1 | <!-- Do not edit this file. It is created by makeTutorial.py from info in GSASIIctrlGUI.py --!> |
---|
2 | <h2>List of GSAS-II tutorials</H2><UL> |
---|
3 | |
---|
4 | <p> A list of available tutorials appears below. Each tutorial is a |
---|
5 | web page that can be opened using the link below, but most tutorials also need |
---|
6 | to have example data files downloaded. This can also be done with links included below, |
---|
7 | but it can be easier to access tutorials using |
---|
8 | <b>Help/Tutorials</b> menu item. |
---|
9 | When this menu entry is used from inside GSAS-II (unless "browse tutorial on web" is selected), |
---|
10 | the data files are downloaded to a local directory and GSAS-II will start from that directory |
---|
11 | for most file open commands. Most tutorials have also been recorded as videos of the computer screen |
---|
12 | along with naration. Links are provided below where videos are available. |
---|
13 | </p> |
---|
14 | </UL><h4>Getting started</H4><UL> |
---|
15 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/StartingGSASII/Starting GSAS.htm">Starting GSAS-II</A> |
---|
16 | [link: <A href="https://anl.box.com/v/StartingGSAS">video</A>, no example data]. |
---|
17 | <blockquote><I>An introduction to GSAS-II with starting instructions and a brief description of the displays.</I></blockquote> |
---|
18 | </UL><h4>Rietveld refinement</H4><UL> |
---|
19 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CWNeutron/Neutron CW Powder Data.htm">CW Neutron Powder fit for Yttrium-Iron Garnet</A> |
---|
20 | [links: <A href="https://anl.box.com/v/NeutronCWPowderData">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CWNeutron/data">Exercise files</A>]. |
---|
21 | <blockquote><I>This shows a simple Rietveld refinement with constraints from CW neutron powder diffraction data.</I></blockquote> |
---|
22 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/LabData/Laboratory X.htm">Fitting laboratory X-ray powder data for fluoroapatite</A> |
---|
23 | [links: <A href="https://anl.box.com/v/LaboratoryX">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/LabData/data">Exercise files</A>]. |
---|
24 | <blockquote><I>This shows a simple Rietveld refinement with CuKa lab Bragg-Brentano powder data.</I></blockquote> |
---|
25 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CWCombined/Combined refinement.htm">Combined X-ray/CW-neutron refinement of PbSO4</A> |
---|
26 | [links: <A href="https://anl.box.com/v/Combinedrefinement">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CWCombined/data">Exercise files</A>]. |
---|
27 | <blockquote><I>This shows Rietveld refinement of a structure with room temperature lab CuKa data and low temperature CW neutron data; |
---|
28 | use is made of the lattice parameter offsets to account for thermal expansion.</I></blockquote> |
---|
29 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF-CW Joint Refinement/TOF combined XN Rietveld refinement in GSAS.htm">Combined X-ray/TOF-neutron Rietveld refinement</A> |
---|
30 | [links: <A href="https://anl.box.com/v/TOFcombinedXNRietveldrefinemen">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF-CW Joint Refinement/data">Exercise files</A>]. |
---|
31 | <blockquote><I>This shows Rietveld refinement with high resolution synchrotron powder data and neutron TOF data</I></blockquote> |
---|
32 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Simulation/SimTutorial.htm">Simulating Powder Diffraction with GSAS-II</A> |
---|
33 | [links: <A href="https://anl.box.com/v/SimTutorial">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Simulation/data">Exercise files</A>]. |
---|
34 | <blockquote><I>This show how to create a simulated powder pattern from a lab diffractometer.</I></blockquote> |
---|
35 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/BkgFit/FitBkgTut.htm">Fitting the Starting Background using Fixed Points</A> |
---|
36 | [links: <A href="https://anl.box.com/v/FitBkgTut">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/BkgFit/data">Exercise files</A>]. |
---|
37 | <blockquote><I>This shows how to get an initial estimate of background parameters from a suite of fixed points |
---|
38 | before beginning Rietveld refinement.</I></blockquote> |
---|
39 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/RietPlot/PublicationPlot.htm">Create a Publication-Ready Rietveld Plot</A> |
---|
40 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/RietPlot/data">Exercise files</A>]. |
---|
41 | <blockquote><I>Shows how to create a customized version of a plot from a fit, |
---|
42 | with enlarged letters, different colors or symbols which can be written |
---|
43 | as a bitmap file, a pdf file or be exported to the Grace or Igor Pro |
---|
44 | plotting programs.</I></blockquote> |
---|
45 | </UL><h4>Magnetic Structure Analysis</H4><UL> |
---|
46 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SimpleMagnetic/SimpleMagnetic.htm">Simple Magnetic Structure Analysis</A> |
---|
47 | [links: <A href="https://anl.box.com/v/SimpleMagnetic">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SimpleMagnetic/data">Exercise files</A>]. |
---|
48 | <blockquote><I>Analysis of a simple antiferromagnet and a simple ferromagnet from CW neutron powder data</I></blockquote> |
---|
49 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-I/Magnetic Structures-I.htm">Magnetic Structure Analysis-I</A> |
---|
50 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-I/data">Exercise files</A>]. |
---|
51 | <blockquote><I>Analysis of a simple antiferromagnet using Bilbao k-SUBGROUPSMAG from CW neutron powder data</I></blockquote> |
---|
52 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-II/Magnetic-II.htm">Magnetic Structure Analysis-II</A> |
---|
53 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-II/data">Exercise files</A>]. |
---|
54 | <blockquote><I>Analysis of a antiferromagnet with change of space group using Bilbao k-SUBGROUPSMAG from CW neutron powder data</I></blockquote> |
---|
55 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-III/Magnetic-III.htm">Magnetic Structure Analysis-III</A> |
---|
56 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-III/data">Exercise files</A>]. |
---|
57 | <blockquote><I>Analysis of a Type IV antiferromagnet with a cell axis doubling using Bilbao k-SUBGROUPSMAG from CW neutron powder data</I></blockquote> |
---|
58 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-IV/Magnetic-IV.htm">Magnetic Structure Analysis-IV</A> |
---|
59 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-IV/data">Exercise files</A>]. |
---|
60 | <blockquote><I>Analysis of a Type IV antiferromagnet with a lattice centering change using Bilbao k-SUBGROUPSMAG from CW neutron powder data</I></blockquote> |
---|
61 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-V/Magnetic-V.htm">Magnetic Structure Analysis-V</A> |
---|
62 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-V/data">Exercise files</A>]. |
---|
63 | <blockquote><I>Analysis of a complex Type IV antiferromagnet with two propagation vectorse using Bilbao k-SUBGROUPSMAG from TOF neutron powder data</I></blockquote> |
---|
64 | </UL><h4>Parametric sequential fitting</H4><UL> |
---|
65 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SeqRefine/SequentialTutorial.htm">Sequential refinement of multiple datasets</A> |
---|
66 | [links: <A href="https://anl.box.com/v/SequentialTutorial">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SeqRefine/data">Exercise files</A>]. |
---|
67 | <blockquote><I>This shows the fitting of a structural model to multiple data sets collected as a function of temperature (7-300K). |
---|
68 | This tutorial is the prerequisite for the next one.</I></blockquote> |
---|
69 | <UL><LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SeqParametric/ParametricFitting.htm">Parametric Fitting and Pseudo Variables for Sequential Fits</A> <A href="#prereq">*</A> |
---|
70 | [link: <A href="https://anl.box.com/v/ParametricFitting">video</A>, no example data]. |
---|
71 | <blockquote><I>This explores the results of the sequential refinement obtained in the previous tutorial; includes |
---|
72 | plotting of variables and fitting the changes with simple equations.</I></blockquote> |
---|
73 | </UL> |
---|
74 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF Sequential Single Peak Fit/TOF Sequential Single Peak Fit.htm">Sequential fitting of single peaks and strain analysis of result</A> |
---|
75 | [links: <A href="https://anl.box.com/v/TOFSequentialSinglePeakFit">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF Sequential Single Peak Fit/data">Exercise files</A>]. |
---|
76 | <blockquote><I>This shows the fitting of single peaks in a sequence of TOF powder patterns from a sample under load; includes |
---|
77 | fitting of the result to get Hookes Law coefficients for elastic deformations.</I></blockquote> |
---|
78 | </UL><h4>Structure solution</H4><UL> |
---|
79 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/FitPeaks/Fit Peaks.htm">Fitting individual peaks & autoindexing</A> |
---|
80 | [links: <A href="https://anl.box.com/v/FitPeaks">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/FitPeaks/data">Exercise files</A>]. |
---|
81 | <blockquote><I>This covers two examples of selecting individual powder diffraction peaks, fitting them and then |
---|
82 | indexing to determine the crystal lattice and possible space group. This is the prerequisite for the next two tutorials.</I></blockquote> |
---|
83 | <UL><LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CFjadarite/Charge Flipping in GSAS.htm">Charge Flipping structure solution for jadarite</A> <A href="#prereq">*</A> |
---|
84 | [no example data or video]. |
---|
85 | <blockquote><I>Solving the structure of jadarite (HLiNaSiB3O8) by charge flipping from Pawley extracted intensities |
---|
86 | from a high resolution synchrotron powder pattern.</I></blockquote> |
---|
87 | </UL> |
---|
88 | <UL><LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CFsucrose/Charge Flipping - sucrose.htm">Charge Flipping structure solution for sucrose</A> <A href="#prereq">*</A> |
---|
89 | [no example data or video]. |
---|
90 | <blockquote><I>Solving the structure of sucrose (C12H22O11) by charge flipping from Pawley extracted intensities |
---|
91 | from a high resolution synchrotron powder pattern.</I></blockquote> |
---|
92 | </UL> |
---|
93 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CFXraySingleCrystal/CFSingleCrystal.htm">Charge Flipping structure solution with Xray single crystal data</A> |
---|
94 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CFXraySingleCrystal/data">Exercise files</A>]. |
---|
95 | <blockquote><I>Solving the structure of dipyridyl disulfate by charge flipping and then refine the structure by least-squares.</I></blockquote> |
---|
96 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF Charge Flipping/Charge Flipping with TOF single crystal data in GSASII.htm">Charge flipping with neutron TOF single crystal data</A> |
---|
97 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF Charge Flipping/data">Exercise files</A>]. |
---|
98 | <blockquote><I>Solving the crystal structure or rubrene (C42H28) from single crystal neutron data |
---|
99 | via charge flipping and then refine the structure by least squares.</I></blockquote> |
---|
100 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/MCsimanneal/MCSA in GSAS.htm">Monte-Carlo simulated annealing structure determination</A> |
---|
101 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/MCsimanneal/data">Exercise files</A>]. |
---|
102 | <blockquote><I>Solving the structures of 3-aminoquinoline and α-d-lactose monohydrate from powder diffraction data |
---|
103 | via Monte Carlo/Simulated Annealing (MC/SA).</I></blockquote> |
---|
104 | </UL><h4>Stacking Fault Modeling</H4><UL> |
---|
105 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/StackingFaults-I/Stacking Faults-I.htm">Stacking fault simulations for diamond</A> |
---|
106 | [link: <A href="https://anl.box.com/v/StackingFaults-I">video</A>, no example data]. |
---|
107 | <blockquote><I>This shows how to simulate the diffraction patterns from faulted diamond.</I></blockquote> |
---|
108 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/StackingFaults-II/Stacking Faults II.htm">Stacking fault simulations for Keokuk kaolinite</A> |
---|
109 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/StackingFaults-II/data">Exercise files</A>]. |
---|
110 | <blockquote><I>This shows how to simulate some diffraction patterns from well ordered Keokuk kaolinite (Al2Si2O5(OH)4) clay.</I></blockquote> |
---|
111 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/StackingFaults-III/Stacking Faults-III.htm">Stacking fault simulations for Georgia kaolinite</A> |
---|
112 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/StackingFaults-III/data">Exercise files</A>]. |
---|
113 | <blockquote><I>This shows how to simulate some diffraction patterns from poorly ordered Georgia kaolinite (Al2Si2O5(OH)4) clay.</I></blockquote> |
---|
114 | </UL><h4>Powder diffractometer calibration</H4><UL> |
---|
115 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CWInstDemo/FindProfParamCW.htm">Determining Starting Profile Parameters from a Standard</A> |
---|
116 | [links: <A href="https://anl.box.com/v/FindProfParamCW">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CWInstDemo/data">Exercise files</A>]. |
---|
117 | <blockquote><I>This shows how to determine profile parameters by fitting individual peaks |
---|
118 | with data collected on a standard using a lab diffractometer.</I></blockquote> |
---|
119 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/FPAfit/FPAfit.htm">Determining Profile Parameters with Fundamental Parameters</A> |
---|
120 | [no example data or video]. |
---|
121 | <blockquote><I>This shows how to determine profile parameters by fitting |
---|
122 | peaks that are computed using the NIST Fundamental Parameters Python |
---|
123 | code. |
---|
124 | Input is formulated to use FPA values similar to those in Topas.</I></blockquote> |
---|
125 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF Calibration/Calibration of a TOF powder diffractometer.htm">Calibration of a Neutron TOF diffractometer</A> |
---|
126 | [links: <A href="https://anl.box.com/v/CalibrationofaTOFpowderdiffrac">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF Calibration/data">Exercise files</A>]. |
---|
127 | <blockquote><I>This uses the fitted positions of all visible peaks in a pattern of NIST SRM 660b La11B6 |
---|
128 | (a=4.15689Ã
) obtained in a multiple single peak fit. The positions are compared to those expected from the |
---|
129 | known lattice parameters to establish the diffractometer constants (difC, difA, difB and Zero) used for |
---|
130 | calculating TOF peak positions from d-spacings. In addition, the peak fitting includes the various profile |
---|
131 | coefficients thus fully describing the instrument contribution to the peak profiles.</I></blockquote> |
---|
132 | </UL><h4>2D Image Processing</H4><UL> |
---|
133 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/2DCalibration/Calibration of an area detector in GSAS.htm">Calibration of an area detector</A> |
---|
134 | [links: <A href="https://anl.box.com/v/CalibrationofanareadetectorinG">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/2DCalibration/data">Exercise files</A>]. |
---|
135 | <blockquote><I>A demonstration of calibrating a Perkin-Elmer area detector, where the detector was intentionally tilted at 45 degrees. |
---|
136 | This exercise is the prerequisite for the next one.</I></blockquote> |
---|
137 | <UL><LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/2DIntegration/Integration of area detector data in GSAS.htm">Integration of area detector data</A> <A href="#prereq">*</A> |
---|
138 | [link: <A href="https://anl.box.com/v/Integrationofareadetectordatai">video</A>, no example data]. |
---|
139 | <blockquote><I>Integration of the image from a Perkin-Elmer area detector, where the detector was intentionally tilted at 45 degrees.</I></blockquote> |
---|
140 | </UL> |
---|
141 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/2DStrain/Strain fitting of 2D data in GSAS-II.htm">Strain fitting of 2D data</A> |
---|
142 | [links: <A href="https://anl.box.com/v/Strainfittingof2DdatainGSAS-II">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/2DStrain/data">Exercise files</A>]. |
---|
143 | <blockquote><I>This show how to determine 3 strain tensor values using the method of He & Smith (Adv. in X-ray Anal. 41, 501, 1997) |
---|
144 | directly froom a sequence of 2D imges from a loaded sample.</I></blockquote> |
---|
145 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/2DTexture/Texture analysis of 2D data in GSAS-II.htm">Texture analysis of 2D data</A> |
---|
146 | [links: <A href="https://anl.box.com/v/Textureanalysisof2DdatainGSAS-">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/2DTexture/data">Exercise files</A>]. |
---|
147 | <blockquote><I>This shows 3 different methods for determining texture via spherical harmonics from 2D x-ray diffraction images. </I></blockquote> |
---|
148 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/DeterminingWavelength/DeterminingWavelength.html">Area Detector Calibration with Multiple Distances: Determine Wavelength</A> |
---|
149 | [links: <A href="https://anl.box.com/v/DeterminingWavelength">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/DeterminingWavelength/data">Exercise files</A>]. |
---|
150 | <blockquote><I>To get an accurate wavelength, without knowing the sample-to-detector distance accurately, images recorded with |
---|
151 | several different distances can be used. This exercise shows how to determine the wavelength from such a series. |
---|
152 | This exercise is the prerequisite for the next one.</I></blockquote> |
---|
153 | <UL><LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/CalibrationTutorial/CalibrationTutorial.html">Area Detector Calibration with Multiple Distances: Calibrate Detector Distances</A> <A href="#prereq">*</A> |
---|
154 | [link: <A href="https://anl.box.com/v/CalibrationTutorial">video</A>, no example data]. |
---|
155 | <blockquote><I>To get an accurate wavelength, without knowing the sample-to-detector distance accurately, images recorded with |
---|
156 | several different distances can be used. After using the previous exercise to determine the wavelength, |
---|
157 | this exercise calibrates the detector distances and shows examples of how to mask, integrate, and save those parameters |
---|
158 | for future reuse.</I></blockquote> |
---|
159 | </UL> |
---|
160 | </UL><h4>Small-Angle Scattering</H4><UL> |
---|
161 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SAsize/Small Angle Size Distribution.htm">Small angle x-ray data size distribution (alumina powder)</A> |
---|
162 | [links: <A href="https://anl.box.com/v/SmallAngleSizeDistribution">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SAsize/data">Exercise files</A>]. |
---|
163 | <blockquote><I>This shows how to determine the size distribution of particles using data from a constant |
---|
164 | wavelength synchrotron X-ray USAXS instrument. This is the prerequisite for the next tutorial</I></blockquote> |
---|
165 | <UL><LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SAfit/Fitting Small Angle Scattering Data.htm">Fitting small angle x-ray data (alumina powder)</A> <A href="#prereq">*</A> |
---|
166 | [links: <A href="https://anl.box.com/v/FittingSmallAngleScatteringDat">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SAfit/data">Exercise files</A>]. |
---|
167 | <blockquote><I>This shows how to fit small angle scattering data using data from a constant wavelength synchrotron X-ray USAXS instrument. </I></blockquote> |
---|
168 | </UL> |
---|
169 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SAimages/Small Angle Image Processing.htm">Image Processing of small angle x-ray data</A> |
---|
170 | [links: <A href="https://anl.box.com/v/SmallAngleImageProcessing">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SAimages/data">Exercise files</A>]. |
---|
171 | <blockquote><I>This shows how to reduce 2D SAXS data to create 1D absolute scaled data. </I></blockquote> |
---|
172 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SAseqref/Sequential Refinement of Small Angle Scattering Data.htm">Sequential refinement with small angle scattering data</A> |
---|
173 | [links: <A href="https://anl.box.com/v/SequentialRefinementofSmallAng">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/SAseqref/data">Exercise files</A>]. |
---|
174 | <blockquote><I>This shows how to fit USAXS small angle scattering data for a suite of samples to demonstrate the |
---|
175 | sequential refinement technique in GSAS-II for SASD and demonstrates fitting with a hard sphere structure |
---|
176 | factor for non-dilute systems. </I></blockquote> |
---|
177 | </UL><h4>Other</H4><UL> |
---|
178 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/MerohedralTwins/Merohedral twin refinement in GSAS.htm">Merohedral twin refinements</A> |
---|
179 | [links: <A href="https://anl.box.com/v/MerohedraltwinrefinementinGSAS">video</A>, <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/MerohedralTwins/data">Exercise files</A>]. |
---|
180 | <blockquote><I>This shows how to use GSAS-II to refine the structure of a few single crystal structures where there is merohedral twinning. </I></blockquote> |
---|
181 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF Single Crystal Refinement/TOF single crystal refinement in GSAS.htm">Single crystal refinement from TOF data</A> |
---|
182 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/TOF Single Crystal Refinement/data">Exercise files</A>]. |
---|
183 | <blockquote><I>This shows how to refine the structure of sapphire (really corundum, Al2O3) from single crystal diffraction data |
---|
184 | collected at the SNS on the TOPAZ instrument at room temperature. </I></blockquote> |
---|
185 | <LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/PythonScript/Scripting.htm">Scripting a GSAS-II Refinement from Python</A> |
---|
186 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/PythonScript/data">Exercise files</A>]. |
---|
187 | <blockquote><I>This demonstrates the use of the GSASIIscriptable module. This uses a Python script to perform a refinement or |
---|
188 | computation, but without use of the GSAS-II graphical user interface. This is a prerequisite for the next tutorial.</I></blockquote> |
---|
189 | <UL><LI><A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/PythonScript/CommandLine.htm">Running a GSAS-II Refinement from the Command Line</A> <A href="#prereq">*</A> |
---|
190 | [link: <A href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/PythonScript/data">Exercise files</A>]. |
---|
191 | <blockquote><I>This shows a unix script that duplicates the previous Python Scripting GSAS-II tutorial. </I></blockquote> |
---|
192 | </UL> |
---|
193 | </UL> |
---|
194 | <A name=prereq>* Indented tutorials require the previous unindented tutorial as a prerequisite |
---|
195 | <h3>Tutorials with video-recorded examples</H3> |
---|
196 | <UL><LI><A href="https://anl.box.com/v/StartingGSAS">Starting GSAS-II</A></LI> |
---|
197 | <LI><A href="https://anl.box.com/v/NeutronCWPowderData">CW Neutron Powder fit for Yttrium-Iron Garnet</A></LI> |
---|
198 | <LI><A href="https://anl.box.com/v/LaboratoryX">Fitting laboratory X-ray powder data for fluoroapatite</A></LI> |
---|
199 | <LI><A href="https://anl.box.com/v/Combinedrefinement">Combined X-ray/CW-neutron refinement of PbSO4</A></LI> |
---|
200 | <LI><A href="https://anl.box.com/v/TOFcombinedXNRietveldrefinemen">Combined X-ray/TOF-neutron Rietveld refinement</A></LI> |
---|
201 | <LI><A href="https://anl.box.com/v/SimTutorial">Simulating Powder Diffraction with GSAS-II</A></LI> |
---|
202 | <LI><A href="https://anl.box.com/v/FitBkgTut">Fitting the Starting Background using Fixed Points</A></LI> |
---|
203 | <LI><A href="https://anl.box.com/v/SimpleMagnetic">Simple Magnetic Structure Analysis</A></LI> |
---|
204 | <LI><A href="https://anl.box.com/v/SequentialTutorial">Sequential refinement of multiple datasets</A></LI> |
---|
205 | <LI><A href="https://anl.box.com/v/ParametricFitting">Parametric Fitting and Pseudo Variables for Sequential Fits</A></LI> |
---|
206 | <LI><A href="https://anl.box.com/v/TOFSequentialSinglePeakFit">Sequential fitting of single peaks and strain analysis of result</A></LI> |
---|
207 | <LI><A href="https://anl.box.com/v/FitPeaks">Fitting individual peaks & autoindexing</A></LI> |
---|
208 | <LI><A href="https://anl.box.com/v/StackingFaults-I">Stacking fault simulations for diamond</A></LI> |
---|
209 | <LI><A href="https://anl.box.com/v/FindProfParamCW">Determining Starting Profile Parameters from a Standard</A></LI> |
---|
210 | <LI><A href="https://anl.box.com/v/CalibrationofaTOFpowderdiffrac">Calibration of a Neutron TOF diffractometer</A></LI> |
---|
211 | <LI><A href="https://anl.box.com/v/CalibrationofanareadetectorinG">Calibration of an area detector</A></LI> |
---|
212 | <LI><A href="https://anl.box.com/v/Integrationofareadetectordatai">Integration of area detector data</A></LI> |
---|
213 | <LI><A href="https://anl.box.com/v/Strainfittingof2DdatainGSAS-II">Strain fitting of 2D data</A></LI> |
---|
214 | <LI><A href="https://anl.box.com/v/Textureanalysisof2DdatainGSAS-">Texture analysis of 2D data</A></LI> |
---|
215 | <LI><A href="https://anl.box.com/v/DeterminingWavelength">Area Detector Calibration with Multiple Distances: Determine Wavelength</A></LI> |
---|
216 | <LI><A href="https://anl.box.com/v/CalibrationTutorial">Area Detector Calibration with Multiple Distances: Calibrate Detector Distances</A></LI> |
---|
217 | <LI><A href="https://anl.box.com/v/SmallAngleSizeDistribution">Small angle x-ray data size distribution (alumina powder)</A></LI> |
---|
218 | <LI><A href="https://anl.box.com/v/FittingSmallAngleScatteringDat">Fitting small angle x-ray data (alumina powder)</A></LI> |
---|
219 | <LI><A href="https://anl.box.com/v/SmallAngleImageProcessing">Image Processing of small angle x-ray data</A></LI> |
---|
220 | <LI><A href="https://anl.box.com/v/SequentialRefinementofSmallAng">Sequential refinement with small angle scattering data</A></LI> |
---|
221 | <LI><A href="https://anl.box.com/v/MerohedraltwinrefinementinGSAS">Merohedral twin refinements</A></LI> |
---|
222 | </UL> |
---|
223 | |
---|
224 | <P>The video tutorials are also <A href=https://pan.baidu.com/s/1C1jq1amfuVmcY2n91cQcsg> mirrored in China</A></P> |
---|