='font-family: 3972 3977 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3973 minor-latin'>Data</span></b> tab. <span class=GramE>Clear</span> the <span 3974 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 3975 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3976 minor-latin'>microstrain</span></b></span>, <b style='mso-bidi-font-weight: 3977 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3978 minor-latin;mso-hansi-theme-font:minor-latin'>D<sub>11</sub></span></b> and <b 3979 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3978 minor-latin'>Data</span></b> tab. Clear the <span class=SpellE><b 3979 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3980 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>microstrain</span></b></span>, 3981 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3982 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>D<sub>11</sub></span></b> 3983 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3980 3984 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Preferred 3981 3985 orientation</span></b> boxes. Also set the <b style='mso-bidi-font-weight:normal'><span … … 3984 3988 avoid a lot of nasty (but harmless) messages at the start of the refinement). 3985 3989 Then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3986 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Phase/Copy3987 flags</span></b> selecting all data to clear all the flags and an <b3988 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3989 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Phase/Copy3990 selected data</span></b> for <span class=SpellE><b style='mso-bidi-font-weight:3990 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit 3991 Phase/Copy flags</span></b> selecting all data to clear all the flags and an <b 3992 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3993 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit 3994 Phase/Copy selected data</span></b> for <span class=SpellE><b style='mso-bidi-font-weight: 3991 3995 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3992 3996 minor-latin;mso-hansi-theme-font:minor-latin'>Pref.Ori</span></b></span> to … … 4018 4022 avoid a lot of nasty (but harmless) messages at the start of the refinement). 4019 4023 Then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 4020 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Phase/Copy4021 flags</span></b> selecting all data to clear all the flags and an <b4022 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 4023 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Phase/Copy4024 selected data</span></b> for <span class=SpellE><b style='mso-bidi-font-weight:4024 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit 4025 Phase/Copy flags</span></b> selecting all data to clear all the flags and an <b 4026 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 4027 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit 4028 Phase/Copy selected data</span></b> for <span class=SpellE><b style='mso-bidi-font-weight: 4025 4029 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 4026 4030 minor-latin;mso-hansi-theme-font:minor-latin'>Pref.Ori</span></b></span> to … … 4046 4050 id="Picture_x0020_108" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:468pt; 4047 4051 height:177pt;visibility:visible;mso-wrap-style:square'> 4048 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 228.png"4052 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image148.png" 4049 4053 o:title=""/> 4050 4054 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=236 4051 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 229.png"4055 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image149.png" 4052 4056 v:shapes="Picture_x0020_108"><![endif]></span></p> 4053 4057 … … 4069 4073 id="Picture_x0020_109" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:468pt; 4070 4074 height:177pt;visibility:visible;mso-wrap-style:square'> 4071 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 230.png"4075 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image150.png" 4072 4076 o:title=""/> 4073 4077 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=236 4074 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 231.png"4078 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image151.png" 4075 4079 v:shapes="Picture_x0020_109"><![endif]></span></p> 4076 4080 … … 4084 4088 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 4085 4089 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Texture</span></b> 4086 tab. <span class=GramE>Set</span> the <b style='mso-bidi-font-weight:normal'><span4087 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 4088 m so-hansi-theme-font:minor-latin'>Harmonic order</span></b> to zero and then4089 back to <bstyle='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;4090 tab. Set the <b style='mso-bidi-font-weight:normal'><span style='font-family: 4091 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 4092 minor-latin'>Harmonic order</span></b> to zero and then back to <b 4093 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 4090 4094 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>10</span></b>. 4091 4095 Leave the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; … … 4107 4111 o:spid="_x0000_i1029" type="#_x0000_t75" style='width:421.5pt;height:97.5pt; 4108 4112 visibility:visible;mso-wrap-style:square'> 4109 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 232.png"4113 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image152.png" 4110 4114 o:title=""/> 4111 4115 </v:shape><![endif]--><![if !vml]><img border=0 width=562 height=130 4112 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 232.png"4116 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image152.png" 4113 4117 v:shapes="Picture_x0020_110"><![endif]></span></p> 4114 4118 4115 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>In this case you4116 do want to do a <span class=SpellE>nonsequential</span> full refinement, so 4117 press the <bstyle='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;4119 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>In this case 4120 you do want to do a nonsequential full refinement, so press the <b 4121 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 4118 4122 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: 4119 4123 minor-latin'>OK</span></b> button. A quick look at the console will show that … … 4137 4141 o:spid="_x0000_i1028" type="#_x0000_t75" style='width:468pt;height:401.25pt; 4138 4142 visibility:visible;mso-wrap-style:square'> 4139 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 233.png"4143 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image153.png" 4140 4144 o:title=""/> 4141 4145 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 4142 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 234.png"4146 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image154.png" 4143 4147 v:shapes="Picture_x0020_111"><![endif]></span></p> 4144 4148 4145 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span4146 class=GramE>which</span> is almost identical to that from Method A.The4149 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>which is 4150 almost identical to that from Method <span class=GramE>A.</span> The 4147 4151 coefficients are seen in</p> 4148 4152 … … 4151 4155 o:spid="_x0000_i1027" type="#_x0000_t75" style='width:468pt;height:177pt; 4152 4156 visibility:visible;mso-wrap-style:square'> 4153 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 235.png"4157 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image155.png" 4154 4158 o:title=""/> 4155 4159 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=236 4156 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 236.png"4160 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image156.png" 4157 4161 v:shapes="Picture_x0020_112"><![endif]></span></p> 4158 4162 … … 4168 4172 o:spid="_x0000_i1026" type="#_x0000_t75" style='width:468pt;height:401.25pt; 4169 4173 visibility:visible;mso-wrap-style:square'> 4170 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 237.png"4174 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image157.png" 4171 4175 o:title=""/> 4172 4176 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=535 4173 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 238.png"4177 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image158.png" 4174 4178 v:shapes="Picture_x0020_113"><![endif]></span></p> 4175 4179 4176 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span4177 class=GramE>a nd</span> also almost identical to what was obtained in Method A;4178 thecoefficients are seen in</p>4180 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and <span 4181 class=GramE>also</span> almost identical to what was obtained in Method A; the 4182 coefficients are seen in</p> 4179 4183 4180 4184 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 4182 4186 o:spid="_x0000_i1025" type="#_x0000_t75" style='width:468pt;height:242.25pt; 4183 4187 visibility:visible;mso-wrap-style:square'> 4184 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 239.png"4188 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image159.png" 4185 4189 o:title=""/> 4186 4190 </v:shape><![endif]--><![if !vml]><img border=0 width=624 height=323 4187 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image 240.png"4191 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image160.png" 4188 4192 v:shapes="Picture_x0020_114"><![endif]></span></p> 4189 4193 -
Tutorials/2DTexture/Texture analysis of 2D data in GSAS-II_files/filelist.xml
r3055 r4923 4 4 <o:File HRef="colorschememapping.xml"/> 5 5 <o:File HRef="image001.png"/> 6 <o:File HRef="image002.png"/> 7 <o:File HRef="image003.png"/> 8 <o:File HRef="image004.png"/> 9 <o:File HRef="image005.png"/> 10 <o:File HRef="image006.png"/> 11 <o:File HRef="image007.png"/> 12 <o:File HRef="image008.png"/> 13 <o:File HRef="image009.png"/> 14 <o:File HRef="image010.png"/> 15 <o:File HRef="image011.png"/> 16 <o:File HRef="image012.png"/> 17 <o:File HRef="image013.png"/> 18 <o:File HRef="image014.png"/> 19 <o:File HRef="image015.png"/> 20 <o:File HRef="image016.png"/> 21 <o:File HRef="image017.png"/> 22 <o:File HRef="image018.png"/> 23 <o:File HRef="image019.png"/> 24 <o:File HRef="image020.png"/> 25 <o:File HRef="image021.png"/> 26 <o:File HRef="image022.png"/> 27 <o:File HRef="image023.png"/> 28 <o:File HRef="image024.png"/> 29 <o:File HRef="image025.png"/> 30 <o:File HRef="image026.png"/> 31 <o:File HRef="image027.png"/> 32 <o:File HRef="image028.png"/> 33 <o:File HRef="image029.png"/> 34 <o:File HRef="image030.png"/> 35 <o:File HRef="image031.png"/> 36 <o:File HRef="image032.png"/> 37 <o:File HRef="image033.png"/> 38 <o:File HRef="image034.png"/> 39 <o:File HRef="image035.png"/> 40 <o:File HRef="image036.png"/> 41 <o:File HRef="image037.png"/> 42 <o:File HRef="image038.png"/> 43 <o:File HRef="image039.png"/> 44 <o:File HRef="image040.png"/> 45 <o:File HRef="image041.png"/> 46 <o:File HRef="image042.png"/> 47 <o:File HRef="image043.png"/> 48 <o:File HRef="image044.png"/> 49 <o:File HRef="image045.png"/> 50 <o:File HRef="image046.png"/> 51 <o:File HRef="image047.png"/> 52 <o:File HRef="image048.png"/> 53 <o:File HRef="image049.png"/> 54 <o:File HRef="image050.png"/> 6 55 <o:File HRef="image051.png"/> 7 <o:File HRef="image003.png"/>8 56 <o:File HRef="image052.png"/> 9 <o:File HRef="image005.png"/>10 57 <o:File HRef="image053.png"/> 11 <o:File HRef="image007.png"/>12 58 <o:File HRef="image054.png"/> 13 <o:File HRef="image009.png"/>14 59 <o:File HRef="image055.png"/> 15 <o:File HRef="image011.png"/>16 60 <o:File HRef="image056.png"/> 17 <o:File HRef="image013.png"/>18 61 <o:File HRef="image057.png"/> 19 <o:File HRef="image015.png"/>20 62 <o:File HRef="image058.png"/> 21 <o:File HRef="image017.png"/>22 63 <o:File HRef="image059.png"/> 23 <o:File HRef="image019.png"/>24 64 <o:File HRef="image060.png"/> 25 <o:File HRef="image021.png"/>26 65 <o:File HRef="image061.png"/> 27 <o:File HRef="image023.png"/>28 66 <o:File HRef="image062.png"/> 29 <o:File HRef="image025.png"/>30 67 <o:File HRef="image063.png"/> 31 <o:File HRef="image027.png"/>32 68 <o:File HRef="image064.png"/> 33 <o:File HRef="image029.png"/> 69 <o:File HRef="image065.png"/> 70 <o:File HRef="image066.png"/> 34 71 <o:File HRef="image067.png"/> 35 <o:File HRef="image031.png"/>36 72 <o:File HRef="image068.png"/> 37 <o:File HRef="image033.png"/>38 73 <o:File HRef="image069.png"/> 39 <o:File HRef="image035.png"/>40 74 <o:File HRef="image070.png"/> 41 <o:File HRef="image037.png"/>42 75 <o:File HRef="image071.png"/> 43 <o:File HRef="image039.png"/>44 76 <o:File HRef="image072.png"/> 45 <o:File HRef="image041.png"/>46 77 <o:File HRef="image073.png"/> 47 <o:File HRef="image043.png"/>48 78 <o:File HRef="image074.png"/> 49 <o:File HRef="image045.png"/>50 79 <o:File HRef="image075.png"/> 51 <o:File HRef="image047.png"/>52 80 <o:File HRef="image076.png"/> 53 <o:File HRef="image049.png"/>54 81 <o:File HRef="image077.png"/> 82 <o:File HRef="image078.png"/> 83 <o:File HRef="image079.png"/> 84 <o:File HRef="image080.png"/> 85 <o:File HRef="image081.png"/> 86 <o:File HRef="image082.png"/> 87 <o:File HRef="image083.png"/> 88 <o:File HRef="image084.png"/> 89 <o:File HRef="image085.png"/> 90 <o:File HRef="image086.png"/> 91 <o:File HRef="image087.png"/> 92 <o:File HRef="image088.png"/> 93 <o:File HRef="image089.png"/> 94 <o:File HRef="image090.png"/> 95 <o:File HRef="image091.png"/> 96 <o:File HRef="image092.png"/> 97 <o:File HRef="image093.png"/> 98 <o:File HRef="image094.png"/> 99 <o:File HRef="image095.png"/> 100 <o:File HRef="image096.png"/> 101 <o:File HRef="image097.png"/> 102 <o:File HRef="image098.png"/> 103 <o:File HRef="image099.png"/> 104 <o:File HRef="image100.png"/> 105 <o:File HRef="image101.png"/> 106 <o:File HRef="image102.png"/> 107 <o:File HRef="image103.png"/> 108 <o:File HRef="image104.png"/> 55 109 <o:File HRef="image105.png"/> 56 <o:File HRef="image 078.png"/>110 <o:File HRef="image106.png"/> 57 111 <o:File HRef="image107.png"/> 58 <o:File HRef="image1 63.png"/>112 <o:File HRef="image108.png"/> 59 113 <o:File HRef="image109.png"/> 60 <o:File HRef="image1 64.png"/>114 <o:File HRef="image110.png"/> 61 115 <o:File HRef="image111.png"/> 62 <o:File HRef="image1 65.png"/>116 <o:File HRef="image112.png"/> 63 117 <o:File HRef="image113.png"/> 64 <o:File HRef="image1 66.png"/>118 <o:File HRef="image114.png"/> 65 119 <o:File HRef="image115.png"/> 66 <o:File HRef="image1 67.png"/>120 <o:File HRef="image116.png"/> 67 121 <o:File HRef="image117.png"/> 68 <o:File HRef="image1 68.png"/>122 <o:File HRef="image118.png"/> 69 123 <o:File HRef="image119.png"/> 70 <o:File HRef="image1 69.png"/>124 <o:File HRef="image120.png"/> 71 125 <o:File HRef="image121.png"/> 72 <o:File HRef="image1 70.png"/>126 <o:File HRef="image122.png"/> 73 127 <o:File HRef="image123.png"/> 74 <o:File HRef="image1 71.png"/>128 <o:File HRef="image124.png"/> 75 129 <o:File HRef="image125.png"/> 76 <o:File HRef="image1 72.png"/>130 <o:File HRef="image126.png"/> 77 131 <o:File HRef="image127.png"/> 78 <o:File HRef="image1 73.png"/>132 <o:File HRef="image128.png"/> 79 133 <o:File HRef="image129.png"/> 80 <o:File HRef="image1 74.png"/>134 <o:File HRef="image130.png"/> 81 135 <o:File HRef="image131.png"/> 82 <o:File HRef="image1 75.png"/>136 <o:File HRef="image132.png"/> 83 137 <o:File HRef="image133.png"/> 84 <o:File HRef="image1 76.png"/>138 <o:File HRef="image134.png"/> 85 139 <o:File HRef="image135.png"/> 86 <o:File HRef="image1 77.png"/>140 <o:File HRef="image136.png"/> 87 141 <o:File HRef="image137.png"/> 88 <o:File HRef="image1 78.png"/>142 <o:File HRef="image138.png"/> 89 143 <o:File HRef="image139.png"/> 90 <o:File HRef="image1 79.png"/>144 <o:File HRef="image140.png"/> 91 145 <o:File HRef="image141.png"/> 92 <o:File HRef="image1 80.png"/>146 <o:File HRef="image142.png"/> 93 147 <o:File HRef="image143.png"/> 94 <o:File HRef="image1 81.png"/>148 <o:File HRef="image144.png"/> 95 149 <o:File HRef="image145.png"/> 96 <o:File HRef="image1 82.png"/>150 <o:File HRef="image146.png"/> 97 151 <o:File HRef="image147.png"/> 98 <o:File HRef="image1 83.png"/>152 <o:File HRef="image148.png"/> 99 153 <o:File HRef="image149.png"/> 100 <o:File HRef="image1 84.png"/>154 <o:File HRef="image150.png"/> 101 155 <o:File HRef="image151.png"/> 102 <o:File HRef="image1 85.png"/>156 <o:File HRef="image152.png"/> 103 157 <o:File HRef="image153.png"/> 104 <o:File HRef="image1 86.png"/>158 <o:File HRef="image154.png"/> 105 159 <o:File HRef="image155.png"/> 106 <o:File HRef="image1 87.png"/>160 <o:File HRef="image156.png"/> 107 161 <o:File HRef="image157.png"/> 108 <o:File HRef="image1 88.png"/>162 <o:File HRef="image158.png"/> 109 163 <o:File HRef="image159.png"/> 110 <o:File HRef="image189.png"/> 111 <o:File HRef="image161.png"/> 112 <o:File HRef="image190.png"/> 113 <o:File HRef="image191.png"/> 114 <o:File HRef="image192.png"/> 115 <o:File HRef="image193.png"/> 116 <o:File HRef="image194.png"/> 117 <o:File HRef="image195.png"/> 118 <o:File HRef="image196.png"/> 119 <o:File HRef="image197.png"/> 120 <o:File HRef="image198.png"/> 121 <o:File HRef="image083.png"/> 122 <o:File HRef="image199.png"/> 123 <o:File HRef="image200.png"/> 124 <o:File HRef="image201.png"/> 125 <o:File HRef="image202.png"/> 126 <o:File HRef="image203.png"/> 127 <o:File HRef="image204.png"/> 128 <o:File HRef="image205.png"/> 129 <o:File HRef="image206.png"/> 130 <o:File HRef="image207.png"/> 131 <o:File HRef="image208.png"/> 132 <o:File HRef="image209.png"/> 133 <o:File HRef="image210.png"/> 134 <o:File HRef="image211.png"/> 135 <o:File HRef="image212.png"/> 136 <o:File HRef="image213.png"/> 137 <o:File HRef="image214.png"/> 138 <o:File HRef="image215.png"/> 139 <o:File HRef="image216.png"/> 140 <o:File HRef="image217.png"/> 141 <o:File HRef="image065.png"/> 142 <o:File HRef="image218.png"/> 143 <o:File HRef="image219.png"/> 144 <o:File HRef="image220.png"/> 145 <o:File HRef="image221.png"/> 146 <o:File HRef="image222.png"/> 147 <o:File HRef="image223.png"/> 148 <o:File HRef="image224.png"/> 149 <o:File HRef="image225.png"/> 150 <o:File HRef="image226.png"/> 151 <o:File HRef="image227.png"/> 152 <o:File HRef="image228.png"/> 153 <o:File HRef="image229.png"/> 154 <o:File HRef="image230.png"/> 155 <o:File HRef="image231.png"/> 156 <o:File HRef="image232.png"/> 157 <o:File HRef="image233.png"/> 158 <o:File HRef="image234.png"/> 159 <o:File HRef="image235.png"/> 160 <o:File HRef="image236.png"/> 161 <o:File HRef="image237.png"/> 162 <o:File HRef="image238.png"/> 163 <o:File HRef="image239.png"/> 164 <o:File HRef="image240.png"/> 164 <o:File HRef="image160.png"/> 165 165 <o:File HRef="filelist.xml"/> 166 166 </xml>
Note: See TracChangeset
for help on using the changeset viewer.