Changeset 1349
- Timestamp:
- May 15, 2014 10:45:46 AM (9 years ago)
- Location:
- trunk
- Files:
-
- 4 edited
Legend:
- Unmodified
- Added
- Removed
-
trunk/GSASIIplot.py
r1344 r1349 660 660 def OnRelease(event): 661 661 if G2frame.itemPicked is None: return 662 if DifLine[0] .get_label() in str(G2frame.itemPicked):662 if DifLine[0] and DifLine[0].get_label() in str(G2frame.itemPicked): 663 663 ypos = event.ydata 664 664 G2frame.delOffset = -ypos/Ymax … … 937 937 X += G2frame.Offset[1]*.005*N 938 938 Xum = ma.getdata(X) 939 939 DifLine = [''] 940 940 if ifpicked: 941 941 Z = xye[3]+offset*N -
trunk/GSASIIpwdGUI.py
r1339 r1349 1400 1400 refData = [refProfile,refLimits,refSample] 1401 1401 G2sasd.SetScale(Data,refData) 1402 G2plt.PlotPatterns(G2frame,plotType='SASD',newPlot=True) 1402 1403 UpdateSampleGrid(G2frame,data) 1403 G2plt.PlotPatterns(G2frame,plotType='SASD',newPlot=False)1404 1404 1405 1405 def OnSampleCopy(event): … … 1483 1483 sampleData.update(copy.deepcopy(copyDict)) 1484 1484 finally: 1485 dlg.Destroy() 1485 dlg.Destroy() 1486 G2plt.PlotPatterns(G2frame,plotType='SASD',newPlot=False) 1486 1487 1487 1488 def OnSampleFlagCopy(event): -
trunk/help/Small Angle Image Processing.htm
r1346 r1349 24 24 <o:Author>Von Dreele</o:Author> 25 25 <o:LastAuthor>Von Dreele</o:LastAuthor> 26 <o:Revision> 9</o:Revision>27 <o:TotalTime>2 395</o:TotalTime>26 <o:Revision>10</o:Revision> 27 <o:TotalTime>2411</o:TotalTime> 28 28 <o:Created>2014-05-13T20:30:00Z</o:Created> 29 <o:LastSaved>2014-05-1 4T21:32:00Z</o:LastSaved>29 <o:LastSaved>2014-05-15T15:43:00Z</o:LastSaved> 30 30 <o:Pages>18</o:Pages> 31 <o:Words> 1995</o:Words>32 <o:Characters>11 378</o:Characters>31 <o:Words>2004</o:Words> 32 <o:Characters>11426</o:Characters> 33 33 <o:Company>Argonne National Laboratory</o:Company> 34 <o:Lines>9 4</o:Lines>34 <o:Lines>95</o:Lines> 35 35 <o:Paragraphs>26</o:Paragraphs> 36 <o:CharactersWithSpaces>13 347</o:CharactersWithSpaces>36 <o:CharactersWithSpaces>13404</o:CharactersWithSpaces> 37 37 <o:Version>14.00</o:Version> 38 38 </o:DocumentProperties> … … 42 42 </xml><![endif]--> 43 43 <link rel=dataStoreItem 44 href="Small%20Angle%20Image%20Processing_files/item00 33.xml"45 target="Small%20Angle%20Image%20Processing_files/props0 34.xml">44 href="Small%20Angle%20Image%20Processing_files/item0048.xml" 45 target="Small%20Angle%20Image%20Processing_files/props049.xml"> 46 46 <link rel=themeData 47 47 href="Small%20Angle%20Image%20Processing_files/themedata.thmx"> … … 392 392 font-weight:bold;} 393 393 h2 394 {mso-style-priority:9; 394 {mso-style-noshow:yes; 395 mso-style-priority:9; 395 396 mso-style-qformat:yes; 396 397 mso-style-link:"Heading 2 Char"; … … 468 469 font-weight:bold;} 469 470 a:link, span.MsoHyperlink 470 {mso-style-priority:99; 471 {mso-style-noshow:yes; 472 mso-style-priority:99; 471 473 color:blue; 472 474 text-decoration:underline; … … 637 639 span.Heading2Char 638 640 {mso-style-name:"Heading 2 Char"; 641 mso-style-noshow:yes; 639 642 mso-style-priority:9; 640 643 mso-style-unhide:no; … … 839 842 this tutorial you will reduce 2D SAXS data to create 1D absolute scaled data. 840 843 The data were collected at APS on beam line 15ID on some polymer base materials 841 to be used for liquid crystal displays. The processing has several steps including842 detector calibration (i.e. determine sample-detector distance & tilt), 843 integration and scaling to an absolute scaled glassy carbon measurement. The 844 data were collected at a wavelength of 1.0332Å with a <span class=SpellE>MarCCD</span>844 to be used for liquid crystal displays. The processing has several steps 845 including detector calibration (i.e. determine sample-detector distance & 846 tilt), integration and scaling to an absolute scaled glassy carbon measurement. 847 The data were collected at a wavelength of 1.0332Å with a <span class=SpellE>MarCCD</span> 845 848 detector placed ~570mm from the sample. Note that menu entries are listed in 846 849 bold face below as <b style='mso-bidi-font-weight:normal'><span … … 891 894 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> 892 895 <o:lock v:ext="edit" aspectratio="t"/> 893 </v:shapetype><v:shape id=" _x0000_i1065" type="#_x0000_t75" style='width:537pt;894 height:397.5pt;visibility:visible;mso-wrap-style:square'>896 </v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1065" type="#_x0000_t75" 897 style='width:537pt;height:397.5pt;visibility:visible;mso-wrap-style:square'> 895 898 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image001.png" 896 899 o:title=""/> 897 900 </v:shape><![endif]--><![if !vml]><img border=0 width=716 height=530 898 src="Small%20Angle%20Image%20Processing_files/image001.png" v:shapes=" _x0000_i1065"><![endif]></span></p>901 src="Small%20Angle%20Image%20Processing_files/image001.png" v:shapes="Picture_x0020_1"><![endif]></span></p> 899 902 900 903 <p class=MsoNormal><o:p> </o:p></p> … … 905 908 and select <b style='mso-bidi-font-weight:normal'><span style='font-family: 906 909 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 907 minor-latin'>AgBehenate_003.tif</span></b> with either a mouse button double click908 or <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";910 minor-latin'>AgBehenate_003.tif</span></b> with either a mouse button double 911 click or <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 909 912 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Open</span></b>; 910 913 the image will appear</p> … … 925 928 926 929 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 927 id=" _x0000_i1063" type="#_x0000_t75" style='width:472.5pt;height:388.5pt;928 visibility:visible;mso-wrap-style:square'>930 id="Picture_x0020_3" o:spid="_x0000_i1063" type="#_x0000_t75" style='width:472.5pt; 931 height:388.5pt;visibility:visible;mso-wrap-style:square'> 929 932 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image003.png" 930 933 o:title=""/> 931 934 </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 932 src="Small%20Angle%20Image%20Processing_files/image003.png" v:shapes=" _x0000_i1063"><![endif]></span></p>935 src="Small%20Angle%20Image%20Processing_files/image003.png" v:shapes="Picture_x0020_3"><![endif]></span></p> 933 936 934 937 <p class=MsoNormal><o:p> </o:p></p> … … 966 969 You should move the <b style='mso-bidi-font-weight:normal'><span 967 970 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 968 mso-hansi-theme-font:minor-latin'>Max intensity</span></b> slider to near the 969 middle of the range that will improve the image. When done the <b 970 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 971 m so-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image972 controls</span></b> windowshould look like</p>973 974 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 975 id=" _x0000_i1062" type="#_x0000_t75" style='width:472.5pt;height:388.5pt;976 visibility:visible;mso-wrap-style:square'>971 mso-hansi-theme-font:minor-latin'>Max intensity</span></b> slider to near the middle 972 of the range that will improve the image. When done the <b style='mso-bidi-font-weight: 973 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 974 minor-latin;mso-hansi-theme-font:minor-latin'>Image controls</span></b> window 975 should look like</p> 976 977 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 978 id="Picture_x0020_4" o:spid="_x0000_i1062" type="#_x0000_t75" style='width:472.5pt; 979 height:388.5pt;visibility:visible;mso-wrap-style:square'> 977 980 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image004.png" 978 981 o:title=""/> 979 982 </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 980 src="Small%20Angle%20Image%20Processing_files/image004.png" v:shapes=" _x0000_i1062"><![endif]></span></p>983 src="Small%20Angle%20Image%20Processing_files/image004.png" v:shapes="Picture_x0020_4"><![endif]></span></p> 981 984 982 985 <p class=MsoNormal><o:p> </o:p></p> … … 1007 1010 22YiTra2kYMu1l1tQD30/bPm3wwYN0x18gb45AdQl1tp5j/sFB2T0FQ7R0nTNEV3j6o9feQzro1i 1008 1011 OWA14Fm+Q8a1a8+Bvu/d/dMb2JY5uiPbhG/ktn4cqGU/er3pcvwCAAD//wMAUEsDBBQABgAIAAAA 1009 IQB C+GEV6wEAACkEAAAOAAAAZHJzL2Uyb0RvYy54bWysU02P0zAQvSPxHyzfadIgKoiarlAXuKxg1010 RYG717EbC9tjjU2T/nvGThs+pZUQFyv2zHsz781kezM5y04KowHf8fWq5kx5Cb3xx45//vT22UvO 1011 YhK+Fxa86vhZRX6ze/pkO4ZWNTCA7RUyIvGxHUPHh5RCW1VRDsqJuIKgPAU1oBOJrnisehQjsTtb 1012 NXW9qUbAPiBIFSO93s5Bviv8WiuZPmgdVWK249RbKieW8yGf1W4r2iOKMBh5aUP8QxdOGE9FF6pb 1013 kQT7huYPKmckQgSdVhJcBVobqYoGUrOuf1NzGERQRQuZE8NiU/x/tPL96R6Z6TverDnzwtGMDgmF 1014 OQ6JvUaEke3Be/IRkFEK+TWG2BJs7+8xK5aTP4Q7kF8jxapfgvkSw5w2aXRMWxO+0JoUq0g8m8ok 1015 zssk1JSYpMdN/WpT07wkhWjMdfMiV65Em2ly1YAxvVPgWP7oeLy0vPQ6lxCnu5hm4BWQwdbnMwlj 1016 3/iepXMg0SJrvRTJ8aJkbr7ISGerZuxHpckwavJ5kVFWVe0tspOgJRNSKp+ahYmyM0wbaxdg/Tjw 1017 kp+hqqzxAm4eBy+IUhl8WsDOeMC/EaSpzJYc1nP+1YFZd7bgAfrzPV6HTPtYBnL5d/LC/3wv8B9/ 1018 +O47AAAA//8DAFBLAwQUAAYACAAAACEAgdKpXd8AAAALAQAADwAAAGRycy9kb3ducmV2LnhtbEyP1012 IQB9d1Df6wEAACkEAAAOAAAAZHJzL2Uyb0RvYy54bWysU02P0zAQvSPxHyzfadIAFURNV6gLXFZQ 1013 bYG717EbC8djjU2T/nvGTho+pZUQl1Hs8Xsz781kezP2lp0VBgOu4etVyZlyElrjTg3//Onds1ec 1014 hShcKyw41fCLCvxm9/TJdvC1qqAD2ypkROJCPfiGdzH6uiiC7FQvwgq8cpTUgL2IdMRT0aIYiL23 1015 RVWWm2IAbD2CVCHQ7e2U5LvMr7WS8aPWQUVmG069xRwxx4cUi91W1CcUvjNybkP8Qxe9MI6KLlS3 1016 Igr2Dc0fVL2RCAF0XEnoC9DaSJU1kJp1+ZuaYye8ylrInOAXm8L/o5Ufzgdkpm34i4ozJ3qa0TGi 1017 MKcusjeIMLA9OEc+ArJqnfwafKgJtncHTIrl6I7+DuTXQLnil2Q6BD89GzX2TFvjv9CaZKtIPBvz 1018 JC7LJNQYmaTLTfl6U9K8JKVozGX1MlUuRJ1oUlWPIb5X0LP00fAwt7z0OpUQ57sQJ+AVkMDWpRiF 1019 sW9dy+LFk2iRtM5FUj4rmZrPMuLFqgl7rzQZRk0+zzLyqqq9RXYWtGRCSuVitTDR6wTTxtoFWD4O 1020 nN8nqMprvICrx8ELIlcGFxdwbxzg3wjimGdLDuvp/dWBSXey4AHaywGvQ6Z9zAOZ/5208D+fM/zH 1021 H777DgAA//8DAFBLAwQUAAYACAAAACEAgdKpXd8AAAALAQAADwAAAGRycy9kb3ducmV2LnhtbEyP 1019 1022 wU7DMBBE70j8g7VI3KjTklQQ4lQVohfEpS1FHLfxkgTidRS7Tfh7lhPc3mhHszPFanKdOtMQWs8G 1020 1023 5rMEFHHlbcu1gdf95uYOVIjIFjvPZOCbAqzKy4sCc+tH3tJ5F2slIRxyNNDE2Odah6ohh2Hme2K5 … … 1023 1026 AAYACAAAACEAtoM4kv4AAADhAQAAEwAAAAAAAAAAAAAAAAAAAAAAW0NvbnRlbnRfVHlwZXNdLnht 1024 1027 bFBLAQItABQABgAIAAAAIQA4/SH/1gAAAJQBAAALAAAAAAAAAAAAAAAAAC8BAABfcmVscy8ucmVs 1025 c1BLAQItABQABgAIAAAAIQB C+GEV6wEAACkEAAAOAAAAAAAAAAAAAAAAAC4CAABkcnMvZTJvRG9j1028 c1BLAQItABQABgAIAAAAIQB9d1Df6wEAACkEAAAOAAAAAAAAAAAAAAAAAC4CAABkcnMvZTJvRG9j 1026 1029 LnhtbFBLAQItABQABgAIAAAAIQCB0qld3wAAAAsBAAAPAAAAAAAAAAAAAAAAAEUEAABkcnMvZG93 1027 1030 bnJldi54bWxQSwUGAAAAAAQABADzAAAAUQUAAAAA … … 1033 1036 absolute;z-index:251659264;margin-left:234px;margin-top:274px;width:73px; 1034 1037 height:38px'><img width=73 height=38 1035 src="Small%20Angle%20Image%20Processing_files/image005.png" v:shapes="Straight_x0020_Arrow_x0020_Connector_x0020_21"></span><![endif]><span 1036 style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="_x0000_i1061" type="#_x0000_t75" 1037 style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'> 1038 src="Small%20Angle%20Image%20Processing_files/image012.png" v:shapes="Straight_x0020_Arrow_x0020_Connector_x0020_21"></span><![endif]><span 1039 style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_5" 1040 o:spid="_x0000_i1061" type="#_x0000_t75" style='width:525pt;height:450pt; 1041 visibility:visible;mso-wrap-style:square'> 1038 1042 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image006.png" 1039 1043 o:title=""/> 1040 1044 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 1041 src="Small%20Angle%20Image%20Processing_files/image006.png" v:shapes=" _x0000_i1061"><![endif]></span></p>1045 src="Small%20Angle%20Image%20Processing_files/image006.png" v:shapes="Picture_x0020_5"><![endif]></span></p> 1042 1046 1043 1047 <p class=MsoNormal><o:p> </o:p></p> … … 1059 1063 mso-hansi-theme-font:minor-latin'>Image Controls</span></b> window). The <b 1060 1064 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1061 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 1062 Controls</span></b>window will show the results of the calibration</p>1063 1064 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1065 id=" _x0000_i1060" type="#_x0000_t75" style='width:472.5pt;height:388.5pt;1066 visibility:visible;mso-wrap-style:square'>1065 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> 1066 window will show the results of the calibration</p> 1067 1068 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1069 id="Picture_x0020_6" o:spid="_x0000_i1060" type="#_x0000_t75" style='width:472.5pt; 1070 height:388.5pt;visibility:visible;mso-wrap-style:square'> 1067 1071 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image007.png" 1068 1072 o:title=""/> 1069 1073 </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 1070 src="Small%20Angle%20Image%20Processing_files/image007.png" v:shapes=" _x0000_i1060"><![endif]></span></p>1074 src="Small%20Angle%20Image%20Processing_files/image007.png" v:shapes="Picture_x0020_6"><![endif]></span></p> 1071 1075 1072 1076 <p class=MsoNormal><o:p> </o:p></p> … … 1085 1089 <p class=MsoNormal><o:p> </o:p></p> 1086 1090 1087 <p class=MsoNormal>You would like to use more points from just the visible rings.1088 I suggest you change <b style='mso-bidi-font-weight:normal'><span1091 <p class=MsoNormal>You would like to use more points from just the visible 1092 rings. I suggest you change <b style='mso-bidi-font-weight:normal'><span 1089 1093 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1090 1094 mso-hansi-theme-font:minor-latin'>Min ring I/<span class=SpellE><span … … 1103 1107 1104 1108 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1105 id=" _x0000_i1058" type="#_x0000_t75" style='width:525pt;height:450pt;1106 visibility:visible;mso-wrap-style:square'>1109 id="Picture_x0020_8" o:spid="_x0000_i1058" type="#_x0000_t75" style='width:525pt; 1110 height:450pt;visibility:visible;mso-wrap-style:square'> 1107 1111 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image009.png" 1108 1112 o:title=""/> 1109 1113 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 1110 src="Small%20Angle%20Image%20Processing_files/image009.png" v:shapes=" _x0000_i1058"><![endif]></span></p>1114 src="Small%20Angle%20Image%20Processing_files/image009.png" v:shapes="Picture_x0020_8"><![endif]></span></p> 1111 1115 1112 1116 <p class=MsoNormal><o:p> </o:p></p> … … 1395 1399 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. 1396 1400 Next go <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1397 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>to IMG Sa3_40s_059.tif</span></b>1398 and change <b style='mso-bidi-font-weight:normal'><span style='font-family: 1399 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1400 m inor-latin'>transmission</span></b> to <b style='mso-bidi-font-weight:normal'><span1401 style=' font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;1402 mso- hansi-theme-font:minor-latin'>0.960</span></b>; <b style='mso-bidi-font-weight:1403 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1404 m inor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> to <b1405 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";1401 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>to IMG 1402 Sa3_40s_059.tif</span></b> and change <b style='mso-bidi-font-weight:normal'><span 1403 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1404 mso-hansi-theme-font:minor-latin'>transmission</span></b> to <b 1405 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1406 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.960</span></b>; 1407 <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1408 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> 1409 to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1406 1410 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. 1407 1411 Finally, go to <b style='mso-bidi-font-weight:normal'><span style='font-family: … … 1418 1422 The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1419 1423 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image 1420 Controls</span></b> data window for this should look like< o:p></o:p></p>1424 Controls</span></b> data window for this should look like</p> 1421 1425 1422 1426 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1426 1430 o:title=""/> 1427 1431 </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 1428 src="Small%20Angle%20Image%20Processing_files/image020.png" v:shapes="Picture_x0020_38"><![endif]></span>< o:p></o:p></p>1432 src="Small%20Angle%20Image%20Processing_files/image020.png" v:shapes="Picture_x0020_38"><![endif]></span></p> 1429 1433 1430 1434 <p class=MsoNormal><o:p> </o:p></p> … … 1440 1444 directory. </p> 1441 1445 1442 <p class=MsoNormal>As noted earlier, th is image containssome unwanted features;1446 <p class=MsoNormal>As noted earlier, the images contain some unwanted features; 1443 1447 so lets create masks to remove them. Select <b style='mso-bidi-font-weight: 1444 1448 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: … … 1475 1479 o:title=""/> 1476 1480 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 1477 src="Small%20Angle%20Image%20Processing_files/image022.png" v:shapes="Picture_x0020_30"><![endif]></span>< o:p></o:p></p>1481 src="Small%20Angle%20Image%20Processing_files/image022.png" v:shapes="Picture_x0020_30"><![endif]></span></p> 1478 1482 1479 1483 <p class=MsoNormal><o:p> </o:p></p> … … 1541 1545 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> 1542 1546 data window, you can change the angular range of the arc by dragging either end 1543 of the arc, and you can move the arc <span1544 style='mso-spacerun:yes'> </span>along a constant 2Θ angle by dragging on any 1545 point inside the mask. The curvature is centered on the beam center position and 1546 follows a constant 2Θ curve established by the detector calibration.<span 1547 style='mso-no-proof:yes'> <!--[if gte vml 1]><v:shape id="Picture_x0020_34"1548 o:spid="_x0000_i1042" type="#_x0000_t75" style='width:525pt;height:450pt;1549 visibility:visible;mso-wrap-style:square'>1547 of the arc, and you can move the arc<span style='mso-spacerun:yes'> 1548 </span>along a constant 2Θ angle by dragging on any point inside the mask. 1549 The curvature is centered on the beam center position and follows a constant 1550 2Θ curve established by the detector calibration.<span style='mso-no-proof: 1551 yes'> <!--[if gte vml 1]><v:shape id="Picture_x0020_34" o:spid="_x0000_i1042" 1552 type="#_x0000_t75" style='width:525pt;height:450pt;visibility:visible; 1553 mso-wrap-style:square'> 1550 1554 <v:imagedata src="Small%20Angle%20Image%20Processing_files/image026.png" 1551 1555 o:title=""/> … … 1556 1560 1557 1561 <p class=MsoNormal>Next lets deal with the beam stop. Im going to use both a 1558 polygon and a spot to cover it. Move the zoom area to be around the center, make1559 sure the zoom buttons are off, enter <b style='mso-bidi-font-weight:normal'><span1562 polygon and a spot to cover it. Move the zoom area to be around the center, 1563 make sure the zoom buttons are off, enter <b style='mso-bidi-font-weight:normal'><span 1560 1564 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1561 1565 mso-hansi-theme-font:minor-latin'>s</span></b> on the plot and press mouse <b … … 1658 1662 1659 1663 <p class=MsoNormal>We are now ready to integrate the glassy carbon and the four 1660 <span class=GramE>Sa</span> images. Select any Image Controls and then do 1661 Operations/Integrate all. A selection dialog will appear; select only the GC 1662 and Sa1-Sa4 data sets and press Ok. The image integration will proceed; a 1663 progress bar shows as each one is done. Five SASD data items will appear on the 1664 GSAS-II data tree; the last one (<b style='mso-bidi-font-weight:normal'><span 1664 <span class=GramE>Sa</span> images. Select any <b style='mso-bidi-font-weight: 1665 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1666 minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> and 1667 then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1668 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Integrate 1669 all</span></b>. A selection dialog will appear; select only the GC and Sa1-Sa4 1670 data sets and press Ok. The image integration will proceed; a progress bar 1671 shows as each one is done. Five SASD data items will appear on the GSAS-II data 1672 tree; the last one (<b style='mso-bidi-font-weight:normal'><span 1665 1673 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1666 1674 mso-hansi-theme-font:minor-latin'>SASD Sa4_40s_061.tif <span class=SpellE>Azm</span>=45.00</span></b>) 1667 will be expanded and plotted.</p> 1675 will be expanded and plotted (you may have to select the <b style='mso-bidi-font-weight: 1676 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1677 minor-latin;mso-hansi-theme-font:minor-latin'>Powder Patterns</span></b> tab to 1678 see it).</p> 1668 1679 1669 1680 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1677 1688 <p class=MsoNormal><o:p> </o:p></p> 1678 1689 1679 <p class=MsoNormal>Pretty obviously the SASD pattern is down to background at Q~0.25Å<sup>-1</sup>;1680 the other Sa1-Sa4 patterns are similar. The glassy carbon pattern extends 1681 nicely to the highest Q (~1.0Å<sup>-1</sup>) measured.</p>1690 <p class=MsoNormal>Pretty obviously the SASD pattern is down to background at 1691 Q~0.25Å<sup>-1</sup>; the other Sa1-Sa4 patterns are similar. The glassy carbon 1692 pattern extends nicely to the highest Q (~1.0Å<sup>-1</sup>) measured.</p> 1682 1693 1683 1694 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1787 1798 mso-hansi-theme-font:minor-latin'>Ok</span></b>; the <b style='mso-bidi-font-weight: 1788 1799 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1789 minor-latin;mso-hansi-theme-font:minor-latin'>GC_5s_200.tif</span></b> data 1790 willbe rescaled to the <b style='mso-bidi-font-weight:normal'><span1800 minor-latin;mso-hansi-theme-font:minor-latin'>GC_5s_200.tif</span></b> data will 1801 be rescaled to the <b style='mso-bidi-font-weight:normal'><span 1791 1802 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1792 1803 mso-hansi-theme-font:minor-latin'>GC calibrated data</span></b> and the <b … … 1818 1829 mso-hansi-theme-font:minor-latin'>Sample Parameters</span></b> menu; a <b 1819 1830 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1820 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Select 1821 sampleparameters</span></b> dialog will appear</p>1831 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Select sample 1832 parameters</span></b> dialog will appear</p> 1822 1833 1823 1834 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1869 1880 <p class=MsoNormal>Ive changed the zoom to show all the data. We are not quite 1870 1881 done; the scales for the Sa1-Sa4 data sets have to be further reduced by a 1871 factor of 8 to account for the longer exposure time. Select SASD 1872 Sa1_40s_067.tif from the GSAS-II data tree, expand it and choose Sample 1873 Parameters</p> 1882 factor of 8 to account for the longer exposure time. Select <b 1883 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1884 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD 1885 Sa1_40s_067.tif</span></b> from the GSAS-II data tree, expand it and choose <b 1886 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1887 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sample 1888 Parameters</span></b></p> 1874 1889 1875 1890 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1879 1894 o:title=""/> 1880 1895 </v:shape><![endif]--><![if !vml]><img border=0 width=389 height=518 1881 src="Small%20Angle%20Image%20Processing_files/image041.png" v:shapes="Picture_x0020_49"><![endif]></span>< o:p></o:p></p>1896 src="Small%20Angle%20Image%20Processing_files/image041.png" v:shapes="Picture_x0020_49"><![endif]></span></p> 1882 1897 1883 1898 <p class=MsoNormal><o:p> </o:p></p> 1884 1899 1885 1900 <p class=MsoNormal>The data items here can take simple mathematical expressions 1886 so change Histogram scale factor to 0.0008536/8 and press Enter. The value will 1887 change to 0.0001067 and the plot redrawn.</p> 1901 so change <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1902 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Histogram 1903 scale factor</span></b> to <b style='mso-bidi-font-weight:normal'><span 1904 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1905 mso-hansi-theme-font:minor-latin'>0.0008536/8</span></b> and press <b 1906 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1907 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Enter</span></b>. 1908 The value will change to <b style='mso-bidi-font-weight:normal'><span 1909 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1910 mso-hansi-theme-font:minor-latin'>0.0001067</span></b> and the plot redrawn.</p> 1888 1911 1889 1912 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape … … 1897 1920 <p class=MsoNormal><o:p> </o:p></p> 1898 1921 1899 <p class=MsoNormal>Next do Command/Copy selected as before to copy this new 1900 scale factor to the other <span class=GramE>Sa</span> data sets. The plot will 1901 again be redrawn</p> 1922 <p class=MsoNormal>Next do <b style='mso-bidi-font-weight:normal'><span 1923 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1924 mso-hansi-theme-font:minor-latin'>Command/Copy selected</span></b> as before to 1925 copy this new scale factor to the other <span class=GramE>Sa</span> data sets. 1926 The plot will again be redrawn</p> 1902 1927 1903 1928 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape -
trunk/help/Small Angle Image Processing_files/filelist.xml
r1346 r1349 1 1 <xml xmlns:o="urn:schemas-microsoft-com:office:office"> 2 2 <o:MainFile HRef="../Small%20Angle%20Image%20Processing.htm"/> 3 <o:File HRef="item00 33.xml"/>4 <o:File HRef="props0 34.xml"/>3 <o:File HRef="item0048.xml"/> 4 <o:File HRef="props049.xml"/> 5 5 <o:File HRef="themedata.thmx"/> 6 6 <o:File HRef="colorschememapping.xml"/> … … 9 9 <o:File HRef="image003.png"/> 10 10 <o:File HRef="image004.png"/> 11 <o:File HRef="image0 05.png"/>11 <o:File HRef="image012.png"/> 12 12 <o:File HRef="image006.png"/> 13 13 <o:File HRef="image007.png"/>
Note: See TracChangeset
for help on using the changeset viewer.