Changeset 3032
- Timestamp:
- Aug 30, 2017 2:58:02 PM (6 years ago)
- Location:
- Tutorials/SAfit
- Files:
-
- 26 added
- 6 deleted
- 18 edited
Legend:
- Unmodified
- Added
- Removed
-
Tutorials/SAfit/Fitting Small Angle Scattering Data.htm
r2791 r3032 25 25 <o:Author>Von Dreele</o:Author> 26 26 <o:LastAuthor>vondreele</o:LastAuthor> 27 <o:Revision> 9</o:Revision>28 <o:TotalTime>21 28</o:TotalTime>27 <o:Revision>11</o:Revision> 28 <o:TotalTime>2156</o:TotalTime> 29 29 <o:Created>2014-05-01T13:58:00Z</o:Created> 30 <o:LastSaved>2017-0 4-19T15:50:00Z</o:LastSaved>30 <o:LastSaved>2017-08-30T19:56:00Z</o:LastSaved> 31 31 <o:Pages>22</o:Pages> 32 32 <o:Words>1464</o:Words> 33 <o:Characters>834 7</o:Characters>33 <o:Characters>8345</o:Characters> 34 34 <o:Company>Argonne National Laboratory</o:Company> 35 35 <o:Lines>69</o:Lines> 36 36 <o:Paragraphs>19</o:Paragraphs> 37 <o:CharactersWithSpaces>979 2</o:CharactersWithSpaces>37 <o:CharactersWithSpaces>9790</o:CharactersWithSpaces> 38 38 <o:Version>16.00</o:Version> 39 39 </o:DocumentProperties> … … 663 663 {font-family:"Cambria Math"; 664 664 panose-1:2 4 5 3 5 4 6 3 2 4; 665 mso-font-charset: 0;665 mso-font-charset:1; 666 666 mso-generic-font-family:roman; 667 667 mso-font-pitch:variable; 668 mso-font-signature: -536870145 1107305727 0 0 4150;}668 mso-font-signature:0 0 0 0 0 0;} 669 669 @font-face 670 670 {font-family:Calibri; … … 1224 1224 <p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In 1225 1225 this tutorial you will fit small angle scattering data for an alumina polishing 1226 powder using data from a constant wavelength synchrotron X-ray USAXS instrument.1227 You will use both a lognormal distribution of spherical particles model and a 1228 unified <span class=SpellE>Guinier-Porod</span> model. The data were collected 1229 from <span style='mso-fareast-font-family:Calibri;mso-fareast-theme-font:minor-latin; 1230 m so-bidi-font-weight:bold;mso-bidi-font-style:italic'>powders spread onto1231 s ticky tape and covered with another layer of the same tape. The data were1232 corrected for background using data collected from two layers of sticky tape. 1233 However, the sample thickness is not</span> accurately known <span1226 powder using data from a constant wavelength synchrotron X-ray USAXS 1227 instrument. You will use both a lognormal distribution of spherical particles 1228 model and a unified <span class=SpellE>Guinier-Porod</span> model. The data 1229 were collected from <span style='mso-fareast-font-family:Calibri;mso-fareast-theme-font: 1230 minor-latin;mso-bidi-font-weight:bold;mso-bidi-font-style:italic'>powders 1231 spread onto sticky tape and covered with another layer of the same tape. The 1232 data were corrected for background using data collected from two layers of 1233 sticky tape. However, the sample thickness is not</span> accurately known <span 1234 1234 style='mso-fareast-font-family:Calibri;mso-fareast-theme-font:minor-latin; 1235 1235 mso-bidi-font-weight:bold;mso-bidi-font-style:italic'>so the data are not … … 1330 1330 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> 1331 1331 <o:lock v:ext="edit" aspectratio="t"/> 1332 </v:shapetype><v:shape id="Picture_x0020_ 6" o:spid="_x0000_i1047" type="#_x0000_t75"1333 style='width: 525pt;height:450pt;visibility:visible;mso-wrap-style:square'>1334 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image00 1.png"1335 o:title=""/> 1336 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001337 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image001.png" v:shapes="Picture_x0020_ 6"><![endif]></span></p>1332 </v:shapetype><v:shape id="Picture_x0020_24" o:spid="_x0000_i1047" type="#_x0000_t75" 1333 style='width:468pt;height:401.25pt;visibility:visible;mso-wrap-style:square'> 1334 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image002.png" 1335 o:title=""/> 1336 </v:shape><![endif]--><![if !vml]><img width=624 height=535 1337 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image001.png" v:shapes="Picture_x0020_24"><![endif]></span></p> 1338 1338 1339 1339 <h2><a name="_Ref386704789">Step 2: Set Limits</a></h2> … … 1348 1348 GSAS-II tree. Set the upper limit using the cursor on the plot by picking the 1349 1349 next-to-last point on the curve with the left or right mouse button. If needed 1350 reposition the lower limit to be the 1<sup>st</sup> data <span class=SpellE>point.The</span>1351 limits windowshould look like</p>1350 reposition the lower limit to be the 1<sup>st</sup> data point. The limits window 1351 should look like</p> 1352 1352 1353 1353 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1354 id="Picture_x0020_2 4" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:225pt;1355 height: 96.75pt;visibility:visible;mso-wrap-style:square'>1356 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 24.png"1357 o:title=""/> 1358 </v:shape><![endif]--><![if !vml]><img width= 300 height=1291359 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 24.png" v:shapes="Picture_x0020_24"><![endif]></span><span1354 id="Picture_x0020_25" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:382.5pt; 1355 height:276pt;visibility:visible;mso-wrap-style:square'> 1356 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image005.png" 1357 o:title=""/> 1358 </v:shape><![endif]--><![if !vml]><img width=510 height=368 1359 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image005.png" v:shapes="Picture_x0020_25"><![endif]></span><span 1360 1360 style='mso-spacerun:yes'> </span></p> 1361 1361 … … 1373 1373 style='mso-spacerun:yes'> </span>\* MERGEFORMAT <span style='mso-element:field-separator'></span></span></b><![endif]--><b 1374 1374 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1375 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Step 4 1376 Creation and Refinement of Log Normal Particle Model<span style='mso-no-proof: 1377 yes'><!--[if gte mso 9]><xml> 1375 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Step 4 Creation 1376 and Refinement of Log Normal Particle Model<span style='mso-no-proof:yes'><!--[if gte mso 9]><xml> 1378 1377 <w:data>08D0C9EA79F9BACE118C8200AA004BA90B02000000080000000E0000005F005200650066003300380036003600390039003400330039000000</w:data> 1379 1378 </xml><![endif]--></span></span></b><!--[if supportFields]><b style='mso-bidi-font-weight: … … 1401 1400 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit</span></b></span><b 1402 1401 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1403 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> substance/Load</span></b>1404 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1405 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: 1406 m inor-latin'>substance</span></b> from the menu; a popup window will appear1407 with possible selections</p>1402 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> 1403 substance/Load</span></b> <b style='mso-bidi-font-weight:normal'><span 1404 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1405 mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>substance</span></b> 1406 from the menu; a popup window will appear with possible selections</p> 1408 1407 1409 1408 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1425 1424 1426 1425 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1427 id=" _x0000_i1044" type="#_x0000_t75" style='width:280.5pt;height:246pt;1428 visibility:visible;mso-wrap-style:square'>1429 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 25.png"1430 o:title=""/> 1431 </v:shape><![endif]--><![if !vml]><img width= 374 height=3281432 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 25.png" v:shapes="_x0000_i1044"><![endif]></span><span1426 id="Picture_x0020_26" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:417pt; 1427 height:269.25pt;visibility:visible;mso-wrap-style:square'> 1428 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image017.png" 1429 o:title=""/> 1430 </v:shape><![endif]--><![if !vml]><img width=556 height=359 1431 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image017.png" v:shapes="Picture_x0020_26"><![endif]></span><span 1433 1432 style='mso-spacerun:yes'> </span></p> 1434 1433 … … 1445 1444 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1446 1445 mso-hansi-theme-font:minor-latin'> substance/Add substance</span></b> to create 1447 a new one (you will be asked for a name and the set of elements in two 1448 successive popup windows). From this information the scattering density and 1449 that as affected by resonant scattering for the listed wavelength is displayed 1450 (thewavelength can be changed in the <b style='mso-bidi-font-weight:normal'><span1446 a new one (you will be asked for a name and the set of elements in two successive 1447 popup windows). From this information the scattering density and that as 1448 affected by resonant scattering for the listed wavelength is displayed (the 1449 wavelength can be changed in the <b style='mso-bidi-font-weight:normal'><span 1451 1450 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1452 1451 mso-hansi-theme-font:minor-latin'>Instrument Parameters</span></b> GSAS-II tree … … 1478 1477 1479 1478 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1480 id=" _x0000_i1043" type="#_x0000_t75" style='width:420.75pt;height:133.5pt;1481 visibility:visible;mso-wrap-style:square'>1482 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image02 6.png"1483 o:title=""/> 1484 </v:shape><![endif]--><![if !vml]><img width= 561 height=1781485 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 26.png" v:shapes="_x0000_i1043"><![endif]></span></p>1479 id="Picture_x0020_27" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:468pt; 1480 height:227.25pt;visibility:visible;mso-wrap-style:square'> 1481 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image029.png" 1482 o:title=""/> 1483 </v:shape><![endif]--><![if !vml]><img width=624 height=303 1484 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image006.png" v:shapes="Picture_x0020_27"><![endif]></span></p> 1486 1485 1487 1486 <p class=MsoNormal><o:p> </o:p></p> … … 1510 1509 1511 1510 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1512 id="Picture_x0020_2 5" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:379.5pt;1513 height: 315pt;visibility:visible;mso-wrap-style:square'>1514 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 06.png"1515 o:title=""/> 1516 </v:shape><![endif]--><![if !vml]><img width= 506 height=4201517 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image00 6.png" v:shapes="Picture_x0020_25"><![endif]></span></p>1511 id="Picture_x0020_28" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:468pt; 1512 height:258pt;visibility:visible;mso-wrap-style:square'> 1513 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image031.png" 1514 o:title=""/> 1515 </v:shape><![endif]--><![if !vml]><img width=624 height=344 1516 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image007.png" v:shapes="Picture_x0020_28"><![endif]></span></p> 1518 1517 1519 1518 <p class=MsoNormal><o:p> </o:p></p> … … 1523 1522 1524 1523 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1525 id="Picture_x0020_2 6" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:525pt;1526 height: 450pt;visibility:visible;mso-wrap-style:square'>1527 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 07.png"1528 o:title=""/> 1529 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001530 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image00 7.png" v:shapes="Picture_x0020_26"><![endif]></span></p>1524 id="Picture_x0020_29" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:412.5pt; 1525 height:354pt;visibility:visible;mso-wrap-style:square'> 1526 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image033.png" 1527 o:title=""/> 1528 </v:shape><![endif]--><![if !vml]><img width=550 height=472 1529 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image008.png" v:shapes="Picture_x0020_29"><![endif]></span></p> 1531 1530 1532 1531 <p class=MsoNormal><o:p> </o:p></p> … … 1569 1568 1570 1569 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1571 id=" _x0000_i1040" type="#_x0000_t75" style='width:525pt;height:450pt;1572 visibility:visible;mso-wrap-style:square'>1573 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 08.png"1574 o:title=""/> 1575 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001576 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image00 8.png" v:shapes="_x0000_i1040"><![endif]></span></p>1570 id="Picture_x0020_30" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:441.75pt; 1571 height:378.75pt;visibility:visible;mso-wrap-style:square'> 1572 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image035.png" 1573 o:title=""/> 1574 </v:shape><![endif]--><![if !vml]><img width=589 height=505 1575 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image009.png" v:shapes="Picture_x0020_30"><![endif]></span></p> 1577 1576 1578 1577 <p class=MsoNormal><o:p> </o:p></p> … … 1588 1587 1589 1588 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1590 id="Picture_x0020_ 28" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:379.5pt;1591 height: 487.5pt;visibility:visible;mso-wrap-style:square'>1592 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 09.png"1593 o:title=""/> 1594 </v:shape><![endif]--><![if !vml]><img width= 506 height=6501595 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 09.png" v:shapes="Picture_x0020_28"><![endif]></span></p>1589 id="Picture_x0020_31" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:468pt; 1590 height:398.25pt;visibility:visible;mso-wrap-style:square'> 1591 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image037.png" 1592 o:title=""/> 1593 </v:shape><![endif]--><![if !vml]><img width=624 height=531 1594 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image010.png" v:shapes="Picture_x0020_31"><![endif]></span></p> 1596 1595 1597 1596 <p class=MsoNormal><o:p> </o:p></p> … … 1623 1622 1624 1623 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1625 id="Picture_x0020_ 29" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:525pt;1626 height: 450pt;visibility:visible;mso-wrap-style:square'>1627 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 10.png"1628 o:title=""/> 1629 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001630 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image01 0.png" v:shapes="Picture_x0020_29"><![endif]></span></p>1624 id="Picture_x0020_32" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:435pt; 1625 height:372.75pt;visibility:visible;mso-wrap-style:square'> 1626 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image039.png" 1627 o:title=""/> 1628 </v:shape><![endif]--><![if !vml]><img width=580 height=497 1629 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image011.png" v:shapes="Picture_x0020_32"><![endif]></span></p> 1631 1630 1632 1631 <p class=MsoNormal><o:p> </o:p></p> … … 1646 1645 1647 1646 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1648 id="Picture_x0020_ 22" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:379.5pt;1649 height: 270.75pt;visibility:visible;mso-wrap-style:square'>1650 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 11.png"1651 o:title=""/> 1652 </v:shape><![endif]--><![if !vml]><img width= 506 height=3611653 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image01 1.png" v:shapes="Picture_x0020_22"><![endif]></span></p>1647 id="Picture_x0020_33" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:468pt; 1648 height:313.5pt;visibility:visible;mso-wrap-style:square'> 1649 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image041.png" 1650 o:title=""/> 1651 </v:shape><![endif]--><![if !vml]><img width=624 height=418 1652 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image012.png" v:shapes="Picture_x0020_33"><![endif]></span></p> 1654 1653 1655 1654 <p class=MsoNormal><o:p> </o:p></p> … … 1658 1657 1659 1658 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1660 id="Picture_x0020_ 12" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt;1661 height: 450pt;visibility:visible;mso-wrap-style:square'>1662 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 12.png"1663 o:title=""/> 1664 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001665 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image01 2.png" v:shapes="Picture_x0020_12"><![endif]></span></p>1659 id="Picture_x0020_34" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:444pt; 1660 height:380.25pt;visibility:visible;mso-wrap-style:square'> 1661 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image043.png" 1662 o:title=""/> 1663 </v:shape><![endif]--><![if !vml]><img width=592 height=507 1664 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image013.png" v:shapes="Picture_x0020_34"><![endif]></span></p> 1666 1665 1667 1666 <p class=MsoNormal><o:p> </o:p></p> … … 1677 1676 1678 1677 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1679 id="Picture_x0020_3 1" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:525pt;1680 height:4 50pt;visibility:visible;mso-wrap-style:square'>1681 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 13.png"1682 o:title=""/> 1683 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001684 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image01 3.png" v:shapes="Picture_x0020_31"><![endif]></span></p>1678 id="Picture_x0020_35" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:468pt; 1679 height:401.25pt;visibility:visible;mso-wrap-style:square'> 1680 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image045.png" 1681 o:title=""/> 1682 </v:shape><![endif]--><![if !vml]><img width=624 height=535 1683 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image014.png" v:shapes="Picture_x0020_35"><![endif]></span></p> 1685 1684 1686 1685 <p class=MsoNormal><o:p> </o:p></p> … … 1707 1706 1708 1707 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1709 id="Picture_x0020_3 2" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt;1710 height:4 50pt;visibility:visible;mso-wrap-style:square'>1711 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 14.png"1712 o:title=""/> 1713 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001714 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image01 4.png" v:shapes="Picture_x0020_32"><![endif]></span></p>1708 id="Picture_x0020_36" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:468pt; 1709 height:401.25pt;visibility:visible;mso-wrap-style:square'> 1710 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image047.png" 1711 o:title=""/> 1712 </v:shape><![endif]--><![if !vml]><img width=624 height=535 1713 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image015.png" v:shapes="Picture_x0020_36"><![endif]></span></p> 1715 1714 1716 1715 <p class=MsoNormal><o:p> </o:p></p> … … 1730 1729 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1731 1730 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background</span></b> 1732 parameter s(one might be able to refine everything at once, but then again it1731 parameter (one might be able to refine everything at once, but then again it 1733 1732 might not work). Check the <b style='mso-bidi-font-weight:normal'><span 1734 1733 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; … … 1756 1755 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1757 1756 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1758 mso-hansi-theme-font:minor-latin'> <span class=SpellE>StdDev</span></span></b> and1759 <span class=SpellE><b style='mso-bidi-font-weight:normal'><span1757 mso-hansi-theme-font:minor-latin'> <span class=SpellE>StdDev</span></span></b> 1758 and <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1760 1759 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1761 1760 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: … … 1766 1765 1767 1766 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1768 id="Picture_x0020_3 3" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:609.75pt;1769 height: 206.25pt;visibility:visible;mso-wrap-style:square'>1770 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 15.png"1771 o:title=""/> 1772 </v:shape><![endif]--><![if !vml]><img width= 813 height=2751773 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image01 5.png" v:shapes="Picture_x0020_33"><![endif]></span></p>1767 id="Picture_x0020_37" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:468pt; 1768 height:196.5pt;visibility:visible;mso-wrap-style:square'> 1769 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image049.png" 1770 o:title=""/> 1771 </v:shape><![endif]--><![if !vml]><img width=624 height=262 1772 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image016.png" v:shapes="Picture_x0020_37"><![endif]></span></p> 1774 1773 1775 1774 <p class=MsoNormal><o:p> </o:p></p> 1776 1775 1777 1776 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1778 id="Picture_x0020_3 4" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt;1779 height: 450pt;visibility:visible;mso-wrap-style:square'>1780 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 16.png"1781 o:title=""/> 1782 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001783 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 16.png" v:shapes="Picture_x0020_34"><![endif]></span></p>1777 id="Picture_x0020_38" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:429pt; 1778 height:367.5pt;visibility:visible;mso-wrap-style:square'> 1779 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image051.png" 1780 o:title=""/> 1781 </v:shape><![endif]--><![if !vml]><img width=572 height=490 1782 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image024.png" v:shapes="Picture_x0020_38"><![endif]></span></p> 1784 1783 1785 1784 <p class=MsoNormal><o:p> </o:p></p> … … 1791 1790 1792 1791 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1793 id="Picture_x0020_ 27" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:468pt;1792 id="Picture_x0020_39" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:468pt; 1794 1793 height:401.25pt;visibility:visible;mso-wrap-style:square'> 1795 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 27.png"1794 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image053.png" 1796 1795 o:title=""/> 1797 1796 </v:shape><![endif]--><![if !vml]><img width=624 height=535 1798 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image02 8.png" v:shapes="Picture_x0020_27"><![endif]></span></p>1799 1800 <p class=MsoNormal><o:p> </o:p></p> 1801 1802 <p class=MsoNormal>This is the sort of agreement one should expect between the 1803 best log normal fit and the size distribution. To save these results you must 1804 do <bstyle='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;1797 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image025.png" v:shapes="Picture_x0020_39"><![endif]></span></p> 1798 1799 <p class=MsoNormal><o:p> </o:p></p> 1800 1801 <p class=MsoNormal>This is the sort of agreement one should expect between the best 1802 log normal fit and the size distribution. To save these results you must do <b 1803 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1805 1804 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/Save 1806 1805 project </span></b>in the main <b style='mso-bidi-font-weight:normal'><span 1807 1806 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1808 mso-hansi-theme-font:minor-latin'>GSAS-II data tree</span></b> window.</p>1807 mso-hansi-theme-font:minor-latin'>GSAS-II data tree</span></b> menu.</p> 1809 1808 1810 1809 <h2>Step 6 Creation of a Unified <span class=SpellE>Guinier-Porod</span> Model</h2> 1811 1810 1812 <p class=MsoNormal>For the Unified model there is assumed to be particles with 1813 some radius of gyration (<span class=SpellE>Guinier</span> model) with a power 1814 law distribution tail (<span class=SpellE>Porod</span> model). This can be set 1815 foryour model by changing the <b style='mso-bidi-font-weight:normal'><span1811 <p class=MsoNormal>For the Unified model there is assumed to be particles with some 1812 radius of gyration (<span class=SpellE>Guinier</span> model) with a power law 1813 distribution tail (<span class=SpellE>Porod</span> model). This can be set for 1814 your model by changing the <b style='mso-bidi-font-weight:normal'><span 1816 1815 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1817 1816 mso-hansi-theme-font:minor-latin'>Distribution</span></b> for the first two … … 1828 1827 1829 1828 <p class=MsoNormal><span style='mso-no-proof:yes'><span 1830 style='mso-spacerun:yes'> </span><!--[if gte vml 1]><v:shape id="Picture_x0020_ 30"1831 o:spid="_x0000_i1030" type="#_x0000_t75" style='width: 379.5pt;height:546pt;1829 style='mso-spacerun:yes'> </span><!--[if gte vml 1]><v:shape id="Picture_x0020_40" 1830 o:spid="_x0000_i1030" type="#_x0000_t75" style='width:468pt;height:459.75pt; 1832 1831 visibility:visible;mso-wrap-style:square'> 1833 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 18.png"1834 o:title=""/> 1835 </v:shape><![endif]--><![if !vml]><img width= 506 height=7281836 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 18.png" v:shapes="Picture_x0020_30"><![endif]></span></p>1832 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image026.png" 1833 o:title=""/> 1834 </v:shape><![endif]--><![if !vml]><img width=624 height=613 1835 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image027.png" v:shapes="Picture_x0020_40"><![endif]></span></p> 1837 1836 1838 1837 <p class=MsoNormal><o:p> </o:p></p> … … 1841 1840 1842 1841 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1843 id="Picture_x0020_ 36" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt;1844 height:4 50pt;visibility:visible;mso-wrap-style:square'>1845 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 19.png"1846 o:title=""/> 1847 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001848 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 19.png" v:shapes="Picture_x0020_36"><![endif]></span></p>1842 id="Picture_x0020_41" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:468pt; 1843 height:401.25pt;visibility:visible;mso-wrap-style:square'> 1844 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image028.png" 1845 o:title=""/> 1846 </v:shape><![endif]--><![if !vml]><img width=624 height=535 1847 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image055.png" v:shapes="Picture_x0020_41"><![endif]></span></p> 1849 1848 1850 1849 <p class=MsoNormal><o:p> </o:p></p> … … 1904 1903 1905 1904 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1906 id="Picture_x0020_ 37" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:379.5pt;1907 height: 546pt;visibility:visible;mso-wrap-style:square'>1908 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 20.png"1909 o:title=""/> 1910 </v:shape><![endif]--><![if !vml]><img width=5 06 height=7281911 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 20.png" v:shapes="Picture_x0020_37"><![endif]></span></p>1905 id="Picture_x0020_42" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:446.25pt; 1906 height:438.75pt;visibility:visible;mso-wrap-style:square'> 1907 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image056.png" 1908 o:title=""/> 1909 </v:shape><![endif]--><![if !vml]><img width=595 height=585 1910 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image057.png" v:shapes="Picture_x0020_42"><![endif]></span></p> 1912 1911 1913 1912 <p class=MsoNormal><o:p> </o:p></p> … … 1916 1915 1917 1916 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1918 id="Picture_x0020_ 38" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:525pt;1919 height:4 50pt;visibility:visible;mso-wrap-style:square'>1920 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 21.png"1921 o:title=""/> 1922 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001923 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 21.png" v:shapes="Picture_x0020_38"><![endif]></span></p>1917 id="Picture_x0020_43" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:468pt; 1918 height:401.25pt;visibility:visible;mso-wrap-style:square'> 1919 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image058.png" 1920 o:title=""/> 1921 </v:shape><![endif]--><![if !vml]><img width=624 height=535 1922 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image059.png" v:shapes="Picture_x0020_43"><![endif]></span></p> 1924 1923 1925 1924 <p class=MsoNormal><o:p> </o:p></p> … … 1960 1959 1961 1960 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1962 id="Picture_x0020_ 39" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:609.75pt;1963 height: 224.25pt;visibility:visible;mso-wrap-style:square'>1964 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 22.png"1965 o:title=""/> 1966 </v:shape><![endif]--><![if !vml]><img width= 813 height=2991967 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 22.png" v:shapes="Picture_x0020_39"><![endif]></span></p>1961 id="Picture_x0020_44" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:449.25pt; 1962 height:198pt;visibility:visible;mso-wrap-style:square'> 1963 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image060.png" 1964 o:title=""/> 1965 </v:shape><![endif]--><![if !vml]><img width=599 height=264 1966 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image061.png" v:shapes="Picture_x0020_44"><![endif]></span></p> 1968 1967 1969 1968 <p class=MsoNormal><o:p> </o:p></p> … … 1972 1971 1973 1972 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1974 id="Picture_x0020_4 0" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;1975 height: 450pt;visibility:visible;mso-wrap-style:square'>1976 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 23.png"1977 o:title=""/> 1978 </v:shape><![endif]--><![if !vml]><img width= 700 height=6001979 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image0 23.png" v:shapes="Picture_x0020_40"><![endif]></span></p>1973 id="Picture_x0020_45" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:439.5pt; 1974 height:376.5pt;visibility:visible;mso-wrap-style:square'> 1975 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image062.png" 1976 o:title=""/> 1977 </v:shape><![endif]--><![if !vml]><img width=586 height=502 1978 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image063.png" v:shapes="Picture_x0020_45"><![endif]></span></p> 1980 1979 1981 1980 <p class=MsoNormal><o:p> </o:p></p> -
Tutorials/SAfit/Fitting Small Angle Scattering Data_files/filelist.xml
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