Changeset 1114


Ignore:
Timestamp:
Oct 18, 2013 3:53:58 PM (8 years ago)
Author:
toby
Message:

fix help error by reverting and editing html by hand

File:
1 edited

Legend:

Unmodified
Added
Removed
  • trunk/help/Calibration of an area detector in GSAS.htm

    r1112 r1114  
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    66
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    9 <meta name=Keywords content="">
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    2624 <o:DocumentProperties>
    2725  <o:Author>Von Dreele</o:Author>
    28   <o:LastAuthor>B Toby</o:LastAuthor>
    29   <o:Revision>15</o:Revision>
    30   <o:TotalTime>143</o:TotalTime>
     26  <o:LastAuthor>Von Dreele</o:LastAuthor>
     27  <o:Revision>14</o:Revision>
     28  <o:TotalTime>137</o:TotalTime>
    3129  <o:Created>2012-05-04T19:00:00Z</o:Created>
    32   <o:LastSaved>2013-10-17T14:38:00Z</o:LastSaved>
     30  <o:LastSaved>2013-04-30T17:13:00Z</o:LastSaved>
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    3634  <o:Company>Argonne National Laboratory</o:Company>
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    847833
    848834<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
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     835href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
     836text-underline:none'>start GSAS-II</span></a></span></u>.</p>
    851837
    852838<h1>Step 1: read in the data file</h1>
    853839
    854 <p class=MsoNormal><span style="mso-spacerun:yes"> </span>Use the <b
     840<p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the <b
    855841style='mso-bidi-font-weight:normal'>Data/Read image data</b> menu item to read
    856842the data file into the current GSAS-II project. </p>
    857843
    858 <p class=MsoNormal><span style="mso-spacerun:yes"> </span></p>
     844<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
    859845
    860846<p class=MsoNormal>A file selection dialog will be shown; its appearance will
    861847depend on your OS. Change the search directory to <b style='mso-bidi-font-weight:
    862 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin;
    863 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:
    864 minor-latin'>/Exercises/images</span></b> and then select the file </p>
     848normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     849minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
     850mso-bidi-theme-font:minor-latin'>/Exercises/images</span></b> and then select
     851the file </p>
    865852
    866853<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
    867 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    868 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>La_hex_+45deg-00015.tif</span></b>
    869 and press <b style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
    870 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    871 Cambria;mso-bidi-theme-font:minor-latin'>Open</span></b>.<span
    872 style='mso-no-proof:yes'> <o:p></o:p></span></p>
     854style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     855mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
     856minor-latin'>La_hex_+45deg-00015.tif</span></b> and press <b style='mso-bidi-font-weight:
     857normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     858minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
     859mso-bidi-theme-font:minor-latin'>Open</span></b>.<span style='mso-no-proof:
     860yes'> <o:p></o:p></span></p>
    873861
    874862<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype
     
    892880 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
    893881 <o:lock v:ext="edit" aspectratio="t"/>
    894 </v:shapetype><v:shape id="_x0000_i1025" type="#_x0000_t75" style='width:300pt;
    895  height:188pt;visibility:visible;mso-wrap-style:square'>
     882</v:shapetype><v:shape id="_x0000_i1032" type="#_x0000_t75" style='width:300pt;
     883 height:187.5pt;visibility:visible;mso-wrap-style:square'>
    896884 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png"
    897885  o:title=""/>
    898 </v:shape><![endif]--><![if !vml]><img border=0 width=302 height=190
    899 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png"
    900 v:shapes="_x0000_i1025"><![endif]></span></p>
     886</v:shape><![endif]--><![if !vml]><img border=0 width=400 height=250
     887src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png"
     888v:shapes="_x0000_i1032"><![endif]></span></p>
    901889
    902890<p class=MsoNormal>At this point the data tree window will have several
    903891entries; the highlighted one specifies the contents of the data window as <b
    904 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
     892style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    905893mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    906 Cambria;mso-bidi-theme-font:minor-latin'>Image Controls</span><o:p></o:p></b></p>
     894Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span><o:p></o:p></b></p>
    907895
    908896<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    909  id="Picture_x0020_10" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:473pt;
     897 id="Picture_x0020_10" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:472.5pt;
    910898 height:342pt;visibility:visible;mso-wrap-style:square'>
     899 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png"
     900  o:title=""/>
     901</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=456
     902src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png"
     903v:shapes="Picture_x0020_10"><![endif]></span></p>
     904
     905<p class=MsoNormal><span style='mso-spacerun:yes'> </span>The plot window shows
     906the image; notice the elliptical shape of the powder diffraction rings
     907due to the 45 degree detector tilt. The
     908blue <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     909mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
     910Calibri;mso-bidi-theme-font:minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span></b>
     911marks the beam location (which defaults to the image center); the
     912calibration you will perform here will find the correct
     913placement for it. Also note that as the mouse is moved across the plot
     914the plot window status bar (at bottom of plot window) shows the
     915cursor position, as computed from the default (incorrect)
     916calibration values. These constants will be correctly determined after you finish the calibration.</p>
     917
     918<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
     919style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_11"
     920 o:spid="_x0000_i1030" type="#_x0000_t75" style='width:525pt;height:450pt;
     921 visibility:visible;mso-wrap-style:square'>
    911922 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
    912923  o:title=""/>
    913 </v:shape><![endif]--><![if !vml]><img border=0 width=475 height=344
    914 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
    915 v:shapes="Picture_x0020_10"><![endif]></span></p>
    916 
    917 <p class=MsoNormal><span style="mso-spacerun:yes"> </span>The plot window shows
    918 the image; notice the elliptical shape of the powder diffraction rings due to
    919 the 45 degree detector tilt. The blue <b style='mso-bidi-font-weight:normal'><span
    920 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    921 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin;
    922 color:#4F81BD;mso-themecolor:accent1'>X</span></b> marks the beam location
    923 (which defaults to the image center); the calibration you will perform here
    924 will find the correct placement for it. Also note that as the mouse is moved
    925 across the plot the plot window status bar (at bottom of plot window) shows the
    926 cursor position, as computed from the default (incorrect) calibration values.
    927 These constants will be correctly determined after you finish the calibration.</p>
    928 
    929 <p class=MsoNormal><span style="mso-spacerun:yes"> </span><span
    930 style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_11"
    931  o:spid="_x0000_i1027" type="#_x0000_t75" style='width:525pt;height:450pt;
    932  visibility:visible;mso-wrap-style:square'>
    933  <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
    934   o:title=""/>
    935 </v:shape><![endif]--><![if !vml]><img border=0 width=527 height=452
    936 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png"
     924</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
     925src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
    937926v:shapes="Picture_x0020_11"><![endif]></span></p>
    938927
    939 <h1><span style="mso-spacerun:yes"> </span>Step 2: Edit image parameters</h1>
    940 
    941 <p class=MsoNormal><span style="mso-spacerun:yes"> </span>Note that, alas, very
     928<h1><span style='mso-spacerun:yes'> </span>Step 2: Edit image parameters</h1>
     929
     930<p class=MsoNormal><span style='mso-spacerun:yes'> </span>Note that, alas, very
    942931few image formats contain all of the important metadata about the image, so it
    943932needs to be added manually. In this case set the <b style='mso-bidi-font-weight:
    944 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin;
    945 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:
    946 minor-latin'>wavelength</span></b> to <b style='mso-bidi-font-weight:normal'><span
    947 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    948 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>0.10798</span></b>.
    949 It is also helpful to change the display of the image so that it is easier to
    950 see the diffraction rings. Lowering the maximum intensity to 10,000 to 20,000
    951 counts will help (note that this can be done by moving the slider, or by typing
    952 a value in the box and then clicking on another control or pressing the <b
    953 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
     933normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     934minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
     935mso-bidi-theme-font:minor-latin'>wavelength</span></b> to <b style='mso-bidi-font-weight:
     936normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     937minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
     938mso-bidi-theme-font:minor-latin'>0.10798</span></b>. It is also helpful to
     939change the display of the image so that it is easier to see the diffraction
     940rings. Lowering the maximum intensity to 10,000 to 20,000 counts will help
     941(note that this can be done by moving the <span class=GramE>slider,</span> or
     942by typing a value in the box and then clicking on another control or pressing
     943the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    954944mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    955 Cambria;mso-bidi-theme-font:minor-latin'>Enter</span></b> or <b
    956 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
     945Calibri;mso-bidi-theme-font:minor-latin'>Enter</span></b> or <b
     946style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    957947mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    958 Cambria;mso-bidi-theme-font:minor-latin'>Tab</span></b> key). You may also wish
     948Calibri;mso-bidi-theme-font:minor-latin'>Tab</span></b> key). You may also wish
    959949to select another color scheme using the <b style='mso-bidi-font-weight:normal'><span
    960 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    961 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>Color
    962 bar</span></b> selector. </p>
    963 
    964 <h1><span style="mso-spacerun:yes"> </span>Step 3: Calibrate</h1>
    965 
    966 <h3><span style="mso-spacerun:yes"> </span>First: </h3>
    967 
    968 <p class=MsoNormal><span style="mso-spacerun:yes">   </span>Set the material
     950style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     951mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
     952minor-latin'>Color bar</span></b> selector. </p>
     953
     954<h1><span style='mso-spacerun:yes'> </span>Step 3: Calibrate</h1>
     955
     956<h3><span style='mso-spacerun:yes'> </span>First: </h3>
     957
     958<p class=MsoNormal><span style='mso-spacerun:yes'>   </span>Set the material
    969959used as a sample in the box labeled <span class=SpellE><b style='mso-bidi-font-weight:
    970 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin;
    971 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:
    972 minor-latin'>Calibrant</span></b></span>; select <b style='mso-bidi-font-weight:
    973 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin;
    974 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:
    975 minor-latin'>LaB6 SRM660a</span></b></p>
    976 
    977 <h3><span style="mso-spacerun:yes"> </span>Second: </h3>
    978 
    979 <p class=MsoNormal><span style="mso-spacerun:yes">   </span>Use the <b
    980 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
     960normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     961minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
     962mso-bidi-theme-font:minor-latin'>Calibrant</span></b></span>; select <b
     963style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    981964mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    982 Cambria;mso-bidi-theme-font:minor-latin'>Operations/Calibrate</span></b> menu
     965Calibri;mso-bidi-theme-font:minor-latin'>LaB6 SRM660a</span></b></p>
     966
     967<h3><span style='mso-spacerun:yes'> </span>Second: </h3>
     968
     969<p class=MsoNormal><span style='mso-spacerun:yes'>   </span>Use the <b
     970style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
     971mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
     972Calibri;mso-bidi-theme-font:minor-latin'>Operations/Calibrate</span></b> menu
    983973item (note this menu is on the <b style='mso-bidi-font-weight:normal'><span
    984 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    985 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>Image
    986 Controls</span></b> window or for the Mac, when the <span class=GramE><b
    987 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
    988 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    989 Cambria;mso-bidi-theme-font:minor-latin'>Image<span style="mso-spacerun:yes"> 
    990 </span>Controls</span></b></span> window is made active this menu is added to the
    991 system menu bar). At this point the status line on the bottom of the <b
    992 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
    993 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    994 Cambria;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window
    995 changes with a prompt to select points for calibration.</p>
     974style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     975mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
     976minor-latin'>Image Controls</span></b> window or for the Mac, the <span
     977class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family:
     978"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
     979minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Image<span
     980style='mso-spacerun:yes'>  </span>Controls</span></b></span> window must be
     981active to place this into the system menu bar). At this point the status line
     982on the bottom of the <b style='mso-bidi-font-weight:normal'><span
     983style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     984mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
     985minor-latin'>Image Controls</span></b> window changes with a prompt to select
     986points for calibration.</p>
    996987
    997988<h3>Third: </h3>
    998989
    999 <p class=MsoNormal><span style="mso-spacerun:yes">  </span>Use the left mouse
     990<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>Use the left mouse
    1000991button to click on at least five locations on the innermost ring. As each point
    1001992is defined, a red &quot;<b style='mso-bidi-font-weight:normal'><span
    1002 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1003 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin;
    1004 color:red'>+</span></b>&quot; is added to the plot. You need not hit the ring
    1005 exactly as the code will search for the locally highest point. (On the Mac with
    1006 a two or three button mouse, use the left mouse button, or with a standard Mac
    1007 mouse, use the regular mouse button.)</p>
     993style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     994mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
     995minor-latin;color:red'>+</span></b>&quot; is added to the plot. You need not
     996hit the ring exactly as the code will search for the locally highest
     997point. (On the Mac with a two or three button mouse, also use the left
     998mouse button, or with a standard Mac single-button mouse, use the
     999regular mouse button.)</p>
    10081000
    10091001<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1010  id="Picture_x0020_8" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:525pt;
     1002 id="Picture_x0020_8" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt;
    10111003 height:450pt;visibility:visible;mso-wrap-style:square'>
    1012  <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
     1004 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
    10131005  o:title=""/>
    1014 </v:shape><![endif]--><![if !vml]><img border=0 width=527 height=452
    1015 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
     1006</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
     1007src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
    10161008v:shapes="Picture_x0020_8"><![endif]></span></p>
    10171009
    1018 <p class=MsoNormal><span style="mso-spacerun:yes">  </span>To remove a point
    1019 added in error click on that point with the right mouse button (on the Mac, if
    1020 you have a single-button mouse, hold the control key down and click with the
    1021 mouse). </p>
    1022 
    1023 <h3><span style="mso-spacerun:yes"> </span>Fourth:</h3>
    1024 
    1025 <p class=MsoNormal><span style="mso-spacerun:yes">  </span>When done, press the
    1026 right mouse button well away from any points that have been added (on the Mac,
    1027 if you have a single-button mouse, hold the control key down and click). </p>
     1010<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>To remove a point
     1011added in error click on that point with the right mouse button
     1012(on the Mac, if you have a single-button mouse, hold the control key
     1013down and click).
     1014</p>
     1015
     1016<h3><span style='mso-spacerun:yes'> </span>Fourth:</h3>
     1017
     1018<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>When done, press the
     1019right mouse button well away from any points that have been added
     1020(on the Mac, if you have a single-button mouse, hold the control key
     1021down and click).
     1022</p>
    10281023
    10291024<p class=MsoNormal>The calibration is then performed. First the rings are
     
    10341029have been fitted, the entire ensemble of rings is refitted to the detector
    10351030parameters and the rings are then shown in blue. The beam position (blue “<span
    1036 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1037 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin;
    1038 color:#4F81BD;mso-themecolor:accent1'>X</span>”) is now correctly positioned.</p>
    1039 
    1040 <p class=MsoNormal><span style="mso-spacerun:yes"> </span><span
     1031style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1032mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
     1033minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span>”) is now correctly
     1034positioned.</p>
     1035
     1036<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
    10411037style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_9"
    1042  o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt;height:450pt;
     1038 o:spid="_x0000_i1028" type="#_x0000_t75" style='width:525pt;height:450pt;
    10431039 visibility:visible;mso-wrap-style:square'>
    1044  <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image009.png"
     1040 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
    10451041  o:title=""/>
    1046 </v:shape><![endif]--><![if !vml]><img border=0 width=527 height=452
    1047 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image010.png"
     1042</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
     1043src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
    10481044v:shapes="Picture_x0020_9"><![endif]></span><span
    1049 style="mso-spacerun:yes"> </span></p>
     1045style='mso-spacerun:yes'> </span></p>
    10501046
    10511047<p class=MsoNormal>The derived calibration results are shown in the <b
    1052 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
     1048style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    10531049mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    1054 Cambria;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window.</p>
     1050Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window.</p>
    10551051
    10561052<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1057  id="Picture_x0020_13" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:473pt;
     1053 id="Picture_x0020_13" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:472.5pt;
    10581054 height:342pt;visibility:visible;mso-wrap-style:square'>
    1059  <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image011.png"
     1055 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png"
    10601056  o:title=""/>
    1061 </v:shape><![endif]--><![if !vml]><img border=0 width=475 height=344
    1062 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image012.png"
     1057</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=456
     1058src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png"
    10631059v:shapes="Picture_x0020_13"><![endif]></span><span
    1064 style="mso-spacerun:yes"> </span></p>
     1060style='mso-spacerun:yes'> </span></p>
    10651061
    10661062<p class=MsoNormal><span class=GramE>and</span> the console window shows
     
    10681064
    10691065<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1070  id="Picture_x0020_14" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:397pt;
    1071  height:134pt;visibility:visible;mso-wrap-style:square'>
    1072  <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image013.png"
     1066 id="Picture_x0020_14" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:396.75pt;
     1067 height:134.25pt;visibility:visible;mso-wrap-style:square'>
     1068 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
    10731069  o:title=""/>
    1074 </v:shape><![endif]--><![if !vml]><img border=0 width=399 height=136
    1075 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image014.png"
     1070</v:shape><![endif]--><![if !vml]><img border=0 width=529 height=179
     1071src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
    10761072v:shapes="Picture_x0020_14"><![endif]></span></p>
    10771073
    1078 <p class=MsoNormal><span style="mso-spacerun:yes"> </span>To see the actual points
    1079 selected by the program, click on the <b style='mso-bidi-font-weight:normal'><span
    1080 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1081 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>show
    1082 ring picks?</span></b> <span class=GramE>check</span> box </p>
     1074<p class=MsoNormal><span style='mso-spacerun:yes'> </span>To see the actual
     1075points selected by the program, click on the <b style='mso-bidi-font-weight:
     1076normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1077minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
     1078mso-bidi-theme-font:minor-latin'>show ring picks?</span></b> <span class=GramE>check</span>
     1079box </p>
    10831080
    10841081<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
    1085  id="Picture_x0020_15" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt;
     1082 id="Picture_x0020_15" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;
    10861083 height:450pt;visibility:visible;mso-wrap-style:square'>
    1087  <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image015.png"
     1084 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
    10881085  o:title=""/>
    1089 </v:shape><![endif]--><![if !vml]><img border=0 width=527 height=452
    1090 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image016.png"
     1086</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
     1087src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
    10911088v:shapes="Picture_x0020_15"><![endif]></span><span
    1092 style="mso-spacerun:yes"> </span><span style='color:#1F497D;mso-themecolor:
     1089style='mso-spacerun:yes'> </span><span style='color:#1F497D;mso-themecolor:
    10931090text2'><o:p></o:p></span></p>
    10941091
     
    10961093selected for the outermost rings are scattered between that and the next ring.
    10971094This can be repaired by changing the pixel search range to 10 and using the <b
    1098 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
     1095style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    10991096mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    1100 Cambria;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b> menu
     1097Calibri;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b> menu
    11011098item.</p>
    11021099
    11031100<p class=MsoNormal>Assuming that these calibration results will be applied to
    11041101other images in the same GSAS-II project, click on <b style='mso-bidi-font-weight:
    1105 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin;
    1106 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:
    1107 minor-latin'>Use as default for all images</span></b>. You may also save a copy
    1108 of the calibration values to a file <span style='font-family:Cambria;
     1102normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1103minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
     1104mso-bidi-theme-font:minor-latin'>Use as default for all images</span></b>. You
     1105may also save a copy of the calibration values to a file <span
     1106style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1107mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
     1108minor-latin'>(<span class=SpellE><i style='mso-bidi-font-style:normal'>name</i><b
     1109style='mso-bidi-font-weight:normal'>.imctrl</b></span></span>) with the <b
     1110style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    11091111mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    1110 Cambria;mso-bidi-theme-font:minor-latin'>(<span class=SpellE><i
    1111 style='mso-bidi-font-style:normal'>name</i><b style='mso-bidi-font-weight:normal'>.imctrl</b></span></span>)
    1112 with the <b style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
     1112Calibri;mso-bidi-theme-font:minor-latin'>Operations/Save Controls</span></b>
     1113menu item. To save the project, including the now-derived calibration information,
     1114use the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    11131115mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    1114 Cambria;mso-bidi-theme-font:minor-latin'>Operations/Save Controls</span></b>
    1115 menu item. To save the project, including the now-derived calibration
    1116 information, use the <b style='mso-bidi-font-weight:normal'><span
    1117 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1118 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>File/Save</span>
    1119 </b><b style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;
     1116Calibri;mso-bidi-theme-font:minor-latin'>File/Save</span> </b><b
     1117style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
    11201118mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
    1121 Cambria;mso-bidi-theme-font:minor-latin'>Project</span></b><span
    1122 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1123 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'> </span>menu
    1124 item associated with the data tree window; as this project has not been saved
    1125 before the file save dialog will need a file name. Don’t enter the extension;
    1126 it will be set to “<b style='mso-bidi-font-weight:normal'><span
    1127 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
    1128 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>.<span
    1129 class=SpellE>gpx</span></span></b>”.</p>
     1119Calibri;mso-bidi-theme-font:minor-latin'>Project</span></b><span
     1120style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
     1121mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
     1122minor-latin'> </span>menu item associated with the data tree window; as this
     1123project has not been saved before the file save dialog will need a file name.
     1124Don’t enter the extension; it will be set to “<b style='mso-bidi-font-weight:
     1125normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
     1126minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
     1127mso-bidi-theme-font:minor-latin'>.<span class=SpellE>gpx</span></span></b>”.</p>
    11301128
    11311129<h2>Next step: <span class=MsoHyperlink><span style='color:#0070C0'><a
    1132 href="Integration%2520of%2520area%2520detector%2520data%2520in%2520GSAS.htm"><u><span
     1130href="Integration%20of%20area%20detector%20data%20in%20GSAS.htm"><u><span
    11331131style='color:black'>Integrate the Data</span></u></a></span></span></h2>
    11341132
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