Changeset 1739


Ignore:
Timestamp:
Mar 18, 2015 12:24:28 PM (7 years ago)
Author:
vondreele
Message:

update small angle size tutorial

Location:
Tutorials/SAsize
Files:
8 edited

Legend:

Unmodified
Added
Removed
  • Tutorials/SAsize/Small Angle Size Distribution.htm

    r1705 r1739  
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    2525  <o:Author>Von Dreele</o:Author>
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     138  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
     139   UnhideWhenUsed="true" Name="toc 6"/>
     140  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
     141   UnhideWhenUsed="true" Name="toc 7"/>
     142  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
     143   UnhideWhenUsed="true" Name="toc 8"/>
     144  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
     145   UnhideWhenUsed="true" Name="toc 9"/>
     146  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     147   Name="Normal Indent"/>
     148  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     149   Name="footnote text"/>
     150  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     151   Name="annotation text"/>
     152  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     153   Name="header"/>
     154  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     155   Name="footer"/>
     156  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     157   Name="index heading"/>
     158  <w:LsdException Locked="false" Priority="35" SemiHidden="true"
     159   UnhideWhenUsed="true" QFormat="true" Name="caption"/>
     160  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     161   Name="table of figures"/>
     162  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     163   Name="envelope address"/>
     164  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     165   Name="envelope return"/>
     166  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     167   Name="footnote reference"/>
     168  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     169   Name="annotation reference"/>
     170  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     171   Name="line number"/>
     172  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     173   Name="page number"/>
     174  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     175   Name="endnote reference"/>
     176  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     177   Name="endnote text"/>
     178  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     179   Name="table of authorities"/>
     180  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     181   Name="macro"/>
     182  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     183   Name="toa heading"/>
     184  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     185   Name="List"/>
     186  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     187   Name="List Bullet"/>
     188  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     189   Name="List Number"/>
     190  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     191   Name="List 2"/>
     192  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     193   Name="List 3"/>
     194  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     195   Name="List 4"/>
     196  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     197   Name="List 5"/>
     198  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     199   Name="List Bullet 2"/>
     200  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     201   Name="List Bullet 3"/>
     202  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     203   Name="List Bullet 4"/>
     204  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     205   Name="List Bullet 5"/>
     206  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     207   Name="List Number 2"/>
     208  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     209   Name="List Number 3"/>
     210  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     211   Name="List Number 4"/>
     212  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     213   Name="List Number 5"/>
     214  <w:LsdException Locked="false" Priority="10" QFormat="true" Name="Title"/>
     215  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     216   Name="Closing"/>
     217  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     218   Name="Signature"/>
     219  <w:LsdException Locked="false" Priority="1" SemiHidden="true"
     220   UnhideWhenUsed="true" Name="Default Paragraph Font"/>
     221  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     222   Name="Body Text"/>
     223  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     224   Name="Body Text Indent"/>
     225  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     226   Name="List Continue"/>
     227  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     228   Name="List Continue 2"/>
     229  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     230   Name="List Continue 3"/>
     231  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     232   Name="List Continue 4"/>
     233  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     234   Name="List Continue 5"/>
     235  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     236   Name="Message Header"/>
     237  <w:LsdException Locked="false" Priority="11" QFormat="true" Name="Subtitle"/>
     238  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     239   Name="Salutation"/>
     240  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     241   Name="Date"/>
     242  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     243   Name="Body Text First Indent"/>
     244  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     245   Name="Body Text First Indent 2"/>
     246  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     247   Name="Note Heading"/>
     248  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     249   Name="Body Text 2"/>
     250  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     251   Name="Body Text 3"/>
     252  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     253   Name="Body Text Indent 2"/>
     254  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     255   Name="Body Text Indent 3"/>
     256  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     257   Name="Block Text"/>
     258  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     259   Name="Hyperlink"/>
     260  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     261   Name="FollowedHyperlink"/>
     262  <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/>
     263  <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/>
     264  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     265   Name="Document Map"/>
     266  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     267   Name="Plain Text"/>
     268  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     269   Name="E-mail Signature"/>
     270  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     271   Name="HTML Top of Form"/>
     272  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     273   Name="HTML Bottom of Form"/>
     274  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     275   Name="Normal (Web)"/>
     276  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     277   Name="HTML Acronym"/>
     278  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     279   Name="HTML Address"/>
     280  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     281   Name="HTML Cite"/>
     282  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     283   Name="HTML Code"/>
     284  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     285   Name="HTML Definition"/>
     286  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     287   Name="HTML Keyboard"/>
     288  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     289   Name="HTML Preformatted"/>
     290  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     291   Name="HTML Sample"/>
     292  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     293   Name="HTML Typewriter"/>
     294  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     295   Name="HTML Variable"/>
     296  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     297   Name="Normal Table"/>
     298  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     299   Name="annotation subject"/>
     300  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     301   Name="No List"/>
     302  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     303   Name="Outline List 1"/>
     304  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     305   Name="Outline List 2"/>
     306  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     307   Name="Outline List 3"/>
     308  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     309   Name="Table Simple 1"/>
     310  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     311   Name="Table Simple 2"/>
     312  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     313   Name="Table Simple 3"/>
     314  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     315   Name="Table Classic 1"/>
     316  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     317   Name="Table Classic 2"/>
     318  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     319   Name="Table Classic 3"/>
     320  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     321   Name="Table Classic 4"/>
     322  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     323   Name="Table Colorful 1"/>
     324  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     325   Name="Table Colorful 2"/>
     326  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     327   Name="Table Colorful 3"/>
     328  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     329   Name="Table Columns 1"/>
     330  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     331   Name="Table Columns 2"/>
     332  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     333   Name="Table Columns 3"/>
     334  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     335   Name="Table Columns 4"/>
     336  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     337   Name="Table Columns 5"/>
     338  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     339   Name="Table Grid 1"/>
     340  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     341   Name="Table Grid 2"/>
     342  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     343   Name="Table Grid 3"/>
     344  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     345   Name="Table Grid 4"/>
     346  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     347   Name="Table Grid 5"/>
     348  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     349   Name="Table Grid 6"/>
     350  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     351   Name="Table Grid 7"/>
     352  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     353   Name="Table Grid 8"/>
     354  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     355   Name="Table List 1"/>
     356  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     357   Name="Table List 2"/>
     358  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     359   Name="Table List 3"/>
     360  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     361   Name="Table List 4"/>
     362  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     363   Name="Table List 5"/>
     364  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     365   Name="Table List 6"/>
     366  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     367   Name="Table List 7"/>
     368  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     369   Name="Table List 8"/>
     370  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     371   Name="Table 3D effects 1"/>
     372  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     373   Name="Table 3D effects 2"/>
     374  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     375   Name="Table 3D effects 3"/>
     376  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     377   Name="Table Contemporary"/>
     378  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     379   Name="Table Elegant"/>
     380  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     381   Name="Table Professional"/>
     382  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     383   Name="Table Subtle 1"/>
     384  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     385   Name="Table Subtle 2"/>
     386  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     387   Name="Table Web 1"/>
     388  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     389   Name="Table Web 2"/>
     390  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     391   Name="Table Web 3"/>
     392  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     393   Name="Balloon Text"/>
     394  <w:LsdException Locked="false" Priority="59" Name="Table Grid"/>
     395  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
     396   Name="Table Theme"/>
     397  <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/>
     398  <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/>
     399  <w:LsdException Locked="false" Priority="60" Name="Light Shading"/>
     400  <w:LsdException Locked="false" Priority="61" Name="Light List"/>
     401  <w:LsdException Locked="false" Priority="62" Name="Light Grid"/>
     402  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/>
     403  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/>
     404  <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/>
     405  <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/>
     406  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/>
     407  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/>
     408  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/>
     409  <w:LsdException Locked="false" Priority="70" Name="Dark List"/>
     410  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/>
     411  <w:LsdException Locked="false" Priority="72" Name="Colorful List"/>
     412  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
     413  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
     414  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
     415  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
     416  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
     417  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
     418  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
     419  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
     420  <w:LsdException Locked="false" Priority="34" QFormat="true"
     421   Name="List Paragraph"/>
     422  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
     423  <w:LsdException Locked="false" Priority="30" QFormat="true"
     424   Name="Intense Quote"/>
     425  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
     426  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
     427  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
     428  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
     429  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
     430  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
     431  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
     432  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
     433  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
     434  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
     435  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
     436  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
     437  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
     438  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
     439  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
     440  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
     441  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
     442  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
     443  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
     444  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
     445  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
     446  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
     447  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
     448  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
     449  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
     450  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
     451  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
     452  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
     453  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
     454  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
     455  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
     456  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
     457  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
     458  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
     459  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
     460  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
     461  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
     462  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
     463  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
     464  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
     465  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
     466  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
     467  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
     468  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
     469  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
     470  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
     471  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
     472  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
     473  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
     474  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
     475  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
     476  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
     477  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
     478  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
     479  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
     480  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
     481  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
     482  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
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    8881207<p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In
    8891208this tutorial you will determine the size distribution of particles in an
    890 alumina polishing powder using data from a constant wavelength synchrotron X-ray
    891 USAXS instrument. You will use both Maximum Entropy (<span class=SpellE>MaxEnt</span>)
     1209alumina polishing powder using data from a constant wavelength synchrotron
     1210X-ray USAXS instrument. You will use both Maximum Entropy (<span class=SpellE>MaxEnt</span>)
    8921211and Total Non-Negative Least Squares (TNNLS) methods assuming spherical
    8931212particles. The data were collected from <span style='mso-fareast-font-family:
     
    9001219italic'>so the data are not calibrated on an absolute scale.<o:p></o:p></span></p>
    9011220
    902 <p class=MsoNormal>If you have not done so already, <a
    903 href="Starting%20GSAS.htm">start GSAS-II</a>.</p>
     1221<p class=MsoNormal>If you have not done so already, start GSAS-II.</p>
    9041222
    9051223<h2>Step 1: read in the data file</h2>
     
    9081226style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span
    9091227style='font:7.0pt "Times New Roman"'>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp; </span></span></span><![endif]>Use
    910 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1228the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    9111229mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    912 Calibri;mso-bidi-theme-font:minor-latin'>Import/Small Angle Data/from a q step
    913 QIE data file</span></b> menu item to read the data file into GSAS-II. This
    914 read option is set to read three column small angle scattering data (SASD) as Q
    915 in Å<sup>-1</sup>, intensity and estimated standard deviation in intensity;
    916 there may be a header with metadata information in the front of this file.<span
    917 style='mso-spacerun:yes'>  </span>Change the file directory to <b
    918 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1230Calibri;mso-bidi-theme-font:minor-latin'>Import/Small Angle Data/from q (A-1) step
     1231X-ray QIE data file</span></b> menu item to read the data file into GSAS-II.
     1232This read option is set to read three column small angle scattering data (SASD)
     1233as Q in Å<sup>-1</sup>, intensity and estimated standard deviation in
     1234intensity; there may be a header with metadata information in the front of this
     1235file.<span style='mso-spacerun:yes'>  </span>Change the file directory to <b
     1236style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    9191237mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    920 Calibri;mso-bidi-theme-font:minor-latin'>Exercises/Small angle</span></b><span
    921 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1238Calibri;mso-bidi-theme-font:minor-latin'>exercises/<span class=SpellE>SAsize</span></span></b><span
     1239style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    9221240mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
    9231241minor-latin'> to find the file</span>; you will have to select the ‘<b
    924 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1242style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    9251243mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>any file
    9261244(*.*)</span></b>’ filter to see it.</p>
     
    9291247style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span
    9301248style='font:7.0pt "Times New Roman"'>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp; </span></span></span><![endif]>Select
    931 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1249the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    9321250mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    9331251Calibri;mso-bidi-theme-font:minor-latin'>alumina data.dat</span></b><span
    934 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1252style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    9351253mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
    9361254minor-latin'> data</span> file in the first dialog and press <b
    937 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1255style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    9381256mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    9391257Calibri;mso-bidi-theme-font:minor-latin'>Open</span></b>. There will be a
    9401258Dialog box asking <span class=GramE><b style='mso-bidi-font-weight:normal'><span
    941 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1259style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    9421260mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
    9431261minor-latin'>Is</span></b></span><b style='mso-bidi-font-weight:normal'><span
    944 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1262style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    9451263mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
    9461264minor-latin'> this the file you want?</span></b> Press <span class=GramE><b
    947 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1265style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    9481266mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    9491267Calibri;mso-bidi-theme-font:minor-latin'>Yes</span></b></span> button to
     
    9511269
    9521270<p class=MsoNormal>At this point the <b style='mso-bidi-font-weight:normal'><span
    953 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1271style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    9541272mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
    9551273minor-latin'>GSAS-II data tree</span></b> window will have several entries and
     
    9761294 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
    9771295 <o:lock v:ext="edit" aspectratio="t"/>
    978 </v:shapetype><v:shape id="Picture_x0020_6" o:spid="_x0000_i1038" type="#_x0000_t75"
     1296</v:shapetype><v:shape id="Picture_x0020_15" o:spid="_x0000_i1038" type="#_x0000_t75"
    9791297 style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'>
    9801298 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image001.png"
    9811299  o:title=""/>
    982 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
    983 src="Small%20Angle%20Size%20Distribution_files/image001.png" v:shapes="Picture_x0020_6"><![endif]></span></p>
     1300</v:shape><![endif]--><![if !vml]><img width=700 height=600
     1301src="Small%20Angle%20Size%20Distribution_files/image001.png" v:shapes="Picture_x0020_15"><![endif]></span></p>
    9841302
    9851303<h2>Step 2: Set Limits</h2>
     
    9901308range scattering is from very large objects not readily described by the size
    9911309distribution analysis and above the scattering is mostly background. Select <b
    992 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1310style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    9931311mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Limits</span></b>
    994 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1312under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    9951313mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina
    9961314data.dat</span></b> from the GSAS-II tree. Then set <b style='mso-bidi-font-weight:
    997 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1315normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    9981316minor-latin;mso-hansi-theme-font:minor-latin'>changed</span></b> to <b
    999 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1317style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    10001318mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.001</span></b>
    10011319for <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
    1002 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1320style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    10031321mso-hansi-theme-font:minor-latin'>Tmin</span></b></span> and <b
    1004 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1322style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    10051323mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.1</span></b>
    10061324for <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
    1007 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1325style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    10081326mso-hansi-theme-font:minor-latin'>Tmax</span></b></span>. You can also set the
    10091327limits using the cursor on the plot by either picking a point on the curve with
     
    10121330
    10131331<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1014  id="Picture_x0020_22" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:225pt;
    1015  height:195pt;visibility:visible;mso-wrap-style:square'>
     1332 id="_x0000_i1037" type="#_x0000_t75" style='width:225pt;height:195pt;
     1333 visibility:visible;mso-wrap-style:square'>
    10161334 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image002.png"
    10171335  o:title=""/>
    1018 </v:shape><![endif]--><![if !vml]><img border=0 width=300 height=260
    1019 src="Small%20Angle%20Size%20Distribution_files/image002.png" v:shapes="Picture_x0020_22"><![endif]></span><span
     1336</v:shape><![endif]--><![if !vml]><img width=300 height=260
     1337src="Small%20Angle%20Size%20Distribution_files/image002.png" v:shapes="_x0000_i1037"><![endif]></span><span
    10201338style='mso-spacerun:yes'> </span></p>
    10211339
    10221340<h2>Step 3 Select the scattering substances for your sample</h2>
    10231341
    1024 <p class=MsoNormal><span style='mso-no-proof:yes'>Two scsttering substances
    1025 need to be defined for your sample to give the anticipated scattering contrast;
    1026 in this case one is alumina and the other is “vacuum” (really air). Parameters
    1027 for a number of substances are defined in the file </span><b style='mso-bidi-font-weight:
    1028 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1342<p class=MsoNormal><span style='mso-no-proof:yes'>Two scsttering substances need
     1343to be defined for your sample to give the anticipated scattering contrast; in
     1344this case one is alumina and the other is “vacuum” (really air). Parameters for
     1345a number of substances are defined in the file </span><b style='mso-bidi-font-weight:
     1346normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    10291347minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span
    1030 style='mso-no-proof:yes'>. You can add your own substances to this or better put
    1031 them in </span><b style='mso-bidi-font-weight:normal'><span style='font-family:
    1032 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1033 minor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span
     1348style='mso-no-proof:yes'>. You can add your own substances to this or better
     1349put them in </span><b style='mso-bidi-font-weight:normal'><span
     1350style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
     1351mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span
    10341352style='mso-no-proof:yes'>; this is read after </span><b style='mso-bidi-font-weight:
    1035 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1353normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    10361354minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span
    10371355style='mso-no-proof:yes'> when you load substances for your selection. </span>Select
    1038 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1356<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    10391357mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Substances</span></b>
    1040 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1358under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    10411359mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina
    10421360data.dat</span></b> from the GSAS-II tree. Then do <b style='mso-bidi-font-weight:
    1043 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
    1044 minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Load</span></b> substance
     1361normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
     1362minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Load</span></b> <b
     1363style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     1364mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>substance</span></b>
    10451365from the menu; a popup window will appear with possible selections</p>
    10461366
     
    10501370 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image003.png"
    10511371  o:title=""/>
    1052 </v:shape><![endif]--><![if !vml]><img border=0 width=346 height=336
     1372</v:shape><![endif]--><![if !vml]><img width=346 height=336
    10531373src="Small%20Angle%20Size%20Distribution_files/image003.png" v:shapes="Picture_x0020_23"><![endif]><o:p></o:p></span></p>
    10541374
     
    10561376
    10571377<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
    1058 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1378style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    10591379mso-hansi-theme-font:minor-latin'>Alumina</span></b> and press <b
    1060 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1380style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    10611381mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>;
    10621382the relevant data for alumina (and vacuum) are displayed next</p>
    10631383
    10641384<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1065  id="Picture_x0020_24" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:259.5pt;
     1385 id="Picture_x0020_16" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:259.5pt;
    10661386 height:195pt;visibility:visible;mso-wrap-style:square'>
    10671387 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image004.png"
    10681388  o:title=""/>
    1069 </v:shape><![endif]--><![if !vml]><img border=0 width=346 height=260
    1070 src="Small%20Angle%20Size%20Distribution_files/image004.png" v:shapes="Picture_x0020_24"><![endif]></span><span
     1389</v:shape><![endif]--><![if !vml]><img width=346 height=260
     1390src="Small%20Angle%20Size%20Distribution_files/image004.png" v:shapes="Picture_x0020_16"><![endif]></span><span
    10711391style='mso-spacerun:yes'> </span></p>
    10721392
     
    10781398are given for each substance. These can each be edited; the other values will
    10791399change accordingly. If your substance isn’t in the list, you can <b
    1080 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1400style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    10811401mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Add
    10821402substance</span></b> to create a new one (you will be asked for a name and the
     
    10841404scattering density and that as affected by resonant scattering for the listed
    10851405wavelength is displayed (the wavelength can be changed in the <b
    1086 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1406style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    10871407mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Instrument
    10881408Parameters</span></b> GSAS-II tree item if needed). The resonant scattering
     
    10931413<p class=MsoNormal>Two of the substances you have loaded into GSAS-II next need
    10941414to be selected for this size distribution analysis; Select <b style='mso-bidi-font-weight:
    1095 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1415normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    10961416minor-latin;mso-hansi-theme-font:minor-latin'>Sample Parameters</span></b>
    1097 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1417under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    10981418mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina
    10991419data.dat</span></b> from the GSAS-II tree. Near the bottom of the window will
    11001420be two rows marked “<b style='mso-bidi-font-weight:normal'><span
    1101 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1421style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    11021422mso-hansi-theme-font:minor-latin'>Material</span></b>”; select <b
    1103 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1423style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    11041424mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Alumina</span></b>
    11051425from one of the pull downs (leave the other as <b style='mso-bidi-font-weight:
    1106 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1426normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    11071427minor-latin;mso-hansi-theme-font:minor-latin'>vacuum</span></b>). The window
    11081428will show at the bottom the computed contrast between alumina and vacuum
    1109 without and with consideration of resonant scattering effects; the latter is used
    1110 in subsequent calculations.</p>
     1429without and with consideration of resonant scattering effects; the latter is
     1430used in subsequent calculations.</p>
    11111431
    11121432<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1113  id="Picture_x0020_25" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:305.25pt;
    1114  height:369pt;visibility:visible;mso-wrap-style:square'>
     1433 id="Picture_x0020_17" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:305.25pt;
     1434 height:408pt;visibility:visible;mso-wrap-style:square'>
    11151435 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image005.png"
    11161436  o:title=""/>
    1117 </v:shape><![endif]--><![if !vml]><img border=0 width=407 height=492
    1118 src="Small%20Angle%20Size%20Distribution_files/image005.png" v:shapes="Picture_x0020_25"><![endif]></span></p>
     1437</v:shape><![endif]--><![if !vml]><img width=407 height=544
     1438src="Small%20Angle%20Size%20Distribution_files/image005.png" v:shapes="Picture_x0020_17"><![endif]></span></p>
    11191439
    11201440<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    11221442<p class=MsoNormal>For experiments for which you know the transmission and the
    11231443sample thickness, you can manipulate the <b style='mso-bidi-font-weight:normal'><span
    1124 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1444style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    11251445mso-hansi-theme-font:minor-latin'>volume fractions</span></b> to make the
    11261446calculated transmission match the observed one. Additionally, if you have
    11271447absolute scaling information, you can rescale the data by adjusting the <b
    1128 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1448style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    11291449mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>histogram
    11301450scale factor</span></b>; multiple data sets can be scaled together via the <b
    1131 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1451style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    11321452mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Command/Set
    11331453scale</span></b> menu item.</p>
     
    11371457<p class=MsoNormal>You are now ready to attempt a size distribution analysis
    11381458using the maximum entropy method. Select <b style='mso-bidi-font-weight:normal'><span
    1139 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1459style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    11401460mso-hansi-theme-font:minor-latin'>Models</span></b> under <b style='mso-bidi-font-weight:
    1141 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1461normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    11421462minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina data.dat</span></b>
    11431463from the GSAS-II tree; the window will display</p>
    11441464
    11451465<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1146  id="Picture_x0020_15" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:355.5pt;
     1466 id="Picture_x0020_18" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:361.5pt;
    11471467 height:191.25pt;visibility:visible;mso-wrap-style:square'>
    11481468 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image006.png"
    11491469  o:title=""/>
    1150 </v:shape><![endif]--><![if !vml]><img border=0 width=474 height=255
    1151 src="Small%20Angle%20Size%20Distribution_files/image006.png" v:shapes="Picture_x0020_15"><![endif]></span></p>
     1470</v:shape><![endif]--><![if !vml]><img width=482 height=255
     1471src="Small%20Angle%20Size%20Distribution_files/image006.png" v:shapes="Picture_x0020_18"><![endif]></span></p>
    11521472
    11531473<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    11581478
    11591479<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1160  id="Picture_x0020_27" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt;
     1480 id="Picture_x0020_19" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt;
    11611481 height:450pt;visibility:visible;mso-wrap-style:square'>
    11621482 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image007.png"
    11631483  o:title=""/>
    1164 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
    1165 src="Small%20Angle%20Size%20Distribution_files/image007.png" v:shapes="Picture_x0020_27"><![endif]></span><span
     1484</v:shape><![endif]--><![if !vml]><img width=700 height=600
     1485src="Small%20Angle%20Size%20Distribution_files/image007.png" v:shapes="Picture_x0020_19"><![endif]></span><span
    11661486style='mso-spacerun:yes'> </span></p>
    11671487
     
    11701490<p class=MsoNormal>It is clear that the intensity levels off at an apparent
    11711491background level of ~<b style='mso-bidi-font-weight:normal'><span
    1172 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1492style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    11731493mso-hansi-theme-font:minor-latin'>0.12</span></b>; enter that into the
    11741494appropriate place in the data window. The plot will be redrawn showing a horizontal
    11751495red line for the background. All the other parameters seem reasonable for a 1<sup>st</sup>
    11761496attempt at a <span class=SpellE>MaxEnt</span> solution. Do <b style='mso-bidi-font-weight:
    1177 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1497normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    11781498minor-latin;mso-hansi-theme-font:minor-latin'>Models/Fit</span></b>; the
    11791499console window will show that the calculation did not converge and the <b
    1180 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1500style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    11811501mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Size
    11821502Distribution</span></b> plot has a “choppy” appearance.</p>
     
    11871507 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image008.png"
    11881508  o:title=""/>
    1189 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
     1509</v:shape><![endif]--><![if !vml]><img width=700 height=600
    11901510src="Small%20Angle%20Size%20Distribution_files/image008.png" v:shapes="Picture_x0020_28"><![endif]></span></p>
    11911511
     
    11941514<p class=MsoNormal>This is not a satisfactory result, but the suggestion given
    11951515in the console window is worth trying. Change the <b style='mso-bidi-font-weight:
    1196 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1516normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    11971517minor-latin;mso-hansi-theme-font:minor-latin'>Error multiplier</span></b> to <b
    1198 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1518style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    11991519mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>5</span></b>
    12001520(notice the increased error bars on the data plot) and repeat <b
    1201 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1521style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    12021522mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Model/Fit</span></b>.
    12031523Convergence is now achieved in &lt;10 cycles (see console window for details)
     
    12091529 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image009.png"
    12101530  o:title=""/>
    1211 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
     1531</v:shape><![endif]--><![if !vml]><img width=700 height=600
    12121532src="Small%20Angle%20Size%20Distribution_files/image009.png" v:shapes="Picture_x0020_29"><![endif]></span></p>
    12131533
     
    12201540<p class=MsoNormal>You may wish to explore the effect of some of the other
    12211541parameters in the data window. Most are obvious but <b style='mso-bidi-font-weight:
    1222 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1542normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    12231543minor-latin;mso-hansi-theme-font:minor-latin'>Log floor factor</span></b> needs
    12241544a bit of explanation. This is the log of the minimum size distribution (scaled
    1225 by the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1545by the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    12261546mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>histogram
    12271547scale factor</span></b> and the <b style='mso-bidi-font-weight:normal'><span
    1228 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1548style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    12291549mso-hansi-theme-font:minor-latin'>contrast</span></b>). This size distribution
    12301550minimum needs to be set within 1-2 orders of magnitude of the optimal value and
     
    12351555
    12361556<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1237  id="Picture_x0020_30" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:621.75pt;
     1557 id="Picture_x0020_20" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt;
    12381558 height:450pt;visibility:visible;mso-wrap-style:square'>
    12391559 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image010.png"
    12401560  o:title=""/>
    1241 </v:shape><![endif]--><![if !vml]><img border=0 width=829 height=600
    1242 src="Small%20Angle%20Size%20Distribution_files/image010.png" v:shapes="Picture_x0020_30"><![endif]></span></p>
     1561</v:shape><![endif]--><![if !vml]><img width=700 height=600
     1562src="Small%20Angle%20Size%20Distribution_files/image010.png" v:shapes="Picture_x0020_20"><![endif]></span></p>
    12431563
    12441564<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    12581578a gradient refinement method for the special case of all positive data and
    12591579parameter values. To try it on this alumina data, select <b style='mso-bidi-font-weight:
    1260 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1580normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    12611581minor-latin;mso-hansi-theme-font:minor-latin'>IPG</span></b> from the <b
    1262 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1582style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    12631583mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Fitting
    12641584method</span></b> pull down. The data window will change to give</p>
    12651585
    12661586<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1267  id="Picture_x0020_16" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:375.75pt;
     1587 id="Picture_x0020_21" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:375.75pt;
    12681588 height:191.25pt;visibility:visible;mso-wrap-style:square'>
    12691589 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image011.png"
    12701590  o:title=""/>
    1271 </v:shape><![endif]--><![if !vml]><img border=0 width=501 height=255
    1272 src="Small%20Angle%20Size%20Distribution_files/image011.png" v:shapes="Picture_x0020_16"><![endif]></span></p>
     1591</v:shape><![endif]--><![if !vml]><img width=501 height=255
     1592src="Small%20Angle%20Size%20Distribution_files/image011.png" v:shapes="Picture_x0020_21"><![endif]></span></p>
    12731593
    12741594<p class=MsoNormal><o:p>&nbsp;</o:p></p>
    12751595
    12761596<p class=MsoNormal>Reset the Error multiplier back to <b style='mso-bidi-font-weight:
    1277 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1597normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    12781598minor-latin;mso-hansi-theme-font:minor-latin'>1.0</span></b> and then do <b
    1279 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1599style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    12801600mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Fit</span></b>
    12811601to run the IPG fitting. The IPG algorithm did not converge in 100 cycles and
     
    12881608 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image012.png"
    12891609  o:title=""/>
    1290 </v:shape><![endif]--><![if !vml]><img border=0 width=829 height=600
     1610</v:shape><![endif]--><![if !vml]><img width=829 height=600
    12911611src="Small%20Angle%20Size%20Distribution_files/image012.png" v:shapes="Picture_x0020_289"><![endif]></span></p>
    12921612
     
    12941614
    12951615<p class=MsoNormal>This can be considerably improved by setting the <b
    1296 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1616style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    12971617mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Error
    12981618multiplier</span></b> to <b style='mso-bidi-font-weight:normal'><span
    1299 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1619style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    13001620mso-hansi-theme-font:minor-latin'>2.0</span></b>; the IPG fit con<span
    13011621style='mso-no-proof:yes'>verges in &lt;20 cycles and gives a smoother size
     
    13071627 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image013.png"
    13081628  o:title=""/>
    1309 </v:shape><![endif]--><![if !vml]><img border=0 width=829 height=600
     1629</v:shape><![endif]--><![if !vml]><img width=829 height=600
    13101630src="Small%20Angle%20Size%20Distribution_files/image013.png" v:shapes="Picture_x0020_291"><![endif]></span></p>
    13111631
     
    13181638
    13191639<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1320  id="Picture_x0020_292" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:621.75pt;
     1640 id="Picture_x0020_22" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;
    13211641 height:450pt;visibility:visible;mso-wrap-style:square'>
    13221642 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image014.png"
    13231643  o:title=""/>
    1324 </v:shape><![endif]--><![if !vml]><img border=0 width=829 height=600
    1325 src="Small%20Angle%20Size%20Distribution_files/image014.png" v:shapes="Picture_x0020_292"><![endif]></span></p>
     1644</v:shape><![endif]--><![if !vml]><img width=700 height=600
     1645src="Small%20Angle%20Size%20Distribution_files/image014.png" v:shapes="Picture_x0020_22"><![endif]></span></p>
    13261646
    13271647<p class=MsoNormal><o:p>&nbsp;</o:p></p>
     
    13291649<p class=MsoNormal>You may wish to explore the other parameters for the IPG
    13301650fitting. If <b style='mso-bidi-font-weight:normal'><span style='font-family:
    1331 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
     1651"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    13321652minor-latin'>Q power weight</span></b> is set to <b style='mso-bidi-font-weight:
    1333 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1653normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    13341654minor-latin;mso-hansi-theme-font:minor-latin'>0-4</span></b>, that changes the
    13351655data weighting to <span class=SpellE><span class=GramE>Q<sup>p</sup></span></span>.
    13361656This can change the convergence of the IPG method and yield improved results if
    13371657one is unsuccessful with the default settings. I got a nice fit with a <b
    1338 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1658style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    13391659mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Q power
    13401660weight</span></b> of <b style='mso-bidi-font-weight:normal'><span
    1341 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1661style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
    13421662mso-hansi-theme-font:minor-latin'>3</span></b> and <b style='mso-bidi-font-weight:
    1343 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1663normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
    13441664minor-latin;mso-hansi-theme-font:minor-latin'>Error multiplier</span></b> of <b
    1345 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     1665style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
    13461666mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>2.0</span></b>.</p>
    13471667
    1348 <p class=MsoNormal>You should save this GSAS-II project as it will be used in
    1349 the tutorial for fitting small angle scattering data; I used <span
    1350 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
    1351 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1352 minor-latin'>alumina.gpx</span></b></span>.</p>
     1668<p class=MsoNormal>You should save this GSAS-II project as it will be used in the
     1669tutorial for fitting small angle scattering data; I used <span class=SpellE><b
     1670style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
     1671mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>alumina.gpx</span></b></span>.</p>
    13531672
    13541673</div>
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