Changeset 1114
- Timestamp:
- Oct 18, 2013 3:53:58 PM (10 years ago)
- File:
-
- 1 edited
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trunk/help/Calibration of an area detector in GSAS.htm
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764 mso-ascii-font-family:Calibri; 779 765 mso-ascii-theme-font:minor-latin; 780 mso-fareast-font-family:Ca mbria;766 mso-fareast-font-family:Calibri; 781 767 mso-fareast-theme-font:minor-latin; 782 mso-hansi-font-family:Ca mbria;768 mso-hansi-font-family:Calibri; 783 769 mso-hansi-theme-font:minor-latin; 784 770 mso-bidi-font-family:"Times New Roman"; … … 797 783 <style> 798 784 /* Style Definitions */ 799 table.MsoNormalTable785 table.MsoNormalTable 800 786 {mso-style-name:"Table Normal"; 801 787 mso-tstyle-rowband-size:0; … … 809 795 mso-pagination:widow-orphan; 810 796 font-size:10.0pt; 811 font-family: Cambria;812 mso-ascii-font-family:Ca mbria;797 font-family:"Calibri","sans-serif"; 798 mso-ascii-font-family:Calibri; 813 799 mso-ascii-theme-font:minor-latin; 814 mso-hansi-font-family:Ca mbria;800 mso-hansi-font-family:Calibri; 815 801 mso-hansi-theme-font:minor-latin;} 816 802 </style> 817 803 <![endif]--><!--[if gte mso 9]><xml> 818 <o:shapedefaults v:ext="edit" spidmax="10 36"/>804 <o:shapedefaults v:ext="edit" spidmax="1026"/> 819 805 </xml><![endif]--><!--[if gte mso 9]><xml> 820 806 <o:shapelayout v:ext="edit"> … … 835 821 intentionally tilted at 45 degrees, are used. Note that menu entries are listed 836 822 in bold face below as <b style='mso-bidi-font-weight:normal'><span 837 style='font-family: Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:838 m inor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>Help/About839 GSAS-II</span></b>, which lists first the name of the menu (here <b 840 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria; 841 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:842 Cambria;mso-bidi-theme-font:minor-latin'>Help</span></b>) and second the name 843 of the entry in the menu (here <b style='mso-bidi-font-weight:normal'><span 844 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:845 minor-latin;mso- bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>About846 GSAS-II</span></b>).</p>823 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 824 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 825 minor-latin'>Help/About GSAS-II</span></b>, which lists first the name of the 826 menu (here <b style='mso-bidi-font-weight:normal'><span style='font-family: 827 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 828 minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Help</span></b>) 829 and second the name of the entry in the menu (here <b style='mso-bidi-font-weight: 830 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 831 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 832 mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).</p> 847 833 848 834 <p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a 849 href="Starting%2 520GSAS.htm"><span style='color:windowtext;text-decoration:850 none;text-underline:none'>start GSAS-II</span></a></span></u>.</p>835 href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none; 836 text-underline:none'>start GSAS-II</span></a></span></u>.</p> 851 837 852 838 <h1>Step 1: read in the data file</h1> 853 839 854 <p class=MsoNormal><span style= "mso-spacerun:yes"> </span>Use the <b840 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the <b 855 841 style='mso-bidi-font-weight:normal'>Data/Read image data</b> menu item to read 856 842 the data file into the current GSAS-II project. </p> 857 843 858 <p class=MsoNormal><span style= "mso-spacerun:yes"> </span></p>844 <p class=MsoNormal><span style='mso-spacerun:yes'> </span></p> 859 845 860 846 <p class=MsoNormal>A file selection dialog will be shown; its appearance will 861 847 depend on your OS. Change the search directory to <b style='mso-bidi-font-weight: 862 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin; 863 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font: 864 minor-latin'>/Exercises/images</span></b> and then select the file </p> 848 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 849 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 850 mso-bidi-theme-font:minor-latin'>/Exercises/images</span></b> and then select 851 the file </p> 865 852 866 853 <p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span 867 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 868 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>La_hex_+45deg-00015.tif</span></b> 869 and press <b style='mso-bidi-font-weight:normal'><span style='font-family:Cambria; 870 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 871 Cambria;mso-bidi-theme-font:minor-latin'>Open</span></b>.<span 872 style='mso-no-proof:yes'> <o:p></o:p></span></p> 854 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 855 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 856 minor-latin'>La_hex_+45deg-00015.tif</span></b> and press <b style='mso-bidi-font-weight: 857 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 858 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 859 mso-bidi-theme-font:minor-latin'>Open</span></b>.<span style='mso-no-proof: 860 yes'> <o:p></o:p></span></p> 873 861 874 862 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype … … 892 880 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> 893 881 <o:lock v:ext="edit" aspectratio="t"/> 894 </v:shapetype><v:shape id="_x0000_i10 25" type="#_x0000_t75" style='width:300pt;895 height:18 8pt;visibility:visible;mso-wrap-style:square'>882 </v:shapetype><v:shape id="_x0000_i1032" type="#_x0000_t75" style='width:300pt; 883 height:187.5pt;visibility:visible;mso-wrap-style:square'> 896 884 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png" 897 885 o:title=""/> 898 </v:shape><![endif]--><![if !vml]><img border=0 width= 302 height=190899 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image00 2.png"900 v:shapes="_x0000_i10 25"><![endif]></span></p>886 </v:shape><![endif]--><![if !vml]><img border=0 width=400 height=250 887 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png" 888 v:shapes="_x0000_i1032"><![endif]></span></p> 901 889 902 890 <p class=MsoNormal>At this point the data tree window will have several 903 891 entries; the highlighted one specifies the contents of the data window as <b 904 style='mso-bidi-font-weight:normal'><span style='font-family: Cambria;892 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 905 893 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 906 Ca mbria;mso-bidi-theme-font:minor-latin'>Image Controls</span><o:p></o:p></b></p>894 Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span><o:p></o:p></b></p> 907 895 908 896 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 909 id="Picture_x0020_10" o:spid="_x0000_i10 26" type="#_x0000_t75" style='width:473pt;897 id="Picture_x0020_10" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:472.5pt; 910 898 height:342pt;visibility:visible;mso-wrap-style:square'> 899 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png" 900 o:title=""/> 901 </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=456 902 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png" 903 v:shapes="Picture_x0020_10"><![endif]></span></p> 904 905 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>The plot window shows 906 the image; notice the elliptical shape of the powder diffraction rings 907 due to the 45 degree detector tilt. The 908 blue <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 909 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 910 Calibri;mso-bidi-theme-font:minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span></b> 911 marks the beam location (which defaults to the image center); the 912 calibration you will perform here will find the correct 913 placement for it. Also note that as the mouse is moved across the plot 914 the plot window status bar (at bottom of plot window) shows the 915 cursor position, as computed from the default (incorrect) 916 calibration values. These constants will be correctly determined after you finish the calibration.</p> 917 918 <p class=MsoNormal><span style='mso-spacerun:yes'> </span><span 919 style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_11" 920 o:spid="_x0000_i1030" type="#_x0000_t75" style='width:525pt;height:450pt; 921 visibility:visible;mso-wrap-style:square'> 911 922 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png" 912 923 o:title=""/> 913 </v:shape><![endif]--><![if !vml]><img border=0 width=475 height=344 914 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png" 915 v:shapes="Picture_x0020_10"><![endif]></span></p> 916 917 <p class=MsoNormal><span style="mso-spacerun:yes"> </span>The plot window shows 918 the image; notice the elliptical shape of the powder diffraction rings due to 919 the 45 degree detector tilt. The blue <b style='mso-bidi-font-weight:normal'><span 920 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 921 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin; 922 color:#4F81BD;mso-themecolor:accent1'>X</span></b> marks the beam location 923 (which defaults to the image center); the calibration you will perform here 924 will find the correct placement for it. Also note that as the mouse is moved 925 across the plot the plot window status bar (at bottom of plot window) shows the 926 cursor position, as computed from the default (incorrect) calibration values. 927 These constants will be correctly determined after you finish the calibration.</p> 928 929 <p class=MsoNormal><span style="mso-spacerun:yes"> </span><span 930 style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_11" 931 o:spid="_x0000_i1027" type="#_x0000_t75" style='width:525pt;height:450pt; 932 visibility:visible;mso-wrap-style:square'> 933 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png" 934 o:title=""/> 935 </v:shape><![endif]--><![if !vml]><img border=0 width=527 height=452 936 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png" 924 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 925 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png" 937 926 v:shapes="Picture_x0020_11"><![endif]></span></p> 938 927 939 <h1><span style= "mso-spacerun:yes"> </span>Step 2: Edit image parameters</h1>940 941 <p class=MsoNormal><span style= "mso-spacerun:yes"> </span>Note that, alas, very928 <h1><span style='mso-spacerun:yes'> </span>Step 2: Edit image parameters</h1> 929 930 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>Note that, alas, very 942 931 few image formats contain all of the important metadata about the image, so it 943 932 needs to be added manually. In this case set the <b style='mso-bidi-font-weight: 944 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin; 945 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font: 946 minor-latin'>wavelength</span></b> to <b style='mso-bidi-font-weight:normal'><span 947 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 948 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>0.10798</span></b>. 949 It is also helpful to change the display of the image so that it is easier to 950 see the diffraction rings. Lowering the maximum intensity to 10,000 to 20,000 951 counts will help (note that this can be done by moving the slider, or by typing 952 a value in the box and then clicking on another control or pressing the <b 953 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria; 933 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 934 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 935 mso-bidi-theme-font:minor-latin'>wavelength</span></b> to <b style='mso-bidi-font-weight: 936 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 937 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 938 mso-bidi-theme-font:minor-latin'>0.10798</span></b>. It is also helpful to 939 change the display of the image so that it is easier to see the diffraction 940 rings. Lowering the maximum intensity to 10,000 to 20,000 counts will help 941 (note that this can be done by moving the <span class=GramE>slider,</span> or 942 by typing a value in the box and then clicking on another control or pressing 943 the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 954 944 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 955 Ca mbria;mso-bidi-theme-font:minor-latin'>Enter</span></b> or <b956 style='mso-bidi-font-weight:normal'><span style='font-family: Cambria;945 Calibri;mso-bidi-theme-font:minor-latin'>Enter</span></b> or <b 946 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 957 947 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 958 Ca mbria;mso-bidi-theme-font:minor-latin'>Tab</span></b> key). You may also wish948 Calibri;mso-bidi-theme-font:minor-latin'>Tab</span></b> key). You may also wish 959 949 to select another color scheme using the <b style='mso-bidi-font-weight:normal'><span 960 style='font-family: Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:961 m inor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>Color962 bar</span></b> selector. </p>963 964 <h1><span style= "mso-spacerun:yes"> </span>Step 3: Calibrate</h1>965 966 <h3><span style= "mso-spacerun:yes"> </span>First: </h3>967 968 <p class=MsoNormal><span style= "mso-spacerun:yes"> </span>Set the material950 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 951 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 952 minor-latin'>Color bar</span></b> selector. </p> 953 954 <h1><span style='mso-spacerun:yes'> </span>Step 3: Calibrate</h1> 955 956 <h3><span style='mso-spacerun:yes'> </span>First: </h3> 957 958 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>Set the material 969 959 used as a sample in the box labeled <span class=SpellE><b style='mso-bidi-font-weight: 970 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin; 971 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font: 972 minor-latin'>Calibrant</span></b></span>; select <b style='mso-bidi-font-weight: 973 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin; 974 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font: 975 minor-latin'>LaB6 SRM660a</span></b></p> 976 977 <h3><span style="mso-spacerun:yes"> </span>Second: </h3> 978 979 <p class=MsoNormal><span style="mso-spacerun:yes"> </span>Use the <b 980 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria; 960 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 961 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 962 mso-bidi-theme-font:minor-latin'>Calibrant</span></b></span>; select <b 963 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 981 964 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 982 Cambria;mso-bidi-theme-font:minor-latin'>Operations/Calibrate</span></b> menu 965 Calibri;mso-bidi-theme-font:minor-latin'>LaB6 SRM660a</span></b></p> 966 967 <h3><span style='mso-spacerun:yes'> </span>Second: </h3> 968 969 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the <b 970 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 971 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 972 Calibri;mso-bidi-theme-font:minor-latin'>Operations/Calibrate</span></b> menu 983 973 item (note this menu is on the <b style='mso-bidi-font-weight:normal'><span 984 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 985 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>Image 986 Controls</span></b> window or for the Mac, when the <span class=GramE><b 987 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria; 988 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 989 Cambria;mso-bidi-theme-font:minor-latin'>Image<span style="mso-spacerun:yes"> 990 </span>Controls</span></b></span> window is made active this menu is added to the 991 system menu bar). At this point the status line on the bottom of the <b 992 style='mso-bidi-font-weight:normal'><span style='font-family:Cambria; 993 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 994 Cambria;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window 995 changes with a prompt to select points for calibration.</p> 974 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 975 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 976 minor-latin'>Image Controls</span></b> window or for the Mac, the <span 977 class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family: 978 "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 979 minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Image<span 980 style='mso-spacerun:yes'> </span>Controls</span></b></span> window must be 981 active to place this into the system menu bar). At this point the status line 982 on the bottom of the <b style='mso-bidi-font-weight:normal'><span 983 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 984 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 985 minor-latin'>Image Controls</span></b> window changes with a prompt to select 986 points for calibration.</p> 996 987 997 988 <h3>Third: </h3> 998 989 999 <p class=MsoNormal><span style= "mso-spacerun:yes"> </span>Use the left mouse990 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the left mouse 1000 991 button to click on at least five locations on the innermost ring. As each point 1001 992 is defined, a red "<b style='mso-bidi-font-weight:normal'><span 1002 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1003 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin; 1004 color:red'>+</span></b>" is added to the plot. You need not hit the ring 1005 exactly as the code will search for the locally highest point. (On the Mac with 1006 a two or three button mouse, use the left mouse button, or with a standard Mac 1007 mouse, use the regular mouse button.)</p> 993 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 994 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 995 minor-latin;color:red'>+</span></b>" is added to the plot. You need not 996 hit the ring exactly as the code will search for the locally highest 997 point. (On the Mac with a two or three button mouse, also use the left 998 mouse button, or with a standard Mac single-button mouse, use the 999 regular mouse button.)</p> 1008 1000 1009 1001 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1010 id="Picture_x0020_8" o:spid="_x0000_i102 8" type="#_x0000_t75" style='width:525pt;1002 id="Picture_x0020_8" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt; 1011 1003 height:450pt;visibility:visible;mso-wrap-style:square'> 1012 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image00 7.png"1004 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png" 1013 1005 o:title=""/> 1014 </v:shape><![endif]--><![if !vml]><img border=0 width= 527 height=4521015 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image00 8.png"1006 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 1007 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png" 1016 1008 v:shapes="Picture_x0020_8"><![endif]></span></p> 1017 1009 1018 <p class=MsoNormal><span style="mso-spacerun:yes"> </span>To remove a point 1019 added in error click on that point with the right mouse button (on the Mac, if 1020 you have a single-button mouse, hold the control key down and click with the 1021 mouse). </p> 1022 1023 <h3><span style="mso-spacerun:yes"> </span>Fourth:</h3> 1024 1025 <p class=MsoNormal><span style="mso-spacerun:yes"> </span>When done, press the 1026 right mouse button well away from any points that have been added (on the Mac, 1027 if you have a single-button mouse, hold the control key down and click). </p> 1010 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>To remove a point 1011 added in error click on that point with the right mouse button 1012 (on the Mac, if you have a single-button mouse, hold the control key 1013 down and click). 1014 </p> 1015 1016 <h3><span style='mso-spacerun:yes'> </span>Fourth:</h3> 1017 1018 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>When done, press the 1019 right mouse button well away from any points that have been added 1020 (on the Mac, if you have a single-button mouse, hold the control key 1021 down and click). 1022 </p> 1028 1023 1029 1024 <p class=MsoNormal>The calibration is then performed. First the rings are … … 1034 1029 have been fitted, the entire ensemble of rings is refitted to the detector 1035 1030 parameters and the rings are then shown in blue. The beam position (blue <span 1036 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1037 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin; 1038 color:#4F81BD;mso-themecolor:accent1'>X</span>) is now correctly positioned.</p> 1039 1040 <p class=MsoNormal><span style="mso-spacerun:yes"> </span><span 1031 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1032 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 1033 minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span>) is now correctly 1034 positioned.</p> 1035 1036 <p class=MsoNormal><span style='mso-spacerun:yes'> </span><span 1041 1037 style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_9" 1042 o:spid="_x0000_i102 9" type="#_x0000_t75" style='width:525pt;height:450pt;1038 o:spid="_x0000_i1028" type="#_x0000_t75" style='width:525pt;height:450pt; 1043 1039 visibility:visible;mso-wrap-style:square'> 1044 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image00 9.png"1040 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png" 1045 1041 o:title=""/> 1046 </v:shape><![endif]--><![if !vml]><img border=0 width= 527 height=4521047 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image0 10.png"1042 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 1043 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png" 1048 1044 v:shapes="Picture_x0020_9"><![endif]></span><span 1049 style= "mso-spacerun:yes"> </span></p>1045 style='mso-spacerun:yes'> </span></p> 1050 1046 1051 1047 <p class=MsoNormal>The derived calibration results are shown in the <b 1052 style='mso-bidi-font-weight:normal'><span style='font-family: Cambria;1048 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1053 1049 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 1054 Ca mbria;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window.</p>1050 Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window.</p> 1055 1051 1056 1052 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1057 id="Picture_x0020_13" o:spid="_x0000_i10 30" type="#_x0000_t75" style='width:473pt;1053 id="Picture_x0020_13" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:472.5pt; 1058 1054 height:342pt;visibility:visible;mso-wrap-style:square'> 1059 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image0 11.png"1055 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png" 1060 1056 o:title=""/> 1061 </v:shape><![endif]--><![if !vml]><img border=0 width= 475 height=3441062 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image0 12.png"1057 </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=456 1058 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png" 1063 1059 v:shapes="Picture_x0020_13"><![endif]></span><span 1064 style= "mso-spacerun:yes"> </span></p>1060 style='mso-spacerun:yes'> </span></p> 1065 1061 1066 1062 <p class=MsoNormal><span class=GramE>and</span> the console window shows … … 1068 1064 1069 1065 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1070 id="Picture_x0020_14" o:spid="_x0000_i10 31" type="#_x0000_t75" style='width:397pt;1071 height:134 pt;visibility:visible;mso-wrap-style:square'>1072 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image0 13.png"1066 id="Picture_x0020_14" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:396.75pt; 1067 height:134.25pt;visibility:visible;mso-wrap-style:square'> 1068 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png" 1073 1069 o:title=""/> 1074 </v:shape><![endif]--><![if !vml]><img border=0 width= 399 height=1361075 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image0 14.png"1070 </v:shape><![endif]--><![if !vml]><img border=0 width=529 height=179 1071 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png" 1076 1072 v:shapes="Picture_x0020_14"><![endif]></span></p> 1077 1073 1078 <p class=MsoNormal><span style="mso-spacerun:yes"> </span>To see the actual points 1079 selected by the program, click on the <b style='mso-bidi-font-weight:normal'><span 1080 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1081 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>show 1082 ring picks?</span></b> <span class=GramE>check</span> box </p> 1074 <p class=MsoNormal><span style='mso-spacerun:yes'> </span>To see the actual 1075 points selected by the program, click on the <b style='mso-bidi-font-weight: 1076 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1077 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 1078 mso-bidi-theme-font:minor-latin'>show ring picks?</span></b> <span class=GramE>check</span> 1079 box </p> 1083 1080 1084 1081 <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape 1085 id="Picture_x0020_15" o:spid="_x0000_i10 32" type="#_x0000_t75" style='width:525pt;1082 id="Picture_x0020_15" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt; 1086 1083 height:450pt;visibility:visible;mso-wrap-style:square'> 1087 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image0 15.png"1084 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png" 1088 1085 o:title=""/> 1089 </v:shape><![endif]--><![if !vml]><img border=0 width= 527 height=4521090 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image0 16.png"1086 </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 1087 src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png" 1091 1088 v:shapes="Picture_x0020_15"><![endif]></span><span 1092 style= "mso-spacerun:yes"> </span><span style='color:#1F497D;mso-themecolor:1089 style='mso-spacerun:yes'> </span><span style='color:#1F497D;mso-themecolor: 1093 1090 text2'><o:p></o:p></span></p> 1094 1091 … … 1096 1093 selected for the outermost rings are scattered between that and the next ring. 1097 1094 This can be repaired by changing the pixel search range to 10 and using the <b 1098 style='mso-bidi-font-weight:normal'><span style='font-family: Cambria;1095 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1099 1096 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 1100 Ca mbria;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b> menu1097 Calibri;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b> menu 1101 1098 item.</p> 1102 1099 1103 1100 <p class=MsoNormal>Assuming that these calibration results will be applied to 1104 1101 other images in the same GSAS-II project, click on <b style='mso-bidi-font-weight: 1105 normal'><span style='font-family:Cambria;mso-ascii-theme-font:minor-latin; 1106 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font: 1107 minor-latin'>Use as default for all images</span></b>. You may also save a copy 1108 of the calibration values to a file <span style='font-family:Cambria; 1102 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1103 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 1104 mso-bidi-theme-font:minor-latin'>Use as default for all images</span></b>. You 1105 may also save a copy of the calibration values to a file <span 1106 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1107 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 1108 minor-latin'>(<span class=SpellE><i style='mso-bidi-font-style:normal'>name</i><b 1109 style='mso-bidi-font-weight:normal'>.imctrl</b></span></span>) with the <b 1110 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1109 1111 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 1110 Ca mbria;mso-bidi-theme-font:minor-latin'>(<span class=SpellE><i1111 style='mso-bidi-font-style:normal'>name</i><b style='mso-bidi-font-weight:normal'>.imctrl</b></span></span>) 1112 with the <b style='mso-bidi-font-weight:normal'><span style='font-family:Cambria;1112 Calibri;mso-bidi-theme-font:minor-latin'>Operations/Save Controls</span></b> 1113 menu item. To save the project, including the now-derived calibration information, 1114 use the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1113 1115 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 1114 Cambria;mso-bidi-theme-font:minor-latin'>Operations/Save Controls</span></b> 1115 menu item. To save the project, including the now-derived calibration 1116 information, use the <b style='mso-bidi-font-weight:normal'><span 1117 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: 1118 minor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>File/Save</span> 1119 </b><b style='mso-bidi-font-weight:normal'><span style='font-family:Cambria; 1116 Calibri;mso-bidi-theme-font:minor-latin'>File/Save</span> </b><b 1117 style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; 1120 1118 mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: 1121 Ca mbria;mso-bidi-theme-font:minor-latin'>Project</span></b><span1122 style='font-family: Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1123 m inor-latin;mso-bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'> </span>menu1124 item associated with the data tree window; as this project has not been saved 1125 before the file save dialog will need a file name. Dont enter the extension; 1126 it will be set to <b style='mso-bidi-font-weight:normal'><span 1127 style='font-family:Cambria;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:1128 minor-latin;mso- bidi-font-family:Cambria;mso-bidi-theme-font:minor-latin'>.<span1129 class=SpellE>gpx</span></span></b>.</p>1119 Calibri;mso-bidi-theme-font:minor-latin'>Project</span></b><span 1120 style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; 1121 mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: 1122 minor-latin'> </span>menu item associated with the data tree window; as this 1123 project has not been saved before the file save dialog will need a file name. 1124 Dont enter the extension; it will be set to <b style='mso-bidi-font-weight: 1125 normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: 1126 minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; 1127 mso-bidi-theme-font:minor-latin'>.<span class=SpellE>gpx</span></span></b>.</p> 1130 1128 1131 1129 <h2>Next step: <span class=MsoHyperlink><span style='color:#0070C0'><a 1132 href="Integration%2 520of%2520area%2520detector%2520data%2520in%2520GSAS.htm"><u><span1130 href="Integration%20of%20area%20detector%20data%20in%20GSAS.htm"><u><span 1133 1131 style='color:black'>Integrate the Data</span></u></a></span></span></h2> 1134 1132
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