Changeset 2390 for Tutorials/SAimages/Small Angle Image Processing.htm
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- Jul 28, 2016 2:18:10 PM (7 years ago)
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Tutorials/SAimages/Small Angle Image Processing.htm
r1741 r2390 24 24 <o:Author>Von Dreele</o:Author> 25 25 <o:LastAuthor>Von Dreele</o:LastAuthor> 26 <o:Revision>1 3</o:Revision>26 <o:Revision>14</o:Revision> 27 27 <o:TotalTime>2504</o:TotalTime> 28 28 <o:Created>2014-05-13T20:30:00Z</o:Created> 29 <o:LastSaved>201 5-03-18T20:33:00Z</o:LastSaved>29 <o:LastSaved>2016-07-28T18:47:00Z</o:LastSaved> 30 30 <o:Pages>1</o:Pages> 31 <o:Words>198 2</o:Words>32 <o:Characters>1129 9</o:Characters>31 <o:Words>1981</o:Words> 32 <o:Characters>11295</o:Characters> 33 33 <o:Company>Argonne National Laboratory</o:Company> 34 34 <o:Lines>94</o:Lines> 35 35 <o:Paragraphs>26</o:Paragraphs> 36 <o:CharactersWithSpaces>1325 5</o:CharactersWithSpaces>37 <o:Version>1 5.00</o:Version>36 <o:CharactersWithSpaces>13250</o:CharactersWithSpaces> 37 <o:Version>16.00</o:Version> 38 38 </o:DocumentProperties> 39 39 <o:OfficeDocumentSettings> … … 661 661 {font-family:"Cambria Math"; 662 662 panose-1:2 4 5 3 5 4 6 3 2 4; 663 mso-font-charset: 0;663 mso-font-charset:1; 664 664 mso-generic-font-family:roman; 665 665 mso-font-pitch:variable; 666 mso-font-signature: -536870145 1107305727 0 0 4150;}666 mso-font-signature:0 0 0 0 0 0;} 667 667 @font-face 668 668 {font-family:Calibri; … … 1036 1036 mso-hansi-font-family:"Courier New"; 1037 1037 mso-bidi-font-family:"Courier New";} 1038 p.msonormal0, li.msonormal0, div.msonormal0 1039 {mso-style-name:msonormal; 1040 mso-style-noshow:yes; 1041 mso-style-priority:99; 1042 mso-style-unhide:no; 1043 mso-margin-top-alt:auto; 1044 margin-right:0in; 1045 mso-margin-bottom-alt:auto; 1046 margin-left:0in; 1047 mso-pagination:widow-orphan; 1048 font-size:12.0pt; 1049 font-family:"Times New Roman",serif; 1050 mso-fareast-font-family:"Times New Roman"; 1051 mso-fareast-theme-font:minor-fareast;} 1038 1052 span.DocumentMapChar 1039 1053 {mso-style-name:"Document Map Char"; … … 1187 1201 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Data/Read 1188 1202 Image data 1189 </span></b> and a file selection dialog box will appear. Go to <b 1190 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1191 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>exercises/<span 1192 class=SpellE>SAimages</span></span></b> and select <b style='mso-bidi-font-weight: 1193 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1194 minor-latin;mso-hansi-theme-font:minor-latin'>AgBehenate_003.tif</span></b> 1203 </span></b> and a file selection dialog box will appear. Go to <span 1204 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1205 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1206 minor-latin'>SAimages</span></b></span><b style='mso-bidi-font-weight:normal'><span 1207 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1208 mso-hansi-theme-font:minor-latin'>/data</span></b> and select <b 1209 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1210 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>AgBehenate_003.tif</span></b> 1195 1211 with either a mouse button double click or <b style='mso-bidi-font-weight:normal'><span 1196 1212 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; … … 1337 1353 <o:lock v:ext="edit" shapetype="f"/> 1338 1354 </v:shape><![endif]--><![if !vml]><span style='mso-ignore:vglayout;position: 1339 absolute;z-index:251659264;margin-left:234px;margin-top:27 4px;width:73px;1355 absolute;z-index:251659264;margin-left:234px;margin-top:273px;width:73px; 1340 1356 height:38px'><img width=73 height=38 1341 src="Small%20Angle%20Image%20Processing_files/image0 04.png" v:shapes="Straight_x0020_Arrow_x0020_Connector_x0020_21"></span><![endif]><span1357 src="Small%20Angle%20Image%20Processing_files/image040.png" v:shapes="Straight_x0020_Arrow_x0020_Connector_x0020_21"></span><![endif]><span 1342 1358 style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_4" 1343 1359 o:spid="_x0000_i1059" type="#_x0000_t75" style='width:525pt;height:450pt; … … 1395 1411 rings. I suggest you change <b style='mso-bidi-font-weight:normal'><span 1396 1412 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1397 mso-hansi-theme-font:minor-latin'>Min ring I/<span class=SpellE><span 1398 class=GramE>Ib</span></span></span></b> to <b style='mso-bidi-font-weight:normal'><span 1399 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1400 mso-hansi-theme-font:minor-latin'>0.5</span></b> and <b style='mso-bidi-font-weight: 1401 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1402 minor-latin;mso-hansi-theme-font:minor-latin'>Min <span class=SpellE>calib</span> 1403 d-spacing</span></b> to <b style='mso-bidi-font-weight:normal'><span 1404 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1405 mso-hansi-theme-font:minor-latin'>10.0</span></b>. Do <b style='mso-bidi-font-weight: 1406 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1407 minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Recalibrate</span></b>; 1413 mso-hansi-theme-font:minor-latin'>Min ring I/<span class=SpellE>Ib</span></span></b> 1414 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1415 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.5</span></b> 1416 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1417 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Min <span 1418 class=SpellE>calib</span> d-spacing</span></b> to <b style='mso-bidi-font-weight: 1419 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1420 minor-latin;mso-hansi-theme-font:minor-latin'>10.0</span></b>. Do <b 1421 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1422 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Recalibrate</span></b>; 1408 1423 more points will be used and they will be limited to the 5 visible rings in the 1409 1424 pattern.</p> … … 1475 1490 1476 1491 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1477 id=" _x0000_i1054" type="#_x0000_t75" style='width:300pt;height:310.5pt;1478 visibility:visible;mso-wrap-style:square'>1492 id="Picture_x0020_9" o:spid="_x0000_i1054" type="#_x0000_t75" style='width:300pt; 1493 height:310.5pt;visibility:visible;mso-wrap-style:square'> 1479 1494 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image010.png" 1480 1495 o:title=""/> 1481 1496 </v:shape><![endif]--><![if !vml]><img width=400 height=414 1482 src="Small%20Angle%20Image%20Processing_files/image010.png" v:shapes=" _x0000_i1054"><![endif]></span></p>1497 src="Small%20Angle%20Image%20Processing_files/image010.png" v:shapes="Picture_x0020_9"><![endif]></span></p> 1483 1498 1484 1499 <p class=MsoNormal><o:p> </o:p></p> … … 1500 1515 1501 1516 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1502 id=" _x0000_i1053" type="#_x0000_t75" style='width:472.5pt;height:388.5pt;1503 visibility:visible;mso-wrap-style:square'>1517 id="Picture_x0020_10" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:472.5pt; 1518 height:388.5pt;visibility:visible;mso-wrap-style:square'> 1504 1519 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image011.png" 1505 1520 o:title=""/> 1506 1521 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1507 src="Small%20Angle%20Image%20Processing_files/image011.png" v:shapes=" _x0000_i1053"><![endif]></span></p>1522 src="Small%20Angle%20Image%20Processing_files/image011.png" v:shapes="Picture_x0020_10"><![endif]></span></p> 1508 1523 1509 1524 <p class=MsoNormal><o:p> </o:p></p> … … 1524 1539 1525 1540 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1526 id=" _x0000_i1052" type="#_x0000_t75" style='width:472.5pt;height:388.5pt;1527 visibility:visible;mso-wrap-style:square'>1541 id="Picture_x0020_11" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:472.5pt; 1542 height:388.5pt;visibility:visible;mso-wrap-style:square'> 1528 1543 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image012.png" 1529 1544 o:title=""/> 1530 1545 </v:shape><![endif]--><![if !vml]><img width=630 height=518 1531 src="Small%20Angle%20Image%20Processing_files/image012.png" v:shapes="_x0000_i1052"><![endif]></span></p> 1532 1533 <p class=MsoNormal><o:p> </o:p></p> 1534 1535 <p class=MsoNormal><span class=GramE>and</span> the image will be that of 1536 glassy carbon. Changing the <b style='mso-bidi-font-weight:normal'><span 1537 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1538 mso-hansi-theme-font:minor-latin'>Max intensity</span></b> slider on the <b 1539 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1540 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 1541 Controls</span></b> window will show that the image from the <span 1542 class=SpellE>MarCCD</span> is circular and slightly offset from the beam 1546 src="Small%20Angle%20Image%20Processing_files/image012.png" v:shapes="Picture_x0020_11"><![endif]></span></p> 1547 1548 <p class=MsoNormal><o:p> </o:p></p> 1549 1550 <p class=MsoNormal>and the image will be that of glassy carbon. Changing the <b 1551 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1552 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Max intensity</span></b> 1553 slider on the <b style='mso-bidi-font-weight:normal'><span style='font-family: 1554 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1555 minor-latin'>Image Controls</span></b> window will show that the image from the 1556 <span class=SpellE>MarCCD</span> is circular and slightly offset from the beam 1543 1557 center. A beam stop shadow is evident as well as an arc-like fault in the image 1544 1558 (toward the upper left corner of the image). We will sort those out later.</p> … … 1573 1587 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1574 1588 minor-latin;mso-hansi-theme-font:minor-latin'>Show integration limits?</span></b> 1575 <span class=GramE>and</span> <b style='mso-bidi-font-weight:normal'><span 1576 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1577 mso-hansi-theme-font:minor-latin'>Do full integration?</span></b> A pair of 1578 circles with a connecting diagonal line will appear on the plot. Set the <b 1579 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1580 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Inner/Outer 1581 q</span></b> values to <b style='mso-bidi-font-weight:normal'><span 1582 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1583 mso-hansi-theme-font:minor-latin'>0.05</span></b> and <b style='mso-bidi-font-weight: 1584 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1585 minor-latin;mso-hansi-theme-font:minor-latin'>0.9</span></b>, respectively, and 1586 set the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1587 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Start 1588 azimuth</span></b> to <b style='mso-bidi-font-weight:normal'><span 1589 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1590 mso-hansi-theme-font:minor-latin'>0</span></b>. Set the <b style='mso-bidi-font-weight: 1591 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1592 minor-latin;mso-hansi-theme-font:minor-latin'>No. 2-theta bins</span></b> to <b 1593 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1594 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>250</span></b>, 1595 which is more appropriate for small angle scattering, and set the <b 1596 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1597 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Bin style: 1598 Constant step bins in</span></b> to <span class=GramE><b style='mso-bidi-font-weight: 1599 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1600 minor-latin;mso-hansi-theme-font:minor-latin'>log(</span></b></span><b 1601 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1602 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>q)</span></b>. 1589 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1590 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Do full 1591 integration?</span></b> A pair of circles with a connecting diagonal line will 1592 appear on the plot. Set the <b style='mso-bidi-font-weight:normal'><span 1593 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1594 mso-hansi-theme-font:minor-latin'>Inner/Outer q</span></b> values to <b 1595 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1596 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.05</span></b> 1597 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1598 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.9</span></b>, 1599 respectively, and set the <b style='mso-bidi-font-weight:normal'><span 1600 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1601 mso-hansi-theme-font:minor-latin'>Start azimuth</span></b> to <b 1602 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1603 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0</span></b>. 1604 Set the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1605 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>No. 2-theta 1606 bins</span></b> to <b style='mso-bidi-font-weight:normal'><span 1607 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1608 mso-hansi-theme-font:minor-latin'>250</span></b>, which is more appropriate for 1609 small angle scattering, and set the <b style='mso-bidi-font-weight:normal'><span 1610 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1611 mso-hansi-theme-font:minor-latin'>Bin style: Constant step bins in</span></b> 1612 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1613 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>log(q)</span></b>. 1603 1614 You should also check the <b style='mso-bidi-font-weight:normal'><span 1604 1615 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1605 mso-hansi-theme-font:minor-latin'>Apply sample absorption?</span></b> <span 1606 class=GramE>and</span> <b style='mso-bidi-font-weight:normal'><span 1607 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1608 mso-hansi-theme-font:minor-latin'>Apply polarization?</span></b> <span 1609 class=GramE>boxes</span>; enter the measured <b style='mso-bidi-font-weight: 1616 mso-hansi-theme-font:minor-latin'>Apply sample absorption?</span></b> and <b 1617 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1618 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Apply 1619 polarization?</span></b> boxes; enter the measured <b style='mso-bidi-font-weight: 1610 1620 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1611 1621 minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> (<b … … 1783 1793 1784 1794 <p class=MsoNormal>To add the mask 1: be sure the focus is on the image and the 1785 zoom buttons are off, 2: type <span class=GramE><b style='mso-bidi-font-weight: 1786 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1787 minor-latin;mso-hansi-theme-font:minor-latin'>a</span></b> to</span> activate 1788 the arc mask entry 3: press the left mouse button (<b style='mso-bidi-font-weight: 1789 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1790 minor-latin;mso-hansi-theme-font:minor-latin'>LB</span></b>) with the cursor 1791 centered on the bad arc. The <b style='mso-bidi-font-weight:normal'><span 1792 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1793 mso-hansi-theme-font:minor-latin'>Masks</span></b> window will show a new entry 1794 </p> 1795 zoom buttons are off, 2: type <b style='mso-bidi-font-weight:normal'><span 1796 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1797 mso-hansi-theme-font:minor-latin'>a</span></b> to activate the arc mask entry 1798 3: press the left mouse button (<b style='mso-bidi-font-weight:normal'><span 1799 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1800 mso-hansi-theme-font:minor-latin'>LB</span></b>) with the cursor centered on 1801 the bad arc. The <b style='mso-bidi-font-weight:normal'><span style='font-family: 1802 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1803 minor-latin'>Masks</span></b> window will show a new entry </p> 1795 1804 1796 1805 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1805 1814 <p class=MsoNormal><o:p> </o:p></p> 1806 1815 1807 <p class=MsoNormal><span class=GramE>and</span> an arc mask will be drawn on 1808 the plot.</p> 1816 <p class=MsoNormal>and an arc mask will be drawn on the plot.</p> 1809 1817 1810 1818 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1839 1847 1840 1848 <p class=MsoNormal>Next lets deal with the beam stop. Im going to use both a 1841 polygon and a spot to cover it. Move the zoom area to be around the center, make1842 sure the zoom buttons are off, enter <b style='mso-bidi-font-weight:normal'><span1849 polygon and a spot to cover it. Move the zoom area to be around the center, 1850 make sure the zoom buttons are off, enter <b style='mso-bidi-font-weight:normal'><span 1843 1851 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1844 1852 mso-hansi-theme-font:minor-latin'>s</span></b> on the plot and press mouse <b … … 1916 1924 closely dragging it with mouse <b style='mso-bidi-font-weight:normal'><span 1917 1925 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1918 mso-hansi-theme-font:minor-latin'>LB</span></b> pressed; a new vertex can be added1919 by dragging an existing vertex with the mouse <b style='mso-bidi-font-weight:1926 mso-hansi-theme-font:minor-latin'>LB</span></b> pressed; a new vertex can be 1927 added by dragging an existing vertex with the mouse <b style='mso-bidi-font-weight: 1920 1928 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1921 1929 minor-latin;mso-hansi-theme-font:minor-latin'>RB</span></b> pressed. If you … … 1927 1935 mask</span></b>; a <b style='mso-bidi-font-weight:normal'><span 1928 1936 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1929 mso-hansi-theme-font:minor-latin'>Copy mask information</span></b> dialog box will1930 appear. Select the <b style='mso-bidi-font-weight:normal'><span1937 mso-hansi-theme-font:minor-latin'>Copy mask information</span></b> dialog box 1938 will appear. Select the <b style='mso-bidi-font-weight:normal'><span 1931 1939 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1932 1940 mso-hansi-theme-font:minor-latin'>Sa1-4</span></b> items and press <b … … 1941 1949 1942 1950 <p class=MsoNormal>We are now ready to integrate the glassy carbon and the four 1943 <span class=GramE>Sa</span> images. Select any <b style='mso-bidi-font-weight: 1944 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1945 m inor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> and1946 then do <bstyle='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;1951 Sa images. Select any <b style='mso-bidi-font-weight:normal'><span 1952 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1953 mso-hansi-theme-font:minor-latin'>Image Controls</span></b> and then do <b 1954 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1947 1955 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Integrate 1948 1956 all</span></b>. A selection dialog will appear; select only the <b … … 1954 1962 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1955 1963 mso-hansi-theme-font:minor-latin'>Ok</span></b>. The image integration will 1956 proceed; a progress bar shows as each one is done. Five SASD data items will appear1957 on the GSAS-II data tree; the last one (<b style='mso-bidi-font-weight:normal'><span 1958 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1959 m so-hansi-theme-font:minor-latin'>SASD Sa4_40s_061.tif <span class=SpellE>Azm</span>=45.00</span></b>)1960 will be expanded and plotted (you may have to select the <b style='mso-bidi-font-weight: 1961 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1962 minor-latin;mso-hansi-theme-font:minor-latin'>Powder Patterns</span></b> tab to 1963 see it).</p>1964 1965 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1966 id=" _x0000_i1037" type="#_x0000_t75" style='width:525pt;height:450pt;1967 visibility:visible;mso-wrap-style:square'>1964 proceed; a progress bar shows as each one is done. Five SASD data items will 1965 appear on the GSAS-II data tree; the last one (<b style='mso-bidi-font-weight: 1966 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1967 minor-latin;mso-hansi-theme-font:minor-latin'>SASD Sa4_40s_061.tif <span 1968 class=SpellE>Azm</span>=45.00</span></b>) will be expanded and plotted (you may 1969 have to select the <b style='mso-bidi-font-weight:normal'><span 1970 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1971 mso-hansi-theme-font:minor-latin'>Powder Patterns</span></b> tab to see it).</p> 1972 1973 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1974 id="Picture_x0020_26" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:525pt; 1975 height:450pt;visibility:visible;mso-wrap-style:square'> 1968 1976 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image027.png" 1969 1977 o:title=""/> 1970 1978 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1971 src="Small%20Angle%20Image%20Processing_files/image027.png" v:shapes=" _x0000_i1037"><![endif]></span></p>1979 src="Small%20Angle%20Image%20Processing_files/image027.png" v:shapes="Picture_x0020_26"><![endif]></span></p> 1972 1980 1973 1981 <p class=MsoNormal><o:p> </o:p></p> … … 1993 2001 the image data; do <b style='mso-bidi-font-weight:normal'><span 1994 2002 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1995 mso-hansi-theme-font:minor-latin'>Import/Small Angle Data/ from <span 1996 class=GramE>q(</span>A-1) step X-ray QIE data file</span></b> and select <b 1997 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1998 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>GC 1999 calibrated data.txt</span></b> from the file selection dialog. You will need to 2000 select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2001 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>any <span 2002 class=GramE>file(</span>*.*)</span></b> to see it. A <b style='mso-bidi-font-weight: 2003 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2004 minor-latin;mso-hansi-theme-font:minor-latin'>Is this the file you want</span></b> 2005 dialog will appear respond <b style='mso-bidi-font-weight:normal'><span 2006 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2007 mso-hansi-theme-font:minor-latin'>Yes</span></b> to read the file; it will be 2008 plotted.</p> 2003 mso-hansi-theme-font:minor-latin'>Import/Small Angle Data/ from q(A-1) step 2004 X-ray QIE data file</span></b> and select <b style='mso-bidi-font-weight:normal'><span 2005 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2006 mso-hansi-theme-font:minor-latin'>GC calibrated data.txt</span></b> from the 2007 file selection dialog. You will need to select <b style='mso-bidi-font-weight: 2008 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2009 minor-latin;mso-hansi-theme-font:minor-latin'>any <span class=GramE>file(</span>*.*)</span></b> 2010 to see it. A <b style='mso-bidi-font-weight:normal'><span style='font-family: 2011 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 2012 minor-latin'>Is this the file you want</span></b> dialog will appear respond <b 2013 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2014 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Yes</span></b> 2015 to read the file; it will be plotted.</p> 2009 2016 2010 2017 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 2088 2095 mso-hansi-theme-font:minor-latin'>GC calibrated data</span></b> and the <b 2089 2096 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2090 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Histogram 2091 scalefactor</span></b> will be changed to the new scaling factor (<b2097 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Histogram scale 2098 factor</span></b> will be changed to the new scaling factor (<b 2092 2099 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2093 2100 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.0008536</span></b>). … … 2164 2171 2165 2172 <p class=MsoNormal>Ive changed the zoom to show all the data. We are not quite 2166 done; the scales for the Sa1-Sa4 data sets have to be further reduced by a 2167 factor of 8 to account for the longer exposure time. Select <b 2168 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2169 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD 2170 Sa1_40s_067.tif</span></b> from the GSAS-II data tree, expand it and choose <b 2171 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2172 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sample 2173 Parameters</span></b></p> 2173 done; the scales for the Sa1-Sa4 data sets have to be further reduced by a factor 2174 of 8 to account for the longer exposure time. Select <b style='mso-bidi-font-weight: 2175 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2176 minor-latin;mso-hansi-theme-font:minor-latin'>SASD Sa1_40s_067.tif</span></b> 2177 from the GSAS-II data tree, expand it and choose <b style='mso-bidi-font-weight: 2178 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2179 minor-latin;mso-hansi-theme-font:minor-latin'>Sample Parameters</span></b></p> 2174 2180 2175 2181 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 2208 2214 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2209 2215 mso-hansi-theme-font:minor-latin'>Command/Copy selected</span></b> as before to 2210 copy this new scale factor to the other <span class=GramE>Sa</span> data sets.2211 The plot will again beredrawn</p>2216 copy this new scale factor to the other Sa data sets. The plot will again be 2217 redrawn</p> 2212 2218 2213 2219 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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