Changeset 1739
- Timestamp:
- Mar 18, 2015 12:24:28 PM (9 years ago)
- Location:
- Tutorials/SAsize
- Files:
-
- 8 edited
Legend:
- Unmodified
- Added
- Removed
-
Tutorials/SAsize/Small Angle Size Distribution.htm
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Name="Salutation"/> 240 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 241 Name="Date"/> 242 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 243 Name="Body Text First Indent"/> 244 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 245 Name="Body Text First Indent 2"/> 246 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 247 Name="Note Heading"/> 248 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 249 Name="Body Text 2"/> 250 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 251 Name="Body Text 3"/> 252 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 253 Name="Body Text Indent 2"/> 254 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 255 Name="Body Text Indent 3"/> 256 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 257 Name="Block Text"/> 258 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 259 Name="Hyperlink"/> 260 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 261 Name="FollowedHyperlink"/> 262 <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/> 263 <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/> 264 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 265 Name="Document Map"/> 266 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 267 Name="Plain Text"/> 268 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 269 Name="E-mail Signature"/> 270 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 271 Name="HTML Top of Form"/> 272 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 273 Name="HTML Bottom of Form"/> 274 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 275 Name="Normal (Web)"/> 276 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 277 Name="HTML Acronym"/> 278 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 279 Name="HTML Address"/> 280 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 281 Name="HTML Cite"/> 282 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 283 Name="HTML Code"/> 284 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 285 Name="HTML Definition"/> 286 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 287 Name="HTML Keyboard"/> 288 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 289 Name="HTML Preformatted"/> 290 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 291 Name="HTML Sample"/> 292 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 293 Name="HTML Typewriter"/> 294 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 295 Name="HTML Variable"/> 296 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 297 Name="Normal Table"/> 298 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 299 Name="annotation subject"/> 300 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 301 Name="No List"/> 302 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 303 Name="Outline List 1"/> 304 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 305 Name="Outline List 2"/> 306 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 307 Name="Outline List 3"/> 308 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 309 Name="Table Simple 1"/> 310 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 311 Name="Table Simple 2"/> 312 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 313 Name="Table Simple 3"/> 314 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 315 Name="Table Classic 1"/> 316 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 317 Name="Table Classic 2"/> 318 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 319 Name="Table Classic 3"/> 320 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 321 Name="Table Classic 4"/> 322 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 323 Name="Table Colorful 1"/> 324 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 325 Name="Table Colorful 2"/> 326 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 327 Name="Table Colorful 3"/> 328 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 329 Name="Table Columns 1"/> 330 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 331 Name="Table Columns 2"/> 332 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 333 Name="Table Columns 3"/> 334 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 335 Name="Table Columns 4"/> 336 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 337 Name="Table Columns 5"/> 338 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 339 Name="Table Grid 1"/> 340 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 341 Name="Table Grid 2"/> 342 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 343 Name="Table Grid 3"/> 344 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 345 Name="Table Grid 4"/> 346 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 347 Name="Table Grid 5"/> 348 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 349 Name="Table Grid 6"/> 350 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 351 Name="Table Grid 7"/> 352 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 353 Name="Table Grid 8"/> 354 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 355 Name="Table List 1"/> 356 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 357 Name="Table List 2"/> 358 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 359 Name="Table List 3"/> 360 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 361 Name="Table List 4"/> 362 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 363 Name="Table List 5"/> 364 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 365 Name="Table List 6"/> 366 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 367 Name="Table List 7"/> 368 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 369 Name="Table List 8"/> 370 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 371 Name="Table 3D effects 1"/> 372 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 373 Name="Table 3D effects 2"/> 374 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 375 Name="Table 3D effects 3"/> 376 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 377 Name="Table Contemporary"/> 378 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 379 Name="Table Elegant"/> 380 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 381 Name="Table Professional"/> 382 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 383 Name="Table Subtle 1"/> 384 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 385 Name="Table Subtle 2"/> 386 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 387 Name="Table Web 1"/> 388 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 389 Name="Table Web 2"/> 390 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 391 Name="Table Web 3"/> 392 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 393 Name="Balloon Text"/> 394 <w:LsdException Locked="false" Priority="59" Name="Table Grid"/> 395 <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" 396 Name="Table Theme"/> 397 <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/> 398 <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/> 399 <w:LsdException Locked="false" Priority="60" Name="Light Shading"/> 400 <w:LsdException Locked="false" Priority="61" Name="Light List"/> 401 <w:LsdException Locked="false" Priority="62" Name="Light Grid"/> 402 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/> 403 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/> 404 <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/> 405 <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/> 406 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/> 407 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/> 408 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/> 409 <w:LsdException Locked="false" Priority="70" Name="Dark List"/> 410 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/> 411 <w:LsdException Locked="false" Priority="72" Name="Colorful List"/> 412 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/> 413 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/> 414 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/> 415 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/> 416 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/> 417 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/> 418 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/> 419 <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/> 420 <w:LsdException Locked="false" Priority="34" QFormat="true" 421 Name="List Paragraph"/> 422 <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/> 423 <w:LsdException Locked="false" Priority="30" QFormat="true" 424 Name="Intense Quote"/> 425 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/> 426 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/> 427 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/> 428 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/> 429 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/> 430 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/> 431 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/> 432 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/> 433 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/> 434 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/> 435 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/> 436 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/> 437 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/> 438 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/> 439 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/> 440 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/> 441 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/> 442 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/> 443 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/> 444 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/> 445 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/> 446 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/> 447 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/> 448 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/> 449 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/> 450 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/> 451 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/> 452 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/> 453 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/> 454 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/> 455 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/> 456 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/> 457 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/> 458 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/> 459 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/> 460 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/> 461 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/> 462 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/> 463 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/> 464 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/> 465 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/> 466 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/> 467 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/> 468 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/> 469 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/> 470 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/> 471 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/> 472 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/> 473 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/> 474 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/> 475 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/> 476 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/> 477 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/> 478 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/> 479 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/> 480 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/> 481 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/> 482 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/> 483 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/> 484 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/> 485 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/> 486 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/> 487 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/> 488 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/> 489 <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/> 490 <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/> 491 <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/> 492 <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/> 493 <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/> 494 <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/> 495 <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/> 496 <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/> 497 <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/> 498 <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/> 499 <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/> 500 <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/> 501 <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/> 502 <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/> 503 <w:LsdException Locked="false" Priority="19" QFormat="true" 504 Name="Subtle Emphasis"/> 505 <w:LsdException Locked="false" Priority="21" QFormat="true" 506 Name="Intense Emphasis"/> 507 <w:LsdException Locked="false" Priority="31" QFormat="true" 508 Name="Subtle Reference"/> 509 <w:LsdException Locked="false" Priority="32" QFormat="true" 510 Name="Intense Reference"/> 511 <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/> 512 <w:LsdException Locked="false" Priority="37" SemiHidden="true" 513 UnhideWhenUsed="true" Name="Bibliography"/> 514 <w:LsdException Locked="false" Priority="39" SemiHidden="true" 515 UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/> 516 <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/> 517 <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/> 518 <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/> 519 <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/> 520 <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/> 521 <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/> 522 <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/> 523 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/> 524 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/> 525 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/> 526 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/> 527 <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/> 528 <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/> 529 <w:LsdException Locked="false" Priority="46" 530 Name="Grid Table 1 Light Accent 1"/> 531 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/> 532 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/> 533 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/> 534 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/> 535 <w:LsdException Locked="false" Priority="51" 536 Name="Grid Table 6 Colorful Accent 1"/> 537 <w:LsdException Locked="false" Priority="52" 538 Name="Grid Table 7 Colorful Accent 1"/> 539 <w:LsdException Locked="false" Priority="46" 540 Name="Grid Table 1 Light Accent 2"/> 541 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/> 542 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/> 543 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/> 544 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/> 545 <w:LsdException Locked="false" Priority="51" 546 Name="Grid Table 6 Colorful Accent 2"/> 547 <w:LsdException Locked="false" Priority="52" 548 Name="Grid Table 7 Colorful Accent 2"/> 549 <w:LsdException Locked="false" Priority="46" 550 Name="Grid Table 1 Light Accent 3"/> 551 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/> 552 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/> 553 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/> 554 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/> 555 <w:LsdException Locked="false" Priority="51" 556 Name="Grid Table 6 Colorful Accent 3"/> 557 <w:LsdException Locked="false" Priority="52" 558 Name="Grid Table 7 Colorful Accent 3"/> 559 <w:LsdException Locked="false" Priority="46" 560 Name="Grid Table 1 Light Accent 4"/> 561 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/> 562 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/> 563 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/> 564 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/> 565 <w:LsdException Locked="false" Priority="51" 566 Name="Grid Table 6 Colorful Accent 4"/> 567 <w:LsdException Locked="false" Priority="52" 568 Name="Grid Table 7 Colorful Accent 4"/> 569 <w:LsdException Locked="false" Priority="46" 570 Name="Grid Table 1 Light Accent 5"/> 571 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/> 572 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/> 573 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/> 574 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/> 575 <w:LsdException Locked="false" Priority="51" 576 Name="Grid Table 6 Colorful Accent 5"/> 577 <w:LsdException Locked="false" Priority="52" 578 Name="Grid Table 7 Colorful Accent 5"/> 579 <w:LsdException Locked="false" Priority="46" 580 Name="Grid Table 1 Light Accent 6"/> 581 <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/> 582 <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/> 583 <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/> 584 <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/> 585 <w:LsdException Locked="false" Priority="51" 586 Name="Grid Table 6 Colorful Accent 6"/> 587 <w:LsdException Locked="false" Priority="52" 588 Name="Grid Table 7 Colorful Accent 6"/> 589 <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/> 590 <w:LsdException Locked="false" Priority="47" Name="List Table 2"/> 591 <w:LsdException Locked="false" Priority="48" 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1021 mso-fareast-font-family:"Times New Roman"; … … 727 1046 mso-ansi-font-size:8.0pt; 728 1047 mso-bidi-font-size:8.0pt; 729 font-family:"Tahoma", "sans-serif";1048 font-family:"Tahoma",sans-serif; 730 1049 mso-ascii-font-family:Tahoma; 731 1050 mso-fareast-font-family:"Times New Roman"; … … 742 1061 mso-ansi-font-size:8.0pt; 743 1062 mso-bidi-font-size:8.0pt; 744 font-family:"Tahoma", "sans-serif";1063 font-family:"Tahoma",sans-serif; 745 1064 mso-ascii-font-family:Tahoma; 746 1065 mso-fareast-font-family:"Times New Roman"; … … 760 1079 mso-ansi-font-size:10.0pt; 761 1080 mso-bidi-font-size:10.0pt; 762 font-family:"Calibri", "sans-serif";1081 font-family:"Calibri",sans-serif; 763 1082 mso-ascii-font-family:Calibri; 764 1083 mso-ascii-theme-font:minor-latin; … … 845 1164 mso-pagination:widow-orphan; 846 1165 font-size:10.0pt; 847 font-family:"Calibri", "sans-serif";1166 font-family:"Calibri",sans-serif; 848 1167 mso-ascii-font-family:Calibri; 849 1168 mso-ascii-theme-font:minor-latin; … … 865 1184 mso-pagination:widow-orphan; 866 1185 font-size:10.0pt; 867 font-family:"Calibri", "sans-serif";1186 font-family:"Calibri",sans-serif; 868 1187 mso-ascii-font-family:Calibri; 869 1188 mso-ascii-theme-font:minor-latin; … … 888 1207 <p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In 889 1208 this tutorial you will determine the size distribution of particles in an 890 alumina polishing powder using data from a constant wavelength synchrotron X-ray891 USAXS instrument. You will use both Maximum Entropy (<span class=SpellE>MaxEnt</span>)1209 alumina polishing powder using data from a constant wavelength synchrotron 1210 X-ray USAXS instrument. You will use both Maximum Entropy (<span class=SpellE>MaxEnt</span>) 892 1211 and Total Non-Negative Least Squares (TNNLS) methods assuming spherical 893 1212 particles. The data were collected from <span style='mso-fareast-font-family: … … 900 1219 italic'>so the data are not calibrated on an absolute scale.<o:p></o:p></span></p> 901 1220 902 <p class=MsoNormal>If you have not done so already, <a 903 href="Starting%20GSAS.htm">start GSAS-II</a>.</p> 1221 <p class=MsoNormal>If you have not done so already, start GSAS-II.</p> 904 1222 905 1223 <h2>Step 1: read in the data file</h2> … … 908 1226 style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span 909 1227 style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Use 910 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1228 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 911 1229 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 912 Calibri;mso-bidi-theme-font:minor-latin'>Import/Small Angle Data/from a qstep913 QIE data file</span></b> menu item to read the data file into GSAS-II. This 914 read option is set to read three column small angle scattering data (SASD) as Q 915 in Å<sup>-1</sup>, intensity and estimated standard deviation in intensity; 916 there may be a header with metadata information in the front of this file.<span 917 style='mso-spacerun:yes'> </span>Change the file directory to <b918 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1230 Calibri;mso-bidi-theme-font:minor-latin'>Import/Small Angle Data/from q (A-1) step 1231 X-ray QIE data file</span></b> menu item to read the data file into GSAS-II. 1232 This read option is set to read three column small angle scattering data (SASD) 1233 as Q in Å<sup>-1</sup>, intensity and estimated standard deviation in 1234 intensity; there may be a header with metadata information in the front of this 1235 file.<span style='mso-spacerun:yes'> </span>Change the file directory to <b 1236 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 919 1237 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 920 Calibri;mso-bidi-theme-font:minor-latin'> Exercises/Small angle</span></b><span921 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1238 Calibri;mso-bidi-theme-font:minor-latin'>exercises/<span class=SpellE>SAsize</span></span></b><span 1239 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 922 1240 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 923 1241 minor-latin'> to find the file</span>; you will have to select the <b 924 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1242 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 925 1243 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>any file 926 1244 (*.*)</span></b> filter to see it.</p> … … 929 1247 style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span 930 1248 style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Select 931 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1249 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 932 1250 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 933 1251 Calibri;mso-bidi-theme-font:minor-latin'>alumina data.dat</span></b><span 934 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1252 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 935 1253 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 936 1254 minor-latin'> data</span> file in the first dialog and press <b 937 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1255 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 938 1256 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 939 1257 Calibri;mso-bidi-theme-font:minor-latin'>Open</span></b>. There will be a 940 1258 Dialog box asking <span class=GramE><b style='mso-bidi-font-weight:normal'><span 941 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1259 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 942 1260 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 943 1261 minor-latin'>Is</span></b></span><b style='mso-bidi-font-weight:normal'><span 944 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1262 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 945 1263 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 946 1264 minor-latin'> this the file you want?</span></b> Press <span class=GramE><b 947 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1265 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 948 1266 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 949 1267 Calibri;mso-bidi-theme-font:minor-latin'>Yes</span></b></span> button to … … 951 1269 952 1270 <p class=MsoNormal>At this point the <b style='mso-bidi-font-weight:normal'><span 953 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1271 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 954 1272 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 955 1273 minor-latin'>GSAS-II data tree</span></b> window will have several entries and … … 976 1294 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> 977 1295 <o:lock v:ext="edit" aspectratio="t"/> 978 </v:shapetype><v:shape id="Picture_x0020_ 6" o:spid="_x0000_i1038" type="#_x0000_t75"1296 </v:shapetype><v:shape id="Picture_x0020_15" o:spid="_x0000_i1038" type="#_x0000_t75" 979 1297 style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'> 980 1298 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image001.png" 981 1299 o:title=""/> 982 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=600983 src="Small%20Angle%20Size%20Distribution_files/image001.png" v:shapes="Picture_x0020_ 6"><![endif]></span></p>1300 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1301 src="Small%20Angle%20Size%20Distribution_files/image001.png" v:shapes="Picture_x0020_15"><![endif]></span></p> 984 1302 985 1303 <h2>Step 2: Set Limits</h2> … … 990 1308 range scattering is from very large objects not readily described by the size 991 1309 distribution analysis and above the scattering is mostly background. Select <b 992 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1310 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 993 1311 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Limits</span></b> 994 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1312 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 995 1313 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina 996 1314 data.dat</span></b> from the GSAS-II tree. Then set <b style='mso-bidi-font-weight: 997 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1315 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 998 1316 minor-latin;mso-hansi-theme-font:minor-latin'>changed</span></b> to <b 999 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1317 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1000 1318 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.001</span></b> 1001 1319 for <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1002 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1320 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1003 1321 mso-hansi-theme-font:minor-latin'>Tmin</span></b></span> and <b 1004 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1322 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1005 1323 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.1</span></b> 1006 1324 for <span class=SpellE><b style='mso-bidi-font-weight:normal'><span 1007 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1325 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1008 1326 mso-hansi-theme-font:minor-latin'>Tmax</span></b></span>. You can also set the 1009 1327 limits using the cursor on the plot by either picking a point on the curve with … … 1012 1330 1013 1331 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1014 id=" Picture_x0020_22" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:225pt;1015 height:195pt;visibility:visible;mso-wrap-style:square'>1332 id="_x0000_i1037" type="#_x0000_t75" style='width:225pt;height:195pt; 1333 visibility:visible;mso-wrap-style:square'> 1016 1334 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image002.png" 1017 1335 o:title=""/> 1018 </v:shape><![endif]--><![if !vml]><img border=0width=300 height=2601019 src="Small%20Angle%20Size%20Distribution_files/image002.png" v:shapes=" Picture_x0020_22"><![endif]></span><span1336 </v:shape><![endif]--><![if !vml]><img width=300 height=260 1337 src="Small%20Angle%20Size%20Distribution_files/image002.png" v:shapes="_x0000_i1037"><![endif]></span><span 1020 1338 style='mso-spacerun:yes'> </span></p> 1021 1339 1022 1340 <h2>Step 3 Select the scattering substances for your sample</h2> 1023 1341 1024 <p class=MsoNormal><span style='mso-no-proof:yes'>Two scsttering substances 1025 need to be defined for your sample to give the anticipated scattering contrast; 1026 in this case one is alumina and the other is vacuum (really air). Parameters 1027 fora number of substances are defined in the file </span><b style='mso-bidi-font-weight:1028 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1342 <p class=MsoNormal><span style='mso-no-proof:yes'>Two scsttering substances need 1343 to be defined for your sample to give the anticipated scattering contrast; in 1344 this case one is alumina and the other is vacuum (really air). Parameters for 1345 a number of substances are defined in the file </span><b style='mso-bidi-font-weight: 1346 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1029 1347 minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span 1030 style='mso-no-proof:yes'>. You can add your own substances to this or better put1031 them in </span><b style='mso-bidi-font-weight:normal'><span style='font-family: 1032 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1033 m inor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span1348 style='mso-no-proof:yes'>. You can add your own substances to this or better 1349 put them in </span><b style='mso-bidi-font-weight:normal'><span 1350 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1351 mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span 1034 1352 style='mso-no-proof:yes'>; this is read after </span><b style='mso-bidi-font-weight: 1035 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1353 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1036 1354 minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span 1037 1355 style='mso-no-proof:yes'> when you load substances for your selection. </span>Select 1038 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1356 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1039 1357 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Substances</span></b> 1040 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1358 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1041 1359 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina 1042 1360 data.dat</span></b> from the GSAS-II tree. Then do <b style='mso-bidi-font-weight: 1043 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1044 minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Load</span></b> substance 1361 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1362 minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Load</span></b> <b 1363 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1364 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>substance</span></b> 1045 1365 from the menu; a popup window will appear with possible selections</p> 1046 1366 … … 1050 1370 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image003.png" 1051 1371 o:title=""/> 1052 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=3361372 </v:shape><![endif]--><![if !vml]><img width=346 height=336 1053 1373 src="Small%20Angle%20Size%20Distribution_files/image003.png" v:shapes="Picture_x0020_23"><![endif]><o:p></o:p></span></p> 1054 1374 … … 1056 1376 1057 1377 <p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span 1058 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1378 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1059 1379 mso-hansi-theme-font:minor-latin'>Alumina</span></b> and press <b 1060 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1380 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1061 1381 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>; 1062 1382 the relevant data for alumina (and vacuum) are displayed next</p> 1063 1383 1064 1384 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1065 id="Picture_x0020_ 24" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:259.5pt;1385 id="Picture_x0020_16" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:259.5pt; 1066 1386 height:195pt;visibility:visible;mso-wrap-style:square'> 1067 1387 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image004.png" 1068 1388 o:title=""/> 1069 </v:shape><![endif]--><![if !vml]><img border=0width=346 height=2601070 src="Small%20Angle%20Size%20Distribution_files/image004.png" v:shapes="Picture_x0020_ 24"><![endif]></span><span1389 </v:shape><![endif]--><![if !vml]><img width=346 height=260 1390 src="Small%20Angle%20Size%20Distribution_files/image004.png" v:shapes="Picture_x0020_16"><![endif]></span><span 1071 1391 style='mso-spacerun:yes'> </span></p> 1072 1392 … … 1078 1398 are given for each substance. These can each be edited; the other values will 1079 1399 change accordingly. If your substance isnt in the list, you can <b 1080 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1400 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1081 1401 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit/Add 1082 1402 substance</span></b> to create a new one (you will be asked for a name and the … … 1084 1404 scattering density and that as affected by resonant scattering for the listed 1085 1405 wavelength is displayed (the wavelength can be changed in the <b 1086 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1406 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1087 1407 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Instrument 1088 1408 Parameters</span></b> GSAS-II tree item if needed). The resonant scattering … … 1093 1413 <p class=MsoNormal>Two of the substances you have loaded into GSAS-II next need 1094 1414 to be selected for this size distribution analysis; Select <b style='mso-bidi-font-weight: 1095 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1415 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1096 1416 minor-latin;mso-hansi-theme-font:minor-latin'>Sample Parameters</span></b> 1097 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1417 under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1098 1418 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina 1099 1419 data.dat</span></b> from the GSAS-II tree. Near the bottom of the window will 1100 1420 be two rows marked <b style='mso-bidi-font-weight:normal'><span 1101 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1421 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1102 1422 mso-hansi-theme-font:minor-latin'>Material</span></b>; select <b 1103 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1423 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1104 1424 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Alumina</span></b> 1105 1425 from one of the pull downs (leave the other as <b style='mso-bidi-font-weight: 1106 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1426 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1107 1427 minor-latin;mso-hansi-theme-font:minor-latin'>vacuum</span></b>). The window 1108 1428 will show at the bottom the computed contrast between alumina and vacuum 1109 without and with consideration of resonant scattering effects; the latter is used1110 in subsequent calculations.</p>1429 without and with consideration of resonant scattering effects; the latter is 1430 used in subsequent calculations.</p> 1111 1431 1112 1432 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1113 id="Picture_x0020_ 25" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:305.25pt;1114 height: 369pt;visibility:visible;mso-wrap-style:square'>1433 id="Picture_x0020_17" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:305.25pt; 1434 height:408pt;visibility:visible;mso-wrap-style:square'> 1115 1435 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image005.png" 1116 1436 o:title=""/> 1117 </v:shape><![endif]--><![if !vml]><img border=0 width=407 height=4921118 src="Small%20Angle%20Size%20Distribution_files/image005.png" v:shapes="Picture_x0020_ 25"><![endif]></span></p>1437 </v:shape><![endif]--><![if !vml]><img width=407 height=544 1438 src="Small%20Angle%20Size%20Distribution_files/image005.png" v:shapes="Picture_x0020_17"><![endif]></span></p> 1119 1439 1120 1440 <p class=MsoNormal><o:p> </o:p></p> … … 1122 1442 <p class=MsoNormal>For experiments for which you know the transmission and the 1123 1443 sample thickness, you can manipulate the <b style='mso-bidi-font-weight:normal'><span 1124 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1444 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1125 1445 mso-hansi-theme-font:minor-latin'>volume fractions</span></b> to make the 1126 1446 calculated transmission match the observed one. Additionally, if you have 1127 1447 absolute scaling information, you can rescale the data by adjusting the <b 1128 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1448 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1129 1449 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>histogram 1130 1450 scale factor</span></b>; multiple data sets can be scaled together via the <b 1131 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1451 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1132 1452 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Command/Set 1133 1453 scale</span></b> menu item.</p> … … 1137 1457 <p class=MsoNormal>You are now ready to attempt a size distribution analysis 1138 1458 using the maximum entropy method. Select <b style='mso-bidi-font-weight:normal'><span 1139 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1459 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1140 1460 mso-hansi-theme-font:minor-latin'>Models</span></b> under <b style='mso-bidi-font-weight: 1141 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1461 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1142 1462 minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina data.dat</span></b> 1143 1463 from the GSAS-II tree; the window will display</p> 1144 1464 1145 1465 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1146 id="Picture_x0020_1 5" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:355.5pt;1466 id="Picture_x0020_18" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:361.5pt; 1147 1467 height:191.25pt;visibility:visible;mso-wrap-style:square'> 1148 1468 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image006.png" 1149 1469 o:title=""/> 1150 </v:shape><![endif]--><![if !vml]><img border=0 width=474height=2551151 src="Small%20Angle%20Size%20Distribution_files/image006.png" v:shapes="Picture_x0020_1 5"><![endif]></span></p>1470 </v:shape><![endif]--><![if !vml]><img width=482 height=255 1471 src="Small%20Angle%20Size%20Distribution_files/image006.png" v:shapes="Picture_x0020_18"><![endif]></span></p> 1152 1472 1153 1473 <p class=MsoNormal><o:p> </o:p></p> … … 1158 1478 1159 1479 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1160 id="Picture_x0020_ 27" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt;1480 id="Picture_x0020_19" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt; 1161 1481 height:450pt;visibility:visible;mso-wrap-style:square'> 1162 1482 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image007.png" 1163 1483 o:title=""/> 1164 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001165 src="Small%20Angle%20Size%20Distribution_files/image007.png" v:shapes="Picture_x0020_ 27"><![endif]></span><span1484 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1485 src="Small%20Angle%20Size%20Distribution_files/image007.png" v:shapes="Picture_x0020_19"><![endif]></span><span 1166 1486 style='mso-spacerun:yes'> </span></p> 1167 1487 … … 1170 1490 <p class=MsoNormal>It is clear that the intensity levels off at an apparent 1171 1491 background level of ~<b style='mso-bidi-font-weight:normal'><span 1172 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1492 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1173 1493 mso-hansi-theme-font:minor-latin'>0.12</span></b>; enter that into the 1174 1494 appropriate place in the data window. The plot will be redrawn showing a horizontal 1175 1495 red line for the background. All the other parameters seem reasonable for a 1<sup>st</sup> 1176 1496 attempt at a <span class=SpellE>MaxEnt</span> solution. Do <b style='mso-bidi-font-weight: 1177 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1497 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1178 1498 minor-latin;mso-hansi-theme-font:minor-latin'>Models/Fit</span></b>; the 1179 1499 console window will show that the calculation did not converge and the <b 1180 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1500 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1181 1501 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Size 1182 1502 Distribution</span></b> plot has a choppy appearance.</p> … … 1187 1507 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image008.png" 1188 1508 o:title=""/> 1189 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001509 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1190 1510 src="Small%20Angle%20Size%20Distribution_files/image008.png" v:shapes="Picture_x0020_28"><![endif]></span></p> 1191 1511 … … 1194 1514 <p class=MsoNormal>This is not a satisfactory result, but the suggestion given 1195 1515 in the console window is worth trying. Change the <b style='mso-bidi-font-weight: 1196 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1516 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1197 1517 minor-latin;mso-hansi-theme-font:minor-latin'>Error multiplier</span></b> to <b 1198 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1518 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1199 1519 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>5</span></b> 1200 1520 (notice the increased error bars on the data plot) and repeat <b 1201 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1521 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1202 1522 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Model/Fit</span></b>. 1203 1523 Convergence is now achieved in <10 cycles (see console window for details) … … 1209 1529 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image009.png" 1210 1530 o:title=""/> 1211 </v:shape><![endif]--><![if !vml]><img border=0width=700 height=6001531 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1212 1532 src="Small%20Angle%20Size%20Distribution_files/image009.png" v:shapes="Picture_x0020_29"><![endif]></span></p> 1213 1533 … … 1220 1540 <p class=MsoNormal>You may wish to explore the effect of some of the other 1221 1541 parameters in the data window. Most are obvious but <b style='mso-bidi-font-weight: 1222 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1542 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1223 1543 minor-latin;mso-hansi-theme-font:minor-latin'>Log floor factor</span></b> needs 1224 1544 a bit of explanation. This is the log of the minimum size distribution (scaled 1225 by the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1545 by the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1226 1546 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>histogram 1227 1547 scale factor</span></b> and the <b style='mso-bidi-font-weight:normal'><span 1228 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1548 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1229 1549 mso-hansi-theme-font:minor-latin'>contrast</span></b>). This size distribution 1230 1550 minimum needs to be set within 1-2 orders of magnitude of the optimal value and … … 1235 1555 1236 1556 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1237 id="Picture_x0020_ 30" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:621.75pt;1557 id="Picture_x0020_20" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt; 1238 1558 height:450pt;visibility:visible;mso-wrap-style:square'> 1239 1559 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image010.png" 1240 1560 o:title=""/> 1241 </v:shape><![endif]--><![if !vml]><img border=0 width=829height=6001242 src="Small%20Angle%20Size%20Distribution_files/image010.png" v:shapes="Picture_x0020_ 30"><![endif]></span></p>1561 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1562 src="Small%20Angle%20Size%20Distribution_files/image010.png" v:shapes="Picture_x0020_20"><![endif]></span></p> 1243 1563 1244 1564 <p class=MsoNormal><o:p> </o:p></p> … … 1258 1578 a gradient refinement method for the special case of all positive data and 1259 1579 parameter values. To try it on this alumina data, select <b style='mso-bidi-font-weight: 1260 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1580 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1261 1581 minor-latin;mso-hansi-theme-font:minor-latin'>IPG</span></b> from the <b 1262 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1582 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1263 1583 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Fitting 1264 1584 method</span></b> pull down. The data window will change to give</p> 1265 1585 1266 1586 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1267 id="Picture_x0020_ 16" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:375.75pt;1587 id="Picture_x0020_21" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:375.75pt; 1268 1588 height:191.25pt;visibility:visible;mso-wrap-style:square'> 1269 1589 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image011.png" 1270 1590 o:title=""/> 1271 </v:shape><![endif]--><![if !vml]><img border=0width=501 height=2551272 src="Small%20Angle%20Size%20Distribution_files/image011.png" v:shapes="Picture_x0020_ 16"><![endif]></span></p>1591 </v:shape><![endif]--><![if !vml]><img width=501 height=255 1592 src="Small%20Angle%20Size%20Distribution_files/image011.png" v:shapes="Picture_x0020_21"><![endif]></span></p> 1273 1593 1274 1594 <p class=MsoNormal><o:p> </o:p></p> 1275 1595 1276 1596 <p class=MsoNormal>Reset the Error multiplier back to <b style='mso-bidi-font-weight: 1277 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1597 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1278 1598 minor-latin;mso-hansi-theme-font:minor-latin'>1.0</span></b> and then do <b 1279 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1599 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1280 1600 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Fit</span></b> 1281 1601 to run the IPG fitting. The IPG algorithm did not converge in 100 cycles and … … 1288 1608 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image012.png" 1289 1609 o:title=""/> 1290 </v:shape><![endif]--><![if !vml]><img border=0width=829 height=6001610 </v:shape><![endif]--><![if !vml]><img width=829 height=600 1291 1611 src="Small%20Angle%20Size%20Distribution_files/image012.png" v:shapes="Picture_x0020_289"><![endif]></span></p> 1292 1612 … … 1294 1614 1295 1615 <p class=MsoNormal>This can be considerably improved by setting the <b 1296 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1616 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1297 1617 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Error 1298 1618 multiplier</span></b> to <b style='mso-bidi-font-weight:normal'><span 1299 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1619 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1300 1620 mso-hansi-theme-font:minor-latin'>2.0</span></b>; the IPG fit con<span 1301 1621 style='mso-no-proof:yes'>verges in <20 cycles and gives a smoother size … … 1307 1627 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image013.png" 1308 1628 o:title=""/> 1309 </v:shape><![endif]--><![if !vml]><img border=0width=829 height=6001629 </v:shape><![endif]--><![if !vml]><img width=829 height=600 1310 1630 src="Small%20Angle%20Size%20Distribution_files/image013.png" v:shapes="Picture_x0020_291"><![endif]></span></p> 1311 1631 … … 1318 1638 1319 1639 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1320 id="Picture_x0020_2 92" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:621.75pt;1640 id="Picture_x0020_22" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt; 1321 1641 height:450pt;visibility:visible;mso-wrap-style:square'> 1322 1642 <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image014.png" 1323 1643 o:title=""/> 1324 </v:shape><![endif]--><![if !vml]><img border=0 width=829height=6001325 src="Small%20Angle%20Size%20Distribution_files/image014.png" v:shapes="Picture_x0020_2 92"><![endif]></span></p>1644 </v:shape><![endif]--><![if !vml]><img width=700 height=600 1645 src="Small%20Angle%20Size%20Distribution_files/image014.png" v:shapes="Picture_x0020_22"><![endif]></span></p> 1326 1646 1327 1647 <p class=MsoNormal><o:p> </o:p></p> … … 1329 1649 <p class=MsoNormal>You may wish to explore the other parameters for the IPG 1330 1650 fitting. If <b style='mso-bidi-font-weight:normal'><span style='font-family: 1331 "Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1651 "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1332 1652 minor-latin'>Q power weight</span></b> is set to <b style='mso-bidi-font-weight: 1333 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1653 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1334 1654 minor-latin;mso-hansi-theme-font:minor-latin'>0-4</span></b>, that changes the 1335 1655 data weighting to <span class=SpellE><span class=GramE>Q<sup>p</sup></span></span>. 1336 1656 This can change the convergence of the IPG method and yield improved results if 1337 1657 one is unsuccessful with the default settings. I got a nice fit with a <b 1338 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1658 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1339 1659 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Q power 1340 1660 weight</span></b> of <b style='mso-bidi-font-weight:normal'><span 1341 style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:minor-latin;1661 style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; 1342 1662 mso-hansi-theme-font:minor-latin'>3</span></b> and <b style='mso-bidi-font-weight: 1343 normal'><span style='font-family:"Calibri", "sans-serif";mso-ascii-theme-font:1663 normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: 1344 1664 minor-latin;mso-hansi-theme-font:minor-latin'>Error multiplier</span></b> of <b 1345 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri", "sans-serif";1665 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1346 1666 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>2.0</span></b>.</p> 1347 1667 1348 <p class=MsoNormal>You should save this GSAS-II project as it will be used in 1349 the tutorial for fitting small angle scattering data; I used <span 1350 class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: 1351 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1352 minor-latin'>alumina.gpx</span></b></span>.</p> 1668 <p class=MsoNormal>You should save this GSAS-II project as it will be used in the 1669 tutorial for fitting small angle scattering data; I used <span class=SpellE><b 1670 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; 1671 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>alumina.gpx</span></b></span>.</p> 1353 1672 1354 1673 </div>
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