| 1 | <html xmlns:v="urn:schemas-microsoft-com:vml" |
|---|
| 2 | xmlns:o="urn:schemas-microsoft-com:office:office" |
|---|
| 3 | xmlns:w="urn:schemas-microsoft-com:office:word" |
|---|
| 4 | xmlns:m="http://schemas.microsoft.com/office/2004/12/omml" |
|---|
| 5 | xmlns="http://www.w3.org/TR/REC-html40"> |
|---|
| 6 | |
|---|
| 7 | <head> |
|---|
| 8 | <meta http-equiv=Content-Type content="text/html; charset=windows-1252"> |
|---|
| 9 | <meta name=ProgId content=Word.Document> |
|---|
| 10 | <meta name=Generator content="Microsoft Word 14"> |
|---|
| 11 | <meta name=Originator content="Microsoft Word 14"> |
|---|
| 12 | <link rel=File-List href="Small%20Angle%20Image%20Processing_files/filelist.xml"> |
|---|
| 13 | <link rel=Edit-Time-Data |
|---|
| 14 | href="Small%20Angle%20Image%20Processing_files/editdata.mso"> |
|---|
| 15 | <!--[if !mso]> |
|---|
| 16 | <style> |
|---|
| 17 | v\:* {behavior:url(#default#VML);} |
|---|
| 18 | o\:* {behavior:url(#default#VML);} |
|---|
| 19 | w\:* {behavior:url(#default#VML);} |
|---|
| 20 | .shape {behavior:url(#default#VML);} |
|---|
| 21 | </style> |
|---|
| 22 | <![endif]--><!--[if gte mso 9]><xml> |
|---|
| 23 | <o:DocumentProperties> |
|---|
| 24 | <o:Author>Von Dreele</o:Author> |
|---|
| 25 | <o:LastAuthor>Von Dreele</o:LastAuthor> |
|---|
| 26 | <o:Revision>9</o:Revision> |
|---|
| 27 | <o:TotalTime>2395</o:TotalTime> |
|---|
| 28 | <o:Created>2014-05-13T20:30:00Z</o:Created> |
|---|
| 29 | <o:LastSaved>2014-05-14T21:32:00Z</o:LastSaved> |
|---|
| 30 | <o:Pages>18</o:Pages> |
|---|
| 31 | <o:Words>1995</o:Words> |
|---|
| 32 | <o:Characters>11378</o:Characters> |
|---|
| 33 | <o:Company>Argonne National Laboratory</o:Company> |
|---|
| 34 | <o:Lines>94</o:Lines> |
|---|
| 35 | <o:Paragraphs>26</o:Paragraphs> |
|---|
| 36 | <o:CharactersWithSpaces>13347</o:CharactersWithSpaces> |
|---|
| 37 | <o:Version>14.00</o:Version> |
|---|
| 38 | </o:DocumentProperties> |
|---|
| 39 | <o:OfficeDocumentSettings> |
|---|
| 40 | <o:AllowPNG/> |
|---|
| 41 | </o:OfficeDocumentSettings> |
|---|
| 42 | </xml><![endif]--> |
|---|
| 43 | <link rel=dataStoreItem |
|---|
| 44 | href="Small%20Angle%20Image%20Processing_files/item0033.xml" |
|---|
| 45 | target="Small%20Angle%20Image%20Processing_files/props034.xml"> |
|---|
| 46 | <link rel=themeData |
|---|
| 47 | href="Small%20Angle%20Image%20Processing_files/themedata.thmx"> |
|---|
| 48 | <link rel=colorSchemeMapping |
|---|
| 49 | href="Small%20Angle%20Image%20Processing_files/colorschememapping.xml"> |
|---|
| 50 | <!--[if gte mso 9]><xml> |
|---|
| 51 | <w:WordDocument> |
|---|
| 52 | <w:Zoom>110</w:Zoom> |
|---|
| 53 | <w:SpellingState>Clean</w:SpellingState> |
|---|
| 54 | <w:GrammarState>Clean</w:GrammarState> |
|---|
| 55 | <w:TrackMoves>false</w:TrackMoves> |
|---|
| 56 | <w:TrackFormatting/> |
|---|
| 57 | <w:PunctuationKerning/> |
|---|
| 58 | <w:ValidateAgainstSchemas/> |
|---|
| 59 | <w:SaveIfXMLInvalid>false</w:SaveIfXMLInvalid> |
|---|
| 60 | <w:IgnoreMixedContent>false</w:IgnoreMixedContent> |
|---|
| 61 | <w:AlwaysShowPlaceholderText>false</w:AlwaysShowPlaceholderText> |
|---|
| 62 | <w:DoNotPromoteQF/> |
|---|
| 63 | <w:LidThemeOther>EN-US</w:LidThemeOther> |
|---|
| 64 | <w:LidThemeAsian>X-NONE</w:LidThemeAsian> |
|---|
| 65 | <w:LidThemeComplexScript>X-NONE</w:LidThemeComplexScript> |
|---|
| 66 | <w:Compatibility> |
|---|
| 67 | <w:BreakWrappedTables/> |
|---|
| 68 | <w:SnapToGridInCell/> |
|---|
| 69 | <w:WrapTextWithPunct/> |
|---|
| 70 | <w:UseAsianBreakRules/> |
|---|
| 71 | <w:DontGrowAutofit/> |
|---|
| 72 | <w:SplitPgBreakAndParaMark/> |
|---|
| 73 | <w:EnableOpenTypeKerning/> |
|---|
| 74 | <w:DontFlipMirrorIndents/> |
|---|
| 75 | <w:OverrideTableStyleHps/> |
|---|
| 76 | </w:Compatibility> |
|---|
| 77 | <w:BrowserLevel>MicrosoftInternetExplorer4</w:BrowserLevel> |
|---|
| 78 | <m:mathPr> |
|---|
| 79 | <m:mathFont m:val="Cambria Math"/> |
|---|
| 80 | <m:brkBin m:val="before"/> |
|---|
| 81 | <m:brkBinSub m:val="--"/> |
|---|
| 82 | <m:smallFrac m:val="off"/> |
|---|
| 83 | <m:dispDef/> |
|---|
| 84 | <m:lMargin m:val="0"/> |
|---|
| 85 | <m:rMargin m:val="0"/> |
|---|
| 86 | <m:defJc m:val="centerGroup"/> |
|---|
| 87 | <m:wrapIndent m:val="1440"/> |
|---|
| 88 | <m:intLim m:val="subSup"/> |
|---|
| 89 | <m:naryLim m:val="undOvr"/> |
|---|
| 90 | </m:mathPr></w:WordDocument> |
|---|
| 91 | </xml><![endif]--><!--[if gte mso 9]><xml> |
|---|
| 92 | <w:LatentStyles DefLockedState="false" DefUnhideWhenUsed="true" |
|---|
| 93 | DefSemiHidden="true" DefQFormat="false" DefPriority="99" |
|---|
| 94 | LatentStyleCount="267"> |
|---|
| 95 | <w:LsdException Locked="false" Priority="0" SemiHidden="false" |
|---|
| 96 | UnhideWhenUsed="false" QFormat="true" Name="Normal"/> |
|---|
| 97 | <w:LsdException Locked="false" Priority="9" SemiHidden="false" |
|---|
| 98 | UnhideWhenUsed="false" QFormat="true" Name="heading 1"/> |
|---|
| 99 | <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 2"/> |
|---|
| 100 | <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 3"/> |
|---|
| 101 | <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 4"/> |
|---|
| 102 | <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 5"/> |
|---|
| 103 | <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 6"/> |
|---|
| 104 | <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 7"/> |
|---|
| 105 | <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 8"/> |
|---|
| 106 | <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 9"/> |
|---|
| 107 | <w:LsdException Locked="false" Priority="39" Name="toc 1"/> |
|---|
| 108 | <w:LsdException Locked="false" Priority="39" Name="toc 2"/> |
|---|
| 109 | <w:LsdException Locked="false" Priority="39" Name="toc 3"/> |
|---|
| 110 | <w:LsdException Locked="false" Priority="39" Name="toc 4"/> |
|---|
| 111 | <w:LsdException Locked="false" Priority="39" Name="toc 5"/> |
|---|
| 112 | <w:LsdException Locked="false" Priority="39" Name="toc 6"/> |
|---|
| 113 | <w:LsdException Locked="false" Priority="39" Name="toc 7"/> |
|---|
| 114 | <w:LsdException Locked="false" Priority="39" Name="toc 8"/> |
|---|
| 115 | <w:LsdException Locked="false" Priority="39" Name="toc 9"/> |
|---|
| 116 | <w:LsdException Locked="false" Priority="35" QFormat="true" Name="caption"/> |
|---|
| 117 | <w:LsdException Locked="false" Priority="10" SemiHidden="false" |
|---|
| 118 | UnhideWhenUsed="false" QFormat="true" Name="Title"/> |
|---|
| 119 | <w:LsdException Locked="false" Priority="1" Name="Default Paragraph Font"/> |
|---|
| 120 | <w:LsdException Locked="false" Priority="11" SemiHidden="false" |
|---|
| 121 | UnhideWhenUsed="false" QFormat="true" Name="Subtitle"/> |
|---|
| 122 | <w:LsdException Locked="false" Priority="22" SemiHidden="false" |
|---|
| 123 | UnhideWhenUsed="false" QFormat="true" Name="Strong"/> |
|---|
| 124 | <w:LsdException Locked="false" Priority="20" SemiHidden="false" |
|---|
| 125 | UnhideWhenUsed="false" QFormat="true" Name="Emphasis"/> |
|---|
| 126 | <w:LsdException Locked="false" Priority="59" SemiHidden="false" |
|---|
| 127 | UnhideWhenUsed="false" Name="Table Grid"/> |
|---|
| 128 | <w:LsdException Locked="false" UnhideWhenUsed="false" Name="Placeholder Text"/> |
|---|
| 129 | <w:LsdException Locked="false" Priority="1" SemiHidden="false" |
|---|
| 130 | UnhideWhenUsed="false" QFormat="true" Name="No Spacing"/> |
|---|
| 131 | <w:LsdException Locked="false" Priority="60" SemiHidden="false" |
|---|
| 132 | UnhideWhenUsed="false" Name="Light Shading"/> |
|---|
| 133 | <w:LsdException Locked="false" Priority="61" SemiHidden="false" |
|---|
| 134 | UnhideWhenUsed="false" Name="Light List"/> |
|---|
| 135 | <w:LsdException Locked="false" Priority="62" SemiHidden="false" |
|---|
| 136 | UnhideWhenUsed="false" Name="Light Grid"/> |
|---|
| 137 | <w:LsdException Locked="false" Priority="63" SemiHidden="false" |
|---|
| 138 | UnhideWhenUsed="false" Name="Medium Shading 1"/> |
|---|
| 139 | <w:LsdException Locked="false" Priority="64" SemiHidden="false" |
|---|
| 140 | UnhideWhenUsed="false" Name="Medium Shading 2"/> |
|---|
| 141 | <w:LsdException Locked="false" Priority="65" SemiHidden="false" |
|---|
| 142 | UnhideWhenUsed="false" Name="Medium List 1"/> |
|---|
| 143 | <w:LsdException Locked="false" Priority="66" SemiHidden="false" |
|---|
| 144 | UnhideWhenUsed="false" Name="Medium List 2"/> |
|---|
| 145 | <w:LsdException Locked="false" Priority="67" SemiHidden="false" |
|---|
| 146 | UnhideWhenUsed="false" Name="Medium Grid 1"/> |
|---|
| 147 | <w:LsdException Locked="false" Priority="68" SemiHidden="false" |
|---|
| 148 | UnhideWhenUsed="false" Name="Medium Grid 2"/> |
|---|
| 149 | <w:LsdException Locked="false" Priority="69" SemiHidden="false" |
|---|
| 150 | UnhideWhenUsed="false" Name="Medium Grid 3"/> |
|---|
| 151 | <w:LsdException Locked="false" Priority="70" SemiHidden="false" |
|---|
| 152 | UnhideWhenUsed="false" Name="Dark List"/> |
|---|
| 153 | <w:LsdException Locked="false" Priority="71" SemiHidden="false" |
|---|
| 154 | UnhideWhenUsed="false" Name="Colorful Shading"/> |
|---|
| 155 | <w:LsdException Locked="false" Priority="72" SemiHidden="false" |
|---|
| 156 | UnhideWhenUsed="false" Name="Colorful List"/> |
|---|
| 157 | <w:LsdException Locked="false" Priority="73" SemiHidden="false" |
|---|
| 158 | UnhideWhenUsed="false" Name="Colorful Grid"/> |
|---|
| 159 | <w:LsdException Locked="false" Priority="60" SemiHidden="false" |
|---|
| 160 | UnhideWhenUsed="false" Name="Light Shading Accent 1"/> |
|---|
| 161 | <w:LsdException Locked="false" Priority="61" SemiHidden="false" |
|---|
| 162 | UnhideWhenUsed="false" Name="Light List Accent 1"/> |
|---|
| 163 | <w:LsdException Locked="false" Priority="62" SemiHidden="false" |
|---|
| 164 | UnhideWhenUsed="false" Name="Light Grid Accent 1"/> |
|---|
| 165 | <w:LsdException Locked="false" Priority="63" SemiHidden="false" |
|---|
| 166 | UnhideWhenUsed="false" Name="Medium Shading 1 Accent 1"/> |
|---|
| 167 | <w:LsdException Locked="false" Priority="64" SemiHidden="false" |
|---|
| 168 | UnhideWhenUsed="false" Name="Medium Shading 2 Accent 1"/> |
|---|
| 169 | <w:LsdException Locked="false" Priority="65" SemiHidden="false" |
|---|
| 170 | UnhideWhenUsed="false" Name="Medium List 1 Accent 1"/> |
|---|
| 171 | <w:LsdException Locked="false" UnhideWhenUsed="false" Name="Revision"/> |
|---|
| 172 | <w:LsdException Locked="false" Priority="34" SemiHidden="false" |
|---|
| 173 | UnhideWhenUsed="false" QFormat="true" Name="List Paragraph"/> |
|---|
| 174 | <w:LsdException Locked="false" Priority="29" SemiHidden="false" |
|---|
| 175 | UnhideWhenUsed="false" QFormat="true" Name="Quote"/> |
|---|
| 176 | <w:LsdException Locked="false" Priority="30" SemiHidden="false" |
|---|
| 177 | UnhideWhenUsed="false" QFormat="true" Name="Intense Quote"/> |
|---|
| 178 | <w:LsdException Locked="false" Priority="66" SemiHidden="false" |
|---|
| 179 | UnhideWhenUsed="false" Name="Medium List 2 Accent 1"/> |
|---|
| 180 | <w:LsdException Locked="false" Priority="67" SemiHidden="false" |
|---|
| 181 | UnhideWhenUsed="false" Name="Medium Grid 1 Accent 1"/> |
|---|
| 182 | <w:LsdException Locked="false" Priority="68" SemiHidden="false" |
|---|
| 183 | UnhideWhenUsed="false" Name="Medium Grid 2 Accent 1"/> |
|---|
| 184 | <w:LsdException Locked="false" Priority="69" SemiHidden="false" |
|---|
| 185 | UnhideWhenUsed="false" Name="Medium Grid 3 Accent 1"/> |
|---|
| 186 | <w:LsdException Locked="false" Priority="70" SemiHidden="false" |
|---|
| 187 | UnhideWhenUsed="false" Name="Dark List Accent 1"/> |
|---|
| 188 | <w:LsdException Locked="false" Priority="71" SemiHidden="false" |
|---|
| 189 | UnhideWhenUsed="false" Name="Colorful Shading Accent 1"/> |
|---|
| 190 | <w:LsdException Locked="false" Priority="72" SemiHidden="false" |
|---|
| 191 | UnhideWhenUsed="false" Name="Colorful List Accent 1"/> |
|---|
| 192 | <w:LsdException Locked="false" Priority="73" SemiHidden="false" |
|---|
| 193 | UnhideWhenUsed="false" Name="Colorful Grid Accent 1"/> |
|---|
| 194 | <w:LsdException Locked="false" Priority="60" SemiHidden="false" |
|---|
| 195 | UnhideWhenUsed="false" Name="Light Shading Accent 2"/> |
|---|
| 196 | <w:LsdException Locked="false" Priority="61" SemiHidden="false" |
|---|
| 197 | UnhideWhenUsed="false" Name="Light List Accent 2"/> |
|---|
| 198 | <w:LsdException Locked="false" Priority="62" SemiHidden="false" |
|---|
| 199 | UnhideWhenUsed="false" Name="Light Grid Accent 2"/> |
|---|
| 200 | <w:LsdException Locked="false" Priority="63" SemiHidden="false" |
|---|
| 201 | UnhideWhenUsed="false" Name="Medium Shading 1 Accent 2"/> |
|---|
| 202 | <w:LsdException Locked="false" Priority="64" SemiHidden="false" |
|---|
| 203 | UnhideWhenUsed="false" Name="Medium Shading 2 Accent 2"/> |
|---|
| 204 | <w:LsdException Locked="false" Priority="65" SemiHidden="false" |
|---|
| 205 | UnhideWhenUsed="false" Name="Medium List 1 Accent 2"/> |
|---|
| 206 | <w:LsdException Locked="false" Priority="66" SemiHidden="false" |
|---|
| 207 | UnhideWhenUsed="false" Name="Medium List 2 Accent 2"/> |
|---|
| 208 | <w:LsdException Locked="false" Priority="67" SemiHidden="false" |
|---|
| 209 | UnhideWhenUsed="false" Name="Medium Grid 1 Accent 2"/> |
|---|
| 210 | <w:LsdException Locked="false" Priority="68" SemiHidden="false" |
|---|
| 211 | UnhideWhenUsed="false" Name="Medium Grid 2 Accent 2"/> |
|---|
| 212 | <w:LsdException Locked="false" Priority="69" SemiHidden="false" |
|---|
| 213 | UnhideWhenUsed="false" Name="Medium Grid 3 Accent 2"/> |
|---|
| 214 | <w:LsdException Locked="false" Priority="70" SemiHidden="false" |
|---|
| 215 | UnhideWhenUsed="false" Name="Dark List Accent 2"/> |
|---|
| 216 | <w:LsdException Locked="false" Priority="71" SemiHidden="false" |
|---|
| 217 | UnhideWhenUsed="false" Name="Colorful Shading Accent 2"/> |
|---|
| 218 | <w:LsdException Locked="false" Priority="72" SemiHidden="false" |
|---|
| 219 | UnhideWhenUsed="false" Name="Colorful List Accent 2"/> |
|---|
| 220 | <w:LsdException Locked="false" Priority="73" SemiHidden="false" |
|---|
| 221 | UnhideWhenUsed="false" Name="Colorful Grid Accent 2"/> |
|---|
| 222 | <w:LsdException Locked="false" Priority="60" SemiHidden="false" |
|---|
| 223 | UnhideWhenUsed="false" Name="Light Shading Accent 3"/> |
|---|
| 224 | <w:LsdException Locked="false" Priority="61" SemiHidden="false" |
|---|
| 225 | UnhideWhenUsed="false" Name="Light List Accent 3"/> |
|---|
| 226 | <w:LsdException Locked="false" Priority="62" SemiHidden="false" |
|---|
| 227 | UnhideWhenUsed="false" Name="Light Grid Accent 3"/> |
|---|
| 228 | <w:LsdException Locked="false" Priority="63" SemiHidden="false" |
|---|
| 229 | UnhideWhenUsed="false" Name="Medium Shading 1 Accent 3"/> |
|---|
| 230 | <w:LsdException Locked="false" Priority="64" SemiHidden="false" |
|---|
| 231 | UnhideWhenUsed="false" Name="Medium Shading 2 Accent 3"/> |
|---|
| 232 | <w:LsdException Locked="false" Priority="65" SemiHidden="false" |
|---|
| 233 | UnhideWhenUsed="false" Name="Medium List 1 Accent 3"/> |
|---|
| 234 | <w:LsdException Locked="false" Priority="66" SemiHidden="false" |
|---|
| 235 | UnhideWhenUsed="false" Name="Medium List 2 Accent 3"/> |
|---|
| 236 | <w:LsdException Locked="false" Priority="67" SemiHidden="false" |
|---|
| 237 | UnhideWhenUsed="false" Name="Medium Grid 1 Accent 3"/> |
|---|
| 238 | <w:LsdException Locked="false" Priority="68" SemiHidden="false" |
|---|
| 239 | UnhideWhenUsed="false" Name="Medium Grid 2 Accent 3"/> |
|---|
| 240 | <w:LsdException Locked="false" Priority="69" SemiHidden="false" |
|---|
| 241 | UnhideWhenUsed="false" Name="Medium Grid 3 Accent 3"/> |
|---|
| 242 | <w:LsdException Locked="false" Priority="70" SemiHidden="false" |
|---|
| 243 | UnhideWhenUsed="false" Name="Dark List Accent 3"/> |
|---|
| 244 | <w:LsdException Locked="false" Priority="71" SemiHidden="false" |
|---|
| 245 | UnhideWhenUsed="false" Name="Colorful Shading Accent 3"/> |
|---|
| 246 | <w:LsdException Locked="false" Priority="72" SemiHidden="false" |
|---|
| 247 | UnhideWhenUsed="false" Name="Colorful List Accent 3"/> |
|---|
| 248 | <w:LsdException Locked="false" Priority="73" SemiHidden="false" |
|---|
| 249 | UnhideWhenUsed="false" Name="Colorful Grid Accent 3"/> |
|---|
| 250 | <w:LsdException Locked="false" Priority="60" SemiHidden="false" |
|---|
| 251 | UnhideWhenUsed="false" Name="Light Shading Accent 4"/> |
|---|
| 252 | <w:LsdException Locked="false" Priority="61" SemiHidden="false" |
|---|
| 253 | UnhideWhenUsed="false" Name="Light List Accent 4"/> |
|---|
| 254 | <w:LsdException Locked="false" Priority="62" SemiHidden="false" |
|---|
| 255 | UnhideWhenUsed="false" Name="Light Grid Accent 4"/> |
|---|
| 256 | <w:LsdException Locked="false" Priority="63" SemiHidden="false" |
|---|
| 257 | UnhideWhenUsed="false" Name="Medium Shading 1 Accent 4"/> |
|---|
| 258 | <w:LsdException Locked="false" Priority="64" SemiHidden="false" |
|---|
| 259 | UnhideWhenUsed="false" Name="Medium Shading 2 Accent 4"/> |
|---|
| 260 | <w:LsdException Locked="false" Priority="65" SemiHidden="false" |
|---|
| 261 | UnhideWhenUsed="false" Name="Medium List 1 Accent 4"/> |
|---|
| 262 | <w:LsdException Locked="false" Priority="66" SemiHidden="false" |
|---|
| 263 | UnhideWhenUsed="false" Name="Medium List 2 Accent 4"/> |
|---|
| 264 | <w:LsdException Locked="false" Priority="67" SemiHidden="false" |
|---|
| 265 | UnhideWhenUsed="false" Name="Medium Grid 1 Accent 4"/> |
|---|
| 266 | <w:LsdException Locked="false" Priority="68" SemiHidden="false" |
|---|
| 267 | UnhideWhenUsed="false" Name="Medium Grid 2 Accent 4"/> |
|---|
| 268 | <w:LsdException Locked="false" Priority="69" SemiHidden="false" |
|---|
| 269 | UnhideWhenUsed="false" Name="Medium Grid 3 Accent 4"/> |
|---|
| 270 | <w:LsdException Locked="false" Priority="70" SemiHidden="false" |
|---|
| 271 | UnhideWhenUsed="false" Name="Dark List Accent 4"/> |
|---|
| 272 | <w:LsdException Locked="false" Priority="71" SemiHidden="false" |
|---|
| 273 | UnhideWhenUsed="false" Name="Colorful Shading Accent 4"/> |
|---|
| 274 | <w:LsdException Locked="false" Priority="72" SemiHidden="false" |
|---|
| 275 | UnhideWhenUsed="false" Name="Colorful List Accent 4"/> |
|---|
| 276 | <w:LsdException Locked="false" Priority="73" SemiHidden="false" |
|---|
| 277 | UnhideWhenUsed="false" Name="Colorful Grid Accent 4"/> |
|---|
| 278 | <w:LsdException Locked="false" Priority="60" SemiHidden="false" |
|---|
| 279 | UnhideWhenUsed="false" Name="Light Shading Accent 5"/> |
|---|
| 280 | <w:LsdException Locked="false" Priority="61" SemiHidden="false" |
|---|
| 281 | UnhideWhenUsed="false" Name="Light List Accent 5"/> |
|---|
| 282 | <w:LsdException Locked="false" Priority="62" SemiHidden="false" |
|---|
| 283 | UnhideWhenUsed="false" Name="Light Grid Accent 5"/> |
|---|
| 284 | <w:LsdException Locked="false" Priority="63" SemiHidden="false" |
|---|
| 285 | UnhideWhenUsed="false" Name="Medium Shading 1 Accent 5"/> |
|---|
| 286 | <w:LsdException Locked="false" Priority="64" SemiHidden="false" |
|---|
| 287 | UnhideWhenUsed="false" Name="Medium Shading 2 Accent 5"/> |
|---|
| 288 | <w:LsdException Locked="false" Priority="65" SemiHidden="false" |
|---|
| 289 | UnhideWhenUsed="false" Name="Medium List 1 Accent 5"/> |
|---|
| 290 | <w:LsdException Locked="false" Priority="66" SemiHidden="false" |
|---|
| 291 | UnhideWhenUsed="false" Name="Medium List 2 Accent 5"/> |
|---|
| 292 | <w:LsdException Locked="false" Priority="67" SemiHidden="false" |
|---|
| 293 | UnhideWhenUsed="false" Name="Medium Grid 1 Accent 5"/> |
|---|
| 294 | <w:LsdException Locked="false" Priority="68" SemiHidden="false" |
|---|
| 295 | UnhideWhenUsed="false" Name="Medium Grid 2 Accent 5"/> |
|---|
| 296 | <w:LsdException Locked="false" Priority="69" SemiHidden="false" |
|---|
| 297 | UnhideWhenUsed="false" Name="Medium Grid 3 Accent 5"/> |
|---|
| 298 | <w:LsdException Locked="false" Priority="70" SemiHidden="false" |
|---|
| 299 | UnhideWhenUsed="false" Name="Dark List Accent 5"/> |
|---|
| 300 | <w:LsdException Locked="false" Priority="71" SemiHidden="false" |
|---|
| 301 | UnhideWhenUsed="false" Name="Colorful Shading Accent 5"/> |
|---|
| 302 | <w:LsdException Locked="false" Priority="72" SemiHidden="false" |
|---|
| 303 | UnhideWhenUsed="false" Name="Colorful List Accent 5"/> |
|---|
| 304 | <w:LsdException Locked="false" Priority="73" SemiHidden="false" |
|---|
| 305 | UnhideWhenUsed="false" Name="Colorful Grid Accent 5"/> |
|---|
| 306 | <w:LsdException Locked="false" Priority="60" SemiHidden="false" |
|---|
| 307 | UnhideWhenUsed="false" Name="Light Shading Accent 6"/> |
|---|
| 308 | <w:LsdException Locked="false" Priority="61" SemiHidden="false" |
|---|
| 309 | UnhideWhenUsed="false" Name="Light List Accent 6"/> |
|---|
| 310 | <w:LsdException Locked="false" Priority="62" SemiHidden="false" |
|---|
| 311 | UnhideWhenUsed="false" Name="Light Grid Accent 6"/> |
|---|
| 312 | <w:LsdException Locked="false" Priority="63" SemiHidden="false" |
|---|
| 313 | UnhideWhenUsed="false" Name="Medium Shading 1 Accent 6"/> |
|---|
| 314 | <w:LsdException Locked="false" Priority="64" SemiHidden="false" |
|---|
| 315 | UnhideWhenUsed="false" Name="Medium Shading 2 Accent 6"/> |
|---|
| 316 | <w:LsdException Locked="false" Priority="65" SemiHidden="false" |
|---|
| 317 | UnhideWhenUsed="false" Name="Medium List 1 Accent 6"/> |
|---|
| 318 | <w:LsdException Locked="false" Priority="66" SemiHidden="false" |
|---|
| 319 | UnhideWhenUsed="false" Name="Medium List 2 Accent 6"/> |
|---|
| 320 | <w:LsdException Locked="false" Priority="67" SemiHidden="false" |
|---|
| 321 | UnhideWhenUsed="false" Name="Medium Grid 1 Accent 6"/> |
|---|
| 322 | <w:LsdException Locked="false" Priority="68" SemiHidden="false" |
|---|
| 323 | UnhideWhenUsed="false" Name="Medium Grid 2 Accent 6"/> |
|---|
| 324 | <w:LsdException Locked="false" Priority="69" SemiHidden="false" |
|---|
| 325 | UnhideWhenUsed="false" Name="Medium Grid 3 Accent 6"/> |
|---|
| 326 | <w:LsdException Locked="false" Priority="70" SemiHidden="false" |
|---|
| 327 | UnhideWhenUsed="false" Name="Dark List Accent 6"/> |
|---|
| 328 | <w:LsdException Locked="false" Priority="71" SemiHidden="false" |
|---|
| 329 | UnhideWhenUsed="false" Name="Colorful Shading Accent 6"/> |
|---|
| 330 | <w:LsdException Locked="false" Priority="72" SemiHidden="false" |
|---|
| 331 | UnhideWhenUsed="false" Name="Colorful List Accent 6"/> |
|---|
| 332 | <w:LsdException Locked="false" Priority="73" SemiHidden="false" |
|---|
| 333 | UnhideWhenUsed="false" Name="Colorful Grid Accent 6"/> |
|---|
| 334 | <w:LsdException Locked="false" Priority="19" SemiHidden="false" |
|---|
| 335 | UnhideWhenUsed="false" QFormat="true" Name="Subtle Emphasis"/> |
|---|
| 336 | <w:LsdException Locked="false" Priority="21" SemiHidden="false" |
|---|
| 337 | UnhideWhenUsed="false" QFormat="true" Name="Intense Emphasis"/> |
|---|
| 338 | <w:LsdException Locked="false" Priority="31" SemiHidden="false" |
|---|
| 339 | UnhideWhenUsed="false" QFormat="true" Name="Subtle Reference"/> |
|---|
| 340 | <w:LsdException Locked="false" Priority="32" SemiHidden="false" |
|---|
| 341 | UnhideWhenUsed="false" QFormat="true" Name="Intense Reference"/> |
|---|
| 342 | <w:LsdException Locked="false" Priority="33" SemiHidden="false" |
|---|
| 343 | UnhideWhenUsed="false" QFormat="true" Name="Book Title"/> |
|---|
| 344 | <w:LsdException Locked="false" Priority="37" Name="Bibliography"/> |
|---|
| 345 | <w:LsdException Locked="false" Priority="39" QFormat="true" Name="TOC Heading"/> |
|---|
| 346 | </w:LatentStyles> |
|---|
| 347 | </xml><![endif]--> |
|---|
| 348 | <style> |
|---|
| 349 | <!-- |
|---|
| 350 | /* Font Definitions */ |
|---|
| 351 | @font-face |
|---|
| 352 | {font-family:Calibri; |
|---|
| 353 | panose-1:2 15 5 2 2 2 4 3 2 4; |
|---|
| 354 | mso-font-charset:0; |
|---|
| 355 | mso-generic-font-family:swiss; |
|---|
| 356 | mso-font-pitch:variable; |
|---|
| 357 | mso-font-signature:-536870145 1073786111 1 0 415 0;} |
|---|
| 358 | @font-face |
|---|
| 359 | {font-family:Tahoma; |
|---|
| 360 | panose-1:2 11 6 4 3 5 4 4 2 4; |
|---|
| 361 | mso-font-charset:0; |
|---|
| 362 | mso-generic-font-family:swiss; |
|---|
| 363 | mso-font-pitch:variable; |
|---|
| 364 | mso-font-signature:-520081665 -1073717157 41 0 66047 0;} |
|---|
| 365 | /* Style Definitions */ |
|---|
| 366 | p.MsoNormal, li.MsoNormal, div.MsoNormal |
|---|
| 367 | {mso-style-unhide:no; |
|---|
| 368 | mso-style-qformat:yes; |
|---|
| 369 | mso-style-parent:""; |
|---|
| 370 | margin:0in; |
|---|
| 371 | margin-bottom:.0001pt; |
|---|
| 372 | mso-pagination:widow-orphan; |
|---|
| 373 | font-size:12.0pt; |
|---|
| 374 | font-family:"Times New Roman","serif"; |
|---|
| 375 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 376 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 377 | h1 |
|---|
| 378 | {mso-style-priority:9; |
|---|
| 379 | mso-style-unhide:no; |
|---|
| 380 | mso-style-qformat:yes; |
|---|
| 381 | mso-style-link:"Heading 1 Char"; |
|---|
| 382 | mso-margin-top-alt:auto; |
|---|
| 383 | margin-right:0in; |
|---|
| 384 | mso-margin-bottom-alt:auto; |
|---|
| 385 | margin-left:0in; |
|---|
| 386 | mso-pagination:widow-orphan; |
|---|
| 387 | mso-outline-level:1; |
|---|
| 388 | font-size:24.0pt; |
|---|
| 389 | font-family:"Times New Roman","serif"; |
|---|
| 390 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 391 | mso-fareast-theme-font:minor-fareast; |
|---|
| 392 | font-weight:bold;} |
|---|
| 393 | h2 |
|---|
| 394 | {mso-style-priority:9; |
|---|
| 395 | mso-style-qformat:yes; |
|---|
| 396 | mso-style-link:"Heading 2 Char"; |
|---|
| 397 | mso-margin-top-alt:auto; |
|---|
| 398 | margin-right:0in; |
|---|
| 399 | mso-margin-bottom-alt:auto; |
|---|
| 400 | margin-left:0in; |
|---|
| 401 | mso-pagination:widow-orphan; |
|---|
| 402 | mso-outline-level:2; |
|---|
| 403 | font-size:18.0pt; |
|---|
| 404 | font-family:"Times New Roman","serif"; |
|---|
| 405 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 406 | mso-fareast-theme-font:minor-fareast; |
|---|
| 407 | font-weight:bold;} |
|---|
| 408 | h3 |
|---|
| 409 | {mso-style-noshow:yes; |
|---|
| 410 | mso-style-priority:9; |
|---|
| 411 | mso-style-qformat:yes; |
|---|
| 412 | mso-style-link:"Heading 3 Char"; |
|---|
| 413 | mso-margin-top-alt:auto; |
|---|
| 414 | margin-right:0in; |
|---|
| 415 | mso-margin-bottom-alt:auto; |
|---|
| 416 | margin-left:0in; |
|---|
| 417 | mso-pagination:widow-orphan; |
|---|
| 418 | mso-outline-level:3; |
|---|
| 419 | font-size:13.5pt; |
|---|
| 420 | font-family:"Times New Roman","serif"; |
|---|
| 421 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 422 | mso-fareast-theme-font:minor-fareast; |
|---|
| 423 | font-weight:bold;} |
|---|
| 424 | h4 |
|---|
| 425 | {mso-style-noshow:yes; |
|---|
| 426 | mso-style-priority:9; |
|---|
| 427 | mso-style-qformat:yes; |
|---|
| 428 | mso-style-link:"Heading 4 Char"; |
|---|
| 429 | mso-style-next:Normal; |
|---|
| 430 | margin-top:10.0pt; |
|---|
| 431 | margin-right:0in; |
|---|
| 432 | margin-bottom:0in; |
|---|
| 433 | margin-left:0in; |
|---|
| 434 | margin-bottom:.0001pt; |
|---|
| 435 | mso-pagination:widow-orphan lines-together; |
|---|
| 436 | page-break-after:avoid; |
|---|
| 437 | mso-outline-level:4; |
|---|
| 438 | font-size:13.0pt; |
|---|
| 439 | font-family:"Cambria","serif"; |
|---|
| 440 | mso-ascii-font-family:Cambria; |
|---|
| 441 | mso-ascii-theme-font:major-latin; |
|---|
| 442 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 443 | mso-fareast-theme-font:major-fareast; |
|---|
| 444 | mso-hansi-font-family:Cambria; |
|---|
| 445 | mso-hansi-theme-font:major-latin; |
|---|
| 446 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 447 | mso-bidi-theme-font:major-bidi; |
|---|
| 448 | color:#4F81BD; |
|---|
| 449 | mso-themecolor:accent1; |
|---|
| 450 | font-weight:bold; |
|---|
| 451 | font-style:italic;} |
|---|
| 452 | h5 |
|---|
| 453 | {mso-style-noshow:yes; |
|---|
| 454 | mso-style-priority:9; |
|---|
| 455 | mso-style-qformat:yes; |
|---|
| 456 | mso-style-link:"Heading 5 Char"; |
|---|
| 457 | mso-margin-top-alt:auto; |
|---|
| 458 | margin-right:0in; |
|---|
| 459 | mso-margin-bottom-alt:auto; |
|---|
| 460 | margin-left:0in; |
|---|
| 461 | mso-pagination:widow-orphan; |
|---|
| 462 | mso-outline-level:5; |
|---|
| 463 | font-size:12.0pt; |
|---|
| 464 | font-family:"Times New Roman","serif"; |
|---|
| 465 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 466 | mso-fareast-theme-font:minor-fareast; |
|---|
| 467 | color:#4F4FFF; |
|---|
| 468 | font-weight:bold;} |
|---|
| 469 | a:link, span.MsoHyperlink |
|---|
| 470 | {mso-style-priority:99; |
|---|
| 471 | color:blue; |
|---|
| 472 | text-decoration:underline; |
|---|
| 473 | text-underline:single;} |
|---|
| 474 | a:visited, span.MsoHyperlinkFollowed |
|---|
| 475 | {mso-style-noshow:yes; |
|---|
| 476 | mso-style-priority:99; |
|---|
| 477 | color:purple; |
|---|
| 478 | text-decoration:underline; |
|---|
| 479 | text-underline:single;} |
|---|
| 480 | p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap |
|---|
| 481 | {mso-style-noshow:yes; |
|---|
| 482 | mso-style-priority:99; |
|---|
| 483 | mso-style-link:"Document Map Char"; |
|---|
| 484 | margin:0in; |
|---|
| 485 | margin-bottom:.0001pt; |
|---|
| 486 | mso-pagination:widow-orphan; |
|---|
| 487 | font-size:8.0pt; |
|---|
| 488 | font-family:"Tahoma","sans-serif"; |
|---|
| 489 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 490 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 491 | p |
|---|
| 492 | {mso-style-noshow:yes; |
|---|
| 493 | mso-style-priority:99; |
|---|
| 494 | mso-margin-top-alt:auto; |
|---|
| 495 | margin-right:0in; |
|---|
| 496 | mso-margin-bottom-alt:auto; |
|---|
| 497 | margin-left:0in; |
|---|
| 498 | mso-pagination:widow-orphan; |
|---|
| 499 | font-size:12.0pt; |
|---|
| 500 | font-family:"Times New Roman","serif"; |
|---|
| 501 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 502 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 503 | pre |
|---|
| 504 | {mso-style-noshow:yes; |
|---|
| 505 | mso-style-priority:99; |
|---|
| 506 | mso-style-link:"HTML Preformatted Char"; |
|---|
| 507 | margin:0in; |
|---|
| 508 | margin-bottom:.0001pt; |
|---|
| 509 | mso-pagination:widow-orphan; |
|---|
| 510 | tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt; |
|---|
| 511 | font-size:10.0pt; |
|---|
| 512 | font-family:"Courier New"; |
|---|
| 513 | mso-fareast-font-family:"Times New Roman";} |
|---|
| 514 | p.MsoAcetate, li.MsoAcetate, div.MsoAcetate |
|---|
| 515 | {mso-style-noshow:yes; |
|---|
| 516 | mso-style-priority:99; |
|---|
| 517 | mso-style-link:"Balloon Text Char"; |
|---|
| 518 | margin:0in; |
|---|
| 519 | margin-bottom:.0001pt; |
|---|
| 520 | mso-pagination:widow-orphan; |
|---|
| 521 | font-size:8.0pt; |
|---|
| 522 | font-family:"Tahoma","sans-serif"; |
|---|
| 523 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 524 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 525 | span.MsoPlaceholderText |
|---|
| 526 | {mso-style-noshow:yes; |
|---|
| 527 | mso-style-priority:99; |
|---|
| 528 | mso-style-unhide:no; |
|---|
| 529 | color:gray;} |
|---|
| 530 | p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing |
|---|
| 531 | {mso-style-noshow:yes; |
|---|
| 532 | mso-style-priority:1; |
|---|
| 533 | mso-style-unhide:no; |
|---|
| 534 | mso-style-qformat:yes; |
|---|
| 535 | mso-style-parent:""; |
|---|
| 536 | margin:0in; |
|---|
| 537 | margin-bottom:.0001pt; |
|---|
| 538 | mso-pagination:widow-orphan; |
|---|
| 539 | font-size:12.0pt; |
|---|
| 540 | font-family:"Times New Roman","serif"; |
|---|
| 541 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 542 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 543 | p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph |
|---|
| 544 | {mso-style-noshow:yes; |
|---|
| 545 | mso-style-priority:34; |
|---|
| 546 | mso-style-unhide:no; |
|---|
| 547 | mso-style-qformat:yes; |
|---|
| 548 | margin-top:0in; |
|---|
| 549 | margin-right:0in; |
|---|
| 550 | margin-bottom:0in; |
|---|
| 551 | margin-left:.5in; |
|---|
| 552 | margin-bottom:.0001pt; |
|---|
| 553 | mso-add-space:auto; |
|---|
| 554 | mso-pagination:widow-orphan; |
|---|
| 555 | font-size:12.0pt; |
|---|
| 556 | font-family:"Times New Roman","serif"; |
|---|
| 557 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 558 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 559 | p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst |
|---|
| 560 | {mso-style-noshow:yes; |
|---|
| 561 | mso-style-priority:34; |
|---|
| 562 | mso-style-unhide:no; |
|---|
| 563 | mso-style-qformat:yes; |
|---|
| 564 | mso-style-type:export-only; |
|---|
| 565 | margin-top:0in; |
|---|
| 566 | margin-right:0in; |
|---|
| 567 | margin-bottom:0in; |
|---|
| 568 | margin-left:.5in; |
|---|
| 569 | margin-bottom:.0001pt; |
|---|
| 570 | mso-add-space:auto; |
|---|
| 571 | mso-pagination:widow-orphan; |
|---|
| 572 | font-size:12.0pt; |
|---|
| 573 | font-family:"Times New Roman","serif"; |
|---|
| 574 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 575 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 576 | p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle |
|---|
| 577 | {mso-style-noshow:yes; |
|---|
| 578 | mso-style-priority:34; |
|---|
| 579 | mso-style-unhide:no; |
|---|
| 580 | mso-style-qformat:yes; |
|---|
| 581 | mso-style-type:export-only; |
|---|
| 582 | margin-top:0in; |
|---|
| 583 | margin-right:0in; |
|---|
| 584 | margin-bottom:0in; |
|---|
| 585 | margin-left:.5in; |
|---|
| 586 | margin-bottom:.0001pt; |
|---|
| 587 | mso-add-space:auto; |
|---|
| 588 | mso-pagination:widow-orphan; |
|---|
| 589 | font-size:12.0pt; |
|---|
| 590 | font-family:"Times New Roman","serif"; |
|---|
| 591 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 592 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 593 | p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast |
|---|
| 594 | {mso-style-noshow:yes; |
|---|
| 595 | mso-style-priority:34; |
|---|
| 596 | mso-style-unhide:no; |
|---|
| 597 | mso-style-qformat:yes; |
|---|
| 598 | mso-style-type:export-only; |
|---|
| 599 | margin-top:0in; |
|---|
| 600 | margin-right:0in; |
|---|
| 601 | margin-bottom:0in; |
|---|
| 602 | margin-left:.5in; |
|---|
| 603 | margin-bottom:.0001pt; |
|---|
| 604 | mso-add-space:auto; |
|---|
| 605 | mso-pagination:widow-orphan; |
|---|
| 606 | font-size:12.0pt; |
|---|
| 607 | font-family:"Times New Roman","serif"; |
|---|
| 608 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 609 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 610 | span.MsoIntenseReference |
|---|
| 611 | {mso-style-priority:32; |
|---|
| 612 | mso-style-unhide:no; |
|---|
| 613 | mso-style-qformat:yes; |
|---|
| 614 | font-variant:small-caps; |
|---|
| 615 | color:#C0504D; |
|---|
| 616 | mso-themecolor:accent2; |
|---|
| 617 | letter-spacing:.25pt; |
|---|
| 618 | font-weight:bold; |
|---|
| 619 | text-decoration:underline; |
|---|
| 620 | text-underline:single;} |
|---|
| 621 | span.Heading1Char |
|---|
| 622 | {mso-style-name:"Heading 1 Char"; |
|---|
| 623 | mso-style-priority:9; |
|---|
| 624 | mso-style-unhide:no; |
|---|
| 625 | mso-style-locked:yes; |
|---|
| 626 | mso-style-link:"Heading 1"; |
|---|
| 627 | mso-ansi-font-size:24.0pt; |
|---|
| 628 | mso-bidi-font-size:24.0pt; |
|---|
| 629 | font-family:"Times New Roman","serif"; |
|---|
| 630 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 631 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 632 | mso-fareast-theme-font:minor-fareast; |
|---|
| 633 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 634 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 635 | mso-font-kerning:18.0pt; |
|---|
| 636 | font-weight:bold;} |
|---|
| 637 | span.Heading2Char |
|---|
| 638 | {mso-style-name:"Heading 2 Char"; |
|---|
| 639 | mso-style-priority:9; |
|---|
| 640 | mso-style-unhide:no; |
|---|
| 641 | mso-style-locked:yes; |
|---|
| 642 | mso-style-link:"Heading 2"; |
|---|
| 643 | mso-ansi-font-size:18.0pt; |
|---|
| 644 | mso-bidi-font-size:18.0pt; |
|---|
| 645 | font-family:"Times New Roman","serif"; |
|---|
| 646 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 647 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 648 | mso-fareast-theme-font:minor-fareast; |
|---|
| 649 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 650 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 651 | font-weight:bold;} |
|---|
| 652 | span.Heading3Char |
|---|
| 653 | {mso-style-name:"Heading 3 Char"; |
|---|
| 654 | mso-style-noshow:yes; |
|---|
| 655 | mso-style-priority:9; |
|---|
| 656 | mso-style-unhide:no; |
|---|
| 657 | mso-style-locked:yes; |
|---|
| 658 | mso-style-link:"Heading 3"; |
|---|
| 659 | mso-ansi-font-size:13.5pt; |
|---|
| 660 | mso-bidi-font-size:13.5pt; |
|---|
| 661 | font-family:"Times New Roman","serif"; |
|---|
| 662 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 663 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 664 | mso-fareast-theme-font:minor-fareast; |
|---|
| 665 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 666 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 667 | font-weight:bold;} |
|---|
| 668 | span.Heading4Char |
|---|
| 669 | {mso-style-name:"Heading 4 Char"; |
|---|
| 670 | mso-style-noshow:yes; |
|---|
| 671 | mso-style-priority:9; |
|---|
| 672 | mso-style-unhide:no; |
|---|
| 673 | mso-style-locked:yes; |
|---|
| 674 | mso-style-link:"Heading 4"; |
|---|
| 675 | mso-ansi-font-size:13.0pt; |
|---|
| 676 | mso-bidi-font-size:13.0pt; |
|---|
| 677 | font-family:"Cambria","serif"; |
|---|
| 678 | mso-ascii-font-family:Cambria; |
|---|
| 679 | mso-ascii-theme-font:major-latin; |
|---|
| 680 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 681 | mso-fareast-theme-font:major-fareast; |
|---|
| 682 | mso-hansi-font-family:Cambria; |
|---|
| 683 | mso-hansi-theme-font:major-latin; |
|---|
| 684 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 685 | mso-bidi-theme-font:major-bidi; |
|---|
| 686 | color:#4F81BD; |
|---|
| 687 | mso-themecolor:accent1; |
|---|
| 688 | font-weight:bold; |
|---|
| 689 | font-style:italic;} |
|---|
| 690 | span.Heading5Char |
|---|
| 691 | {mso-style-name:"Heading 5 Char"; |
|---|
| 692 | mso-style-noshow:yes; |
|---|
| 693 | mso-style-priority:9; |
|---|
| 694 | mso-style-unhide:no; |
|---|
| 695 | mso-style-locked:yes; |
|---|
| 696 | mso-style-link:"Heading 5"; |
|---|
| 697 | mso-ansi-font-size:12.0pt; |
|---|
| 698 | mso-bidi-font-size:12.0pt; |
|---|
| 699 | font-family:"Times New Roman","serif"; |
|---|
| 700 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 701 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 702 | mso-fareast-theme-font:minor-fareast; |
|---|
| 703 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 704 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 705 | color:#4F4FFF; |
|---|
| 706 | font-weight:bold;} |
|---|
| 707 | span.HTMLPreformattedChar |
|---|
| 708 | {mso-style-name:"HTML Preformatted Char"; |
|---|
| 709 | mso-style-noshow:yes; |
|---|
| 710 | mso-style-priority:99; |
|---|
| 711 | mso-style-unhide:no; |
|---|
| 712 | mso-style-locked:yes; |
|---|
| 713 | mso-style-link:"HTML Preformatted"; |
|---|
| 714 | font-family:"Courier New"; |
|---|
| 715 | mso-ascii-font-family:"Courier New"; |
|---|
| 716 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 717 | mso-hansi-font-family:"Courier New"; |
|---|
| 718 | mso-bidi-font-family:"Courier New";} |
|---|
| 719 | span.DocumentMapChar |
|---|
| 720 | {mso-style-name:"Document Map Char"; |
|---|
| 721 | mso-style-noshow:yes; |
|---|
| 722 | mso-style-priority:99; |
|---|
| 723 | mso-style-unhide:no; |
|---|
| 724 | mso-style-locked:yes; |
|---|
| 725 | mso-style-link:"Document Map"; |
|---|
| 726 | mso-ansi-font-size:8.0pt; |
|---|
| 727 | mso-bidi-font-size:8.0pt; |
|---|
| 728 | font-family:"Tahoma","sans-serif"; |
|---|
| 729 | mso-ascii-font-family:Tahoma; |
|---|
| 730 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 731 | mso-fareast-theme-font:minor-fareast; |
|---|
| 732 | mso-hansi-font-family:Tahoma; |
|---|
| 733 | mso-bidi-font-family:Tahoma;} |
|---|
| 734 | span.BalloonTextChar |
|---|
| 735 | {mso-style-name:"Balloon Text Char"; |
|---|
| 736 | mso-style-noshow:yes; |
|---|
| 737 | mso-style-priority:99; |
|---|
| 738 | mso-style-unhide:no; |
|---|
| 739 | mso-style-locked:yes; |
|---|
| 740 | mso-style-link:"Balloon Text"; |
|---|
| 741 | mso-ansi-font-size:8.0pt; |
|---|
| 742 | mso-bidi-font-size:8.0pt; |
|---|
| 743 | font-family:"Tahoma","sans-serif"; |
|---|
| 744 | mso-ascii-font-family:Tahoma; |
|---|
| 745 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 746 | mso-fareast-theme-font:minor-fareast; |
|---|
| 747 | mso-hansi-font-family:Tahoma; |
|---|
| 748 | mso-bidi-font-family:Tahoma;} |
|---|
| 749 | span.SpellE |
|---|
| 750 | {mso-style-name:""; |
|---|
| 751 | mso-spl-e:yes;} |
|---|
| 752 | span.GramE |
|---|
| 753 | {mso-style-name:""; |
|---|
| 754 | mso-gram-e:yes;} |
|---|
| 755 | .MsoChpDefault |
|---|
| 756 | {mso-style-type:export-only; |
|---|
| 757 | mso-default-props:yes; |
|---|
| 758 | font-size:10.0pt; |
|---|
| 759 | mso-ansi-font-size:10.0pt; |
|---|
| 760 | mso-bidi-font-size:10.0pt; |
|---|
| 761 | font-family:"Calibri","sans-serif"; |
|---|
| 762 | mso-ascii-font-family:Calibri; |
|---|
| 763 | mso-ascii-theme-font:minor-latin; |
|---|
| 764 | mso-fareast-font-family:Calibri; |
|---|
| 765 | mso-fareast-theme-font:minor-latin; |
|---|
| 766 | mso-hansi-font-family:Calibri; |
|---|
| 767 | mso-hansi-theme-font:minor-latin; |
|---|
| 768 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 769 | mso-bidi-theme-font:minor-bidi;} |
|---|
| 770 | @page WordSection1 |
|---|
| 771 | {size:8.5in 11.0in; |
|---|
| 772 | margin:1.0in 1.0in 1.0in 1.0in; |
|---|
| 773 | mso-header-margin:.5in; |
|---|
| 774 | mso-footer-margin:.5in; |
|---|
| 775 | mso-paper-source:0;} |
|---|
| 776 | div.WordSection1 |
|---|
| 777 | {page:WordSection1;} |
|---|
| 778 | --> |
|---|
| 779 | </style> |
|---|
| 780 | <!--[if gte mso 10]> |
|---|
| 781 | <style> |
|---|
| 782 | /* Style Definitions */ |
|---|
| 783 | table.MsoNormalTable |
|---|
| 784 | {mso-style-name:"Table Normal"; |
|---|
| 785 | mso-tstyle-rowband-size:0; |
|---|
| 786 | mso-tstyle-colband-size:0; |
|---|
| 787 | mso-style-noshow:yes; |
|---|
| 788 | mso-style-priority:99; |
|---|
| 789 | mso-style-parent:""; |
|---|
| 790 | mso-padding-alt:0in 5.4pt 0in 5.4pt; |
|---|
| 791 | mso-para-margin:0in; |
|---|
| 792 | mso-para-margin-bottom:.0001pt; |
|---|
| 793 | mso-pagination:widow-orphan; |
|---|
| 794 | font-size:10.0pt; |
|---|
| 795 | font-family:"Calibri","sans-serif"; |
|---|
| 796 | mso-ascii-font-family:Calibri; |
|---|
| 797 | mso-ascii-theme-font:minor-latin; |
|---|
| 798 | mso-hansi-font-family:Calibri; |
|---|
| 799 | mso-hansi-theme-font:minor-latin;} |
|---|
| 800 | table.MsoTableGrid |
|---|
| 801 | {mso-style-name:"Table Grid"; |
|---|
| 802 | mso-tstyle-rowband-size:0; |
|---|
| 803 | mso-tstyle-colband-size:0; |
|---|
| 804 | mso-style-priority:59; |
|---|
| 805 | mso-style-unhide:no; |
|---|
| 806 | border:solid windowtext 1.0pt; |
|---|
| 807 | mso-border-alt:solid windowtext .5pt; |
|---|
| 808 | mso-padding-alt:0in 5.4pt 0in 5.4pt; |
|---|
| 809 | mso-border-insideh:.5pt solid windowtext; |
|---|
| 810 | mso-border-insidev:.5pt solid windowtext; |
|---|
| 811 | mso-para-margin:0in; |
|---|
| 812 | mso-para-margin-bottom:.0001pt; |
|---|
| 813 | mso-pagination:widow-orphan; |
|---|
| 814 | font-size:10.0pt; |
|---|
| 815 | font-family:"Calibri","sans-serif"; |
|---|
| 816 | mso-ascii-font-family:Calibri; |
|---|
| 817 | mso-ascii-theme-font:minor-latin; |
|---|
| 818 | mso-hansi-font-family:Calibri; |
|---|
| 819 | mso-hansi-theme-font:minor-latin;} |
|---|
| 820 | </style> |
|---|
| 821 | <![endif]--><!--[if gte mso 9]><xml> |
|---|
| 822 | <o:shapedefaults v:ext="edit" spidmax="1027"/> |
|---|
| 823 | </xml><![endif]--><!--[if gte mso 9]><xml> |
|---|
| 824 | <o:shapelayout v:ext="edit"> |
|---|
| 825 | <o:idmap v:ext="edit" data="1"/> |
|---|
| 826 | <o:rules v:ext="edit"> |
|---|
| 827 | <o:r id="V:Rule1" type="connector" idref="#Straight_x0020_Arrow_x0020_Connector_x0020_21"/> |
|---|
| 828 | </o:rules> |
|---|
| 829 | </o:shapelayout></xml><![endif]--> |
|---|
| 830 | </head> |
|---|
| 831 | |
|---|
| 832 | <body lang=EN-US link=blue vlink=purple style='tab-interval:.5in'> |
|---|
| 833 | |
|---|
| 834 | <div class=WordSection1> |
|---|
| 835 | |
|---|
| 836 | <h1><strong>Small Angle X-Ray Data Image Processing<o:p></o:p></strong></h1> |
|---|
| 837 | |
|---|
| 838 | <p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In |
|---|
| 839 | this tutorial you will reduce 2D SAXS data to create 1D absolute scaled data. |
|---|
| 840 | The data were collected at APS on beam line 15ID on some polymer base materials |
|---|
| 841 | to be used for liquid crystal displays. The processing has several steps including |
|---|
| 842 | detector calibration (i.e. determine sample-detector distance & tilt), |
|---|
| 843 | integration and scaling to an absolute scaled glassy carbon measurement. The |
|---|
| 844 | data were collected at a wavelength of 1.0332Å with a <span class=SpellE>MarCCD</span> |
|---|
| 845 | detector placed ~570mm from the sample. Note that menu entries are listed in |
|---|
| 846 | bold face below as <b style='mso-bidi-font-weight:normal'><span |
|---|
| 847 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 848 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
|---|
| 849 | minor-latin'>Help/About GSAS-II</span></b>, which lists first the name of the |
|---|
| 850 | menu (here <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 851 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 852 | minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Help</span></b>) |
|---|
| 853 | and second the name of the entry in the menu (here <b style='mso-bidi-font-weight: |
|---|
| 854 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 855 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; |
|---|
| 856 | mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).<span |
|---|
| 857 | style='mso-spacerun:yes'> </span><span style='mso-fareast-font-family:Calibri; |
|---|
| 858 | mso-fareast-theme-font:minor-latin;mso-bidi-font-weight:bold;mso-bidi-font-style: |
|---|
| 859 | italic'><o:p></o:p></span></p> |
|---|
| 860 | |
|---|
| 861 | <p class=MsoNormal>If you have not done so already, <a |
|---|
| 862 | href="Starting%20GSAS.htm">start GSAS-II</a>.</p> |
|---|
| 863 | |
|---|
| 864 | <h2>Step 1: Detector calibration</h2> |
|---|
| 865 | |
|---|
| 866 | <p class=MsoNormal>The detector position is determined by using an image |
|---|
| 867 | collected from silver <span class=SpellE>behenate</span>; do <b |
|---|
| 868 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 869 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Data/Read |
|---|
| 870 | Image data
</span></b> and a file selection dialog box will appear</p> |
|---|
| 871 | |
|---|
| 872 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype |
|---|
| 873 | id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t" |
|---|
| 874 | path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f"> |
|---|
| 875 | <v:stroke joinstyle="miter"/> |
|---|
| 876 | <v:formulas> |
|---|
| 877 | <v:f eqn="if lineDrawn pixelLineWidth 0"/> |
|---|
| 878 | <v:f eqn="sum @0 1 0"/> |
|---|
| 879 | <v:f eqn="sum 0 0 @1"/> |
|---|
| 880 | <v:f eqn="prod @2 1 2"/> |
|---|
| 881 | <v:f eqn="prod @3 21600 pixelWidth"/> |
|---|
| 882 | <v:f eqn="prod @3 21600 pixelHeight"/> |
|---|
| 883 | <v:f eqn="sum @0 0 1"/> |
|---|
| 884 | <v:f eqn="prod @6 1 2"/> |
|---|
| 885 | <v:f eqn="prod @7 21600 pixelWidth"/> |
|---|
| 886 | <v:f eqn="sum @8 21600 0"/> |
|---|
| 887 | <v:f eqn="prod @7 21600 pixelHeight"/> |
|---|
| 888 | <v:f eqn="sum @10 21600 0"/> |
|---|
| 889 | </v:formulas> |
|---|
| 890 | <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> |
|---|
| 891 | <o:lock v:ext="edit" aspectratio="t"/> |
|---|
| 892 | </v:shapetype><v:shape id="_x0000_i1065" type="#_x0000_t75" style='width:537pt; |
|---|
| 893 | height:397.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 894 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image001.png" |
|---|
| 895 | o:title=""/> |
|---|
| 896 | </v:shape><![endif]--><![if !vml]><img border=0 width=716 height=530 |
|---|
| 897 | src="Small%20Angle%20Image%20Processing_files/image001.png" v:shapes="_x0000_i1065"><![endif]></span></p> |
|---|
| 898 | |
|---|
| 899 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 900 | |
|---|
| 901 | <p class=MsoNormal>Go to <b style='mso-bidi-font-weight:normal'><span |
|---|
| 902 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 903 | mso-hansi-theme-font:minor-latin'>Exercises/Small angle/Image reduction</span></b> |
|---|
| 904 | and select <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 905 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 906 | minor-latin'>AgBehenate_003.tif</span></b> with either a mouse button double click |
|---|
| 907 | or <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 908 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Open</span></b>; |
|---|
| 909 | the image will appear</p> |
|---|
| 910 | |
|---|
| 911 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 912 | id="Picture_x0020_16" o:spid="_x0000_i1064" type="#_x0000_t75" style='width:525pt; |
|---|
| 913 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 914 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image002.png" |
|---|
| 915 | o:title=""/> |
|---|
| 916 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 917 | src="Small%20Angle%20Image%20Processing_files/image002.png" v:shapes="Picture_x0020_16"><![endif]></span></p> |
|---|
| 918 | |
|---|
| 919 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 920 | |
|---|
| 921 | <p class=MsoNormal>And the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 922 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 923 | mso-hansi-theme-font:minor-latin'>Image controls</span></b> window will show</p> |
|---|
| 924 | |
|---|
| 925 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 926 | id="_x0000_i1063" type="#_x0000_t75" style='width:472.5pt;height:388.5pt; |
|---|
| 927 | visibility:visible;mso-wrap-style:square'> |
|---|
| 928 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image003.png" |
|---|
| 929 | o:title=""/> |
|---|
| 930 | </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 |
|---|
| 931 | src="Small%20Angle%20Image%20Processing_files/image003.png" v:shapes="_x0000_i1063"><![endif]></span></p> |
|---|
| 932 | |
|---|
| 933 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 934 | |
|---|
| 935 | <p class=MsoNormal>Note the default <b style='mso-bidi-font-weight:normal'><span |
|---|
| 936 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 937 | mso-hansi-theme-font:minor-latin'>Type of image data</span></b> is <b |
|---|
| 938 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 939 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>PWDR - |
|---|
| 940 | powder diffraction data</span></b>; you will change that <span |
|---|
| 941 | style='mso-no-proof:yes'>now.</span> Select <b style='mso-bidi-font-weight: |
|---|
| 942 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 943 | minor-latin;mso-hansi-theme-font:minor-latin'>SASD small angle scattering |
|---|
| 944 | data</span></b> (the window will change). Enter the <b style='mso-bidi-font-weight: |
|---|
| 945 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 946 | minor-latin;mso-hansi-theme-font:minor-latin'>wavelength</span></b> (<b |
|---|
| 947 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 948 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1.0332</span></b>), |
|---|
| 949 | and select the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
|---|
| 950 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 951 | mso-hansi-theme-font:minor-latin'>Calibrant</span></b></span> (near bottom of |
|---|
| 952 | window) as <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 953 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 954 | minor-latin'>Ag <span class=SpellE>behenate</span></span></b>. Note that the |
|---|
| 955 | calibration info for Ag <span class=SpellE>behenate</span> was read from a |
|---|
| 956 | python file <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 957 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 958 | minor-latin'>GSASII/ImageCalibrants.py</span></b>. If you have a <span |
|---|
| 959 | class=SpellE>calibrant</span> that isnt in this file you should enter it in |
|---|
| 960 | the file <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 961 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>UserCalibrants.py</span></b>; |
|---|
| 962 | just follow the format of the examples within <b style='mso-bidi-font-weight: |
|---|
| 963 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 964 | minor-latin;mso-hansi-theme-font:minor-latin'>ImageCalibrants.py</span></b>. |
|---|
| 965 | You should move the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 966 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 967 | mso-hansi-theme-font:minor-latin'>Max intensity</span></b> slider to near the |
|---|
| 968 | middle of the range that will improve the image. When done the <b |
|---|
| 969 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 970 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
|---|
| 971 | controls</span></b> window should look like</p> |
|---|
| 972 | |
|---|
| 973 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 974 | id="_x0000_i1062" type="#_x0000_t75" style='width:472.5pt;height:388.5pt; |
|---|
| 975 | visibility:visible;mso-wrap-style:square'> |
|---|
| 976 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image004.png" |
|---|
| 977 | o:title=""/> |
|---|
| 978 | </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 |
|---|
| 979 | src="Small%20Angle%20Image%20Processing_files/image004.png" v:shapes="_x0000_i1062"><![endif]></span></p> |
|---|
| 980 | |
|---|
| 981 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 982 | |
|---|
| 983 | <p class=MsoNormal>And the image will be</p> |
|---|
| 984 | |
|---|
| 985 | <p class=MsoNormal><!--[if gte vml 1]><v:shapetype id="_x0000_t32" coordsize="21600,21600" |
|---|
| 986 | o:spt="32" o:oned="t" path="m,l21600,21600e" filled="f"> |
|---|
| 987 | <v:path arrowok="t" fillok="f" o:connecttype="none"/> |
|---|
| 988 | <o:lock v:ext="edit" shapetype="t"/> |
|---|
| 989 | </v:shapetype><v:shape id="Straight_x0020_Arrow_x0020_Connector_x0020_21" |
|---|
| 990 | o:spid="_x0000_s1026" type="#_x0000_t32" style='position:absolute; |
|---|
| 991 | margin-left:177pt;margin-top:214.5pt;width:48pt;height:15.75pt;flip:y; |
|---|
| 992 | z-index:251659264;visibility:visible;mso-wrap-style:square; |
|---|
| 993 | mso-width-percent:0;mso-height-percent:0;mso-wrap-distance-left:9pt; |
|---|
| 994 | mso-wrap-distance-top:0;mso-wrap-distance-right:9pt; |
|---|
| 995 | mso-wrap-distance-bottom:0;mso-position-horizontal:absolute; |
|---|
| 996 | mso-position-horizontal-relative:text;mso-position-vertical:absolute; |
|---|
| 997 | mso-position-vertical-relative:text;mso-width-percent:0;mso-height-percent:0; |
|---|
| 998 | mso-width-relative:page;mso-height-relative:page' o:gfxdata="UEsDBBQABgAIAAAAIQC2gziS/gAAAOEBAAATAAAAW0NvbnRlbnRfVHlwZXNdLnhtbJSRQU7DMBBF |
|---|
| 999 | 90jcwfIWJU67QAgl6YK0S0CoHGBkTxKLZGx5TGhvj5O2G0SRWNoz/78nu9wcxkFMGNg6quQqL6RA |
|---|
| 1000 | 0s5Y6ir5vt9lD1JwBDIwOMJKHpHlpr69KfdHjyxSmriSfYz+USnWPY7AufNIadK6MEJMx9ApD/oD |
|---|
| 1001 | OlTrorhX2lFEilmcO2RdNtjC5xDF9pCuTyYBB5bi6bQ4syoJ3g9WQ0ymaiLzg5KdCXlKLjvcW893 |
|---|
| 1002 | SUOqXwnz5DrgnHtJTxOsQfEKIT7DmDSUCaxw7Rqn8787ZsmRM9e2VmPeBN4uqYvTtW7jvijg9N/y |
|---|
| 1003 | JsXecLq0q+WD6m8AAAD//wMAUEsDBBQABgAIAAAAIQA4/SH/1gAAAJQBAAALAAAAX3JlbHMvLnJl |
|---|
| 1004 | bHOkkMFqwzAMhu+DvYPRfXGawxijTi+j0GvpHsDYimMaW0Yy2fr2M4PBMnrbUb/Q94l/f/hMi1qR |
|---|
| 1005 | JVI2sOt6UJgd+ZiDgffL8ekFlFSbvV0oo4EbChzGx4f9GRdb25HMsYhqlCwG5lrLq9biZkxWOiqY |
|---|
| 1006 | 22YiTra2kYMu1l1tQD30/bPm3wwYN0x18gb45AdQl1tp5j/sFB2T0FQ7R0nTNEV3j6o9feQzro1i |
|---|
| 1007 | OWA14Fm+Q8a1a8+Bvu/d/dMb2JY5uiPbhG/ktn4cqGU/er3pcvwCAAD//wMAUEsDBBQABgAIAAAA |
|---|
| 1008 | IQBC+GEV6wEAACkEAAAOAAAAZHJzL2Uyb0RvYy54bWysU02P0zAQvSPxHyzfadIgKoiarlAXuKxg |
|---|
| 1009 | RYG717EbC9tjjU2T/nvGThs+pZUQFyv2zHsz781kezM5y04KowHf8fWq5kx5Cb3xx45//vT22UvO |
|---|
| 1010 | YhK+Fxa86vhZRX6ze/pkO4ZWNTCA7RUyIvGxHUPHh5RCW1VRDsqJuIKgPAU1oBOJrnisehQjsTtb |
|---|
| 1011 | NXW9qUbAPiBIFSO93s5Bviv8WiuZPmgdVWK249RbKieW8yGf1W4r2iOKMBh5aUP8QxdOGE9FF6pb |
|---|
| 1012 | kQT7huYPKmckQgSdVhJcBVobqYoGUrOuf1NzGERQRQuZE8NiU/x/tPL96R6Z6TverDnzwtGMDgmF |
|---|
| 1013 | OQ6JvUaEke3Be/IRkFEK+TWG2BJs7+8xK5aTP4Q7kF8jxapfgvkSw5w2aXRMWxO+0JoUq0g8m8ok |
|---|
| 1014 | zssk1JSYpMdN/WpT07wkhWjMdfMiV65Em2ly1YAxvVPgWP7oeLy0vPQ6lxCnu5hm4BWQwdbnMwlj |
|---|
| 1015 | 3/iepXMg0SJrvRTJ8aJkbr7ISGerZuxHpckwavJ5kVFWVe0tspOgJRNSKp+ahYmyM0wbaxdg/Tjw |
|---|
| 1016 | kp+hqqzxAm4eBy+IUhl8WsDOeMC/EaSpzJYc1nP+1YFZd7bgAfrzPV6HTPtYBnL5d/LC/3wv8B9/ |
|---|
| 1017 | +O47AAAA//8DAFBLAwQUAAYACAAAACEAgdKpXd8AAAALAQAADwAAAGRycy9kb3ducmV2LnhtbEyP |
|---|
| 1018 | wU7DMBBE70j8g7VI3KjTklQQ4lQVohfEpS1FHLfxkgTidRS7Tfh7lhPc3mhHszPFanKdOtMQWs8G |
|---|
| 1019 | 5rMEFHHlbcu1gdf95uYOVIjIFjvPZOCbAqzKy4sCc+tH3tJ5F2slIRxyNNDE2Odah6ohh2Hme2K5 |
|---|
| 1020 | ffjBYRQ51NoOOEq46/QiSZbaYcvyocGeHhuqvnYnZ6B9Gt/senw/7A/Ovnxuts/zYNGY66tp/QAq |
|---|
| 1021 | 0hT/zPBbX6pDKZ2O/sQ2qM7AbZbKlmggXdwLiCPNEoGjwDLJQJeF/r+h/AEAAP//AwBQSwECLQAU |
|---|
| 1022 | AAYACAAAACEAtoM4kv4AAADhAQAAEwAAAAAAAAAAAAAAAAAAAAAAW0NvbnRlbnRfVHlwZXNdLnht |
|---|
| 1023 | bFBLAQItABQABgAIAAAAIQA4/SH/1gAAAJQBAAALAAAAAAAAAAAAAAAAAC8BAABfcmVscy8ucmVs |
|---|
| 1024 | c1BLAQItABQABgAIAAAAIQBC+GEV6wEAACkEAAAOAAAAAAAAAAAAAAAAAC4CAABkcnMvZTJvRG9j |
|---|
| 1025 | LnhtbFBLAQItABQABgAIAAAAIQCB0qld3wAAAAsBAAAPAAAAAAAAAAAAAAAAAEUEAABkcnMvZG93 |
|---|
| 1026 | bnJldi54bWxQSwUGAAAAAAQABADzAAAAUQUAAAAA |
|---|
| 1027 | " strokecolor="#c0504d [3205]" strokeweight="3pt"> |
|---|
| 1028 | <v:stroke endarrow="open"/> |
|---|
| 1029 | <v:shadow on="t" color="black" opacity="22937f" origin=",.5" offset="0,.63889mm"/> |
|---|
| 1030 | <o:lock v:ext="edit" shapetype="f"/> |
|---|
| 1031 | </v:shape><![endif]--><![if !vml]><span style='mso-ignore:vglayout;position: |
|---|
| 1032 | absolute;z-index:251659264;margin-left:234px;margin-top:274px;width:73px; |
|---|
| 1033 | height:38px'><img width=73 height=38 |
|---|
| 1034 | src="Small%20Angle%20Image%20Processing_files/image005.png" v:shapes="Straight_x0020_Arrow_x0020_Connector_x0020_21"></span><![endif]><span |
|---|
| 1035 | style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="_x0000_i1061" type="#_x0000_t75" |
|---|
| 1036 | style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1037 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image006.png" |
|---|
| 1038 | o:title=""/> |
|---|
| 1039 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1040 | src="Small%20Angle%20Image%20Processing_files/image006.png" v:shapes="_x0000_i1061"><![endif]></span></p> |
|---|
| 1041 | |
|---|
| 1042 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1043 | |
|---|
| 1044 | <p class=MsoNormal>Next select <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1045 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1046 | mso-hansi-theme-font:minor-latin'>Operations/Calibrate</span></b> from the <b |
|---|
| 1047 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1048 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
|---|
| 1049 | Controls</span></b> menu; a bit of instruction will appear on the status line |
|---|
| 1050 | of this window. Select 5 points on the innermost ring (arrowed above); a small |
|---|
| 1051 | red cross will appear at each selection point. Press the right mouse button to |
|---|
| 1052 | finish; calibration will proceed. A sequence of concentric red rings will |
|---|
| 1053 | appear; they will switch to blue when calibration is finished. Select <b |
|---|
| 1054 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1055 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Show ring |
|---|
| 1056 | picks</span></b> (near bottom right of <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1057 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1058 | mso-hansi-theme-font:minor-latin'>Image Controls</span></b> window). The <b |
|---|
| 1059 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1060 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
|---|
| 1061 | Controls</span></b> window will show the results of the calibration</p> |
|---|
| 1062 | |
|---|
| 1063 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1064 | id="_x0000_i1060" type="#_x0000_t75" style='width:472.5pt;height:388.5pt; |
|---|
| 1065 | visibility:visible;mso-wrap-style:square'> |
|---|
| 1066 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image007.png" |
|---|
| 1067 | o:title=""/> |
|---|
| 1068 | </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 |
|---|
| 1069 | src="Small%20Angle%20Image%20Processing_files/image007.png" v:shapes="_x0000_i1060"><![endif]></span></p> |
|---|
| 1070 | |
|---|
| 1071 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1072 | |
|---|
| 1073 | <p class=MsoNormal>And the plot will show the points (very sparse!) used in the |
|---|
| 1074 | calibration calculations.</p> |
|---|
| 1075 | |
|---|
| 1076 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1077 | id="Picture_x0020_23" o:spid="_x0000_i1059" type="#_x0000_t75" style='width:525pt; |
|---|
| 1078 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1079 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image008.png" |
|---|
| 1080 | o:title=""/> |
|---|
| 1081 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1082 | src="Small%20Angle%20Image%20Processing_files/image008.png" v:shapes="Picture_x0020_23"><![endif]></span></p> |
|---|
| 1083 | |
|---|
| 1084 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1085 | |
|---|
| 1086 | <p class=MsoNormal>You would like to use more points from just the visible rings. |
|---|
| 1087 | I suggest you change <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1088 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1089 | mso-hansi-theme-font:minor-latin'>Min ring I/<span class=SpellE><span |
|---|
| 1090 | class=GramE>Ib</span></span></span></b> to <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1091 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1092 | mso-hansi-theme-font:minor-latin'>0.5</span></b> and <b style='mso-bidi-font-weight: |
|---|
| 1093 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1094 | minor-latin;mso-hansi-theme-font:minor-latin'>Min <span class=SpellE>calib</span> |
|---|
| 1095 | d-spacing</span></b> to <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1096 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1097 | mso-hansi-theme-font:minor-latin'>10.0</span></b>. Do <b style='mso-bidi-font-weight: |
|---|
| 1098 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1099 | minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Recalibrate</span></b>; |
|---|
| 1100 | more points will be used and they will be limited to the 5 visible rings in the |
|---|
| 1101 | pattern.</p> |
|---|
| 1102 | |
|---|
| 1103 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1104 | id="_x0000_i1058" type="#_x0000_t75" style='width:525pt;height:450pt; |
|---|
| 1105 | visibility:visible;mso-wrap-style:square'> |
|---|
| 1106 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image009.png" |
|---|
| 1107 | o:title=""/> |
|---|
| 1108 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1109 | src="Small%20Angle%20Image%20Processing_files/image009.png" v:shapes="_x0000_i1058"><![endif]></span></p> |
|---|
| 1110 | |
|---|
| 1111 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1112 | |
|---|
| 1113 | <p class=MsoNormal>And give the calibration result as</p> |
|---|
| 1114 | |
|---|
| 1115 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1116 | id="Picture_x0020_25" o:spid="_x0000_i1057" type="#_x0000_t75" style='width:472.5pt; |
|---|
| 1117 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1118 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image010.png" |
|---|
| 1119 | o:title=""/> |
|---|
| 1120 | </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 |
|---|
| 1121 | src="Small%20Angle%20Image%20Processing_files/image010.png" v:shapes="Picture_x0020_25"><![endif]></span></p> |
|---|
| 1122 | |
|---|
| 1123 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1124 | |
|---|
| 1125 | <p class=MsoNormal>You will need this calibration information to process the |
|---|
| 1126 | other images in this tutorial. To save it for future use do <b |
|---|
| 1127 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1128 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Save |
|---|
| 1129 | controls</span></b>; a file dialog will appear</p> |
|---|
| 1130 | |
|---|
| 1131 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1132 | id="Picture_x0020_26" o:spid="_x0000_i1056" type="#_x0000_t75" style='width:537pt; |
|---|
| 1133 | height:397.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1134 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image011.png" |
|---|
| 1135 | o:title=""/> |
|---|
| 1136 | </v:shape><![endif]--><![if !vml]><img border=0 width=716 height=530 |
|---|
| 1137 | src="Small%20Angle%20Image%20Processing_files/image011.png" v:shapes="Picture_x0020_26"><![endif]></span></p> |
|---|
| 1138 | |
|---|
| 1139 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1140 | |
|---|
| 1141 | <p class=MsoNormal>Makeup a file name (no extension needed) for this; I chose <b |
|---|
| 1142 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1143 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD</span></b>. |
|---|
| 1144 | Press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1145 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Save</span></b> |
|---|
| 1146 | and the file <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
|---|
| 1147 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1148 | mso-hansi-theme-font:minor-latin'>SASD.imctrl</span></b></span> will be written |
|---|
| 1149 | to the local directory.</p> |
|---|
| 1150 | |
|---|
| 1151 | <p class=MsoNormal>If you are continuing on to the next step do <b |
|---|
| 1152 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1153 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/New |
|---|
| 1154 | Project</span></b> (dont bother saving the project file unless you want it; we |
|---|
| 1155 | will not need it here); otherwise you can exit GSAS-II.</p> |
|---|
| 1156 | |
|---|
| 1157 | <h2>Step 2: Data image integration</h2> |
|---|
| 1158 | |
|---|
| 1159 | <p class=MsoNormal>The objective here is to read in the four polymer sample |
|---|
| 1160 | images, a glassy carbon image, an empty container image and a dark image. The |
|---|
| 1161 | images will be integrated after creating masks to remove the beam stop and |
|---|
| 1162 | other objectionable parts of the images. If you have not done so already, <a |
|---|
| 1163 | href="Starting%20GSAS.htm">start GSAS-II</a>. </p> |
|---|
| 1164 | |
|---|
| 1165 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1166 | |
|---|
| 1167 | <p class=MsoNormal>First do <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1168 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1169 | mso-hansi-theme-font:minor-latin'>Data/Read image data
</span></b>, go to <b |
|---|
| 1170 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1171 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Exercises/Small |
|---|
| 1172 | angle/Image reduction</span></b> and select all images except <b |
|---|
| 1173 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1174 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>AgBehenate_003.tif</span></b>; |
|---|
| 1175 | then press <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1176 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1177 | minor-latin'>Open</span></b> to read all of them. The GSAS-II data tree window |
|---|
| 1178 | will show entries for 7 images and will expand the last one</p> |
|---|
| 1179 | |
|---|
| 1180 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1181 | id="Picture_x0020_11" o:spid="_x0000_i1055" type="#_x0000_t75" style='width:300pt; |
|---|
| 1182 | height:308.25pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1183 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image013.png" |
|---|
| 1184 | o:title=""/> |
|---|
| 1185 | </v:shape><![endif]--><![if !vml]><img border=0 width=400 height=411 |
|---|
| 1186 | src="Small%20Angle%20Image%20Processing_files/image013.png" v:shapes="Picture_x0020_11"><![endif]></span></p> |
|---|
| 1187 | |
|---|
| 1188 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1189 | |
|---|
| 1190 | <p class=MsoNormal>Notice that the Dark, Empty and GC (glassy carbon) are all |
|---|
| 1191 | 5s images and the Sa1-4 ones are 40s images; this time information is needed |
|---|
| 1192 | later to obtain correct scaling. First select the <b style='mso-bidi-font-weight: |
|---|
| 1193 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1194 | minor-latin;mso-hansi-theme-font:minor-latin'>IMG GC_5s_200.tif</span></b> |
|---|
| 1195 | entry from the tree and expand it (press the <b style='mso-bidi-font-weight: |
|---|
| 1196 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1197 | minor-latin;mso-hansi-theme-font:minor-latin'>+</span></b> box); then select <b |
|---|
| 1198 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1199 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
|---|
| 1200 | controls</span></b>. The data window (<b style='mso-bidi-font-weight:normal'><span |
|---|
| 1201 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1202 | mso-hansi-theme-font:minor-latin'>Image Controls</span></b>) will show the |
|---|
| 1203 | default settings.</p> |
|---|
| 1204 | |
|---|
| 1205 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1206 | id="Picture_x0020_12" o:spid="_x0000_i1054" type="#_x0000_t75" style='width:472.5pt; |
|---|
| 1207 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1208 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image014.png" |
|---|
| 1209 | o:title=""/> |
|---|
| 1210 | </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 |
|---|
| 1211 | src="Small%20Angle%20Image%20Processing_files/image014.png" v:shapes="Picture_x0020_12"><![endif]></span></p> |
|---|
| 1212 | |
|---|
| 1213 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1214 | |
|---|
| 1215 | <p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1216 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1217 | mso-hansi-theme-font:minor-latin'>Operations/Load controls</span></b> from the |
|---|
| 1218 | menu; a file selection dialog will appear showing the available *.<span |
|---|
| 1219 | class=SpellE>imctrl</span> files (the one you made in Step 1 should be seen).</p> |
|---|
| 1220 | |
|---|
| 1221 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1222 | id="Picture_x0020_13" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:537pt; |
|---|
| 1223 | height:397.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1224 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image015.png" |
|---|
| 1225 | o:title=""/> |
|---|
| 1226 | </v:shape><![endif]--><![if !vml]><img border=0 width=716 height=530 |
|---|
| 1227 | src="Small%20Angle%20Image%20Processing_files/image015.png" v:shapes="Picture_x0020_13"><![endif]></span></p> |
|---|
| 1228 | |
|---|
| 1229 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1230 | |
|---|
| 1231 | <p class=MsoNormal>Select it and press <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1232 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1233 | mso-hansi-theme-font:minor-latin'>Open</span></b>; the <b style='mso-bidi-font-weight: |
|---|
| 1234 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1235 | minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> window |
|---|
| 1236 | will be redrawn with the settings obtained in <b style='mso-bidi-font-weight: |
|---|
| 1237 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1238 | minor-latin;mso-hansi-theme-font:minor-latin'>Step 1: Detector calibration</span></b></p> |
|---|
| 1239 | |
|---|
| 1240 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1241 | id="Picture_x0020_14" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:472.5pt; |
|---|
| 1242 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1243 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image016.png" |
|---|
| 1244 | o:title=""/> |
|---|
| 1245 | </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 |
|---|
| 1246 | src="Small%20Angle%20Image%20Processing_files/image016.png" v:shapes="Picture_x0020_14"><![endif]></span></p> |
|---|
| 1247 | |
|---|
| 1248 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1249 | |
|---|
| 1250 | <p class=MsoNormal><span class=GramE>and</span> the image will be that of |
|---|
| 1251 | glassy carbon. Changing the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1252 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1253 | mso-hansi-theme-font:minor-latin'>Max intensity</span></b> slider on the <b |
|---|
| 1254 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1255 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
|---|
| 1256 | Controls</span></b> window will show that the image from the <span |
|---|
| 1257 | class=SpellE>MarCCD</span> is circular and slightly offset from the beam |
|---|
| 1258 | center. A beam stop shadow is evident as well as an arc-like fault in the image |
|---|
| 1259 | (toward the upper left corner of the image). We will sort those out later.</p> |
|---|
| 1260 | |
|---|
| 1261 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1262 | id="Picture_x0020_15" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:525pt; |
|---|
| 1263 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1264 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image017.png" |
|---|
| 1265 | o:title=""/> |
|---|
| 1266 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1267 | src="Small%20Angle%20Image%20Processing_files/image017.png" v:shapes="Picture_x0020_15"><![endif]></span></p> |
|---|
| 1268 | |
|---|
| 1269 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1270 | |
|---|
| 1271 | <p class=MsoNormal>The next step we will be doing is to set up the integration |
|---|
| 1272 | controls. The <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1273 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1274 | minor-latin'>Dark image</span></b> is <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1275 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1276 | mso-hansi-theme-font:minor-latin'>IMG Dark_5s_003.tif</span></b>, the <b |
|---|
| 1277 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1278 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background |
|---|
| 1279 | image</span></b> is <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1280 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1281 | mso-hansi-theme-font:minor-latin'>IMG Empty_5s_014.tif</span></b>; select these |
|---|
| 1282 | two. The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1283 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
|---|
| 1284 | for each are <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1285 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1286 | minor-latin'>-1.0</span></b> because their exposures were the same as this |
|---|
| 1287 | glassy carbon image (5s). Next check the boxes for <b style='mso-bidi-font-weight: |
|---|
| 1288 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1289 | minor-latin;mso-hansi-theme-font:minor-latin'>Show integration limits?</span></b> |
|---|
| 1290 | <span class=GramE>and</span> <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1291 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1292 | mso-hansi-theme-font:minor-latin'>Do full integration?</span></b> A pair of |
|---|
| 1293 | circles with a connecting diagonal line will appear on the plot. Set the <b |
|---|
| 1294 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1295 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Inner/Outer |
|---|
| 1296 | 2-theta</span></b> values to <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1297 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1298 | mso-hansi-theme-font:minor-latin'>0.5</span></b> and <b style='mso-bidi-font-weight: |
|---|
| 1299 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1300 | minor-latin;mso-hansi-theme-font:minor-latin'>9.0</span></b>, respectively, and |
|---|
| 1301 | set the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1302 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Start |
|---|
| 1303 | azimuth</span></b> to <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1304 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1305 | mso-hansi-theme-font:minor-latin'>0</span></b>. Set the <b style='mso-bidi-font-weight: |
|---|
| 1306 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1307 | minor-latin;mso-hansi-theme-font:minor-latin'>No. 2-theta bins</span></b> to <b |
|---|
| 1308 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1309 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>250</span></b>, |
|---|
| 1310 | which is more appropriate for small angle scattering, and set the <b |
|---|
| 1311 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1312 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Bin style: |
|---|
| 1313 | Constant step bins in</span></b> to <span class=GramE><b style='mso-bidi-font-weight: |
|---|
| 1314 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1315 | minor-latin;mso-hansi-theme-font:minor-latin'>log(</span></b></span><b |
|---|
| 1316 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1317 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>q)</span></b>. |
|---|
| 1318 | You should also check the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1319 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1320 | mso-hansi-theme-font:minor-latin'>Apply sample transmission?</span></b> <span |
|---|
| 1321 | class=GramE>and</span> <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1322 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1323 | mso-hansi-theme-font:minor-latin'>Apply polarization?</span></b> <span |
|---|
| 1324 | class=GramE>boxes</span>; enter the measured <b style='mso-bidi-font-weight: |
|---|
| 1325 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1326 | minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> (<b |
|---|
| 1327 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1328 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.818</span></b>) |
|---|
| 1329 | for the glassy carbon sample. When done the <b style='mso-bidi-font-weight: |
|---|
| 1330 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1331 | minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> data |
|---|
| 1332 | window should look like</p> |
|---|
| 1333 | |
|---|
| 1334 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1335 | id="Picture_x0020_29" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:472.5pt; |
|---|
| 1336 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1337 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image018.png" |
|---|
| 1338 | o:title=""/> |
|---|
| 1339 | </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 |
|---|
| 1340 | src="Small%20Angle%20Image%20Processing_files/image018.png" v:shapes="Picture_x0020_29"><![endif]></span></p> |
|---|
| 1341 | |
|---|
| 1342 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1343 | |
|---|
| 1344 | <p class=MsoNormal>And the plot should look like</p> |
|---|
| 1345 | |
|---|
| 1346 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1347 | id="Picture_x0020_28" o:spid="_x0000_i1049" type="#_x0000_t75" style='width:525pt; |
|---|
| 1348 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1349 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image019.png" |
|---|
| 1350 | o:title=""/> |
|---|
| 1351 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1352 | src="Small%20Angle%20Image%20Processing_files/image019.png" v:shapes="Picture_x0020_28"><![endif]></span></p> |
|---|
| 1353 | |
|---|
| 1354 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1355 | |
|---|
| 1356 | <p class=MsoNormal>Now copy these controls to the other images. Do <b |
|---|
| 1357 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1358 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Copy |
|---|
| 1359 | controls</span></b> and select just the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1360 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1361 | mso-hansi-theme-font:minor-latin'>Sa1-4</span></b> data names. </p> |
|---|
| 1362 | |
|---|
| 1363 | <p class=MsoNormal>We now need to go to the <b style='mso-bidi-font-weight: |
|---|
| 1364 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1365 | minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> for |
|---|
| 1366 | each of <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1367 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sa1-Sa4</span></b> |
|---|
| 1368 | to enter the correct transmission for each and change the Dark & Background |
|---|
| 1369 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1370 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
|---|
| 1371 | to account for the different exposure times. Start with <b style='mso-bidi-font-weight: |
|---|
| 1372 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1373 | minor-latin;mso-hansi-theme-font:minor-latin'>IMG Sa1_40s_067.tif</span></b> |
|---|
| 1374 | and change <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1375 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1376 | minor-latin'>transmission</span></b> to <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1377 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1378 | mso-hansi-theme-font:minor-latin'>0.943</span></b> and the two <b |
|---|
| 1379 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1380 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
|---|
| 1381 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1382 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. |
|---|
| 1383 | Then go to <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1384 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1385 | minor-latin'>IMG Sa2_40s_069.tif</span></b> and change <b style='mso-bidi-font-weight: |
|---|
| 1386 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1387 | minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> to <b |
|---|
| 1388 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1389 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.979</span></b>; |
|---|
| 1390 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1391 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
|---|
| 1392 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1393 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. |
|---|
| 1394 | Next go <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1395 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>to IMG Sa3_40s_059.tif</span></b> |
|---|
| 1396 | and change <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1397 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1398 | minor-latin'>transmission</span></b> to <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1399 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1400 | mso-hansi-theme-font:minor-latin'>0.960</span></b>; <b style='mso-bidi-font-weight: |
|---|
| 1401 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1402 | minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> to <b |
|---|
| 1403 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1404 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. |
|---|
| 1405 | Finally, go to <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1406 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1407 | minor-latin'>IMG Sa4_40s_061.tif</span></b> and change <b style='mso-bidi-font-weight: |
|---|
| 1408 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1409 | minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> to <b |
|---|
| 1410 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1411 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.968</span></b>; |
|---|
| 1412 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1413 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
|---|
| 1414 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1415 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. |
|---|
| 1416 | The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1417 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
|---|
| 1418 | Controls</span></b> data window for this should look like<o:p></o:p></p> |
|---|
| 1419 | |
|---|
| 1420 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1421 | id="Picture_x0020_38" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:472.5pt; |
|---|
| 1422 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1423 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image020.png" |
|---|
| 1424 | o:title=""/> |
|---|
| 1425 | </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518 |
|---|
| 1426 | src="Small%20Angle%20Image%20Processing_files/image020.png" v:shapes="Picture_x0020_38"><![endif]></span><o:p></o:p></p> |
|---|
| 1427 | |
|---|
| 1428 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1429 | |
|---|
| 1430 | <p class=MsoNormal>This is a reasonable time to save the project; do <b |
|---|
| 1431 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1432 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/Save |
|---|
| 1433 | project as
</span></b> from the main GSAS-II data tree menu. Choose a file name |
|---|
| 1434 | (I assumed <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1435 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1436 | minor-latin'>image</span></b>) and it will be written on the local file |
|---|
| 1437 | directory. </p> |
|---|
| 1438 | |
|---|
| 1439 | <p class=MsoNormal>As noted earlier, this image contains some unwanted features; |
|---|
| 1440 | so lets create masks to remove them. Select <b style='mso-bidi-font-weight: |
|---|
| 1441 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1442 | minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> from the GSAS-II |
|---|
| 1443 | data tree under <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1444 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1445 | minor-latin'>IMG GC_5s_200.tif</span></b>; the data window will show</p> |
|---|
| 1446 | |
|---|
| 1447 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1448 | id="Picture_x0020_17" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:337.5pt; |
|---|
| 1449 | height:99.75pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1450 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image021.png" |
|---|
| 1451 | o:title=""/> |
|---|
| 1452 | </v:shape><![endif]--><![if !vml]><img border=0 width=450 height=133 |
|---|
| 1453 | src="Small%20Angle%20Image%20Processing_files/image021.png" v:shapes="Picture_x0020_17"><![endif]></span></p> |
|---|
| 1454 | |
|---|
| 1455 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1456 | |
|---|
| 1457 | <p class=MsoNormal>To mask out the regions beyond the circular <span |
|---|
| 1458 | class=SpellE>MarCCD</span> image change the <span class=GramE><b |
|---|
| 1459 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1460 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Lower<span |
|---|
| 1461 | style='mso-spacerun:yes'> </span><span class=SpellE>threshhold</span></span></b></span> |
|---|
| 1462 | from <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1463 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0</span></b> |
|---|
| 1464 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1465 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1</span></b>; |
|---|
| 1466 | the image will be redrawn with these regions in red</p> |
|---|
| 1467 | |
|---|
| 1468 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1469 | id="Picture_x0020_30" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:525pt; |
|---|
| 1470 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1471 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image022.png" |
|---|
| 1472 | o:title=""/> |
|---|
| 1473 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1474 | src="Small%20Angle%20Image%20Processing_files/image022.png" v:shapes="Picture_x0020_30"><![endif]></span><o:p></o:p></p> |
|---|
| 1475 | |
|---|
| 1476 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1477 | |
|---|
| 1478 | <p class=MsoNormal>These are now excluded. The status line for the <b |
|---|
| 1479 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1480 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> |
|---|
| 1481 | data window gives the directions for adding additional masks. You can make arcs |
|---|
| 1482 | (well use that here), rings, spots (this too) and polygons (this as well) as |
|---|
| 1483 | masks. These enclose areas to be excluded. The frame works in the opposite |
|---|
| 1484 | sense in that everything outside the frame is excluded (NB: only one frame is |
|---|
| 1485 | allowed). So lets first mask the bad arc in the upper left zoom in on that |
|---|
| 1486 | part of the image</p> |
|---|
| 1487 | |
|---|
| 1488 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1489 | id="Picture_x0020_19" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:525pt; |
|---|
| 1490 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1491 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image023.png" |
|---|
| 1492 | o:title=""/> |
|---|
| 1493 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1494 | src="Small%20Angle%20Image%20Processing_files/image023.png" v:shapes="Picture_x0020_19"><![endif]></span></p> |
|---|
| 1495 | |
|---|
| 1496 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1497 | |
|---|
| 1498 | <p class=MsoNormal>To add the mask 1: be sure the focus is on the image and the |
|---|
| 1499 | zoom buttons are off, 2: type <span class=GramE><b style='mso-bidi-font-weight: |
|---|
| 1500 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1501 | minor-latin;mso-hansi-theme-font:minor-latin'>a</span></b> to</span> activate |
|---|
| 1502 | the arc mask entry 3: press the left mouse button (<b style='mso-bidi-font-weight: |
|---|
| 1503 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1504 | minor-latin;mso-hansi-theme-font:minor-latin'>LB</span></b>) with the cursor |
|---|
| 1505 | centered on the bad arc. The <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1506 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1507 | mso-hansi-theme-font:minor-latin'>Masks</span></b> window will show a new entry |
|---|
| 1508 | </p> |
|---|
| 1509 | |
|---|
| 1510 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1511 | id="Picture_x0020_20" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:337.5pt; |
|---|
| 1512 | height:135pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1513 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image024.png" |
|---|
| 1514 | o:title=""/> |
|---|
| 1515 | </v:shape><![endif]--><![if !vml]><img border=0 width=450 height=180 |
|---|
| 1516 | src="Small%20Angle%20Image%20Processing_files/image024.png" v:shapes="Picture_x0020_20"><![endif]></span><span |
|---|
| 1517 | style='mso-spacerun:yes'> </span></p> |
|---|
| 1518 | |
|---|
| 1519 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1520 | |
|---|
| 1521 | <p class=MsoNormal><span class=GramE>and</span> an arc mask will be drawn on |
|---|
| 1522 | the plot.</p> |
|---|
| 1523 | |
|---|
| 1524 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1525 | id="Picture_x0020_22" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:525pt; |
|---|
| 1526 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1527 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image025.png" |
|---|
| 1528 | o:title=""/> |
|---|
| 1529 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1530 | src="Small%20Angle%20Image%20Processing_files/image025.png" v:shapes="Picture_x0020_22"><![endif]></span></p> |
|---|
| 1531 | |
|---|
| 1532 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1533 | |
|---|
| 1534 | <p class=MsoNormal>You can change the angular width of the arc by changing <b |
|---|
| 1535 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1536 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>thickness</span></b> |
|---|
| 1537 | in the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1538 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> |
|---|
| 1539 | data window, you can change the angular range of the arc by dragging either end |
|---|
| 1540 | of the arc, and you can move the arc <span |
|---|
| 1541 | style='mso-spacerun:yes'> </span>along a constant 2Θ angle by dragging on any |
|---|
| 1542 | point inside the mask. The curvature is centered on the beam center position and |
|---|
| 1543 | follows a constant 2Θ curve established by the detector calibration.<span |
|---|
| 1544 | style='mso-no-proof:yes'> <!--[if gte vml 1]><v:shape id="Picture_x0020_34" |
|---|
| 1545 | o:spid="_x0000_i1042" type="#_x0000_t75" style='width:525pt;height:450pt; |
|---|
| 1546 | visibility:visible;mso-wrap-style:square'> |
|---|
| 1547 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image026.png" |
|---|
| 1548 | o:title=""/> |
|---|
| 1549 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1550 | src="Small%20Angle%20Image%20Processing_files/image026.png" v:shapes="Picture_x0020_34"><![endif]></span></p> |
|---|
| 1551 | |
|---|
| 1552 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1553 | |
|---|
| 1554 | <p class=MsoNormal>Next lets deal with the beam stop. Im going to use both a |
|---|
| 1555 | polygon and a spot to cover it. Move the zoom area to be around the center, make |
|---|
| 1556 | sure the zoom buttons are off, enter <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1557 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1558 | mso-hansi-theme-font:minor-latin'>s</span></b> on the plot and press mouse <b |
|---|
| 1559 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1560 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>LB</span></b> |
|---|
| 1561 | with the cursor positioned where you want the spot. A 1mm diameter red circle |
|---|
| 1562 | will appear on the plot</p> |
|---|
| 1563 | |
|---|
| 1564 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1565 | id="Picture_x0020_35" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:525pt; |
|---|
| 1566 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1567 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image027.png" |
|---|
| 1568 | o:title=""/> |
|---|
| 1569 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1570 | src="Small%20Angle%20Image%20Processing_files/image027.png" v:shapes="Picture_x0020_35"><![endif]></span></p> |
|---|
| 1571 | |
|---|
| 1572 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1573 | |
|---|
| 1574 | <p class=MsoNormal>And the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1575 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1576 | mso-hansi-theme-font:minor-latin'>Masks</span></b> window will have new |
|---|
| 1577 | information</p> |
|---|
| 1578 | |
|---|
| 1579 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1580 | id="Picture_x0020_24" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:337.5pt; |
|---|
| 1581 | height:170.25pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1582 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image028.png" |
|---|
| 1583 | o:title=""/> |
|---|
| 1584 | </v:shape><![endif]--><![if !vml]><img border=0 width=450 height=227 |
|---|
| 1585 | src="Small%20Angle%20Image%20Processing_files/image028.png" v:shapes="Picture_x0020_24"><![endif]></span></p> |
|---|
| 1586 | |
|---|
| 1587 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1588 | |
|---|
| 1589 | <p class=MsoNormal>You can change the diameter of the spot, I used <b |
|---|
| 1590 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1591 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>7.0</span></b>; |
|---|
| 1592 | the plot now shows a ring that just covers the beam stop. You may have to drag |
|---|
| 1593 | it a bit (Hint: drag the center of the spot) to get it well centered.</p> |
|---|
| 1594 | |
|---|
| 1595 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1596 | id="Picture_x0020_36" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:525pt; |
|---|
| 1597 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1598 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image029.png" |
|---|
| 1599 | o:title=""/> |
|---|
| 1600 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1601 | src="Small%20Angle%20Image%20Processing_files/image029.png" v:shapes="Picture_x0020_36"><![endif]></span></p> |
|---|
| 1602 | |
|---|
| 1603 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1604 | |
|---|
| 1605 | <p class=MsoNormal>Next we need to mask the stick holding the beam stop; well |
|---|
| 1606 | use a 4 sided polygon for this. Adjust the zoom & position so you can see |
|---|
| 1607 | the entire beam stop stick. Make sure all zoom buttons are off, press <b |
|---|
| 1608 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1609 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>p</span></b> |
|---|
| 1610 | on the plot, then press the mouse <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1611 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1612 | mso-hansi-theme-font:minor-latin'>LB</span></b> at four points in succession |
|---|
| 1613 | around the beam stop stick. A line segment for the polygon will be drawn |
|---|
| 1614 | following your mouse clicks. Finally press the mouse <b style='mso-bidi-font-weight: |
|---|
| 1615 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1616 | minor-latin;mso-hansi-theme-font:minor-latin'>RB</span></b> to close the |
|---|
| 1617 | polygon. You should see something like</p> |
|---|
| 1618 | |
|---|
| 1619 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1620 | id="Picture_x0020_37" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:525pt; |
|---|
| 1621 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1622 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image030.png" |
|---|
| 1623 | o:title=""/> |
|---|
| 1624 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1625 | src="Small%20Angle%20Image%20Processing_files/image030.png" v:shapes="Picture_x0020_37"><![endif]></span></p> |
|---|
| 1626 | |
|---|
| 1627 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1628 | |
|---|
| 1629 | <p class=MsoNormal>You can adjust the position of the polygon vertices by |
|---|
| 1630 | closely dragging it with mouse <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1631 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1632 | mso-hansi-theme-font:minor-latin'>LB</span></b> pressed; a new vertex can be |
|---|
| 1633 | added by dragging an existing vertex with the mouse <b style='mso-bidi-font-weight: |
|---|
| 1634 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1635 | minor-latin;mso-hansi-theme-font:minor-latin'>RB</span></b> pressed. If you |
|---|
| 1636 | drag one vertex onto another, they are merged and cannot be separated.</p> |
|---|
| 1637 | |
|---|
| 1638 | <p class=MsoNormal>We want to use these masks for all the Sa1-4 images. <span |
|---|
| 1639 | class=GramE>Do</span> <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1640 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1641 | mso-hansi-theme-font:minor-latin'>Operations/Copy mask</span></b>; a <b |
|---|
| 1642 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1643 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Copy mask |
|---|
| 1644 | information</span></b> dialog box will appear. Select the <b style='mso-bidi-font-weight: |
|---|
| 1645 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1646 | minor-latin;mso-hansi-theme-font:minor-latin'>Sa1-4</span></b> items and press <b |
|---|
| 1647 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1648 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ok</span></b>. |
|---|
| 1649 | Here is a useful place to save your project; do <b style='mso-bidi-font-weight: |
|---|
| 1650 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1651 | minor-latin;mso-hansi-theme-font:minor-latin'>File/Save project</span></b> from |
|---|
| 1652 | the main GSAS-II data tree menu.</p> |
|---|
| 1653 | |
|---|
| 1654 | <h2>Step 3: Integration of images</h2> |
|---|
| 1655 | |
|---|
| 1656 | <p class=MsoNormal>We are now ready to integrate the glassy carbon and the four |
|---|
| 1657 | <span class=GramE>Sa</span> images. Select any Image Controls and then do |
|---|
| 1658 | Operations/Integrate all. A selection dialog will appear; select only the GC |
|---|
| 1659 | and Sa1-Sa4 data sets and press Ok. The image integration will proceed; a |
|---|
| 1660 | progress bar shows as each one is done. Five SASD data items will appear on the |
|---|
| 1661 | GSAS-II data tree; the last one (<b style='mso-bidi-font-weight:normal'><span |
|---|
| 1662 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1663 | mso-hansi-theme-font:minor-latin'>SASD Sa4_40s_061.tif <span class=SpellE>Azm</span>=45.00</span></b>) |
|---|
| 1664 | will be expanded and plotted.</p> |
|---|
| 1665 | |
|---|
| 1666 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1667 | id="Picture_x0020_39" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:525pt; |
|---|
| 1668 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1669 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image031.png" |
|---|
| 1670 | o:title=""/> |
|---|
| 1671 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1672 | src="Small%20Angle%20Image%20Processing_files/image031.png" v:shapes="Picture_x0020_39"><![endif]></span></p> |
|---|
| 1673 | |
|---|
| 1674 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1675 | |
|---|
| 1676 | <p class=MsoNormal>Pretty obviously the SASD pattern is down to background at Q~0.25Å<sup>-1</sup>; |
|---|
| 1677 | the other Sa1-Sa4 patterns are similar. The glassy carbon pattern extends |
|---|
| 1678 | nicely to the highest Q (~1.0Å<sup>-1</sup>) measured.</p> |
|---|
| 1679 | |
|---|
| 1680 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1681 | id="Picture_x0020_40" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt; |
|---|
| 1682 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1683 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image032.png" |
|---|
| 1684 | o:title=""/> |
|---|
| 1685 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1686 | src="Small%20Angle%20Image%20Processing_files/image032.png" v:shapes="Picture_x0020_40"><![endif]></span></p> |
|---|
| 1687 | |
|---|
| 1688 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1689 | |
|---|
| 1690 | <h2>Step 4: Scaling of SASD patterns</h2> |
|---|
| 1691 | |
|---|
| 1692 | <p class=MsoNormal>To set this data on an absolute scale, we compare it to an |
|---|
| 1693 | absolute scaled glassy carbon scan. One of these is in the same directory as |
|---|
| 1694 | the image data; do <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1695 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1696 | mso-hansi-theme-font:minor-latin'>Import/Small Angle Data/ from <span |
|---|
| 1697 | class=GramE>q(</span>A-1) step X-ray QIE data file</span></b> and select <b |
|---|
| 1698 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1699 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>GC |
|---|
| 1700 | calibrated data.txt</span></b> from the file selection dialog. You will need to |
|---|
| 1701 | select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1702 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>any <span |
|---|
| 1703 | class=GramE>file(</span>*.*)</span></b> to see it. A <b style='mso-bidi-font-weight: |
|---|
| 1704 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1705 | minor-latin;mso-hansi-theme-font:minor-latin'>Is <span class=GramE>this the</span> |
|---|
| 1706 | file you want</span></b> dialog will appear respond <b style='mso-bidi-font-weight: |
|---|
| 1707 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1708 | minor-latin;mso-hansi-theme-font:minor-latin'>Yes</span></b> to read the file; |
|---|
| 1709 | it will be plotted.</p> |
|---|
| 1710 | |
|---|
| 1711 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1712 | id="Picture_x0020_41" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:525pt; |
|---|
| 1713 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1714 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image033.png" |
|---|
| 1715 | o:title=""/> |
|---|
| 1716 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1717 | src="Small%20Angle%20Image%20Processing_files/image033.png" v:shapes="Picture_x0020_41"><![endif]></span></p> |
|---|
| 1718 | |
|---|
| 1719 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1720 | |
|---|
| 1721 | <p class=MsoNormal>If you <span class=GramE>enter <b style='mso-bidi-font-weight: |
|---|
| 1722 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1723 | minor-latin;mso-hansi-theme-font:minor-latin'>s</span></b></span> on the plot |
|---|
| 1724 | window, all of the SASD patterns will be plotted together (Ive adjusted the |
|---|
| 1725 | zoom to see them all).</p> |
|---|
| 1726 | |
|---|
| 1727 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1728 | id="Picture_x0020_42" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt; |
|---|
| 1729 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1730 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image034.png" |
|---|
| 1731 | o:title=""/> |
|---|
| 1732 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1733 | src="Small%20Angle%20Image%20Processing_files/image034.png" v:shapes="Picture_x0020_42"><![endif]></span></p> |
|---|
| 1734 | |
|---|
| 1735 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1736 | |
|---|
| 1737 | <p class=MsoNormal>Clearly the measured image data need to be scaled down to |
|---|
| 1738 | have them on absolute scale. First is to discover the scaling between the two |
|---|
| 1739 | glassy carbon patterns. Go to the measured one (<b style='mso-bidi-font-weight: |
|---|
| 1740 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1741 | minor-latin;mso-hansi-theme-font:minor-latin'>SASD GC_5s_200.tif</span></b>) |
|---|
| 1742 | and select <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1743 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1744 | minor-latin'>Sample Parameters</span></b>.</p> |
|---|
| 1745 | |
|---|
| 1746 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1747 | id="Picture_x0020_43" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:291.75pt; |
|---|
| 1748 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1749 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image035.png" |
|---|
| 1750 | o:title=""/> |
|---|
| 1751 | </v:shape><![endif]--><![if !vml]><img border=0 width=389 height=518 |
|---|
| 1752 | src="Small%20Angle%20Image%20Processing_files/image035.png" v:shapes="Picture_x0020_43"><![endif]></span></p> |
|---|
| 1753 | |
|---|
| 1754 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1755 | |
|---|
| 1756 | <p class=MsoNormal>We will change <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1757 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1758 | mso-hansi-theme-font:minor-latin'>Histogram scale factor</span></b> by |
|---|
| 1759 | comparison with the absolute glassy carbon scan. Do <b style='mso-bidi-font-weight: |
|---|
| 1760 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1761 | minor-latin;mso-hansi-theme-font:minor-latin'>Command/Set scale</span></b> from |
|---|
| 1762 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1763 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sample |
|---|
| 1764 | Parameters</span></b> menu; a <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1765 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1766 | mso-hansi-theme-font:minor-latin'>Reference histogram</span></b> dialog will |
|---|
| 1767 | appear.</p> |
|---|
| 1768 | |
|---|
| 1769 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1770 | id="Picture_x0020_44" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:259.5pt; |
|---|
| 1771 | height:252pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1772 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image036.png" |
|---|
| 1773 | o:title=""/> |
|---|
| 1774 | </v:shape><![endif]--><![if !vml]><img border=0 width=346 height=336 |
|---|
| 1775 | src="Small%20Angle%20Image%20Processing_files/image036.png" v:shapes="Picture_x0020_44"><![endif]></span></p> |
|---|
| 1776 | |
|---|
| 1777 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1778 | |
|---|
| 1779 | <p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1780 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1781 | mso-hansi-theme-font:minor-latin'>SASD GC calibrated data.txt</span></b> (shown |
|---|
| 1782 | in blue above) and press <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1783 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1784 | mso-hansi-theme-font:minor-latin'>Ok</span></b>; the <b style='mso-bidi-font-weight: |
|---|
| 1785 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1786 | minor-latin;mso-hansi-theme-font:minor-latin'>GC_5s_200.tif</span></b> data |
|---|
| 1787 | will be rescaled to the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1788 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1789 | mso-hansi-theme-font:minor-latin'>GC calibrated data</span></b> and the <b |
|---|
| 1790 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1791 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Histogram |
|---|
| 1792 | scale factor</span></b> will be changed to the new scaling factor (<b |
|---|
| 1793 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1794 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.0008536</span></b>). |
|---|
| 1795 | The plot will be redrawn with the scaled data.</p> |
|---|
| 1796 | |
|---|
| 1797 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1798 | id="Picture_x0020_45" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt; |
|---|
| 1799 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1800 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image037.png" |
|---|
| 1801 | o:title=""/> |
|---|
| 1802 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1803 | src="Small%20Angle%20Image%20Processing_files/image037.png" v:shapes="Picture_x0020_45"><![endif]></span></p> |
|---|
| 1804 | |
|---|
| 1805 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1806 | |
|---|
| 1807 | <p class=MsoNormal>The divergence at high Q is probably from a background |
|---|
| 1808 | contribution to the standard that is not present in our measured one. Next we |
|---|
| 1809 | have to apply this scale factor to the Sa1-Sa4 data sets. Do <b |
|---|
| 1810 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1811 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Command/Copy |
|---|
| 1812 | selected
</span></b> from the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1813 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1814 | mso-hansi-theme-font:minor-latin'>Sample Parameters</span></b> menu; a <b |
|---|
| 1815 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1816 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Select |
|---|
| 1817 | sample parameters</span></b> dialog will appear</p> |
|---|
| 1818 | |
|---|
| 1819 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1820 | id="Picture_x0020_46" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:240pt; |
|---|
| 1821 | height:232.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1822 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image038.png" |
|---|
| 1823 | o:title=""/> |
|---|
| 1824 | </v:shape><![endif]--><![if !vml]><img border=0 width=320 height=310 |
|---|
| 1825 | src="Small%20Angle%20Image%20Processing_files/image038.png" v:shapes="Picture_x0020_46"><![endif]></span></p> |
|---|
| 1826 | |
|---|
| 1827 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1828 | |
|---|
| 1829 | <p class=MsoNormal>Select only <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1830 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1831 | mso-hansi-theme-font:minor-latin'>Histogram scale factor</span></b> and press <b |
|---|
| 1832 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1833 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ok</span></b>; |
|---|
| 1834 | a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1835 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Copy sample |
|---|
| 1836 | parameters</span></b> dialog will appear</p> |
|---|
| 1837 | |
|---|
| 1838 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1839 | id="Picture_x0020_47" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:240pt; |
|---|
| 1840 | height:232.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1841 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image039.png" |
|---|
| 1842 | o:title=""/> |
|---|
| 1843 | </v:shape><![endif]--><![if !vml]><img border=0 width=320 height=310 |
|---|
| 1844 | src="Small%20Angle%20Image%20Processing_files/image039.png" v:shapes="Picture_x0020_47"><![endif]></span></p> |
|---|
| 1845 | |
|---|
| 1846 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1847 | |
|---|
| 1848 | <p class=MsoNormal>Select only the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1849 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1850 | mso-hansi-theme-font:minor-latin'>Sa1-Sa4</span></b> data sets and press <b |
|---|
| 1851 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1852 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ok</span></b>. |
|---|
| 1853 | The copy will occur and the plot redrawn</p> |
|---|
| 1854 | |
|---|
| 1855 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1856 | id="Picture_x0020_48" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:525pt; |
|---|
| 1857 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1858 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image040.png" |
|---|
| 1859 | o:title=""/> |
|---|
| 1860 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1861 | src="Small%20Angle%20Image%20Processing_files/image040.png" v:shapes="Picture_x0020_48"><![endif]></span></p> |
|---|
| 1862 | |
|---|
| 1863 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1864 | |
|---|
| 1865 | <p class=MsoNormal>Ive changed the zoom to show all the data. We are not quite |
|---|
| 1866 | done; the scales for the Sa1-Sa4 data sets have to be further reduced by a |
|---|
| 1867 | factor of 8 to account for the longer exposure time. Select SASD |
|---|
| 1868 | Sa1_40s_067.tif from the GSAS-II data tree, expand it and choose Sample |
|---|
| 1869 | Parameters</p> |
|---|
| 1870 | |
|---|
| 1871 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1872 | id="Picture_x0020_49" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:291.75pt; |
|---|
| 1873 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1874 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image041.png" |
|---|
| 1875 | o:title=""/> |
|---|
| 1876 | </v:shape><![endif]--><![if !vml]><img border=0 width=389 height=518 |
|---|
| 1877 | src="Small%20Angle%20Image%20Processing_files/image041.png" v:shapes="Picture_x0020_49"><![endif]></span><o:p></o:p></p> |
|---|
| 1878 | |
|---|
| 1879 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1880 | |
|---|
| 1881 | <p class=MsoNormal>The data items here can take simple mathematical expressions |
|---|
| 1882 | so change Histogram scale factor to 0.0008536/8 and press Enter. The value will |
|---|
| 1883 | change to 0.0001067 and the plot redrawn.</p> |
|---|
| 1884 | |
|---|
| 1885 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1886 | id="Picture_x0020_50" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:525pt; |
|---|
| 1887 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1888 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image042.png" |
|---|
| 1889 | o:title=""/> |
|---|
| 1890 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1891 | src="Small%20Angle%20Image%20Processing_files/image042.png" v:shapes="Picture_x0020_50"><![endif]></span></p> |
|---|
| 1892 | |
|---|
| 1893 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1894 | |
|---|
| 1895 | <p class=MsoNormal>Next do Command/Copy selected as before to copy this new |
|---|
| 1896 | scale factor to the other <span class=GramE>Sa</span> data sets. The plot will |
|---|
| 1897 | again be redrawn</p> |
|---|
| 1898 | |
|---|
| 1899 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1900 | id="Picture_x0020_51" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt; |
|---|
| 1901 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1902 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image043.png" |
|---|
| 1903 | o:title=""/> |
|---|
| 1904 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1905 | src="Small%20Angle%20Image%20Processing_files/image043.png" v:shapes="Picture_x0020_51"><![endif]></span></p> |
|---|
| 1906 | |
|---|
| 1907 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1908 | |
|---|
| 1909 | <p class=MsoNormal>Everything is now on absolute scale and these polymer |
|---|
| 1910 | samples are quite weak small angle <span class=SpellE>scatterers</span>. This |
|---|
| 1911 | is a good point to do a <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1912 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1913 | mso-hansi-theme-font:minor-latin'>File/Save project</span></b> from the main |
|---|
| 1914 | GSAS-II data tree menu. You can try to fit unified & <span class=SpellE>Porod</span> |
|---|
| 1915 | models to them following the procedures demonstrated in the <strong><span |
|---|
| 1916 | style='font-weight:normal;mso-bidi-font-weight:bold'><a |
|---|
| 1917 | href="Fitting%20Small%20Angle%20Scattering%20Data.htm"><span style='mso-bidi-font-weight: |
|---|
| 1918 | normal'>Fitting Small Angle X-Ray Data</span></a> tutorial. Id set the high Q |
|---|
| 1919 | limit to about 0.25Å<sup>-1</sup> as above that is only noisy background.</span></strong></p> |
|---|
| 1920 | |
|---|
| 1921 | </div> |
|---|
| 1922 | |
|---|
| 1923 | </body> |
|---|
| 1924 | |
|---|
| 1925 | </html> |
|---|
