Changeset 3036


Ignore:
Timestamp:
Aug 31, 2017 3:27:41 PM (4 years ago)
Author:
vondreele
Message:

update to 2 frame version

Location:
Tutorials/SAseqref
Files:
43 added
29 deleted
2 edited

Legend:

Unmodified
Added
Removed
  • Tutorials/SAseqref/Sequential Refinement of Small Angle Scattering Data.htm

    r2794 r3036  
    2525  <o:Author>Von Dreele</o:Author>
    2626  <o:LastAuthor>vondreele</o:LastAuthor>
    27   <o:Revision>20</o:Revision>
    28   <o:TotalTime>2626</o:TotalTime>
     27  <o:Revision>21</o:Revision>
     28  <o:TotalTime>2677</o:TotalTime>
    2929  <o:Created>2014-05-03T14:24:00Z</o:Created>
    30   <o:LastSaved>2017-04-19T17:19:00Z</o:LastSaved>
     30  <o:LastSaved>2017-08-31T20:26:00Z</o:LastSaved>
    3131  <o:Pages>26</o:Pages>
    32   <o:Words>1538</o:Words>
    33   <o:Characters>8773</o:Characters>
     32  <o:Words>1554</o:Words>
     33  <o:Characters>8859</o:Characters>
    3434  <o:Company>Argonne National Laboratory</o:Company>
    3535  <o:Lines>73</o:Lines>
    3636  <o:Paragraphs>20</o:Paragraphs>
    37   <o:CharactersWithSpaces>10291</o:CharactersWithSpaces>
     37  <o:CharactersWithSpaces>10393</o:CharactersWithSpaces>
    3838  <o:Version>16.00</o:Version>
    3939 </o:DocumentProperties>
     
    13041304 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
    13051305 <o:lock v:ext="edit" aspectratio="t"/>
    1306 </v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1056" type="#_x0000_t75"
    1307  style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'>
    1308  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image001.png"
    1309   o:title=""/>
    1310 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1311 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image001.png"
    1312 v:shapes="Picture_x0020_1"><![endif]></span></p>
     1306</v:shapetype><v:shape id="Picture_x0020_33" o:spid="_x0000_i1055" type="#_x0000_t75"
     1307 style='width:468pt;height:401.25pt;visibility:visible;mso-wrap-style:square'>
     1308 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image002.png"
     1309  o:title=""/>
     1310</v:shape><![endif]--><![if !vml]><img width=624 height=535
     1311src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image005.png"
     1312v:shapes="Picture_x0020_33"><![endif]></span></p>
    13131313
    13141314<h2><a name="_Ref386704789">Step 2: Set Limits</a></h2>
     
    13271327
    13281328<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1329  id="_x0000_i1055" type="#_x0000_t75" style='width:225pt;height:96.75pt;
     1329 id="Picture_x0020_34" o:spid="_x0000_i1054" type="#_x0000_t75" style='width:408pt;
     1330 height:306.75pt;visibility:visible;mso-wrap-style:square'>
     1331 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image007.png"
     1332  o:title=""/>
     1333</v:shape><![endif]--><![if !vml]><img width=544 height=409
     1334src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image007.png"
     1335v:shapes="Picture_x0020_34"><![endif]></span><span
     1336style='mso-spacerun:yes'> </span></p>
     1337
     1338<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     1339
     1340<p class=MsoNormal>To copy these limits to the other data sets use the <b
     1341style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     1342mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit
     1343Limits/Copy</span></b> command from the data window menu; a popup window will
     1344give the selection of targets.<br>
     1345<span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_35"
     1346 o:spid="_x0000_i1053" type="#_x0000_t75" style='width:216.75pt;height:254.25pt;
    13301347 visibility:visible;mso-wrap-style:square'>
    1331  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image033.png"
    1332   o:title=""/>
    1333 </v:shape><![endif]--><![if !vml]><img width=300 height=129
    1334 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image033.png"
    1335 v:shapes="_x0000_i1055"><![endif]></span><span
    1336 style='mso-spacerun:yes'> </span></p>
    1337 
    1338 <p class=MsoNormal><o:p>&nbsp;</o:p></p>
    1339 
    1340 <p class=MsoNormal>To copy these limits to the other data sets use the <b
    1341 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    1342 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Limits/Copy</span></b>
    1343 command from the data window menu; a popup window will give the selection of
    1344 targets.<br>
    1345 <span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_27"
    1346  o:spid="_x0000_i1054" type="#_x0000_t75" style='width:240pt;height:232.5pt;
    1347  visibility:visible;mso-wrap-style:square'>
    1348  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image003.png"
    1349   o:title=""/>
    1350 </v:shape><![endif]--><![if !vml]><img width=320 height=310
    1351 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image003.png"
    1352 v:shapes="Picture_x0020_27"><![endif]></span></p>
     1348 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image008.png"
     1349  o:title=""/>
     1350</v:shape><![endif]--><![if !vml]><img width=289 height=339
     1351src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image008.png"
     1352v:shapes="Picture_x0020_35"><![endif]></span></p>
    13531353
    13541354<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    13591359checked) and then press <b style='mso-bidi-font-weight:normal'><span
    13601360style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    1361 mso-hansi-theme-font:minor-latin'>Enter</span></b> to do the copy.</p>
     1361mso-hansi-theme-font:minor-latin'>OK</span></b> to do the copy.</p>
    13621362
    13631363<h2>Step 3 Select the scattering substances for your sample</h2>
     
    13731373style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    13741374mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span
    1375 style='mso-no-proof:yes'>; this is read after Substances.py when you load substances
    1376 for your selection. </span>Select <b style='mso-bidi-font-weight:normal'><span
    1377 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    1378 mso-hansi-theme-font:minor-latin'>Substances</span></b> from the GSAS-II tree.
    1379 Then do <span class=GramE><b style='mso-bidi-font-weight:normal'><span
     1375style='mso-no-proof:yes'>; this is read after Substances.py when you load
     1376substances for your selection. </span>Select <b style='mso-bidi-font-weight:
     1377normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
     1378minor-latin;mso-hansi-theme-font:minor-latin'>Substances</span></b> from the
     1379GSAS-II tree. Then do <span class=GramE><b style='mso-bidi-font-weight:normal'><span
    13801380style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    13811381mso-hansi-theme-font:minor-latin'>Edit</span></b></span><b style='mso-bidi-font-weight:
     
    13851385
    13861386<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1387  id="Picture_x0020_3" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:259.5pt;
     1387 id="Picture_x0020_3" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:259.5pt;
    13881388 height:252pt;visibility:visible;mso-wrap-style:square'>
    13891389 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image004.png"
     
    13961396
    13971397<p class=MsoNormal>Notice that silica is not one of the choices; we will add it
    1398 in a moment. Select <b style='mso-bidi-font-weight:normal'><span
    1399 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    1400 mso-hansi-theme-font:minor-latin'>Water</span></b> and press <b
     1398in a moment (a-Quartz is but let’s ignore that). Select <b style='mso-bidi-font-weight:
     1399normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
     1400minor-latin;mso-hansi-theme-font:minor-latin'>Water</span></b> and press <b
    14011401style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    14021402mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>;
     
    14041404
    14051405<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1406  id="_x0000_i1052" type="#_x0000_t75" style='width:280.5pt;height:246pt;
    1407  visibility:visible;mso-wrap-style:square'>
    1408  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image034.png"
    1409   o:title=""/>
    1410 </v:shape><![endif]--><![if !vml]><img width=374 height=328
    1411 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image034.png"
    1412 v:shapes="_x0000_i1052"><![endif]></span><span
     1406 id="Picture_x0020_36" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:408pt;
     1407 height:306.75pt;visibility:visible;mso-wrap-style:square'>
     1408 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image029.png"
     1409  o:title=""/>
     1410</v:shape><![endif]--><![if !vml]><img width=544 height=409
     1411src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image029.png"
     1412v:shapes="Picture_x0020_36"><![endif]></span><span
    14131413style='mso-spacerun:yes'> </span></p>
    14141414
     
    14191419The composition, volume occupied by the atoms in the composition and the
    14201420density are given for each substance. These can each be edited; the other
    1421 values will change accordingly. Since silica wasn’t in the list of known
    1422 substances, do <b style='mso-bidi-font-weight:normal'><span style='font-family:
    1423 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1424 minor-latin'>Edit substance/Add substance</span></b> to create it; you will be
    1425 asked for a name – enter <b style='mso-bidi-font-weight:normal'><span
    1426 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    1427 mso-hansi-theme-font:minor-latin'>silica</span></b> and then a periodic table
    1428 of the elements will be shown. Select <b style='mso-bidi-font-weight:normal'><span
    1429 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    1430 mso-hansi-theme-font:minor-latin'>Si</span></b> and <b style='mso-bidi-font-weight:
    1431 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    1432 minor-latin;mso-hansi-theme-font:minor-latin'>O</span></b></p>
    1433 
    1434 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1435  id="Picture_x0020_6" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:435pt;
     1421values will change accordingly. Since we are going to say that silica wasn’t in
     1422the list of known substances, do <b style='mso-bidi-font-weight:normal'><span
     1423style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
     1424mso-hansi-theme-font:minor-latin'>Edit substance/Add substance</span></b> to
     1425create it; you will be asked for a name – enter <b style='mso-bidi-font-weight:
     1426normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
     1427minor-latin;mso-hansi-theme-font:minor-latin'>silica</span></b> and then a
     1428periodic table of the elements will be shown. Select <b style='mso-bidi-font-weight:
     1429normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
     1430minor-latin;mso-hansi-theme-font:minor-latin'>Si</span></b> and <b
     1431style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     1432mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>O</span></b></p>
     1433
     1434<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
     1435 id="Picture_x0020_6" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:435pt;
    14361436 height:270pt;visibility:visible;mso-wrap-style:square'>
    14371437 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image006.png"
     
    14501450
    14511451<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1452  id="Picture_x0020_35" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:280.5pt;
    1453  height:350.25pt;visibility:visible;mso-wrap-style:square'>
    1454  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image035.png"
    1455   o:title=""/>
    1456 </v:shape><![endif]--><![if !vml]><img width=374 height=467
    1457 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image035.png"
    1458 v:shapes="Picture_x0020_35"><![endif]></span></p>
     1452 id="_x0000_i1049" type="#_x0000_t75" style='width:408pt;height:306.75pt;
     1453 visibility:visible;mso-wrap-style:square'>
     1454 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image032.png"
     1455  o:title=""/>
     1456</v:shape><![endif]--><![if !vml]><img width=544 height=409
     1457src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image032.png"
     1458v:shapes="_x0000_i1049"><![endif]></span></p>
    14591459
    14601460<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    14681468
    14691469<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1470  id="_x0000_i1049" type="#_x0000_t75" style='width:280.5pt;height:350.25pt;
    1471  visibility:visible;mso-wrap-style:square'>
    1472  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image036.png"
    1473   o:title=""/>
    1474 </v:shape><![endif]--><![if !vml]><img width=374 height=467
    1475 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image036.png"
    1476 v:shapes="_x0000_i1049"><![endif]></span><span
     1470 id="Picture_x0020_38" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:408pt;
     1471 height:306.75pt;visibility:visible;mso-wrap-style:square'>
     1472 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image040.png"
     1473  o:title=""/>
     1474</v:shape><![endif]--><![if !vml]><img width=544 height=409
     1475src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image040.png"
     1476v:shapes="Picture_x0020_38"><![endif]></span><span
    14771477style='mso-spacerun:yes'> </span></p>
    14781478
     
    15021502
    15031503<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1504  id="Picture_x0020_9" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:291.75pt;
    1505  height:388.5pt;visibility:visible;mso-wrap-style:square'>
    1506  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image009.png"
    1507   o:title=""/>
    1508 </v:shape><![endif]--><![if !vml]><img width=389 height=518
    1509 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image009.png"
    1510 v:shapes="Picture_x0020_9"><![endif]><o:p></o:p></span></p>
     1504 id="Picture_x0020_39" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:438pt;
     1505 height:435.75pt;visibility:visible;mso-wrap-style:square'>
     1506 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image041.png"
     1507  o:title=""/>
     1508</v:shape><![endif]--><![if !vml]><img width=584 height=581
     1509src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image042.png"
     1510v:shapes="Picture_x0020_39"><![endif]><o:p></o:p></span></p>
    15111511
    15121512<p class=MsoNormal><span style='mso-no-proof:yes'><o:p>&nbsp;</o:p></span></p>
     
    15331533
    15341534<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1535  id="Picture_x0020_10" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:291.75pt;
    1536  height:388.5pt;visibility:visible;mso-wrap-style:square'>
    1537  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image010.png"
    1538   o:title=""/>
    1539 </v:shape><![endif]--><![if !vml]><img width=389 height=518
    1540 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image010.png"
    1541 v:shapes="Picture_x0020_10"><![endif]><o:p></o:p></span></p>
     1535 id="Picture_x0020_40" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:447.75pt;
     1536 height:445.5pt;visibility:visible;mso-wrap-style:square'>
     1537 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image043.png"
     1538  o:title=""/>
     1539</v:shape><![endif]--><![if !vml]><img width=597 height=594
     1540src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image043.png"
     1541v:shapes="Picture_x0020_40"><![endif]><o:p></o:p></span></p>
    15421542
    15431543<p class=MsoNormal><span style='mso-no-proof:yes'><o:p>&nbsp;</o:p></span></p>
     
    15611561
    15621562<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1563  id="Picture_x0020_11" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:291.75pt;
    1564  height:388.5pt;visibility:visible;mso-wrap-style:square'>
    1565  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image011.png"
    1566   o:title=""/>
    1567 </v:shape><![endif]--><![if !vml]><img width=389 height=518
    1568 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image011.png"
    1569 v:shapes="Picture_x0020_11"><![endif]></span><span
     1563 id="Picture_x0020_41" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:444pt;
     1564 height:441.75pt;visibility:visible;mso-wrap-style:square'>
     1565 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image044.png"
     1566  o:title=""/>
     1567</v:shape><![endif]--><![if !vml]><img width=592 height=589
     1568src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image044.png"
     1569v:shapes="Picture_x0020_41"><![endif]></span><span
    15701570style='mso-spacerun:yes'> </span><span style='mso-no-proof:yes'><o:p></o:p></span></p>
    15711571
     
    15821582
    15831583<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1584  id="Picture_x0020_12" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:525pt;
    1585  height:450pt;visibility:visible;mso-wrap-style:square'>
    1586  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image012.png"
    1587   o:title=""/>
    1588 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1589 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image012.png"
    1590 v:shapes="Picture_x0020_12"><![endif]></span></p>
     1584 id="Picture_x0020_42" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:453pt;
     1585 height:388.5pt;visibility:visible;mso-wrap-style:square'>
     1586 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image045.png"
     1587  o:title=""/>
     1588</v:shape><![endif]--><![if !vml]><img width=604 height=518
     1589src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image046.png"
     1590v:shapes="Picture_x0020_42"><![endif]></span></p>
    15911591
    15921592<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    16231623
    16241624<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1625  id="Picture_x0020_13" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:525pt;
    1626  height:450pt;visibility:visible;mso-wrap-style:square'>
    1627  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image013.png"
    1628   o:title=""/>
    1629 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1630 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image013.png"
    1631 v:shapes="Picture_x0020_13"><![endif]></span></p>
     1625 id="Picture_x0020_43" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:450.75pt;
     1626 height:386.25pt;visibility:visible;mso-wrap-style:square'>
     1627 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image047.png"
     1628  o:title=""/>
     1629</v:shape><![endif]--><![if !vml]><img width=601 height=515
     1630src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image048.png"
     1631v:shapes="Picture_x0020_43"><![endif]></span></p>
    16321632
    16331633<p class=MsoNormal><span style='mso-no-proof:yes'><o:p>&nbsp;</o:p></span></p>
     
    16591659
    16601660<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1661  id="Picture_x0020_14" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:384.75pt;
    1662  height:358.5pt;visibility:visible;mso-wrap-style:square'>
    1663  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image014.png"
    1664   o:title=""/>
    1665 </v:shape><![endif]--><![if !vml]><img width=513 height=478
    1666 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image014.png"
    1667 v:shapes="Picture_x0020_14"><![endif]></span></p>
     1661 id="Picture_x0020_44" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:468pt;
     1662 height:276pt;visibility:visible;mso-wrap-style:square'>
     1663 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image049.png"
     1664  o:title=""/>
     1665</v:shape><![endif]--><![if !vml]><img width=624 height=368
     1666src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image050.png"
     1667v:shapes="Picture_x0020_44"><![endif]></span></p>
    16681668
    16691669<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    16721672
    16731673<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1674  id="Picture_x0020_34" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:525pt;
    1675  height:450pt;visibility:visible;mso-wrap-style:square'>
    1676  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image015.png"
    1677   o:title=""/>
    1678 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1679 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image015.png"
    1680 v:shapes="Picture_x0020_34"><![endif]></span><br clear=all style='mso-special-character:
     1674 id="Picture_x0020_45" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:438.75pt;
     1675 height:376.5pt;visibility:visible;mso-wrap-style:square'>
     1676 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image051.png"
     1677  o:title=""/>
     1678</v:shape><![endif]--><![if !vml]><img width=585 height=502
     1679src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image052.png"
     1680v:shapes="Picture_x0020_45"><![endif]></span><br clear=all style='mso-special-character:
    16811681line-break'>
    16821682</p>
     
    17061706
    17071707<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1708  id="Picture_x0020_36" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:384.75pt;
    1709  height:358.5pt;visibility:visible;mso-wrap-style:square'>
    1710  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image016.png"
    1711   o:title=""/>
    1712 </v:shape><![endif]--><![if !vml]><img width=513 height=478
    1713 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image016.png"
    1714 v:shapes="Picture_x0020_36"><![endif]></span></p>
     1708 id="Picture_x0020_46" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:468pt;
     1709 height:276pt;visibility:visible;mso-wrap-style:square'>
     1710 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image053.png"
     1711  o:title=""/>
     1712</v:shape><![endif]--><![if !vml]><img width=624 height=368
     1713src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image054.png"
     1714v:shapes="Picture_x0020_46"><![endif]></span></p>
    17151715
    17161716<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    17191719
    17201720<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1721  id="_x0000_i1040" type="#_x0000_t75" style='width:525pt;height:450pt;
    1722  visibility:visible;mso-wrap-style:square'>
    1723  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image017.png"
    1724   o:title=""/>
    1725 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1726 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image017.png"
    1727 v:shapes="_x0000_i1040"><![endif]></span></p>
     1721 id="Picture_x0020_47" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:468pt;
     1722 height:401.25pt;visibility:visible;mso-wrap-style:square'>
     1723 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image055.png"
     1724  o:title=""/>
     1725</v:shape><![endif]--><![if !vml]><img width=624 height=535
     1726src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image056.png"
     1727v:shapes="Picture_x0020_47"><![endif]></span></p>
    17281728
    17291729<h2>Step 6: Initial refinement</h2>
     
    17401740
    17411741<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1742  id="_x0000_i1039" type="#_x0000_t75" style='width:384.75pt;height:358.5pt;
    1743  visibility:visible;mso-wrap-style:square'>
    1744  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image018.png"
    1745   o:title=""/>
    1746 </v:shape><![endif]--><![if !vml]><img width=513 height=478
    1747 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image018.png"
    1748 v:shapes="_x0000_i1039"><![endif]></span></p>
     1742 id="Picture_x0020_48" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:468pt;
     1743 height:276pt;visibility:visible;mso-wrap-style:square'>
     1744 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image057.png"
     1745  o:title=""/>
     1746</v:shape><![endif]--><![if !vml]><img width=624 height=368
     1747src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image058.png"
     1748v:shapes="Picture_x0020_48"><![endif]></span></p>
    17491749
    17501750<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    17531753
    17541754<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1755  id="Picture_x0020_39" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:609.75pt;
    1756  height:152.25pt;visibility:visible;mso-wrap-style:square'>
    1757  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image019.png"
    1758   o:title=""/>
    1759 </v:shape><![endif]--><![if !vml]><img width=813 height=203
    1760 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image019.png"
    1761 v:shapes="Picture_x0020_39"><![endif]></span></p>
     1755 id="Picture_x0020_49" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:468pt;
     1756 height:149.25pt;visibility:visible;mso-wrap-style:square'>
     1757 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image059.png"
     1758  o:title=""/>
     1759</v:shape><![endif]--><![if !vml]><img width=624 height=199
     1760src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image060.png"
     1761v:shapes="Picture_x0020_49"><![endif]></span></p>
    17621762
    17631763<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    17661766
    17671767<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1768  id="Picture_x0020_40" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:525pt;
    1769  height:450pt;visibility:visible;mso-wrap-style:square'>
    1770  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image020.png"
    1771   o:title=""/>
    1772 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1773 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image020.png"
    1774 v:shapes="Picture_x0020_40"><![endif]></span></p>
     1768 id="Picture_x0020_50" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:468pt;
     1769 height:401.25pt;visibility:visible;mso-wrap-style:square'>
     1770 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image061.png"
     1771  o:title=""/>
     1772</v:shape><![endif]--><![if !vml]><img width=624 height=535
     1773src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image062.png"
     1774v:shapes="Picture_x0020_50"><![endif]></span></p>
    17751775
    17761776<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    17891789
    17901790<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1791  id="Picture_x0020_21" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:240pt;
    1792  height:232.5pt;visibility:visible;mso-wrap-style:square'>
    1793  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image021.png"
    1794   o:title=""/>
    1795 </v:shape><![endif]--><![if !vml]><img width=320 height=310
    1796 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image021.png"
    1797 v:shapes="Picture_x0020_21"><![endif]></span></p>
     1791 id="Picture_x0020_51" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:223.5pt;
     1792 height:289.5pt;visibility:visible;mso-wrap-style:square'>
     1793 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image063.png"
     1794  o:title=""/>
     1795</v:shape><![endif]--><![if !vml]><img width=298 height=386
     1796src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image063.png"
     1797v:shapes="Picture_x0020_51"><![endif]></span></p>
    17981798
    17991799<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    18011801<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
    18021802style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    1803 mso-hansi-theme-font:minor-latin'>Set All</span></b>, all boxes will be checked
    1804 showing selection of the data sets. Then press <b style='mso-bidi-font-weight:
    1805 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    1806 minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>; a new dialog box
    1807 will appear</p>
    1808 
    1809 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1810  id="Picture_x0020_33" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:259.5pt;
    1811  height:252pt;visibility:visible;mso-wrap-style:square'>
    1812  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image022.png"
    1813   o:title=""/>
    1814 </v:shape><![endif]--><![if !vml]><img width=346 height=336
    1815 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image022.png"
    1816 v:shapes="Picture_x0020_33"><![endif]></span></p>
    1817 
    1818 <p class=MsoNormal><o:p>&nbsp;</o:p></p>
    1819 
    1820 <p class=MsoNormal>This allows you to instruct the sequential refinement to
    1821 start at the last data set and proceed backwards through them (<b
    1822 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    1823 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Reverse
    1824 sequence</span></b>). It also allows you to instruct the sequential refinement
    1825 to use the current parameters as starting values for the next data set. This
    1826 works in either direction and facilitates the initial sequential refinements.
    1827 NB: some sequential refinements do not work well in both directions; in this
    1828 particular case starting with a fitted 1% pattern and going in reverse through
    1829 the data fails on the 5% data set. Apparently the change in parameters is too
    1830 great for the least squares to handle; going in the forward direction works
    1831 just fine (as you will see next). Select <b style='mso-bidi-font-weight:normal'><span
    1832 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    1833 mso-hansi-theme-font:minor-latin'>Copy from prev.</span></b> and press <b
    1834 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     1803mso-hansi-theme-font:minor-latin'>Set <span class=GramE>All</span></span></b>,
     1804all boxes will be checked showing selection of the data sets. This also allows
     1805you to instruct the sequential refinement to start at the last data set and
     1806proceed backwards through them (<b style='mso-bidi-font-weight:normal'><span
     1807style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
     1808mso-hansi-theme-font:minor-latin'>Reverse order</span></b>). It also allows you
     1809to instruct the sequential refinement to use the current parameters as starting
     1810values for the next data set. This works in either direction and facilitates
     1811the initial sequential refinements. NB: some sequential refinements do not work
     1812well in both directions; in this particular case starting with a fitted 1%
     1813pattern and going in reverse through the data fails on the 5% data set.
     1814Apparently the change in parameters is too great for the least squares to
     1815handle; going in the forward direction works just fine (as you will see next).
     1816Select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     1817mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Copy to next</span></b>
     1818and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    18351819mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>;
    18361820the sequential refinement will proceed very rapidly displaying results for each
    18371821data set on the console and finally ending by displaying the <b
    18381822style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    1839 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sequential
     1823mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sequential refinement
    18401824results.<o:p></o:p></span></b></p>
    18411825
    18421826<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1843  id="Picture_x0020_42" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:564pt;
    1844  height:262.5pt;visibility:visible;mso-wrap-style:square'>
    1845  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image023.png"
    1846   o:title=""/>
    1847 </v:shape><![endif]--><![if !vml]><img width=752 height=350
    1848 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image023.png"
    1849 v:shapes="Picture_x0020_42"><![endif]></span></p>
     1827 id="Picture_x0020_53" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:459pt;
     1828 height:234pt;visibility:visible;mso-wrap-style:square'>
     1829 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image064.png"
     1830  o:title=""/>
     1831</v:shape><![endif]--><![if !vml]><img width=612 height=312
     1832src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image065.png"
     1833v:shapes="Picture_x0020_53"><![endif]></span></p>
    18501834
    18511835<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    18571841
    18581842<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1859  id="Picture_x0020_43" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:525pt;
    1860  height:450pt;visibility:visible;mso-wrap-style:square'>
    1861  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image024.png"
    1862   o:title=""/>
    1863 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1864 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image024.png"
    1865 v:shapes="Picture_x0020_43"><![endif]></span></p>
     1843 id="Picture_x0020_54" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:468pt;
     1844 height:401.25pt;visibility:visible;mso-wrap-style:square'>
     1845 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image066.png"
     1846  o:title=""/>
     1847</v:shape><![endif]--><![if !vml]><img width=624 height=535
     1848src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image067.png"
     1849v:shapes="Picture_x0020_54"><![endif]></span></p>
    18661850
    18671851<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    18751859minor-latin'>s</span></b> from the <b style='mso-bidi-font-weight:normal'><span
    18761860style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    1877 mso-hansi-theme-font:minor-latin'>K</span></b> box); a dialog box will appear
    1878 with a selection of parameters to plot along the x-axis. Select <b
    1879 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    1880 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>fraction</span></b>
    1881 and the plot will be redrawn (it may require selection of another column &amp;
    1882 then <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     1861mso-hansi-theme-font:minor-latin'>K</span></b> box); a dialog box will appear with
     1862a selection of parameters to plot along the x-axis. Select <b style='mso-bidi-font-weight:
     1863normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
     1864minor-latin;mso-hansi-theme-font:minor-latin'>fraction</span></b> and the plot
     1865will be redrawn (it may require selection of another column &amp; then <b
     1866style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    18831867mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0<span
    18841868class=GramE>;Volume</span></span></b> to make it appear).</p>
    18851869
    18861870<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1887  id="Picture_x0020_44" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt;
    1888  height:450pt;visibility:visible;mso-wrap-style:square'>
    1889  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image025.png"
    1890   o:title=""/>
    1891 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1892 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image025.png"
    1893 v:shapes="Picture_x0020_44"><![endif]></span></p>
    1894 
    1895 <p class=MsoNormal><o:p>&nbsp;</o:p></p>
    1896 
    1897 <p class=MsoNormal>It is gratifying how this relation between Volume and the
    1898 composition is linear. You can now determine the slope &amp; intercept (or fit
    1899 to some other function!) directly with GSAS-II; do <b style='mso-bidi-font-weight:
    1900 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    1901 minor-latin;mso-hansi-theme-font:minor-latin'>Parametric Fit/Add equation</span></b>
    1902 and the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     1871 id="Picture_x0020_55" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:445.5pt;
     1872 height:381.75pt;visibility:visible;mso-wrap-style:square'>
     1873 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image068.png"
     1874  o:title=""/>
     1875</v:shape><![endif]--><![if !vml]><img width=594 height=509
     1876src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image069.png"
     1877v:shapes="Picture_x0020_55"><![endif]></span></p>
     1878
     1879<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     1880
     1881<p class=MsoNormal>It is gratifying how this relation between Volume and the composition
     1882is linear. You can now determine the slope &amp; intercept (or fit to some
     1883other function!) directly with GSAS-II; do <b style='mso-bidi-font-weight:normal'><span
     1884style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
     1885mso-hansi-theme-font:minor-latin'>Parametric Fit/Add equation</span></b> and
     1886the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    19031887mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Expression
    19041888Editor</span></b> dialog box will appear.</p>
    19051889
    19061890<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1907  id="Picture_x0020_26" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:465pt;
    1908  height:225pt;visibility:visible;mso-wrap-style:square'>
    1909  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image026.png"
    1910   o:title=""/>
    1911 </v:shape><![endif]--><![if !vml]><img width=620 height=300
    1912 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image026.png"
    1913 v:shapes="Picture_x0020_26"><![endif]></span></p>
     1891 id="Picture_x0020_56" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:465pt;
     1892 height:255pt;visibility:visible;mso-wrap-style:square'>
     1893 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image070.png"
     1894  o:title=""/>
     1895</v:shape><![endif]--><![if !vml]><img width=620 height=340
     1896src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image070.png"
     1897v:shapes="Picture_x0020_56"><![endif]></span></p>
    19141898
    19151899<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    19291913
    19301914<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1931  id="Picture_x0020_45" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:465pt;
     1915 id="Picture_x0020_57" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:465pt;
    19321916 height:255pt;visibility:visible;mso-wrap-style:square'>
    1933  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image027.png"
     1917 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image071.png"
    19341918  o:title=""/>
    19351919</v:shape><![endif]--><![if !vml]><img width=620 height=340
    1936 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image027.png"
    1937 v:shapes="Picture_x0020_45"><![endif]></span></p>
     1920src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image071.png"
     1921v:shapes="Picture_x0020_57"><![endif]></span></p>
    19381922
    19391923<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    19571941
    19581942<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1959  id="Picture_x0020_46" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;
     1943 id="Picture_x0020_58" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;
    19601944 height:255pt;visibility:visible;mso-wrap-style:square'>
    1961  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image028.png"
     1945 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image072.png"
    19621946  o:title=""/>
    19631947</v:shape><![endif]--><![if !vml]><img width=620 height=340
    1964 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image028.png"
    1965 v:shapes="Picture_x0020_46"><![endif]></span></p>
     1948src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image072.png"
     1949v:shapes="Picture_x0020_58"><![endif]></span></p>
    19661950
    19671951<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    20041988
    20051989<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    2006  id="Picture_x0020_47" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt;
     1990 id="Picture_x0020_59" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt;
    20071991 height:255pt;visibility:visible;mso-wrap-style:square'>
    2008  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image030.png"
     1992 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image073.png"
    20091993  o:title=""/>
    20101994</v:shape><![endif]--><![if !vml]><img width=620 height=340
    2011 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image030.png"
    2012 v:shapes="Picture_x0020_47"><![endif]></span></p>
     1995src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image073.png"
     1996v:shapes="Picture_x0020_59"><![endif]></span></p>
    20131997
    20141998<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    20202004
    20212005<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    2022  id="Picture_x0020_49" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:303.75pt;
    2023  height:98.25pt;visibility:visible;mso-wrap-style:square'>
    2024  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image031.png"
    2025   o:title=""/>
    2026 </v:shape><![endif]--><![if !vml]><img width=405 height=131
    2027 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image031.png"
    2028 v:shapes="Picture_x0020_49"><![endif]></span></p>
    2029 
    2030 <p class=MsoNormal><o:p>&nbsp;</o:p></p>
    2031 
    2032 <p class=MsoNormal>And the plot shows the curve (in blue) calculated from the
     2006 id="Picture_x0020_60" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:354pt;
     2007 height:116.25pt;visibility:visible;mso-wrap-style:square'>
     2008 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image074.png"
     2009  o:title=""/>
     2010</v:shape><![endif]--><![if !vml]><img width=472 height=155
     2011src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image074.png"
     2012v:shapes="Picture_x0020_60"><![endif]></span></p>
     2013
     2014<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     2015
     2016<p class=MsoNormal>And the plot shows the curve (in red) calculated from the
    20332017best fit, weighted by the <span class=SpellE>esds</span> on the data points, to
    20342018the model equation for a straight line.</p>
    20352019
    20362020<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    2037  id="Picture_x0020_38" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:468pt;
     2021 id="Picture_x0020_61" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:468pt;
    20382022 height:401.25pt;visibility:visible;mso-wrap-style:square'>
    2039  <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image038.png"
     2023 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image075.png"
    20402024  o:title=""/>
    20412025</v:shape><![endif]--><![if !vml]><img width=624 height=535
    2042 src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image039.png"
    2043 v:shapes="Picture_x0020_38"><![endif]></span></p>
     2026src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image076.png"
     2027v:shapes="Picture_x0020_61"><![endif]></span></p>
    20442028
    20452029<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    20522036explanation for the discrepancy is that the silica particles are partially
    20532037hydrated thus reducing the contrast from 175.6x10<sup>20</sup> cm<sup>-4</sup>
    2054 to something like 98x10<sup>20</sup>cm<sup>-4</sup>.</p>
     2038to something like 98x10<sup>20</sup>cm<sup>-4</sup>. This concludes the small
     2039angle sequential fit tutorial; you may save the project.</p>
    20552040
    20562041</div>
  • Tutorials/SAseqref/Sequential Refinement of Small Angle Scattering Data_files/filelist.xml

    r2794 r3036  
    44 <o:File HRef="themedata.thmx"/>
    55 <o:File HRef="colorschememapping.xml"/>
    6  <o:File HRef="image001.png"/>
    7  <o:File HRef="image033.png"/>
    8  <o:File HRef="image003.png"/>
     6 <o:File HRef="image002.png"/>
     7 <o:File HRef="image005.png"/>
     8 <o:File HRef="image007.png"/>
     9 <o:File HRef="image008.png"/>
    910 <o:File HRef="image004.png"/>
    10  <o:File HRef="image034.png"/>
     11 <o:File HRef="image029.png"/>
    1112 <o:File HRef="image006.png"/>
    12  <o:File HRef="image035.png"/>
    13  <o:File HRef="image036.png"/>
    14  <o:File HRef="image009.png"/>
    15  <o:File HRef="image010.png"/>
    16  <o:File HRef="image011.png"/>
    17  <o:File HRef="image012.png"/>
    18  <o:File HRef="image013.png"/>
    19  <o:File HRef="image014.png"/>
    20  <o:File HRef="image015.png"/>
    21  <o:File HRef="image016.png"/>
    22  <o:File HRef="image017.png"/>
    23  <o:File HRef="image018.png"/>
    24  <o:File HRef="image019.png"/>
    25  <o:File HRef="image020.png"/>
    26  <o:File HRef="image021.png"/>
    27  <o:File HRef="image022.png"/>
    28  <o:File HRef="image023.png"/>
    29  <o:File HRef="image024.png"/>
    30  <o:File HRef="image025.png"/>
    31  <o:File HRef="image026.png"/>
    32  <o:File HRef="image027.png"/>
    33  <o:File HRef="image028.png"/>
     13 <o:File HRef="image032.png"/>
     14 <o:File HRef="image040.png"/>
     15 <o:File HRef="image041.png"/>
     16 <o:File HRef="image042.png"/>
     17 <o:File HRef="image043.png"/>
     18 <o:File HRef="image044.png"/>
     19 <o:File HRef="image045.png"/>
     20 <o:File HRef="image046.png"/>
     21 <o:File HRef="image047.png"/>
     22 <o:File HRef="image048.png"/>
     23 <o:File HRef="image049.png"/>
     24 <o:File HRef="image050.png"/>
     25 <o:File HRef="image051.png"/>
     26 <o:File HRef="image052.png"/>
     27 <o:File HRef="image053.png"/>
     28 <o:File HRef="image054.png"/>
     29 <o:File HRef="image055.png"/>
     30 <o:File HRef="image056.png"/>
     31 <o:File HRef="image057.png"/>
     32 <o:File HRef="image058.png"/>
     33 <o:File HRef="image059.png"/>
     34 <o:File HRef="image060.png"/>
     35 <o:File HRef="image061.png"/>
     36 <o:File HRef="image062.png"/>
     37 <o:File HRef="image063.png"/>
     38 <o:File HRef="image064.png"/>
     39 <o:File HRef="image065.png"/>
     40 <o:File HRef="image066.png"/>
     41 <o:File HRef="image067.png"/>
     42 <o:File HRef="image068.png"/>
     43 <o:File HRef="image069.png"/>
     44 <o:File HRef="image070.png"/>
     45 <o:File HRef="image071.png"/>
     46 <o:File HRef="image072.png"/>
    3447 <o:File HRef="image037.png"/>
    35  <o:File HRef="image030.png"/>
    36  <o:File HRef="image031.png"/>
    37  <o:File HRef="image038.png"/>
    38  <o:File HRef="image039.png"/>
     48 <o:File HRef="image073.png"/>
     49 <o:File HRef="image074.png"/>
     50 <o:File HRef="image075.png"/>
     51 <o:File HRef="image076.png"/>
    3952 <o:File HRef="filelist.xml"/>
    4053</xml>
Note: See TracChangeset for help on using the changeset viewer.