Changeset 1740 for Tutorials/SAfit/Fitting Small Angle Scattering Data.htm
- Timestamp:
- Mar 18, 2015 12:50:51 PM (8 years ago)
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Tutorials/SAfit/Fitting Small Angle Scattering Data.htm
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Name="Salutation"/> 240 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 241 Name="Date"/> 242 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 243 Name="Body Text First Indent"/> 244 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 245 Name="Body Text First Indent 2"/> 246 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 247 Name="Note Heading"/> 248 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 249 Name="Body Text 2"/> 250 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 251 Name="Body Text 3"/> 252 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 253 Name="Body Text Indent 2"/> 254 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 255 Name="Body Text Indent 3"/> 256 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 257 Name="Block Text"/> 258 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 259 Name="Hyperlink"/> 260 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 261 Name="FollowedHyperlink"/> 262 <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/> 263 <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/> 264 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 265 Name="Document Map"/> 266 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 267 Name="Plain Text"/> 268 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 269 Name="E-mail Signature"/> 270 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 271 Name="HTML Top of Form"/> 272 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 273 Name="HTML Bottom of Form"/> 274 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 275 Name="Normal (Web)"/> 276 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 277 Name="HTML Acronym"/> 278 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 279 Name="HTML Address"/> 280 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 281 Name="HTML Cite"/> 282 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 283 Name="HTML Code"/> 284 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 285 Name="HTML Definition"/> 286 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 287 Name="HTML Keyboard"/> 288 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 289 Name="HTML Preformatted"/> 290 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 291 Name="HTML Sample"/> 292 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 293 Name="HTML Typewriter"/> 294 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 295 Name="HTML Variable"/> 296 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 297 Name="Normal Table"/> 298 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 299 Name="annotation subject"/> 300 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 301 Name="No List"/> 302 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 303 Name="Outline List 1"/> 304 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 305 Name="Outline List 2"/> 306 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 307 Name="Outline List 3"/> 308 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 309 Name="Table Simple 1"/> 310 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 311 Name="Table Simple 2"/> 312 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 313 Name="Table Simple 3"/> 314 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 315 Name="Table Classic 1"/> 316 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 317 Name="Table Classic 2"/> 318 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 319 Name="Table Classic 3"/> 320 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 321 Name="Table Classic 4"/> 322 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 323 Name="Table Colorful 1"/> 324 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 325 Name="Table Colorful 2"/> 326 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 327 Name="Table Colorful 3"/> 328 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 329 Name="Table Columns 1"/> 330 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 331 Name="Table Columns 2"/> 332 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 333 Name="Table Columns 3"/> 334 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 335 Name="Table Columns 4"/> 336 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 337 Name="Table Columns 5"/> 338 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 339 Name="Table Grid 1"/> 340 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 341 Name="Table Grid 2"/> 342 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 343 Name="Table Grid 3"/> 344 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 345 Name="Table Grid 4"/> 346 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 347 Name="Table Grid 5"/> 348 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 349 Name="Table Grid 6"/> 350 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 351 Name="Table Grid 7"/> 352 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 353 Name="Table Grid 8"/> 354 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 355 Name="Table List 1"/> 356 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 357 Name="Table List 2"/> 358 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 359 Name="Table List 3"/> 360 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 361 Name="Table List 4"/> 362 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 363 Name="Table List 5"/> 364 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 365 Name="Table List 6"/> 366 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 367 Name="Table List 7"/> 368 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 369 Name="Table List 8"/> 370 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 371 Name="Table 3D effects 1"/> 372 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 373 Name="Table 3D effects 2"/> 374 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 375 Name="Table 3D effects 3"/> 376 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 377 Name="Table Contemporary"/> 378 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 379 Name="Table Elegant"/> 380 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 381 Name="Table Professional"/> 382 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 383 Name="Table Subtle 1"/> 384 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 385 Name="Table Subtle 2"/> 386 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 387 Name="Table Web 1"/> 388 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 389 Name="Table Web 2"/> 390 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 391 Name="Table Web 3"/> 392 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 393 Name="Balloon Text"/> 394 <w:LsdException Locked="false" Priority="59" Name="Table Grid"/> 395 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 396 Name="Table Theme"/> 397 <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/> 398 <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/> 399 <w:LsdException Locked="false" Priority="60" Name="Light Shading"/> 400 <w:LsdException Locked="false" Priority="61" Name="Light List"/> 401 <w:LsdException Locked="false" Priority="62" Name="Light Grid"/> 402 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/> 403 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/> 404 <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/> 405 <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/> 406 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/> 407 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/> 408 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/> 409 <w:LsdException Locked="false" Priority="70" Name="Dark List"/> 410 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/> 411 <w:LsdException Locked="false" Priority="72" Name="Colorful List"/> 412 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/> 413 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/> 414 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/> 415 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/> 416 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/> 417 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/> 418 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/> 419 <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/> 420 <w:LsdException Locked="false" Priority="34" QFormat="true" 421 Name="List Paragraph"/> 422 <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/> 423 <w:LsdException Locked="false" Priority="30" QFormat="true" 424 Name="Intense Quote"/> 425 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/> 426 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/> 427 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/> 428 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/> 429 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/> 430 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/> 431 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/> 432 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/> 433 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/> 434 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/> 435 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/> 436 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/> 437 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/> 438 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/> 439 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/> 440 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/> 441 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/> 442 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/> 443 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/> 444 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/> 445 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/> 446 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/> 447 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/> 448 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/> 449 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/> 450 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/> 451 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/> 452 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/> 453 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/> 454 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/> 455 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/> 456 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/> 457 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/> 458 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/> 459 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/> 460 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/> 461 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/> 462 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/> 463 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/> 464 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/> 465 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/> 466 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/> 467 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/> 468 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/> 469 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/> 470 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/> 471 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/> 472 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/> 473 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/> 474 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/> 475 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/> 476 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/> 477 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/> 478 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/> 479 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/> 480 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/> 481 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/> 482 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/> 483 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/> 484 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/> 485 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/> 486 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/> 487 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/> 488 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/> 489 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/> 490 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/> 491 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/> 492 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/> 493 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/> 494 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/> 495 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/> 496 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/> 497 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/> 498 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/> 499 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/> 500 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/> 501 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/> 502 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/> 503 <w:LsdException Locked="false" Priority="19" QFormat="true" 504 Name="Subtle Emphasis"/> 505 <w:LsdException Locked="false" Priority="21" QFormat="true" 506 Name="Intense Emphasis"/> 507 <w:LsdException Locked="false" Priority="31" QFormat="true" 508 Name="Subtle Reference"/> 509 <w:LsdException Locked="false" Priority="32" QFormat="true" 510 Name="Intense Reference"/> 511 <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/> 512 <w:LsdException Locked="false" Priority="37" SemiHidden="true" 513 UnhideWhenUsed="true" Name="Bibliography"/> 514 <w:LsdException Locked="false" Priority="39" SemiHidden="true" 515 UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/> 516 <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/> 517 <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/> 518 <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/> 519 <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/> 520 <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/> 521 <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/> 522 <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/> 523 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/> 524 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/> 525 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/> 526 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/> 527 <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/> 528 <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/> 529 <w:LsdException Locked="false" Priority="46" 530 Name="Grid Table 1 Light Accent 1"/> 531 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/> 532 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/> 533 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/> 534 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/> 535 <w:LsdException Locked="false" Priority="51" 536 Name="Grid Table 6 Colorful Accent 1"/> 537 <w:LsdException Locked="false" Priority="52" 538 Name="Grid Table 7 Colorful Accent 1"/> 539 <w:LsdException Locked="false" Priority="46" 540 Name="Grid Table 1 Light Accent 2"/> 541 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/> 542 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/> 543 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/> 544 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/> 545 <w:LsdException Locked="false" Priority="51" 546 Name="Grid Table 6 Colorful Accent 2"/> 547 <w:LsdException Locked="false" Priority="52" 548 Name="Grid Table 7 Colorful Accent 2"/> 549 <w:LsdException Locked="false" Priority="46" 550 Name="Grid Table 1 Light Accent 3"/> 551 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/> 552 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/> 553 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/> 554 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/> 555 <w:LsdException Locked="false" Priority="51" 556 Name="Grid Table 6 Colorful Accent 3"/> 557 <w:LsdException Locked="false" Priority="52" 558 Name="Grid Table 7 Colorful Accent 3"/> 559 <w:LsdException Locked="false" Priority="46" 560 Name="Grid Table 1 Light Accent 4"/> 561 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/> 562 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/> 563 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/> 564 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/> 565 <w:LsdException Locked="false" Priority="51" 566 Name="Grid Table 6 Colorful Accent 4"/> 567 <w:LsdException Locked="false" Priority="52" 568 Name="Grid Table 7 Colorful Accent 4"/> 569 <w:LsdException Locked="false" Priority="46" 570 Name="Grid Table 1 Light Accent 5"/> 571 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/> 572 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/> 573 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/> 574 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/> 575 <w:LsdException Locked="false" Priority="51" 576 Name="Grid Table 6 Colorful Accent 5"/> 577 <w:LsdException Locked="false" Priority="52" 578 Name="Grid Table 7 Colorful Accent 5"/> 579 <w:LsdException Locked="false" Priority="46" 580 Name="Grid Table 1 Light Accent 6"/> 581 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/> 582 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/> 583 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/> 584 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/> 585 <w:LsdException Locked="false" Priority="51" 586 Name="Grid Table 6 Colorful Accent 6"/> 587 <w:LsdException Locked="false" Priority="52" 588 Name="Grid Table 7 Colorful Accent 6"/> 589 <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/> 590 <w:LsdException Locked="false" Priority="47" Name="List Table 2"/> 591 <w:LsdException Locked="false" Priority="48" 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1022 mso-fareast-font-family:"Times New Roman"; … … 727 1047 mso-ansi-font-size:8.0pt; 728 1048 mso-bidi-font-size:8.0pt; 729 font-family:"Tahoma", "sans-serif";1049 font-family:"Tahoma",sans-serif; 730 1050 mso-ascii-font-family:Tahoma; 731 1051 mso-fareast-font-family:"Times New Roman"; … … 742 1062 mso-ansi-font-size:8.0pt; 743 1063 mso-bidi-font-size:8.0pt; 744 font-family:"Tahoma", "sans-serif";1064 font-family:"Tahoma",sans-serif; 745 1065 mso-ascii-font-family:Tahoma; 746 1066 mso-fareast-font-family:"Times New Roman"; … … 760 1080 mso-ansi-font-size:10.0pt; 761 1081 mso-bidi-font-size:10.0pt; 762 font-family:"Calibri", "sans-serif";1082 font-family:"Calibri",sans-serif; 763 1083 mso-ascii-font-family:Calibri; 764 1084 mso-ascii-theme-font:minor-latin; … … 845 1165 mso-pagination:widow-orphan; 846 1166 font-size:10.0pt; 847 font-family:"Calibri", "sans-serif";1167 font-family:"Calibri",sans-serif; 848 1168 mso-ascii-font-family:Calibri; 849 1169 mso-ascii-theme-font:minor-latin; … … 865 1185 mso-pagination:widow-orphan; 866 1186 font-size:10.0pt; 867 font-family:"Calibri", "sans-serif";1187 font-family:"Calibri",sans-serif; 868 1188 mso-ascii-font-family:Calibri; 869 1189 mso-ascii-theme-font:minor-latin; … … 888 1208 <p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In 889 1209 this tutorial you will fit small angle scattering data for an alumina polishing 890 powder using data from a constant wavelength synchrotron X-ray USAXS 891 instrument. You will use both a lognormal distribution of spherical particles 892 model and a unified <span class=SpellE>Guinier-Porod</span> model. The data 893 were collected from <span style='mso-fareast-font-family:Calibri;mso-fareast-theme-font: 894 m inor-latin;mso-bidi-font-weight:bold;mso-bidi-font-style:italic'>powders895 s pread onto sticky tape and covered with another layer of the same tape. The896 data were corrected for background using data collected from two layers of 897 sticky tape.However, the sample thickness is not</span> accurately known <span1210 powder using data from a constant wavelength synchrotron X-ray USAXS instrument. 1211 You will use both a lognormal distribution of spherical particles model and a 1212 unified <span class=SpellE>Guinier-Porod</span> model. The data were collected 1213 from <span style='mso-fareast-font-family:Calibri;mso-fareast-theme-font:minor-latin; 1214 mso-bidi-font-weight:bold;mso-bidi-font-style:italic'>powders spread onto 1215 sticky tape and covered with another layer of the same tape. The data were 1216 corrected for background using data collected from two layers of sticky tape. 1217 However, the sample thickness is not</span> accurately known <span 898 1218 style='mso-fareast-font-family:Calibri;mso-fareast-theme-font:minor-latin; 899 1219 mso-bidi-font-weight:bold;mso-bidi-font-style:italic'>so the data are not 900 1220 calibrated on an absolute scale.<o:p></o:p></span></p> 901 1221 902 <p class=MsoNormal>If you have not done so already, <a 903 href="Starting%20GSAS.htm">start GSAS-II</a>.</p> 1222 <p class=MsoNormal>If you have not done so already, start GSAS-II.</p> 904 1223 905 1224 <h2>Step 1: read in the data file</h2> … … 909 1228 style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>If 910 1229 you have saved the GSAS-II project file from the <b style='mso-bidi-font-weight: 911 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1230 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 912 1231 minor-latin;mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> 913 1232 tutorial, use <b style='mso-bidi-font-weight:normal'><span style='font-family: 914 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1233 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 915 1234 minor-latin'>File/Open project 916 1235 </span></b> menu item to retrieve the data; 917 1236 plots of the size distribution and the data will appear. Then go to <!--[if supportFields]><b 918 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1237 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 919 1238 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'><span 920 1239 style='mso-element:field-begin'></span><span 921 1240 style='mso-spacerun:yes'> </span>REF _Ref386704789 \h<span 922 1241 style='mso-spacerun:yes'> </span>\* MERGEFORMAT <span style='mso-element:field-separator'></span></span></b><![endif]--><b 923 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1242 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 924 1243 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Step 2: Set 925 1244 Limits<!--[if gte mso 9]><xml> 926 1245 <w:data>08D0C9EA79F9BACE118C8200AA004BA90B02000000080000000E0000005F005200650066003300380036003700300034003700380039000000</w:data> 927 1246 </xml><![endif]--></span></b><!--[if supportFields]><b style='mso-bidi-font-weight: 928 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1247 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 929 1248 minor-latin;mso-hansi-theme-font:minor-latin'><span style='mso-element:field-end'></span></span></b><![endif]-->. 930 1249 Otherwise, use the <b style='mso-bidi-font-weight:normal'><span 931 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1250 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 932 1251 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 933 minor-latin'>Import/Small Angle Data/from a q stepQIE data file</span></b>1252 minor-latin'>Import/Small Angle Data/from q (A-1) step X-ray QIE data file</span></b> 934 1253 menu item to read the data file into GSAS-II. This read option is set to read 935 1254 three column small angle scattering data (SASD) as Q in Å<sup>-1</sup>, … … 937 1256 with metadata information in the front of this file.<span 938 1257 style='mso-spacerun:yes'> </span>Change the file directory to <b 939 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1258 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 940 1259 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 941 Calibri;mso-bidi-theme-font:minor-latin'> Exercises/Small angle</span></b><span942 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1260 Calibri;mso-bidi-theme-font:minor-latin'>exercises/<span class=SpellE>SAsize</span></span></b><span 1261 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 943 1262 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 944 1263 minor-latin'> to find the file</span>; you will have to select the <b 945 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1264 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 946 1265 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>any file 947 1266 (*.*)</span></b> filter to see it.</p> … … 950 1269 style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span 951 1270 style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Select 952 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1271 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 953 1272 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 954 1273 Calibri;mso-bidi-theme-font:minor-latin'>alumina data.dat</span></b><span 955 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1274 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 956 1275 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 957 1276 minor-latin'> data</span> file in the first dialog and press <b 958 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1277 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 959 1278 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 960 1279 Calibri;mso-bidi-theme-font:minor-latin'>Open</span></b>. There will be a 961 1280 Dialog box asking <span class=GramE><b style='mso-bidi-font-weight:normal'><span 962 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1281 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 963 1282 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 964 1283 minor-latin'>Is</span></b></span><b style='mso-bidi-font-weight:normal'><span 965 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1284 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 966 1285 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 967 1286 minor-latin'> this the file you want?</span></b> Press <span class=GramE><b 968 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1287 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 969 1288 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 970 1289 Calibri;mso-bidi-theme-font:minor-latin'>Yes</span></b></span> button to … … 972 1291 973 1292 <p class=MsoNormal>At this point the <b style='mso-bidi-font-weight:normal'><span 974 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1293 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 975 1294 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 976 1295 minor-latin'>GSAS-II data tree</span></b> window will have several entries and … … 1001 1320 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image001.png" 1002 1321 o:title=""/> 1003 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001322 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1004 1323 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image001.png" v:shapes="Picture_x0020_6"><![endif]></span></p> 1005 1324 … … 1009 1328 the last point in the pattern as it does appear to be somewhat suspect (see 1010 1329 plot). Select <b style='mso-bidi-font-weight:normal'><span style='font-family: 1011 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1330 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1012 1331 minor-latin'>Limits</span></b> under <b style='mso-bidi-font-weight:normal'><span 1013 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1332 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1014 1333 mso-hansi-theme-font:minor-latin'>SASD alumina data.dat</span></b> from the 1015 1334 GSAS-II tree. Set the upper limit using the cursor on the plot by picking the … … 1018 1337 1019 1338 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1020 id="Picture_x0020_ 15" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:225pt;1339 id="Picture_x0020_24" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:225pt; 1021 1340 height:195pt;visibility:visible;mso-wrap-style:square'> 1022 1341 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image002.png" 1023 1342 o:title=""/> 1024 </v:shape><![endif]--><![if !vml]><img border=0width=300 height=2601025 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image002.png" v:shapes="Picture_x0020_ 15"><![endif]></span><span1343 </v:shape><![endif]--><![if !vml]><img width=300 height=260 1344 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image002.png" v:shapes="Picture_x0020_24"><![endif]></span><span 1026 1345 style='mso-spacerun:yes'> </span></p> 1027 1346 … … 1030 1349 <p class=MsoNormal><span style='mso-no-proof:yes'>If you have already done this 1031 1350 step in the </span><b style='mso-bidi-font-weight:normal'><span 1032 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1351 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1033 1352 mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Size Distribution</span></b><span 1034 1353 style='mso-no-proof:yes'> tutorial, skip to </span><!--[if supportFields]><b 1035 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1354 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1036 1355 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof: 1037 1356 yes'><span style='mso-element:field-begin'></span><span 1038 1357 style='mso-spacerun:yes'> </span>REF _Ref386699439 \h<span 1039 1358 style='mso-spacerun:yes'> </span>\* MERGEFORMAT <span style='mso-element:field-separator'></span></span></b><![endif]--><b 1040 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1359 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1041 1360 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Step 4 1042 1361 Creation and Refinement of Log Normal Particle Model<span style='mso-no-proof: … … 1044 1363 <w:data>08D0C9EA79F9BACE118C8200AA004BA90B02000000080000000E0000005F005200650066003300380036003600390039003400330039000000</w:data> 1045 1364 </xml><![endif]--></span></span></b><!--[if supportFields]><b style='mso-bidi-font-weight: 1046 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1365 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1047 1366 minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'><span 1048 1367 style='mso-element:field-end'></span></span></b><![endif]--><span … … 1051 1370 other is vacuum (really air). Parameters for a number of substances are 1052 1371 defined in the file </span><b style='mso-bidi-font-weight:normal'><span 1053 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1372 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1054 1373 mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span 1055 1374 style='mso-no-proof:yes'>. You can add your own substances to this or better 1056 1375 put them in </span><b style='mso-bidi-font-weight:normal'><span 1057 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1376 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1058 1377 mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span 1059 1378 style='mso-no-proof:yes'>; this is read after Substances.py when you load 1060 1379 substances for your selection. </span>Select <b style='mso-bidi-font-weight: 1061 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1380 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1062 1381 minor-latin;mso-hansi-theme-font:minor-latin'>Substances</span></b> under <b 1063 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1382 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1064 1383 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina 1065 1384 data.dat</span></b> from the GSAS-II tree. Then do <b style='mso-bidi-font-weight: 1066 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1385 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1067 1386 minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Load</span></b> substance 1068 1387 from the menu; a popup window will appear with possible selections</p> … … 1073 1392 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image003.png" 1074 1393 o:title=""/> 1075 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=3361394 </v:shape><![endif]--><![if !vml]><img width=346 height=336 1076 1395 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image003.png" v:shapes="Picture_x0020_3"><![endif]><o:p></o:p></span></p> 1077 1396 … … 1079 1398 1080 1399 <p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span 1081 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1400 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1082 1401 mso-hansi-theme-font:minor-latin'>Alumina</span></b> and press <b 1083 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1402 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1084 1403 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>; 1085 1404 the relevant data for alumina (and vacuum) are displayed next</p> … … 1090 1409 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image004.png" 1091 1410 o:title=""/> 1092 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=2601411 </v:shape><![endif]--><![if !vml]><img width=346 height=260 1093 1412 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image004.png" v:shapes="Picture_x0020_4"><![endif]></span><span 1094 1413 style='mso-spacerun:yes'> </span></p> … … 1101 1420 are given for each substance. These can each be edited; the other values will 1102 1421 change accordingly. If your substance isnt in the list, you can <b 1103 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1422 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1104 1423 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Add 1105 1424 substance</span></b> to create a new one (you will be asked for a name and the … … 1107 1426 scattering density and that as affected by resonant scattering for the listed 1108 1427 wavelength is displayed (the wavelength can be changed in the <b 1109 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1428 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1110 1429 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Instrument 1111 1430 Parameters</span></b> GSAS-II tree item if needed). The resonant scattering … … 1118 1437 <p class=MsoNormal>You are now ready to attempt fitting the data with a log 1119 1438 normal distribution of spherical particles. Thus youll need to select <b 1120 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1439 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1121 1440 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models</span></b> 1122 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1441 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1123 1442 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina 1124 1443 data.dat</span></b> from the GSAS-II tree; the data window will display the <b 1125 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1444 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1126 1445 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Size dist.</span></b> 1127 1446 display;<span style='mso-no-proof:yes'> </span>change this to <b 1128 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1447 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1129 1448 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Particle fit</span></b> 1130 using the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1449 using the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1131 1450 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Modeling by</span></b> 1132 1451 pull down. NB: GSAS-II will remember your selection the next time you enter 1133 this <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1452 this <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1134 1453 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models</span></b> 1135 1454 data tree item.</p> … … 1140 1459 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image005.png" 1141 1460 o:title=""/> 1142 </v:shape><![endif]--><![if !vml]><img border=0width=506 height=1901461 </v:shape><![endif]--><![if !vml]><img width=506 height=190 1143 1462 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image005.png" v:shapes="Picture_x0020_16"><![endif]></span></p> 1144 1463 … … 1146 1465 1147 1466 <p class=MsoNormal>If you had done the <b style='mso-bidi-font-weight:normal'><span 1148 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1467 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1149 1468 mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> tutorial, you 1150 1469 would know that there were two populations of particles in the sample. One had 1151 1470 a mean diameter of ~1300A and the other had a mean diameter of ~150A. You will 1152 1471 also need something to describe the very lowest Q portion of the data. Do <b 1153 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1472 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1154 1473 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Add</span></b> 1155 1474 from the menu; the data window will change and the plots will be refreshed. 1156 1475 Your first step is to change the <b style='mso-bidi-font-weight:normal'><span 1157 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1476 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1158 1477 mso-hansi-theme-font:minor-latin'>Material</span></b> to <b style='mso-bidi-font-weight: 1159 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1478 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1160 1479 minor-latin;mso-hansi-theme-font:minor-latin'>Alumina</span></b> and make sure 1161 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1480 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1162 1481 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background</span></b> 1163 1482 is something reasonable (<b style='mso-bidi-font-weight:normal'><span 1164 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1483 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1165 1484 mso-hansi-theme-font:minor-latin'>0.11</span></b>) based on the data at highest 1166 Q; again the data window and plots will be refreshed.</p> 1167 1168 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1169 id="Picture_x0020_17" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:379.5pt; 1485 Q; again the data window and plots will be refreshed. Click on one of the 1486 slider buttons to force a calculation.</p> 1487 1488 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1489 id="Picture_x0020_25" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:379.5pt; 1170 1490 height:315pt;visibility:visible;mso-wrap-style:square'> 1171 1491 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image006.png" 1172 1492 o:title=""/> 1173 </v:shape><![endif]--><![if !vml]><img border=0width=506 height=4201174 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image006.png" v:shapes="Picture_x0020_ 17"><![endif]></span></p>1493 </v:shape><![endif]--><![if !vml]><img width=506 height=420 1494 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image006.png" v:shapes="Picture_x0020_25"><![endif]></span></p> 1175 1495 1176 1496 <p class=MsoNormal><o:p> </o:p></p> … … 1180 1500 1181 1501 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1182 id="Picture_x0020_ 18" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:525pt;1502 id="Picture_x0020_26" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:525pt; 1183 1503 height:450pt;visibility:visible;mso-wrap-style:square'> 1184 1504 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image007.png" 1185 1505 o:title=""/> 1186 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001187 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image007.png" v:shapes="Picture_x0020_ 18"><![endif]></span></p>1506 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1507 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image007.png" v:shapes="Picture_x0020_26"><![endif]></span></p> 1188 1508 1189 1509 <p class=MsoNormal><o:p> </o:p></p> … … 1191 1511 <p class=MsoNormal>You can manually adjust the calculated curve by using the 1192 1512 sliders: increase <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1193 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1513 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1194 1514 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: 1195 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1515 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1196 1516 minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b> and decrease <span 1197 1517 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1198 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1518 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1199 1519 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1200 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1520 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1201 1521 mso-hansi-theme-font:minor-latin'> Mean</span></b> to improve the fit. NB: The <span 1202 1522 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1203 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1523 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1204 1524 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1205 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1525 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1206 1526 mso-hansi-theme-font:minor-latin'> Mean</span></b> is a radius so its value is 1207 1527 roughly œ the <b style='mso-bidi-font-weight:normal'><span style='font-family: 1208 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1528 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1209 1529 minor-latin'>Size Distribution</span></b> result. The sliders cover 2 orders of 1210 1530 magnitude; their range is reset if a value is entered in the value field. After 1211 1531 changing <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1212 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1532 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1213 1533 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: 1214 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1534 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1215 1535 minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b> to <b 1216 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1536 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1217 1537 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>700</span></b> 1218 1538 and <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1219 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1539 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1220 1540 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: 1221 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1541 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1222 1542 minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b> to <b 1223 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1543 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1224 1544 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.0953</span></b> 1225 1545 my plot is</p> 1226 1546 1227 1547 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1228 id="Picture_x0020_ 19" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:525pt;1548 id="Picture_x0020_27" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:525pt; 1229 1549 height:450pt;visibility:visible;mso-wrap-style:square'> 1230 1550 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image008.png" 1231 1551 o:title=""/> 1232 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001233 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image008.png" v:shapes="Picture_x0020_ 19"><![endif]></span></p>1552 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1553 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image008.png" v:shapes="Picture_x0020_27"><![endif]></span></p> 1234 1554 1235 1555 <p class=MsoNormal><o:p> </o:p></p> … … 1238 1558 obvious one at Q~0.03-4Å<sup>-1</sup>; the latter is responsible for the ~150Å 1239 1559 peak in the <b style='mso-bidi-font-weight:normal'><span style='font-family: 1240 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1560 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1241 1561 minor-latin'>Size Distribution</span></b> result. Do another <b 1242 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1562 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1243 1563 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Add</span></b> 1244 1564 to include it. The data window now shows two components</p> 1245 1565 1246 1566 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1247 id="Picture_x0020_2 0" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:379.5pt;1567 id="Picture_x0020_28" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:379.5pt; 1248 1568 height:487.5pt;visibility:visible;mso-wrap-style:square'> 1249 1569 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image009.png" 1250 1570 o:title=""/> 1251 </v:shape><![endif]--><![if !vml]><img border=0width=506 height=6501252 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image009.png" v:shapes="Picture_x0020_2 0"><![endif]></span></p>1571 </v:shape><![endif]--><![if !vml]><img width=506 height=650 1572 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image009.png" v:shapes="Picture_x0020_28"><![endif]></span></p> 1253 1573 1254 1574 <p class=MsoNormal><o:p> </o:p></p> 1255 1575 1256 1576 <p class=MsoNormal>Note the <b style='mso-bidi-font-weight:normal'><span 1257 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1577 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1258 1578 mso-hansi-theme-font:minor-latin'>Material</span></b> for the new one is preset 1259 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1579 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1260 1580 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Alumina</span></b> 1261 1581 to save you the easily forgotten step of setting it. Change <span class=SpellE><b 1262 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1582 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1263 1583 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1264 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1584 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1265 1585 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b> 1266 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1586 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1267 1587 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>75</span></b> 1268 1588 (i.e. œ of 150) and reduce <span class=SpellE><b style='mso-bidi-font-weight: 1269 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1589 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1270 1590 minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1271 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1591 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1272 1592 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b> 1273 1593 to make the green curve better match the data (you can inset <b 1274 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1594 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1275 1595 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0</span></b>s 1276 1596 in the value & play with the slider something like <b style='mso-bidi-font-weight: 1277 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1597 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1278 1598 minor-latin;mso-hansi-theme-font:minor-latin'>0.0003</span></b> looks good). My 1279 1599 fit looked like</p> 1280 1600 1281 1601 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1282 id="Picture_x0020_2 1" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:525pt;1602 id="Picture_x0020_29" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:525pt; 1283 1603 height:450pt;visibility:visible;mso-wrap-style:square'> 1284 1604 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image010.png" 1285 1605 o:title=""/> 1286 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001287 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image010.png" v:shapes="Picture_x0020_2 1"><![endif]></span></p>1606 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1607 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image010.png" v:shapes="Picture_x0020_29"><![endif]></span></p> 1288 1608 1289 1609 <p class=MsoNormal><o:p> </o:p></p> … … 1293 1613 described by a pure <span class=SpellE>Porod</span> power law scattering model. 1294 1614 Do another <b style='mso-bidi-font-weight:normal'><span style='font-family: 1295 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1615 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1296 1616 minor-latin'>Models/Add</span></b> and change the <b style='mso-bidi-font-weight: 1297 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1617 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1298 1618 minor-latin;mso-hansi-theme-font:minor-latin'>Distribution </span></b>selection 1299 1619 to <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1300 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1620 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1301 1621 mso-hansi-theme-font:minor-latin'>Porod</span></b></span>. The third component 1302 1622 is then (Ive shrunk the window & moved the scroll bar).</p> … … 1307 1627 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image011.png" 1308 1628 o:title=""/> 1309 </v:shape><![endif]--><![if !vml]><img border=0width=506 height=3611629 </v:shape><![endif]--><![if !vml]><img width=506 height=361 1310 1630 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image011.png" v:shapes="Picture_x0020_22"><![endif]></span></p> 1311 1631 … … 1315 1635 1316 1636 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1317 id=" Picture_x0020_23" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt;1318 height:450pt;visibility:visible;mso-wrap-style:square'>1637 id="_x0000_i1036" type="#_x0000_t75" style='width:525pt;height:450pt; 1638 visibility:visible;mso-wrap-style:square'> 1319 1639 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image012.png" 1320 1640 o:title=""/> 1321 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001322 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image012.png" v:shapes=" Picture_x0020_23"><![endif]></span></p>1641 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1642 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image012.png" v:shapes="_x0000_i1036"><![endif]></span></p> 1323 1643 1324 1644 <p class=MsoNormal><o:p> </o:p></p> … … 1327 1647 component variables. Remembering that this is likely to be an agglomeration of 1328 1648 1300Å particles; set the <span class=SpellE><b style='mso-bidi-font-weight: 1329 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1649 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1330 1650 minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1331 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1651 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1332 1652 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Cutoff</span></b> 1333 1653 to that value. That immediately restores the higher Q portion of the fit.</p> 1334 1654 1335 1655 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1336 id="Picture_x0020_ 24" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:525pt;1656 id="Picture_x0020_31" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:525pt; 1337 1657 height:450pt;visibility:visible;mso-wrap-style:square'> 1338 1658 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image013.png" 1339 1659 o:title=""/> 1340 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001341 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image013.png" v:shapes="Picture_x0020_ 24"><![endif]></span></p>1660 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1661 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image013.png" v:shapes="Picture_x0020_31"><![endif]></span></p> 1342 1662 1343 1663 <p class=MsoNormal><o:p> </o:p></p> 1344 1664 1345 1665 <p class=MsoNormal>Next use the <span class=SpellE><b style='mso-bidi-font-weight: 1346 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1666 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1347 1667 minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1348 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1668 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1349 1669 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> P</span></b> 1350 1670 (power law exponent) slider to adjust the fit. In this case setting <span 1351 1671 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1352 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1672 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1353 1673 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1354 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1674 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1355 1675 mso-hansi-theme-font:minor-latin'> P</span></b> to ~<b style='mso-bidi-font-weight: 1356 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1676 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1357 1677 minor-latin;mso-hansi-theme-font:minor-latin'>3.25</span></b> gives a pretty 1358 1678 good fit without needing to adjust the <span class=SpellE><b style='mso-bidi-font-weight: 1359 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1679 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1360 1680 minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1361 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1681 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1362 1682 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> B</span></b> 1363 1683 <span class=SpellE>prefactor</span>.</p> 1364 1684 1365 1685 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1366 id="Picture_x0020_ 25" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt;1686 id="Picture_x0020_32" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt; 1367 1687 height:450pt;visibility:visible;mso-wrap-style:square'> 1368 1688 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image014.png" 1369 1689 o:title=""/> 1370 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001371 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image014.png" v:shapes="Picture_x0020_ 25"><![endif]></span></p>1372 1373 <p class=MsoNormal><o:p> </o:p></p> 1374 1375 <p class=MsoNormal>Finally, you can refine these coefficients to find the best fit1376 to the data. As a beginner, Id start by refining just the two <span1690 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1691 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image014.png" v:shapes="Picture_x0020_32"><![endif]></span></p> 1692 1693 <p class=MsoNormal><o:p> </o:p></p> 1694 1695 <p class=MsoNormal>Finally, you can refine these coefficients to find the best 1696 fit to the data. As a beginner, Id start by refining just the two <span 1377 1697 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1378 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1698 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1379 1699 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1380 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1700 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1381 1701 mso-hansi-theme-font:minor-latin'> Volume</span></b> and the <span 1382 1702 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1383 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1703 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1384 1704 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1385 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1705 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1386 1706 mso-hansi-theme-font:minor-latin'> B</span></b> along with the <b 1387 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1707 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1388 1708 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background</span></b> 1389 1709 parameters (one might be able to refine everything at once, but then again it 1390 1710 might not work). Check the <b style='mso-bidi-font-weight:normal'><span 1391 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1711 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1392 1712 mso-hansi-theme-font:minor-latin'>Refine?</span></b> <span class=GramE>boxes</span> 1393 1713 for these parameters. Do <b style='mso-bidi-font-weight:normal'><span 1394 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1714 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1395 1715 mso-hansi-theme-font:minor-latin'>Models/Fit </span></b>to do the least squares 1396 1716 refinement; convergence will occur very quickly. NB: if the refinement messes 1397 1717 up, you can recover the previous result; do <b style='mso-bidi-font-weight: 1398 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1718 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1399 1719 minor-latin;mso-hansi-theme-font:minor-latin'>Models/Undo</span></b> to 1400 1720 recover. Then add the two <span class=SpellE><b style='mso-bidi-font-weight: 1401 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1721 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1402 1722 minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1403 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1723 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1404 1724 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b> 1405 1725 and <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1406 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1726 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1407 1727 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: 1408 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1728 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1409 1729 minor-latin;mso-hansi-theme-font:minor-latin'> P</span></b> parameters to the 1410 1730 refinement, again convergence is easily obtained. Finally, add the two <span 1411 1731 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1412 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1732 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1413 1733 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1414 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1734 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1415 1735 mso-hansi-theme-font:minor-latin'> <span class=SpellE>StdDev</span></span></b> 1416 1736 and <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1417 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1737 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1418 1738 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: 1419 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1739 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1420 1740 minor-latin;mso-hansi-theme-font:minor-latin'> Cutoff</span></b> parameters (a 1421 1741 total of ten) to the list. The result is a really nice fit to the data with … … 1423 1743 1424 1744 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1425 id="Picture_x0020_ 28" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:549.75pt;1745 id="Picture_x0020_33" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:609.75pt; 1426 1746 height:206.25pt;visibility:visible;mso-wrap-style:square'> 1427 1747 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image015.png" 1428 1748 o:title=""/> 1429 </v:shape><![endif]--><![if !vml]><img border=0 width=733 height=2751430 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image015.png" v:shapes="Picture_x0020_ 28"><![endif]></span></p>1431 1432 <p class=MsoNormal><o:p> </o:p></p> 1433 1434 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1435 id="Picture_x0020_ 27" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt;1749 </v:shape><![endif]--><![if !vml]><img width=813 height=275 1750 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image015.png" v:shapes="Picture_x0020_33"><![endif]></span></p> 1751 1752 <p class=MsoNormal><o:p> </o:p></p> 1753 1754 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1755 id="Picture_x0020_34" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt; 1436 1756 height:450pt;visibility:visible;mso-wrap-style:square'> 1437 1757 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image016.png" 1438 1758 o:title=""/> 1439 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001440 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image016.png" v:shapes="Picture_x0020_ 27"><![endif]></span></p>1759 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1760 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image016.png" v:shapes="Picture_x0020_34"><![endif]></span></p> 1441 1761 1442 1762 <p class=MsoNormal><o:p> </o:p></p> 1443 1763 1444 1764 <p class=MsoNormal>If you had done a <b style='mso-bidi-font-weight:normal'><span 1445 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1765 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1446 1766 mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> analysis, these 1447 1767 results are plotted as component curves on that plot as well</p> 1448 1768 1449 1769 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1450 id="Picture_x0020_ 29" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt;1770 id="Picture_x0020_35" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt; 1451 1771 height:450pt;visibility:visible;mso-wrap-style:square'> 1452 1772 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image017.png" 1453 1773 o:title=""/> 1454 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001455 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image017.png" v:shapes="Picture_x0020_ 29"><![endif]></span></p>1774 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1775 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image017.png" v:shapes="Picture_x0020_35"><![endif]></span></p> 1456 1776 1457 1777 <p class=MsoNormal><o:p> </o:p></p> … … 1459 1779 <p class=MsoNormal>This is the sort of agreement one should expect between the 1460 1780 best log normal fit and the size distribution. To save these results you must 1461 do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1781 do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1462 1782 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/Save 1463 1783 project </span></b>in the main <b style='mso-bidi-font-weight:normal'><span 1464 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1784 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1465 1785 mso-hansi-theme-font:minor-latin'>GSAS-II data tree</span></b> window.</p> 1466 1786 … … 1471 1791 law distribution tail (<span class=SpellE>Porod</span> model). This can be set 1472 1792 for your model by changing the <b style='mso-bidi-font-weight:normal'><span 1473 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1793 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1474 1794 mso-hansi-theme-font:minor-latin'>Distribution</span></b> for the first two 1475 1795 components to <b style='mso-bidi-font-weight:normal'><span style='font-family: 1476 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1796 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1477 1797 minor-latin'>Unified</span></b>. NB: the log normal coefficients are not lost 1478 1798 by this step; they can be recovered by simply changing the <b style='mso-bidi-font-weight: 1479 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1799 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1480 1800 minor-latin;mso-hansi-theme-font:minor-latin'>Distribution</span></b> back to <span 1481 1801 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1482 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1802 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1483 1803 minor-latin'>LogNormal</span></b></span>. The data window values give the 1484 1804 defaults for these components</p> … … 1490 1810 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image018.png" 1491 1811 o:title=""/> 1492 </v:shape><![endif]--><![if !vml]><img border=0width=506 height=7281812 </v:shape><![endif]--><![if !vml]><img width=506 height=728 1493 1813 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image018.png" v:shapes="Picture_x0020_30"><![endif]></span></p> 1494 1814 … … 1498 1818 1499 1819 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1500 id="Picture_x0020_3 1" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt;1820 id="Picture_x0020_36" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt; 1501 1821 height:450pt;visibility:visible;mso-wrap-style:square'> 1502 1822 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image019.png" 1503 1823 o:title=""/> 1504 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001505 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image019.png" v:shapes="Picture_x0020_3 1"><![endif]></span></p>1824 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1825 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image019.png" v:shapes="Picture_x0020_36"><![endif]></span></p> 1506 1826 1507 1827 <p class=MsoNormal><o:p> </o:p></p> 1508 1828 1509 1829 <p class=MsoNormal>First, change the <span class=SpellE><b style='mso-bidi-font-weight: 1510 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1830 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1511 1831 minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1512 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1832 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1513 1833 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> <span 1514 1834 class=SpellE>Rg</span></span></b> values to be about œ the <b style='mso-bidi-font-weight: 1515 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1835 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1516 1836 minor-latin;mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> 1517 1837 results (e.g. <b style='mso-bidi-font-weight:normal'><span style='font-family: 1518 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1838 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1519 1839 minor-latin'>700</span></b> & <b style='mso-bidi-font-weight:normal'><span 1520 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1840 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1521 1841 mso-hansi-theme-font:minor-latin'>75</span></b>), then set the <span 1522 1842 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1523 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1843 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1524 1844 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1525 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1845 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1526 1846 mso-hansi-theme-font:minor-latin'> Cutoff</span></b> value for the <span 1527 1847 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1528 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1848 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1529 1849 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1530 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1850 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1531 1851 mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span></span></b>=700 1532 one to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1852 one to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1533 1853 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>100</span></b>. 1534 1854 Next, change the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1535 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1855 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1536 1856 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: 1537 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1857 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1538 1858 minor-latin;mso-hansi-theme-font:minor-latin'> G</span></b> for the <span 1539 1859 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1540 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1860 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1541 1861 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1542 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1862 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1543 1863 mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span>=700</span></b> 1544 1864 one to be about the Intensity value for the lower Q bump in the data (~<b 1545 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1865 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1546 1866 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1.0e6</span></b>). 1547 1867 Finally, reduce the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1548 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1868 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1549 1869 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: 1550 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1870 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1551 1871 minor-latin;mso-hansi-theme-font:minor-latin'> G</span></b> value for the <span 1552 1872 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1553 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1873 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1554 1874 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1555 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1875 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1556 1876 mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span>=75</span></b> 1557 1877 component to get the best fit to the data (~<b style='mso-bidi-font-weight: 1558 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1878 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1559 1879 minor-latin;mso-hansi-theme-font:minor-latin'>210</span></b>). The data window 1560 1880 looks like</p> 1561 1881 1562 1882 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1563 id="Picture_x0020_3 2" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:379.5pt;1883 id="Picture_x0020_37" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:379.5pt; 1564 1884 height:546pt;visibility:visible;mso-wrap-style:square'> 1565 1885 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image020.png" 1566 1886 o:title=""/> 1567 </v:shape><![endif]--><![if !vml]><img border=0width=506 height=7281568 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image020.png" v:shapes="Picture_x0020_3 2"><![endif]></span></p>1887 </v:shape><![endif]--><![if !vml]><img width=506 height=728 1888 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image020.png" v:shapes="Picture_x0020_37"><![endif]></span></p> 1569 1889 1570 1890 <p class=MsoNormal><o:p> </o:p></p> … … 1573 1893 1574 1894 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1575 id="Picture_x0020_3 3" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:525pt;1895 id="Picture_x0020_38" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:525pt; 1576 1896 height:450pt;visibility:visible;mso-wrap-style:square'> 1577 1897 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image021.png" 1578 1898 o:title=""/> 1579 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001580 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image021.png" v:shapes="Picture_x0020_3 3"><![endif]></span></p>1899 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1900 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image021.png" v:shapes="Picture_x0020_38"><![endif]></span></p> 1581 1901 1582 1902 <p class=MsoNormal><o:p> </o:p></p> 1583 1903 1584 1904 <p class=MsoNormal>This is probably close enough to do a refinement. Select <b 1585 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1905 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1586 1906 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Refine?</span></b> 1587 1907 For <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1588 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1908 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1589 1909 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: 1590 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1910 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1591 1911 minor-latin;mso-hansi-theme-font:minor-latin'> G</span></b>, <span 1592 1912 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1593 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1913 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1594 1914 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1595 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1915 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1596 1916 mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span></span></b> and <span 1597 1917 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1598 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1918 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1599 1919 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1600 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1920 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1601 1921 mso-hansi-theme-font:minor-latin'> B</span></b> for both components (the <span 1602 1922 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1603 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1923 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1604 1924 minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span 1605 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1925 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1606 1926 mso-hansi-theme-font:minor-latin'> B</span></b>, <span class=SpellE><b 1607 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1927 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1608 1928 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1609 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1929 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1610 1930 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> P</span></b> 1611 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1931 and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1612 1932 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background 1613 1933 Refine?</span></b> boxes should also be checked). Then do <b style='mso-bidi-font-weight: 1614 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1934 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1615 1935 minor-latin;mso-hansi-theme-font:minor-latin'>Models/Fit</span></b>; it should 1616 1936 rapidly converge to give in the console window</p> 1617 1937 1618 1938 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1619 id="Picture_x0020_3 4" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:549.75pt;1620 height:2 06.25pt;visibility:visible;mso-wrap-style:square'>1939 id="Picture_x0020_39" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:609.75pt; 1940 height:224.25pt;visibility:visible;mso-wrap-style:square'> 1621 1941 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image022.png" 1622 1942 o:title=""/> 1623 </v:shape><![endif]--><![if !vml]><img border=0 width=733 height=2751624 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image022.png" v:shapes="Picture_x0020_3 4"><![endif]></span></p>1943 </v:shape><![endif]--><![if !vml]><img width=813 height=299 1944 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image022.png" v:shapes="Picture_x0020_39"><![endif]></span></p> 1625 1945 1626 1946 <p class=MsoNormal><o:p> </o:p></p> … … 1629 1949 1630 1950 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1631 id="Picture_x0020_ 35" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;1951 id="Picture_x0020_40" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt; 1632 1952 height:450pt;visibility:visible;mso-wrap-style:square'> 1633 1953 <v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image023.png" 1634 1954 o:title=""/> 1635 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001636 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image023.png" v:shapes="Picture_x0020_ 35"><![endif]></span></p>1955 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1956 src="Fitting%20Small%20Angle%20Scattering%20Data_files/image023.png" v:shapes="Picture_x0020_40"><![endif]></span></p> 1637 1957 1638 1958 <p class=MsoNormal><o:p> </o:p></p> … … 1640 1960 <p class=MsoNormal>This fit is almost as close as the log normal one done 1641 1961 earlier. However, the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1642 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1962 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1643 1963 mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight: 1644 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1964 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1645 1965 minor-latin;mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span></span></b> 1646 1966 values are a bit less than the corresponding <span class=SpellE><b 1647 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1967 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1648 1968 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b 1649 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1969 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1650 1970 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b> 1651 values obtained earlier. Also note that this model makes no reference to the substance1652 contrast used earlier (the <b style='mso-bidi-font-weight:normal'><span1653 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1971 values obtained earlier. Also note that this model makes no reference to the 1972 substance contrast used earlier (the <b style='mso-bidi-font-weight:normal'><span 1973 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1654 1974 mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> plot will not 1655 1975 have curves calculated from this model). To save these results you must do <b 1656 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1976 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1657 1977 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/Save 1658 1978 project </span></b>in the main <b style='mso-bidi-font-weight:normal'><span 1659 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1979 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1660 1980 mso-hansi-theme-font:minor-latin'>GSAS-II data tree</span></b> window.</p> 1661 1981
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