Changeset 2385 for Tutorials/2DTexture
- Timestamp:
- Jul 28, 2016 2:16:36 PM (7 years ago)
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- 1 edited
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Tutorials/2DTexture/Texture analysis of 2D data in GSAS-II.htm
r1870 r2385 25 25 <o:Author>Von Dreele</o:Author> 26 26 <o:LastAuthor>Von Dreele</o:LastAuthor> 27 <o:Revision> 9</o:Revision>28 <o:TotalTime>214 2</o:TotalTime>27 <o:Revision>10</o:Revision> 28 <o:TotalTime>2143</o:TotalTime> 29 29 <o:Created>2015-05-14T17:06:00Z</o:Created> 30 <o:LastSaved>201 5-05-14T17:39:00Z</o:LastSaved>31 <o:Pages> 1</o:Pages>32 <o:Words>43 40</o:Words>33 <o:Characters>247 41</o:Characters>30 <o:LastSaved>2016-07-28T18:35:00Z</o:LastSaved> 31 <o:Pages>54</o:Pages> 32 <o:Words>4339</o:Words> 33 <o:Characters>24736</o:Characters> 34 34 <o:Company>Argonne National Laboratory</o:Company> 35 35 <o:Lines>206</o:Lines> 36 36 <o:Paragraphs>58</o:Paragraphs> 37 <o:CharactersWithSpaces>290 23</o:CharactersWithSpaces>38 <o:Version>1 5.00</o:Version>37 <o:CharactersWithSpaces>29017</o:CharactersWithSpaces> 38 <o:Version>16.00</o:Version> 39 39 </o:DocumentProperties> 40 40 <o:OfficeDocumentSettings> … … 48 48 <!--[if gte mso 9]><xml> 49 49 <w:WordDocument> 50 <w: Zoom>108</w:Zoom>50 <w:View>Print</w:View> 51 51 <w:SpellingState>Clean</w:SpellingState> 52 52 <w:GrammarState>Clean</w:GrammarState> … … 1181 1181 mso-hansi-font-family:"Courier New"; 1182 1182 mso-bidi-font-family:"Courier New";} 1183 p.msonormal0, li.msonormal0, div.msonormal0 1184 {mso-style-name:msonormal; 1185 mso-style-noshow:yes; 1186 mso-style-priority:99; 1187 mso-style-unhide:no; 1188 mso-margin-top-alt:auto; 1189 margin-right:0in; 1190 mso-margin-bottom-alt:auto; 1191 margin-left:0in; 1192 mso-pagination:widow-orphan; 1193 font-size:12.0pt; 1194 font-family:"Times New Roman",serif; 1195 mso-fareast-font-family:"Times New Roman"; 1196 mso-fareast-theme-font:minor-fareast;} 1183 1197 span.TitleChar 1184 1198 {mso-style-name:"Title Char"; … … 1513 1527 1514 1528 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 1515 margin-left:0in;line-height:115%'> <span class=GramE>is</span> used to give the1516 intensity corrections dueto texture. The two harmonic terms, <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span1529 margin-left:0in;line-height:115%'>is used to give the intensity corrections due 1530 to texture. The two harmonic terms, <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 1517 1531 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 1518 1532 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 1535 1549 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image004.png" 1536 1550 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 1537 style='mso-spacerun:yes'> </span> <span class=GramE>and </span><!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span1551 style='mso-spacerun:yes'> </span>and <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 1538 1552 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 1539 1553 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 1579 1593 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 1580 1594 style='mso-spacerun:yes'> </span>terms are nonzero so the rest are excluded 1581 from the <span class=GramE>summations</span>and the set of <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span1595 from the summations and the set of <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 1582 1596 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 1583 1597 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 1710 1724 "Times New Roman";mso-fareast-theme-font:minor-fareast;mso-ansi-language:EN-US; 1711 1725 mso-fareast-language:EN-US;mso-bidi-language:AR-SA'><!--[if gte vml 1]><v:shape 1712 id="_x0000_i1025" type="#_x0000_t75" style='width:32 1pt;height:54pt'>1726 id="_x0000_i1025" type="#_x0000_t75" style='width:320.95pt;height:54pt'> 1713 1727 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image013.png" 1714 1728 o:title="" chromakey="white"/> … … 1762 1776 margin-left:0in;line-height:115%'><b style='mso-bidi-font-weight:normal'>M = -</b><b 1763 1777 style='mso-bidi-font-weight:normal'><span style='font-family:Symbol'>Q</span>A</b><b 1764 style='mso-bidi-font-weight:normal'><span style='font-family:Symbol'>W <span1765 class=GramE>C<span style='font-family:"Times New Roman",serif'>(</span></span>F</span>+</b><b1778 style='mso-bidi-font-weight:normal'><span style='font-family:Symbol'>WC</span>(</b><b 1779 style='mso-bidi-font-weight:normal'><span style='font-family:Symbol'>F</span>+</b><b 1766 1780 style='mso-bidi-font-weight:normal'><span style='font-family:Symbol'>F</span><sub>s</sub>)</b><b 1767 1781 style='mso-bidi-font-weight:normal'><span style='font-family:Symbol'>C</span><span … … 1770 1784 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 1771 1785 margin-left:0in;line-height:115%'>By transformation of unit Cartesian vectors 1772 (100, 010 and 001) with this rotation matrix, the sample orientation 1773 coordinates (<span style='font-family:Symbol'>y</span>, <span style='font-family: 1774 Symbol'>g</span>)are given by</p>1786 (100, 010 and 001) with this rotation matrix, the sample orientation coordinates 1787 (<span style='font-family:Symbol'>y</span>, <span style='font-family:Symbol'>g</span>) 1788 are given by</p> 1775 1789 1776 1790 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 1777 margin-left:0in;line-height:115%'>< span class=GramE><i>cos</i>(</span><span1778 style='font-family:Symbol'>y</span>) = <!--[if gte msEquation 12]><m:oMath><i 1779 style=' mso-bidi-font-style:normal'><span style='font-family:"Cambria Math",serif'><m:r>M</m:r></span></i><m:d><m:dPr><span1791 margin-left:0in;line-height:115%'><i>cos</i>(<span style='font-family:Symbol'>y</span>) 1792 = <!--[if gte msEquation 12]><m:oMath><i style='mso-bidi-font-style:normal'><span 1793 style='font-family:"Cambria Math",serif'><m:r>M</m:r></span></i><m:d><m:dPr><span 1780 1794 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 1781 1795 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 1855 1869 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image020.png" 1856 1870 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 1857 style='mso-spacerun:yes'> </span> <span class=GramE>and </span><!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span1871 style='mso-spacerun:yes'> </span>and <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 1858 1872 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 1859 1873 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 1930 1944 1931 1945 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 1932 margin-left:0in;line-height:115%'> <span class=GramE>where</span> the normalized1933 associated Legendrefunctions, <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span1946 margin-left:0in;line-height:115%'>where the normalized associated Legendre 1947 functions, <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 1934 1948 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 1935 1949 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 2006 2020 2007 2021 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 2008 margin-left:0in;line-height:115%'> <span class=GramE>for</span>m even and</p>2022 margin-left:0in;line-height:115%'>for m even and</p> 2009 2023 2010 2024 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; … … 2060 2074 2061 2075 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 2062 margin-left:0in;line-height:115%'><span class=GramE>for</span> m odd.<span 2063 style='mso-spacerun:yes'> </span>Each sum is only over either the even or odd 2064 values of s, respectively, because of the properties of the Fourier 2065 coefficients<span class=GramE>, </span><!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 2076 margin-left:0in;line-height:115%'>for m odd.<span style='mso-spacerun:yes'> 2077 </span>Each sum is only over either the even or odd values of s, respectively, 2078 because of the properties of the Fourier coefficients, <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 2066 2079 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 2067 2080 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 2202 2215 "Times New Roman";mso-fareast-theme-font:minor-fareast;mso-ansi-language:EN-US; 2203 2216 mso-fareast-language:EN-US;mso-bidi-language:AR-SA'><!--[if gte vml 1]><v:shape 2204 id="_x0000_i1025" type="#_x0000_t75" style='width:423.7 5pt;height:55.5pt'>2217 id="_x0000_i1025" type="#_x0000_t75" style='width:423.7pt;height:55.5pt'> 2205 2218 <v:imagedata src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image033.png" 2206 2219 o:title="" chromakey="white"/> … … 2210 2223 2211 2224 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 2212 margin-left:0in;line-height:115%'> <span class=GramE>is</span> satisfied.<span2213 style='mso-spacerun:yes'></span>Terms of the form <!--[if gte msEquation 12]><m:oMath><m:func><m:funcPr><span2225 margin-left:0in;line-height:115%'>is satisfied.<span style='mso-spacerun:yes'> 2226 </span>Terms of the form <!--[if gte msEquation 12]><m:oMath><m:func><m:funcPr><span 2214 2227 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 2215 2228 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 2302 2315 src="Texture%20analysis%20of%202D%20data%20in%20GSAS-II_files/image040.png" 2303 2316 v:shapes="_x0000_i1025"><![endif]></span><![endif]><span 2304 style='mso-spacerun:yes'> </span> <span class=GramE>and </span><!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span2317 style='mso-spacerun:yes'> </span>and <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 2305 2318 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 2306 2319 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 2403 2416 2404 2417 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 2405 margin-left:0in;line-height:115%'><span class=GramE>using</span> the 2406 coefficients, <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 2418 margin-left:0in;line-height:115%'>using the coefficients, <!--[if gte msEquation 12]><m:oMath><m:sSubSup><m:sSubSupPr><span 2407 2419 style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math"; 2408 2420 mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style: … … 2466 2478 style='mso-spacerun:yes'> </span>and the sample orientation angles <span 2467 2479 style='font-family:Symbol'>W</span><sub>s</sub>, <span style='font-family:Symbol'>C</span><sub>s</sub>, 2468 <span class=GramE><span style='font-family:Symbol'>F</span></span><sub>s</sub>. 2469 </p> 2480 <span style='font-family:Symbol'>F</span><sub>s</sub>. </p> 2470 2481 2471 2482 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; … … 2525 2536 2526 2537 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 2527 margin-left:0in;line-height:115%'>If the texture is random then J = 1, 2528 otherwise J > 1; for a single crystal J = <span style='font-family:Symbol'>¥.</span> 2529 </p> 2538 margin-left:0in;line-height:115%'>If the texture is random then J = 1, otherwise 2539 J > 1; for a single crystal J = <span style='font-family:Symbol'>¥.</span> </p> 2530 2540 2531 2541 <p class=gsastext style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; … … 2582 2592 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Use the <b 2583 2593 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2584 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Data/Read 2585 imagedata</span></b> menu item to read the data file into the current GSAS-II2594 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Data/Read image 2595 data</span></b> menu item to read the data file into the current GSAS-II 2586 2596 project. A file selection dialog will be shown; its appearance will depend on 2587 2597 your OS. Change the search directory to <b style='mso-bidi-font-weight:normal'><span 2588 2598 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2589 2599 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 2590 minor-latin'> /exercises/2DTexture</span></b>and then select the file <b2600 minor-latin'>2DTexture/data </span></b>and then select the file <b 2591 2601 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2592 2602 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>NDC5_01588_1.ge2</span></b>. … … 2603 2613 v:shapes="Picture_x0020_29"><![endif]></span></p> 2604 2614 2605 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span2606 class=GramE>and</span> the <b style='mso-bidi-font-weight:normal'><span 2607 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2608 mso-hansi-theme-font:minor-latin'>ImageControls</span></b> data page will show</p>2615 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and the <b 2616 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2617 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 2618 Controls</span></b> data page will show</p> 2609 2619 2610 2620 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 2656 2666 is suitable) and shows that the diffraction rings show the effect of texture 2657 2667 and that the image has a fairly high background. Placing the cursor in the 2658 corners or inside the inner ring shows a background >1700. This can be suppressed2659 by adjusting the <b style='mso-bidi-font-weight:normal'><span style='font-family: 2660 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 2661 m inor-latin'>Flat <span class=SpellE>Bkg</span></span></b> (I chose <b2662 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;2668 corners or inside the inner ring shows a background >1700. This can be 2669 suppressed by adjusting the <b style='mso-bidi-font-weight:normal'><span 2670 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2671 mso-hansi-theme-font:minor-latin'>Flat <span class=SpellE>Bkg</span></span></b> 2672 (I chose <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2663 2673 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1700</span></b> 2664 2674 for this). The image will now show the rings much more clearly.</p> … … 2675 2685 2676 2686 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>For texture 2677 analysis we will need to integrate the image into a number of slices sampling 2678 the changing ring intensity with azimuthal angle. Also note that the image 2679 seems to have <b style='mso-bidi-font-weight:normal'><span style='font-family: 2687 analysis we will need to integrate the image into a number of slices sampling the 2688 changing ring intensity with azimuthal angle. Also note that the image seems to 2689 have <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2690 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>mm</span></b> 2691 symmetry so that the unique part of this intensity variation covers 0-90° of 2692 azimuth. In addition the ring intensity variation is such that using 10° slices 2693 will capture it reasonably well. However, we want to include both 0° and 90° as 2694 slice centers. Thus there will be 10 slices beginning at -5° and ending at 95°. 2695 Check the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2696 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Show 2697 integration limits?</span></b> box and uncheck the <b style='mso-bidi-font-weight: 2698 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2699 minor-latin;mso-hansi-theme-font:minor-latin'>Do full integration? </span></b>box, 2700 enter <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2701 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>10</span></b> 2702 in the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2703 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>No. azimuth 2704 bins</span></b>, enter <b style='mso-bidi-font-weight:normal'><span 2705 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2706 mso-hansi-theme-font:minor-latin'>-5</span></b> in the <b style='mso-bidi-font-weight: 2707 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2708 minor-latin;mso-hansi-theme-font:minor-latin'>Start azimuth</span></b> box (it 2709 will change to 355) and enter <b style='mso-bidi-font-weight:normal'><span 2710 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2711 mso-hansi-theme-font:minor-latin'>455</span></b> in the <b style='mso-bidi-font-weight: 2712 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2713 minor-latin;mso-hansi-theme-font:minor-latin'>End azimuth</span></b> box. In 2714 addition, recall that the sample was mounted vertically and thus is aligned 2715 with the defined laboratory I axis. Thus, the sample coordinate system needs to 2716 be rotated by 90° to match the sample axis with the K axis; this can be done by 2717 making the <b style='mso-bidi-font-weight:normal'><span style='font-family: 2680 2718 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 2681 minor-latin'>mm</span></b> symmetry so that the unique part of this intensity 2682 variation covers 0-90° of azimuth. In addition the ring intensity variation is 2683 such that using 10° slices will capture it reasonably well. However, we want to 2684 include both 0° and 90° as slice centers. Thus there will be 10 slices 2685 beginning at -5° and ending at 95°. Check the <b style='mso-bidi-font-weight: 2719 minor-latin'>Sample goniometer axis Chi</span></b> = <b style='mso-bidi-font-weight: 2686 2720 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2687 minor-latin;mso-hansi-theme-font:minor-latin'>Show integration limits?</span></b> 2688 <span class=GramE>box</span> and uncheck the <b style='mso-bidi-font-weight: 2689 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2690 minor-latin;mso-hansi-theme-font:minor-latin'>Do full integration? </span></b><span 2691 class=GramE>box</span>, enter <b style='mso-bidi-font-weight:normal'><span 2692 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2693 mso-hansi-theme-font:minor-latin'>10</span></b> in the <b style='mso-bidi-font-weight: 2694 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2695 minor-latin;mso-hansi-theme-font:minor-latin'>No. azimuth bins</span></b>, 2696 enter <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2697 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-5</span></b> 2698 in the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2699 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Start 2700 azimuth</span></b> box (it will change to 355) and enter <b style='mso-bidi-font-weight: 2701 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 2702 minor-latin;mso-hansi-theme-font:minor-latin'>455</span></b> in the <b 2703 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2704 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>End azimuth</span></b> 2705 box. In addition, recall that the sample was mounted vertically and thus is 2706 aligned with the defined laboratory I axis. Thus, the sample coordinate system 2707 needs to be rotated by 90° to match the sample axis with the K axis; this can 2708 be done by making the <b style='mso-bidi-font-weight:normal'><span 2709 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2710 mso-hansi-theme-font:minor-latin'>Sample goniometer axis Chi</span></b> = <b 2711 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2712 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>90</span></b>. 2713 The plot will change with each entry and at the end should look like</p> 2721 minor-latin;mso-hansi-theme-font:minor-latin'>90</span></b>. The plot will 2722 change with each entry and at the end should look like</p> 2714 2723 2715 2724 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 2775 2784 v:shapes="Picture_x0020_36"><![endif]></span></p> 2776 2785 2777 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span2778 class=GramE>for</span> one ring. This level is too low. Return to the <b 2779 style=' mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;2780 mso- ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image2781 Controls</span></b> item in the datatree.</p>2786 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>for one ring. 2787 This level is too low. Return to the <b style='mso-bidi-font-weight:normal'><span 2788 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2789 mso-hansi-theme-font:minor-latin'>Image Controls</span></b> item in the data 2790 tree.</p> 2782 2791 2783 2792 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>We are now … … 2805 2814 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>This <span 2806 2815 class=SpellE>NiTi</span> alloy consists of two phases, cubic B2 and monoclinic 2807 B19. Their parameters are <span class=GramE>:</span><br>2816 B19. Their parameters are:<br> 2808 2817 B2: <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2809 2818 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>P m 3 m</span></b>, … … 2831 2840 <span class=SpellE>Ti</span> <b style='mso-bidi-font-weight:normal'><span 2832 2841 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 2833 mso-hansi-theme-font:minor-latin'>0.5787 <span class=GramE>,0.2841,Œ</span></span></b>,2834 Ni <bstyle='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;2842 mso-hansi-theme-font:minor-latin'>0.5787,0.2841,Œ</span></b>, Ni <b 2843 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 2835 2844 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.9700,0.8209,Œ</span></b>, 2836 2845 <span class=SpellE>U<sub>iso</sub></span>=<b style='mso-bidi-font-weight:normal'><span … … 2876 2885 v:shapes="Picture_x0020_38"><![endif]></span></p> 2877 2886 2878 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span2879 class=GramE>and</span> the B19Atoms table should be</p>2887 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and the B19 2888 Atoms table should be</p> 2880 2889 2881 2890 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 2912 2921 v:shapes="Picture_x0020_40"><![endif]></span></p> 2913 2922 2914 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span2915 class=GramE>and</span> that forB19 will be</p>2923 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and that for 2924 B19 will be</p> 2916 2925 2917 2926 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3010 3019 mso-hansi-theme-font:minor-latin'>Edit/Copy data</span></b>, select <b 3011 3020 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3012 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Set <span 3013 class=GramE>All</span></span></b> & press <b style='mso-bidi-font-weight: 3014 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3015 minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b> to copy these to 3016 the other histograms. Next select the <b style='mso-bidi-font-weight:normal'><span 3017 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3018 mso-hansi-theme-font:minor-latin'>B19</span></b> phase and repeat this process. 3019 We are now ready for the first refinement; do <b style='mso-bidi-font-weight: 3020 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3021 minor-latin;mso-hansi-theme-font:minor-latin'>Calculate/Refine</span></b> from 3022 the main GSAS-II data tree window. A progress bar popup will appear and when 3023 done a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3024 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Refinement 3025 results</span></b> popup will show with Rw~32%. Press <b style='mso-bidi-font-weight: 3026 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3027 minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b> to load this 3028 result; GSAS-II will return you to the last window you were using and display 3029 the 1<sup>st</sup> powder pattern showing you the fit</p> 3021 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Set All</span></b> 3022 & press <b style='mso-bidi-font-weight:normal'><span style='font-family: 3023 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3024 minor-latin'>OK</span></b> to copy these to the other histograms. Next select 3025 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3026 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>B19</span></b> 3027 phase and repeat this process. We are now ready for the first refinement; do <b 3028 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3029 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Calculate/Refine</span></b> 3030 from the main GSAS-II data tree window. A progress bar popup will appear and 3031 when done a <b style='mso-bidi-font-weight:normal'><span style='font-family: 3032 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3033 minor-latin'>Refinement results</span></b> popup will show with Rw~32%. Press <b 3034 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3035 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b> 3036 to load this result; GSAS-II will return you to the last window you were using 3037 and display the 1<sup>st</sup> powder pattern showing you the fit</p> 3030 3038 3031 3039 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3247 3255 3248 3256 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Next go to the 3249 Texture tab for the B19 phase. Again a <span class=SpellE>bullseye</span> pole3250 figure is drawn; changethat to an Inverse pole figure.</p>3257 Texture tab for the B19 phase. Again a bullseye pole figure is drawn; change 3258 that to an Inverse pole figure.</p> 3251 3259 3252 3260 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3287 3295 v:shapes="Picture_x0020_54"><![endif]></span></p> 3288 3296 3289 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span3290 class=GramE>and</span> inversepole figure</p>3297 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and inverse 3298 pole figure</p> 3291 3299 3292 3300 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3313 3321 v:shapes="Picture_x0020_56"><![endif]></span></p> 3314 3322 3315 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span3316 class=GramE>and</span> inversepole figure</p>3323 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and inverse 3324 pole figure</p> 3317 3325 3318 3326 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3328 3336 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>This completes 3329 3337 the tutorial on Method A for doing texture analysis. It is useful for a case 3330 like this one where there are very few data sets required for the texture 3331 analysis. However, for the case of lower sample symmetry one must several dozen 3332 or even a few hundred histograms and then the suite of parameters can easily be 3333 > 1000 of which only a few dozen describe the texture. This leads to the 3334 next Methodsfor texture analysis in GSAS-II.</p>3338 like this one where there are very few data sets required for the texture analysis. 3339 However, for the case of lower sample symmetry one must several dozen or even a 3340 few hundred histograms and then the suite of parameters can easily be > 1000 3341 of which only a few dozen describe the texture. This leads to the next Methods 3342 for texture analysis in GSAS-II.</p> 3335 3343 3336 3344 <h2 style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt;margin-left: … … 3342 3350 3343 3351 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>This begins 3344 the texture analysis in much the same way as Method A except that all the 3345 initial refinements are done sequentially, that is refinements are done for 3346 theparameters associated with each powder pattern to convergence in a serial3352 the texture analysis in much the same way as Method A except that all the initial 3353 refinements are done sequentially, that is refinements are done for the 3354 parameters associated with each powder pattern to convergence in a serial 3347 3355 fashion. In this case where there are 10 PWDR data sets, there will be 10 3348 3356 refinements done in sequence. Parameters that span all the data (e.g. lattice … … 3396 3404 tab and check the <b style='mso-bidi-font-weight:normal'><span 3397 3405 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3398 mso-hansi-theme-font:minor-latin'>Phase fraction</span></b> box and change the <span 3399 class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family: 3400 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3401 minor-latin'>Preferred</span></b></span><b style='mso-bidi-font-weight:normal'><span 3402 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3403 mso-hansi-theme-font:minor-latin'> orientation model</span></b> to <b 3404 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3405 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Spherical 3406 harmonics</span></b>. Then do <b style='mso-bidi-font-weight:normal'><span 3407 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3408 mso-hansi-theme-font:minor-latin'>Edit/Copy data</span></b> to copy both the 3409 flag and the model to the other PWDR entries.</p> 3406 mso-hansi-theme-font:minor-latin'>Phase fraction</span></b> box and change the <b 3407 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3408 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Preferred 3409 orientation model</span></b> to <b style='mso-bidi-font-weight:normal'><span 3410 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3411 mso-hansi-theme-font:minor-latin'>Spherical harmonics</span></b>. Then do <b 3412 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3413 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Copy 3414 data</span></b> to copy both the flag and the model to the other PWDR entries.</p> 3410 3415 3411 3416 <p class=MsoListParagraphCxSpLast style='margin-bottom:12.0pt;mso-add-space: … … 3419 3424 tab and check the <b style='mso-bidi-font-weight:normal'><span 3420 3425 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3421 mso-hansi-theme-font:minor-latin'>Phase fraction box</span></b> and change the <span 3422 class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family: 3423 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3424 minor-latin'>Preferred</span></b></span><b style='mso-bidi-font-weight:normal'><span 3425 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3426 mso-hansi-theme-font:minor-latin'> orientation model</span></b> to <b 3427 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3428 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Spherical 3429 harmonics</span></b>. Then do <b style='mso-bidi-font-weight:normal'><span 3430 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3431 mso-hansi-theme-font:minor-latin'>Edit/Copy data</span></b> to copy both the 3432 flag and the model to the other PWDR entries.</p> 3426 mso-hansi-theme-font:minor-latin'>Phase fraction box</span></b> and change the <b 3427 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3428 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Preferred 3429 orientation model</span></b> to <b style='mso-bidi-font-weight:normal'><span 3430 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3431 mso-hansi-theme-font:minor-latin'>Spherical harmonics</span></b>. Then do <b 3432 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3433 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Copy 3434 data</span></b> to copy both the flag and the model to the other PWDR entries.</p> 3433 3435 3434 3436 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Now select <b … … 3510 3512 3511 3513 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>If you examine 3512 one of the PWDR entries, youll see that just in this point in Method <span3513 class=GramE>A</span> much ofthe misfit is texture and perhaps peak position.</p>3514 one of the PWDR entries, youll see that just in this point in Method A much of 3515 the misfit is texture and perhaps peak position.</p> 3514 3516 3515 3517 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3553 3555 3554 3556 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>This allows 3555 you to select which parameters to copy data and flags. Select Pref. <span3556 class=SpellE>Ori</span>. And press OK; the file selection is next. Do Set <span 3557 c lass=GramE>All</span> and OK to do this copy. That copies the full spherical3558 harmonics model to the other data sets. Select one tocheck if youd like.</p>3557 you to select which parameters to copy data and flags. Select Pref. Ori. And 3558 press OK; the file selection is next. Do Set All and OK to do this copy. That 3559 copies the full spherical harmonics model to the other data sets. Select one to 3560 check if youd like.</p> 3559 3561 3560 3562 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Next do the … … 3576 3578 ready for the next refinement; do Calculate/Sequential refine. Be careful not 3577 3579 (by habit say) pick Refine; a warning popup will appear. After it completes the 3578 Sequential refinement results shows that the fit is better but convergence 3579 wasntquite complete.</p>3580 Sequential refinement results shows that the fit is better but convergence wasnt 3581 quite complete.</p> 3580 3582 3581 3583 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3651 3653 perhaps the B19 phase needs high order spherical harmonics. Select the Data 3652 3654 tab for the B19 phase and change the Harmonic order to 6. Then do Edit/Copy 3653 selected data for <span class=SpellE>Pref.Ori</span>. <span class=GramE>to</span> 3654 the other data sets. This (after few repeats) gives a further improvement in 3655 the fit</p> 3655 selected data for <span class=SpellE>Pref.Ori</span>. to the other data sets. 3656 This (after few repeats) gives a further improvement in the fit</p> 3656 3657 3657 3658 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3672 3673 0in;line-height:115%'>Step 2. Texture analysis</h3> 3673 3674 3674 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>During the 3675 sequential refinements done in Step 1, we fitted the profiles allowing strain 3676 parameters (<span class=SpellE>Dij</span>) for peak position shifts and <span 3677 class=SpellE>microstrain</span> for peak shape. We modeled the intensity 3678 variation with a spherical harmonics preferred orientation correction. If you 3679 select any PWDR entry from the GSAS-II data tree and pick the Reflection List 3680 subentry (at the bottom) you can see the magnitude of this correction for each 3681 reflection in each phase.</p> 3675 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>During the sequential 3676 refinements done in Step 1, we fitted the profiles allowing strain parameters (<span 3677 class=SpellE>Dij</span>) for peak position shifts and <span class=SpellE>microstrain</span> 3678 for peak shape. We modeled the intensity variation with a spherical harmonics 3679 preferred orientation correction. If you select any PWDR entry from the GSAS-II 3680 data tree and pick the Reflection List subentry (at the bottom) you can see the 3681 magnitude of this correction for each reflection in each phase.</p> 3682 3682 3683 3683 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>For the B2 … … 3694 3694 v:shapes="Picture_x0020_14"><![endif]></span></p> 3695 3695 3696 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span3697 class=GramE>and</span> for theB19 phase we see</p>3696 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and for the 3697 B19 phase we see</p> 3698 3698 3699 3699 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3741 3741 3742 3742 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Do 3743 Texture/Refine texture from the menu; the window will be repainted and a <span3744 class=SpellE>bullseye</span>pole figure will appear. </p>3743 Texture/Refine texture from the menu; the window will be repainted and a 3744 bullseye pole figure will appear. </p> 3745 3745 3746 3746 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3768 3768 3769 3769 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>This is 3770 essentially the same as we obtained earlier in Method <span class=GramE>A</span>3771 (maybe not quite asstrong here).</p>3770 essentially the same as we obtained earlier in Method A (maybe not quite as 3771 strong here).</p> 3772 3772 3773 3773 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Now select the … … 3786 3786 v:shapes="Picture_x0020_21"><![endif]></span></p> 3787 3787 3788 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>And a <span 3789 class=SpellE>bullseye</span> pole figure; change that to Inverse pole figure to 3790 see the texture</p> 3788 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>And a bullseye 3789 pole figure; change that to Inverse pole figure to see the texture</p> 3791 3790 3792 3791 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 3800 3799 v:shapes="Picture_x0020_22"><![endif]></span></p> 3801 3800 3802 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Again this is 3803 very similar to what we found in Method A but again not quite as strong (max 3804 MRD ~13instead of ~18).</p>3801 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Again this is very 3802 similar to what we found in Method A but again not quite as strong (max MRD ~13 3803 instead of ~18).</p> 3805 3804 3806 3805 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Now do a … … 3843 3842 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>Here we want 3844 3843 to clear refinement flags for all parameters that need not be varied in a 3845 texture analysis refinement. The general rule is to not refine any parameter 3846 unlesswe expect it to affect the peak intensities. These are listed below:</p>3844 texture analysis refinement. The general rule is to not refine any parameter unless 3845 we expect it to affect the peak intensities. These are listed below:</p> 3847 3846 3848 3847 <p class=MsoListParagraphCxSpFirst style='margin-bottom:12.0pt;mso-add-space: … … 3878 3877 phase and its <b style='mso-bidi-font-weight:normal'><span style='font-family: 3879 3878 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3880 minor-latin'>Data</span></b> tab. <span class=GramE>Clear</span>the <span3879 minor-latin'>Data</span></b> <span class=GramE>tab.</span> Clear the <span 3881 3880 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 3882 3881 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: … … 3894 3893 flags</span></b> selecting all data to clear all the flags and an <b 3895 3894 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3895 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Copy selected 3896 data</span></b> for <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 3897 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3898 mso-hansi-theme-font:minor-latin'>Pref.Ori</span></b></span> to copy the zeroed 3899 out harmonic coefficients.</p> 3900 3901 <p class=MsoListParagraphCxSpLast style='margin-bottom:12.0pt;mso-add-space: 3902 auto;text-indent:-.25in;line-height:115%;mso-list:l1 level1 lfo4'><![if !supportLists]><span 3903 style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>3)<span 3904 style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]><b 3905 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3906 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>B19</span></b>: 3907 we do not want to refine either the <span class=SpellE>microstrain</span>, <span 3908 class=SpellE>Dij</span>, or preferred orientation coefficients. Select the <b 3909 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3910 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>B19</span></b> 3911 phase and its <b style='mso-bidi-font-weight:normal'><span style='font-family: 3912 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3913 minor-latin'>Data</span></b> tab. Clear the <span class=SpellE><b 3914 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3915 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>microstrain</span></b></span>, 3916 four <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 3917 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3918 mso-hansi-theme-font:minor-latin'>Dij</span></b></span> and <b 3919 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3920 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Preferred 3921 orientation</span></b> boxes. Also set the <b style='mso-bidi-font-weight:normal'><span 3922 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3923 mso-hansi-theme-font:minor-latin'>Harmonic order</span></b> to zero (this will 3924 avoid a lot of nasty (but harmless) messages at the start of the refinement). 3925 Then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3926 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Copy 3927 flags</span></b> selecting all data to clear all the flags and an <b 3928 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3896 3929 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Copy 3897 3930 selected data</span></b> for <span class=SpellE><b style='mso-bidi-font-weight: … … 3900 3933 copy the zeroed out harmonic coefficients.</p> 3901 3934 3902 <p class=MsoListParagraphCxSpLast style='margin-bottom:12.0pt;mso-add-space:3903 auto;text-indent:-.25in;line-height:115%;mso-list:l1 level1 lfo4'><![if !supportLists]><span3904 style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>3)<span3905 style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]><b3906 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;3907 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>B19</span></b>:3908 we do not want to refine either the <span class=SpellE>microstrain</span>, <span3909 class=SpellE>Dij</span>, or preferred orientation coefficients. Select the <b3910 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;3911 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>B19</span></b>3912 phase and its <b style='mso-bidi-font-weight:normal'><span style='font-family:3913 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:3914 minor-latin'>Data</span></b> tab. Clear the <span class=SpellE><b3915 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;3916 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>microstrain</span></b></span>,3917 four <span class=SpellE><b style='mso-bidi-font-weight:normal'><span3918 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;3919 mso-hansi-theme-font:minor-latin'>Dij</span></b></span> and <b3920 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;3921 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Preferred3922 orientation</span></b> boxes. Also set the <b style='mso-bidi-font-weight:normal'><span3923 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;3924 mso-hansi-theme-font:minor-latin'>Harmonic order</span></b> to zero (this will3925 avoid a lot of nasty (but harmless) messages at the start of the refinement).3926 Then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;3927 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Copy3928 flags</span></b> selecting all data to clear all the flags and an <b3929 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;3930 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Copy3931 selected data</span></b> for <span class=SpellE><b style='mso-bidi-font-weight:3932 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:3933 minor-latin;mso-hansi-theme-font:minor-latin'>Pref.Ori</span></b></span> to3934 copy the zeroed out harmonic coefficients.</p>3935 3936 3935 <p class=MsoNormal style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; 3937 3936 margin-left:.25in;line-height:115%'><o:p> </o:p></p> … … 3940 3939 margin-left:.25in;line-height:115%'>Notice that we have allowed refinement of 3941 3940 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3942 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Phase fractions</span></b>; 3943 these may change during the texture refinement. Now select the <b 3944 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3945 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Texture</span></b> 3946 tab for the <b style='mso-bidi-font-weight:normal'><span style='font-family: 3941 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Phase 3942 fractions</span></b>; these may change during the texture refinement. Now 3943 select the <b style='mso-bidi-font-weight:normal'><span style='font-family: 3947 3944 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 3948 minor-latin'>B2</span></b> phase (it may still have values from the Method B).</p> 3945 minor-latin'>Texture</span></b> tab for the <b style='mso-bidi-font-weight: 3946 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 3947 minor-latin;mso-hansi-theme-font:minor-latin'>B2</span></b> phase (it may still 3948 have values from the Method B).</p> 3949 3949 3950 3950 <p class=MsoNormal style='margin-top:0in;margin-right:0in;margin-bottom:12.0pt; … … 3990 3990 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 3991 3991 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Texture</span></b> 3992 tab. <span class=GramE>Set</span>the <b style='mso-bidi-font-weight:normal'><span3992 <span class=GramE>tab.</span> Set the <b style='mso-bidi-font-weight:normal'><span 3993 3993 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 3994 3994 mso-hansi-theme-font:minor-latin'>Harmonic order</span></b> to zero and then … … 4047 4047 v:shapes="Picture_x0020_26"><![endif]></span></p> 4048 4048 4049 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'> <span4050 class=GramE>which</span> is almost identical to that from Method A.The4049 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>which is 4050 almost identical to that from Method <span class=GramE>A.</span> The 4051 4051 coefficients are seen in</p> 4052 4052 … … 4078 4078 v:shapes="Picture_x0020_28"><![endif]></span></p> 4079 4079 4080 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span 4081 class=GramE>and</span> also almost identical to what was obtained in Method A; 4082 the coefficients are seen in</p> 4080 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'>and also 4081 almost identical to what was obtained in Method A; the coefficients are seen in</p> 4083 4082 4084 4083 <p class=MsoNormal style='margin-bottom:12.0pt;line-height:115%'><span … … 4097 4096 tutorial that in more complex textures where the data set may consist of slices 4098 4097 obtained from a suite of 2D images collected as the sample is rotated, Method C 4099 will give a relatively fast determination of the texture without resorting to large4100 matrix least-squares refinements.</p>4098 will give a relatively fast determination of the texture without resorting to 4099 large matrix least-squares refinements.</p> 4101 4100 4102 4101 </div>
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