Changeset 3031


Ignore:
Timestamp:
Aug 30, 2017 2:27:07 PM (4 years ago)
Author:
vondreele
Message:

update to 2 frame version

Location:
Tutorials/SAsize
Files:
20 added
11 deleted
2 edited

Legend:

Unmodified
Added
Removed
  • Tutorials/SAsize/Small Angle Size Distribution.htm

    r2790 r3031  
    2525  <o:Author>Von Dreele</o:Author>
    2626  <o:LastAuthor>vondreele</o:LastAuthor>
    27   <o:Revision>16</o:Revision>
    28   <o:TotalTime>1960</o:TotalTime>
     27  <o:Revision>17</o:Revision>
     28  <o:TotalTime>1975</o:TotalTime>
    2929  <o:Created>2014-03-20T16:54:00Z</o:Created>
    30   <o:LastSaved>2017-04-19T15:00:00Z</o:LastSaved>
    31   <o:Pages>1</o:Pages>
     30  <o:LastSaved>2017-08-30T19:25:00Z</o:LastSaved>
     31  <o:Pages>14</o:Pages>
    3232  <o:Words>1274</o:Words>
    3333  <o:Characters>7265</o:Characters>
     
    661661 /* Font Definitions */
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    12171224<p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In
    12181225this tutorial you will determine the size distribution of particles in an
    1219 alumina polishing powder using data from a constant wavelength synchrotron
    1220 X-ray USAXS instrument. You will use both Maximum Entropy (<span class=SpellE>MaxEnt</span>)
     1226alumina polishing powder using data from a constant wavelength synchrotron X-ray
     1227USAXS instrument. You will use both Maximum Entropy (<span class=SpellE>MaxEnt</span>)
    12211228and Total Non-Negative Least Squares (TNNLS) methods assuming spherical
    12221229particles. The data were collected from <span style='mso-fareast-font-family:
     
    13001307 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
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    1307 src="Small%20Angle%20Size%20Distribution_files/image001.png" v:shapes="_x0000_i1038"><![endif]></span></p>
     1314src="Small%20Angle%20Size%20Distribution_files/image001.png" v:shapes="Picture_x0020_1"><![endif]></span></p>
    13081315
    13091316<h2>Step 2: Set Limits</h2>
     
    13361343
    13371344<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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     1346 height:267pt;visibility:visible;mso-wrap-style:square'>
     1347 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image015.png"
    13411348  o:title=""/>
    1342 </v:shape><![endif]--><![if !vml]><img width=300 height=129
    1343 src="Small%20Angle%20Size%20Distribution_files/image002.png" v:shapes="Picture_x0020_15"><![endif]></span><span
     1349</v:shape><![endif]--><![if !vml]><img width=554 height=356
     1350src="Small%20Angle%20Size%20Distribution_files/image016.png" v:shapes="Picture_x0020_15"><![endif]></span><span
    13441351style='mso-spacerun:yes'> </span></p>
    13451352
     
    13681375mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit</span></b></span><b
    13691376style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    1370 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> substance/Load</span></b>
    1371 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    1372 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>substance</span></b>
    1373 from the menu; a popup window will appear with possible selections</p>
     1377mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>
     1378substance/Load</span></b> <b style='mso-bidi-font-weight:normal'><span
     1379style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
     1380mso-hansi-theme-font:minor-latin'>substance</span></b> from the menu; a popup
     1381window will appear with possible selections</p>
    13741382
    13751383<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1376  id="Picture_x0020_23" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:259.5pt;
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     1385 visibility:visible;mso-wrap-style:square'>
    13781386 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image003.png"
    13791387  o:title=""/>
    13801388</v:shape><![endif]--><![if !vml]><img width=346 height=336
    1381 src="Small%20Angle%20Size%20Distribution_files/image003.png" v:shapes="Picture_x0020_23"><![endif]><o:p></o:p></span></p>
     1389src="Small%20Angle%20Size%20Distribution_files/image003.png" v:shapes="_x0000_i1036"><![endif]><o:p></o:p></span></p>
    13821390
    13831391<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    13911399
    13921400<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1393  id="Picture_x0020_16" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:280.5pt;
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    1395  <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image004.png"
     1401 id="Picture_x0020_17" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:431.25pt;
     1402 height:275.25pt;visibility:visible;mso-wrap-style:square'>
     1403 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image017.png"
    13961404  o:title=""/>
    1397 </v:shape><![endif]--><![if !vml]><img width=374 height=328
    1398 src="Small%20Angle%20Size%20Distribution_files/image004.png" v:shapes="Picture_x0020_16"><![endif]></span><span
     1405</v:shape><![endif]--><![if !vml]><img width=575 height=367
     1406src="Small%20Angle%20Size%20Distribution_files/image017.png" v:shapes="Picture_x0020_17"><![endif]></span><span
    13991407style='mso-spacerun:yes'> </span></p>
    14001408
    14011409<p class=MsoNormal><o:p>&nbsp;</o:p></p>
    14021410
    1403 <p class=MsoNormal>If desired you can load/add as many substances as you want into
    1404 this list; you can also delete any of them (except vacuum &amp; unit scatter).
    1405 The composition, volume occupied by the atoms in the composition and the
    1406 density are given for each substance. These can each be edited; the other
     1411<p class=MsoNormal>If desired you can load/add as many substances as you want
     1412into this list; you can also delete any of them (except vacuum &amp; unit
     1413scatter). The composition, volume occupied by the atoms in the composition and
     1414the density are given for each substance. These can each be edited; the other
    14071415values will change accordingly. If your substance isn’t in the list, you can <b
    14081416style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     
    14391447
    14401448<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1441  id="Picture_x0020_17" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:305.25pt;
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    1443  <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image005.png"
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     1450 height:447pt;visibility:visible;mso-wrap-style:square'>
     1451 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image018.png"
    14441452  o:title=""/>
    1445 </v:shape><![endif]--><![if !vml]><img width=407 height=544
    1446 src="Small%20Angle%20Size%20Distribution_files/image005.png" v:shapes="Picture_x0020_17"><![endif]></span></p>
     1453</v:shape><![endif]--><![if !vml]><img width=612 height=596
     1454src="Small%20Angle%20Size%20Distribution_files/image018.png" v:shapes="Picture_x0020_18"><![endif]></span></p>
    14471455
    14481456<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    14721480
    14731481<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1474  id="Picture_x0020_18" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:361.5pt;
    1475  height:191.25pt;visibility:visible;mso-wrap-style:square'>
    1476  <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image006.png"
     1482 id="_x0000_i1033" type="#_x0000_t75" style='width:468pt;height:238.5pt;
     1483 visibility:visible;mso-wrap-style:square'>
     1484 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image019.png"
    14771485  o:title=""/>
    1478 </v:shape><![endif]--><![if !vml]><img width=482 height=255
    1479 src="Small%20Angle%20Size%20Distribution_files/image006.png" v:shapes="Picture_x0020_18"><![endif]></span></p>
     1486</v:shape><![endif]--><![if !vml]><img width=624 height=318
     1487src="Small%20Angle%20Size%20Distribution_files/image020.png" v:shapes="_x0000_i1033"><![endif]></span></p>
    14801488
    14811489<p class=MsoNormal><o:p>&nbsp;</o:p></p>
    14821490
    1483 <p class=MsoNormal>Many selections are made by default for this analysis;
    1484 however it is important that an appropriate value is selected for the
    1485 background. From the high Q end of the data plot</p>
     1491<p class=MsoNormal>Many selections are made by default for this analysis; however
     1492it is important that an appropriate value is selected for the background. From
     1493the high Q end of the data plot</p>
    14861494
    14871495<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
     
    15011509mso-hansi-theme-font:minor-latin'>0.12</span></b>; enter that into the
    15021510appropriate place in the data window. The plot will be redrawn showing a
    1503 horizontal red line for the background. All the other parameters seem reasonable
    1504 for a 1<sup>st</sup> attempt at a <span class=SpellE>MaxEnt</span> solution. Do
    1505 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    1506 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Fit</span></b>;
    1507 the console window will show that the calculation did not converge and the <b
    1508 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    1509 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Size
    1510 Distribution</span></b> plot has a “choppy” appearance.</p>
     1511horizontal red line for the background. All the other parameters seem
     1512reasonable for a 1<sup>st</sup> attempt at a <span class=SpellE>MaxEnt</span>
     1513solution. Do <b style='mso-bidi-font-weight:normal'><span style='font-family:
     1514"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
     1515minor-latin'>Models/Fit</span></b>; the console window will show that the
     1516calculation did not converge and the <b style='mso-bidi-font-weight:normal'><span
     1517style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
     1518mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> plot has a
     1519“choppy” appearance.</p>
    15111520
    15121521<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1513  id="Picture_x0020_28" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt;
    1514  height:450pt;visibility:visible;mso-wrap-style:square'>
    1515  <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image008.png"
     1522 id="Picture_x0020_20" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:468pt;
     1523 height:401.25pt;visibility:visible;mso-wrap-style:square'>
     1524 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image021.png"
    15161525  o:title=""/>
    1517 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1518 src="Small%20Angle%20Size%20Distribution_files/image008.png" v:shapes="Picture_x0020_28"><![endif]></span></p>
     1526</v:shape><![endif]--><![if !vml]><img width=624 height=535
     1527src="Small%20Angle%20Size%20Distribution_files/image022.png" v:shapes="Picture_x0020_20"><![endif]></span></p>
    15191528
    15201529<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    15331542
    15341543<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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    1537  <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image009.png"
     1544 id="Picture_x0020_21" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:468pt;
     1545 height:401.25pt;visibility:visible;mso-wrap-style:square'>
     1546 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image023.png"
    15381547  o:title=""/>
    1539 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1540 src="Small%20Angle%20Size%20Distribution_files/image009.png" v:shapes="Picture_x0020_29"><![endif]></span></p>
     1548</v:shape><![endif]--><![if !vml]><img width=624 height=535
     1549src="Small%20Angle%20Size%20Distribution_files/image024.png" v:shapes="Picture_x0020_21"><![endif]></span></p>
    15411550
    15421551<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    15631572
    15641573<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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    1567  <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image010.png"
     1574 id="Picture_x0020_22" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:426.75pt;
     1575 height:366pt;visibility:visible;mso-wrap-style:square'>
     1576 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image025.png"
    15681577  o:title=""/>
    1569 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1570 src="Small%20Angle%20Size%20Distribution_files/image010.png" v:shapes="Picture_x0020_20"><![endif]></span></p>
     1578</v:shape><![endif]--><![if !vml]><img width=569 height=488
     1579src="Small%20Angle%20Size%20Distribution_files/image026.png" v:shapes="Picture_x0020_22"><![endif]></span></p>
    15711580
    15721581<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    15931602
    15941603<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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     1606 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image027.png"
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    1599 </v:shape><![endif]--><![if !vml]><img width=501 height=255
    1600 src="Small%20Angle%20Size%20Distribution_files/image011.png" v:shapes="Picture_x0020_21"><![endif]></span></p>
     1608</v:shape><![endif]--><![if !vml]><img width=624 height=318
     1609src="Small%20Angle%20Size%20Distribution_files/image028.png" v:shapes="Picture_x0020_23"><![endif]></span></p>
    16011610
    16021611<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    16121621
    16131622<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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    1616  <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image012.png"
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    1618 </v:shape><![endif]--><![if !vml]><img width=829 height=600
    1619 src="Small%20Angle%20Size%20Distribution_files/image012.png" v:shapes="Picture_x0020_289"><![endif]></span></p>
     1627</v:shape><![endif]--><![if !vml]><img width=624 height=535
     1628src="Small%20Angle%20Size%20Distribution_files/image030.png" v:shapes="Picture_x0020_24"><![endif]></span></p>
    16201629
    16211630<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    16311640
    16321641<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1633  id="Picture_x0020_291" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:621.75pt;
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    16361645  o:title=""/>
    1637 </v:shape><![endif]--><![if !vml]><img width=829 height=600
    1638 src="Small%20Angle%20Size%20Distribution_files/image013.png" v:shapes="Picture_x0020_291"><![endif]></span></p>
     1646</v:shape><![endif]--><![if !vml]><img width=624 height=535
     1647src="Small%20Angle%20Size%20Distribution_files/image032.png" v:shapes="Picture_x0020_25"><![endif]></span></p>
    16391648
    16401649<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    16461655
    16471656<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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    1650  <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image014.png"
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     1658 height:385.5pt;visibility:visible;mso-wrap-style:square'>
     1659 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image033.png"
    16511660  o:title=""/>
    1652 </v:shape><![endif]--><![if !vml]><img width=700 height=600
    1653 src="Small%20Angle%20Size%20Distribution_files/image014.png" v:shapes="Picture_x0020_22"><![endif]></span></p>
     1661</v:shape><![endif]--><![if !vml]><img width=600 height=514
     1662src="Small%20Angle%20Size%20Distribution_files/image034.png" v:shapes="Picture_x0020_26"><![endif]></span></p>
    16541663
    16551664<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    16611670normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    16621671minor-latin;mso-hansi-theme-font:minor-latin'>0-4</span></b>, that changes the
    1663 data weighting to <span class=SpellE>Q<sup>p</sup></span>. This can change the
    1664 convergence of the IPG method and yield improved results if one is unsuccessful
    1665 with the default settings. I got a nice fit with a <b style='mso-bidi-font-weight:
    1666 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    1667 minor-latin;mso-hansi-theme-font:minor-latin'>Q power weight</span></b> of <b
     1672data weighting to <span class=SpellE>Q<sup>p</sup></span>. This can change the convergence
     1673of the IPG method and yield improved results if one is unsuccessful with the
     1674default settings. I got a nice fit with a <b style='mso-bidi-font-weight:normal'><span
     1675style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
     1676mso-hansi-theme-font:minor-latin'>Q power weight</span></b> of <b
    16681677style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    16691678mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>3</span></b>
     
    16741683mso-hansi-theme-font:minor-latin'>2.0</span></b>.</p>
    16751684
    1676 <p class=MsoNormal>You should save this GSAS-II project as it will be used in
    1677 the tutorial for fitting small angle scattering data; I used <span
    1678 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
    1679 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1680 minor-latin'>alumina.gpx</span></b></span>.</p>
     1685<p class=MsoNormal>You should save this GSAS-II project as it will be used in the
     1686tutorial for fitting small angle scattering data; I used <span class=SpellE><b
     1687style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     1688mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>alumina.gpx</span></b></span>.</p>
    16811689
    16821690</div>
  • Tutorials/SAsize/Small Angle Size Distribution_files/filelist.xml

    r1705 r3031  
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