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332 | UnhideWhenUsed="false" Name="Colorful Shading Accent 6"/> |
---|
333 | <w:LsdException Locked="false" Priority="72" SemiHidden="false" |
---|
334 | UnhideWhenUsed="false" Name="Colorful List Accent 6"/> |
---|
335 | <w:LsdException Locked="false" Priority="73" SemiHidden="false" |
---|
336 | UnhideWhenUsed="false" Name="Colorful Grid Accent 6"/> |
---|
337 | <w:LsdException Locked="false" Priority="19" SemiHidden="false" |
---|
338 | UnhideWhenUsed="false" QFormat="true" Name="Subtle Emphasis"/> |
---|
339 | <w:LsdException Locked="false" Priority="21" SemiHidden="false" |
---|
340 | UnhideWhenUsed="false" QFormat="true" Name="Intense Emphasis"/> |
---|
341 | <w:LsdException Locked="false" Priority="31" SemiHidden="false" |
---|
342 | UnhideWhenUsed="false" QFormat="true" Name="Subtle Reference"/> |
---|
343 | <w:LsdException Locked="false" Priority="32" SemiHidden="false" |
---|
344 | UnhideWhenUsed="false" QFormat="true" Name="Intense Reference"/> |
---|
345 | <w:LsdException Locked="false" Priority="33" SemiHidden="false" |
---|
346 | UnhideWhenUsed="false" QFormat="true" Name="Book Title"/> |
---|
347 | <w:LsdException Locked="false" Priority="37" Name="Bibliography"/> |
---|
348 | <w:LsdException Locked="false" Priority="39" QFormat="true" Name="TOC Heading"/> |
---|
349 | </w:LatentStyles> |
---|
350 | </xml><![endif]--> |
---|
351 | <style> |
---|
352 | <!-- |
---|
353 | /* Font Definitions */ |
---|
354 | @font-face |
---|
355 | {font-family:Calibri; |
---|
356 | panose-1:2 15 5 2 2 2 4 3 2 4; |
---|
357 | mso-font-charset:0; |
---|
358 | mso-generic-font-family:swiss; |
---|
359 | mso-font-pitch:variable; |
---|
360 | mso-font-signature:-536870145 1073786111 1 0 415 0;} |
---|
361 | @font-face |
---|
362 | {font-family:Tahoma; |
---|
363 | panose-1:2 11 6 4 3 5 4 4 2 4; |
---|
364 | mso-font-charset:0; |
---|
365 | mso-generic-font-family:swiss; |
---|
366 | mso-font-pitch:variable; |
---|
367 | mso-font-signature:-520081665 -1073717157 41 0 66047 0;} |
---|
368 | /* Style Definitions */ |
---|
369 | p.MsoNormal, li.MsoNormal, div.MsoNormal |
---|
370 | {mso-style-unhide:no; |
---|
371 | mso-style-qformat:yes; |
---|
372 | mso-style-parent:""; |
---|
373 | margin:0in; |
---|
374 | margin-bottom:.0001pt; |
---|
375 | mso-pagination:widow-orphan; |
---|
376 | font-size:12.0pt; |
---|
377 | font-family:"Times New Roman","serif"; |
---|
378 | mso-fareast-font-family:"Times New Roman"; |
---|
379 | mso-fareast-theme-font:minor-fareast;} |
---|
380 | h1 |
---|
381 | {mso-style-priority:9; |
---|
382 | mso-style-unhide:no; |
---|
383 | mso-style-qformat:yes; |
---|
384 | mso-style-link:"Heading 1 Char"; |
---|
385 | mso-margin-top-alt:auto; |
---|
386 | margin-right:0in; |
---|
387 | mso-margin-bottom-alt:auto; |
---|
388 | margin-left:0in; |
---|
389 | mso-pagination:widow-orphan; |
---|
390 | mso-outline-level:1; |
---|
391 | font-size:24.0pt; |
---|
392 | font-family:"Times New Roman","serif"; |
---|
393 | mso-fareast-font-family:"Times New Roman"; |
---|
394 | mso-fareast-theme-font:minor-fareast; |
---|
395 | font-weight:bold;} |
---|
396 | h2 |
---|
397 | {mso-style-noshow:yes; |
---|
398 | mso-style-priority:9; |
---|
399 | mso-style-qformat:yes; |
---|
400 | mso-style-link:"Heading 2 Char"; |
---|
401 | mso-margin-top-alt:auto; |
---|
402 | margin-right:0in; |
---|
403 | mso-margin-bottom-alt:auto; |
---|
404 | margin-left:0in; |
---|
405 | mso-pagination:widow-orphan; |
---|
406 | mso-outline-level:2; |
---|
407 | font-size:18.0pt; |
---|
408 | font-family:"Times New Roman","serif"; |
---|
409 | mso-fareast-font-family:"Times New Roman"; |
---|
410 | mso-fareast-theme-font:minor-fareast; |
---|
411 | font-weight:bold;} |
---|
412 | h3 |
---|
413 | {mso-style-noshow:yes; |
---|
414 | mso-style-priority:9; |
---|
415 | mso-style-qformat:yes; |
---|
416 | mso-style-link:"Heading 3 Char"; |
---|
417 | mso-margin-top-alt:auto; |
---|
418 | margin-right:0in; |
---|
419 | mso-margin-bottom-alt:auto; |
---|
420 | margin-left:0in; |
---|
421 | mso-pagination:widow-orphan; |
---|
422 | mso-outline-level:3; |
---|
423 | font-size:13.5pt; |
---|
424 | font-family:"Times New Roman","serif"; |
---|
425 | mso-fareast-font-family:"Times New Roman"; |
---|
426 | mso-fareast-theme-font:minor-fareast; |
---|
427 | font-weight:bold;} |
---|
428 | h4 |
---|
429 | {mso-style-noshow:yes; |
---|
430 | mso-style-priority:9; |
---|
431 | mso-style-qformat:yes; |
---|
432 | mso-style-link:"Heading 4 Char"; |
---|
433 | mso-style-next:Normal; |
---|
434 | margin-top:10.0pt; |
---|
435 | margin-right:0in; |
---|
436 | margin-bottom:0in; |
---|
437 | margin-left:0in; |
---|
438 | margin-bottom:.0001pt; |
---|
439 | mso-pagination:widow-orphan lines-together; |
---|
440 | page-break-after:avoid; |
---|
441 | mso-outline-level:4; |
---|
442 | font-size:13.0pt; |
---|
443 | font-family:"Cambria","serif"; |
---|
444 | mso-ascii-font-family:Cambria; |
---|
445 | mso-ascii-theme-font:major-latin; |
---|
446 | mso-fareast-font-family:"Times New Roman"; |
---|
447 | mso-fareast-theme-font:major-fareast; |
---|
448 | mso-hansi-font-family:Cambria; |
---|
449 | mso-hansi-theme-font:major-latin; |
---|
450 | mso-bidi-font-family:"Times New Roman"; |
---|
451 | mso-bidi-theme-font:major-bidi; |
---|
452 | color:#4F81BD; |
---|
453 | mso-themecolor:accent1; |
---|
454 | font-weight:bold; |
---|
455 | font-style:italic;} |
---|
456 | h5 |
---|
457 | {mso-style-noshow:yes; |
---|
458 | mso-style-priority:9; |
---|
459 | mso-style-qformat:yes; |
---|
460 | mso-style-link:"Heading 5 Char"; |
---|
461 | mso-margin-top-alt:auto; |
---|
462 | margin-right:0in; |
---|
463 | mso-margin-bottom-alt:auto; |
---|
464 | margin-left:0in; |
---|
465 | mso-pagination:widow-orphan; |
---|
466 | mso-outline-level:5; |
---|
467 | font-size:12.0pt; |
---|
468 | font-family:"Times New Roman","serif"; |
---|
469 | mso-fareast-font-family:"Times New Roman"; |
---|
470 | mso-fareast-theme-font:minor-fareast; |
---|
471 | color:#4F4FFF; |
---|
472 | font-weight:bold;} |
---|
473 | p.MsoTitle, li.MsoTitle, div.MsoTitle |
---|
474 | {mso-style-noshow:yes; |
---|
475 | mso-style-priority:10; |
---|
476 | mso-style-unhide:no; |
---|
477 | mso-style-qformat:yes; |
---|
478 | mso-style-link:"Title Char"; |
---|
479 | mso-style-next:Normal; |
---|
480 | margin-top:0in; |
---|
481 | margin-right:0in; |
---|
482 | margin-bottom:15.0pt; |
---|
483 | margin-left:0in; |
---|
484 | mso-add-space:auto; |
---|
485 | mso-pagination:widow-orphan; |
---|
486 | border:none; |
---|
487 | mso-border-bottom-alt:solid #4F81BD 1.0pt; |
---|
488 | mso-border-bottom-themecolor:accent1; |
---|
489 | padding:0in; |
---|
490 | mso-padding-alt:0in 0in 4.0pt 0in; |
---|
491 | font-size:26.0pt; |
---|
492 | font-family:"Cambria","serif"; |
---|
493 | mso-ascii-font-family:Cambria; |
---|
494 | mso-ascii-theme-font:major-latin; |
---|
495 | mso-fareast-font-family:"Times New Roman"; |
---|
496 | mso-fareast-theme-font:major-fareast; |
---|
497 | mso-hansi-font-family:Cambria; |
---|
498 | mso-hansi-theme-font:major-latin; |
---|
499 | mso-bidi-font-family:"Times New Roman"; |
---|
500 | mso-bidi-theme-font:major-bidi; |
---|
501 | color:#17365D; |
---|
502 | mso-themecolor:text2; |
---|
503 | mso-themeshade:191; |
---|
504 | letter-spacing:.25pt; |
---|
505 | mso-font-kerning:14.0pt;} |
---|
506 | p.MsoTitleCxSpFirst, li.MsoTitleCxSpFirst, div.MsoTitleCxSpFirst |
---|
507 | {mso-style-noshow:yes; |
---|
508 | mso-style-priority:10; |
---|
509 | mso-style-unhide:no; |
---|
510 | mso-style-qformat:yes; |
---|
511 | mso-style-link:"Title Char"; |
---|
512 | mso-style-next:Normal; |
---|
513 | mso-style-type:export-only; |
---|
514 | margin:0in; |
---|
515 | margin-bottom:.0001pt; |
---|
516 | mso-add-space:auto; |
---|
517 | mso-pagination:widow-orphan; |
---|
518 | border:none; |
---|
519 | mso-border-bottom-alt:solid #4F81BD 1.0pt; |
---|
520 | mso-border-bottom-themecolor:accent1; |
---|
521 | padding:0in; |
---|
522 | mso-padding-alt:0in 0in 4.0pt 0in; |
---|
523 | font-size:26.0pt; |
---|
524 | font-family:"Cambria","serif"; |
---|
525 | mso-ascii-font-family:Cambria; |
---|
526 | mso-ascii-theme-font:major-latin; |
---|
527 | mso-fareast-font-family:"Times New Roman"; |
---|
528 | mso-fareast-theme-font:major-fareast; |
---|
529 | mso-hansi-font-family:Cambria; |
---|
530 | mso-hansi-theme-font:major-latin; |
---|
531 | mso-bidi-font-family:"Times New Roman"; |
---|
532 | mso-bidi-theme-font:major-bidi; |
---|
533 | color:#17365D; |
---|
534 | mso-themecolor:text2; |
---|
535 | mso-themeshade:191; |
---|
536 | letter-spacing:.25pt; |
---|
537 | mso-font-kerning:14.0pt;} |
---|
538 | p.MsoTitleCxSpMiddle, li.MsoTitleCxSpMiddle, div.MsoTitleCxSpMiddle |
---|
539 | {mso-style-noshow:yes; |
---|
540 | mso-style-priority:10; |
---|
541 | mso-style-unhide:no; |
---|
542 | mso-style-qformat:yes; |
---|
543 | mso-style-link:"Title Char"; |
---|
544 | mso-style-next:Normal; |
---|
545 | mso-style-type:export-only; |
---|
546 | margin:0in; |
---|
547 | margin-bottom:.0001pt; |
---|
548 | mso-add-space:auto; |
---|
549 | mso-pagination:widow-orphan; |
---|
550 | border:none; |
---|
551 | mso-border-bottom-alt:solid #4F81BD 1.0pt; |
---|
552 | mso-border-bottom-themecolor:accent1; |
---|
553 | padding:0in; |
---|
554 | mso-padding-alt:0in 0in 4.0pt 0in; |
---|
555 | font-size:26.0pt; |
---|
556 | font-family:"Cambria","serif"; |
---|
557 | mso-ascii-font-family:Cambria; |
---|
558 | mso-ascii-theme-font:major-latin; |
---|
559 | mso-fareast-font-family:"Times New Roman"; |
---|
560 | mso-fareast-theme-font:major-fareast; |
---|
561 | mso-hansi-font-family:Cambria; |
---|
562 | mso-hansi-theme-font:major-latin; |
---|
563 | mso-bidi-font-family:"Times New Roman"; |
---|
564 | mso-bidi-theme-font:major-bidi; |
---|
565 | color:#17365D; |
---|
566 | mso-themecolor:text2; |
---|
567 | mso-themeshade:191; |
---|
568 | letter-spacing:.25pt; |
---|
569 | mso-font-kerning:14.0pt;} |
---|
570 | p.MsoTitleCxSpLast, li.MsoTitleCxSpLast, div.MsoTitleCxSpLast |
---|
571 | {mso-style-noshow:yes; |
---|
572 | mso-style-priority:10; |
---|
573 | mso-style-unhide:no; |
---|
574 | mso-style-qformat:yes; |
---|
575 | mso-style-link:"Title Char"; |
---|
576 | mso-style-next:Normal; |
---|
577 | mso-style-type:export-only; |
---|
578 | margin-top:0in; |
---|
579 | margin-right:0in; |
---|
580 | margin-bottom:15.0pt; |
---|
581 | margin-left:0in; |
---|
582 | mso-add-space:auto; |
---|
583 | mso-pagination:widow-orphan; |
---|
584 | border:none; |
---|
585 | mso-border-bottom-alt:solid #4F81BD 1.0pt; |
---|
586 | mso-border-bottom-themecolor:accent1; |
---|
587 | padding:0in; |
---|
588 | mso-padding-alt:0in 0in 4.0pt 0in; |
---|
589 | font-size:26.0pt; |
---|
590 | font-family:"Cambria","serif"; |
---|
591 | mso-ascii-font-family:Cambria; |
---|
592 | mso-ascii-theme-font:major-latin; |
---|
593 | mso-fareast-font-family:"Times New Roman"; |
---|
594 | mso-fareast-theme-font:major-fareast; |
---|
595 | mso-hansi-font-family:Cambria; |
---|
596 | mso-hansi-theme-font:major-latin; |
---|
597 | mso-bidi-font-family:"Times New Roman"; |
---|
598 | mso-bidi-theme-font:major-bidi; |
---|
599 | color:#17365D; |
---|
600 | mso-themecolor:text2; |
---|
601 | mso-themeshade:191; |
---|
602 | letter-spacing:.25pt; |
---|
603 | mso-font-kerning:14.0pt;} |
---|
604 | a:link, span.MsoHyperlink |
---|
605 | {mso-style-noshow:yes; |
---|
606 | mso-style-priority:99; |
---|
607 | color:blue; |
---|
608 | text-decoration:underline; |
---|
609 | text-underline:single;} |
---|
610 | a:visited, span.MsoHyperlinkFollowed |
---|
611 | {mso-style-noshow:yes; |
---|
612 | mso-style-priority:99; |
---|
613 | color:purple; |
---|
614 | text-decoration:underline; |
---|
615 | text-underline:single;} |
---|
616 | p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap |
---|
617 | {mso-style-noshow:yes; |
---|
618 | mso-style-priority:99; |
---|
619 | mso-style-link:"Document Map Char"; |
---|
620 | margin:0in; |
---|
621 | margin-bottom:.0001pt; |
---|
622 | mso-pagination:widow-orphan; |
---|
623 | font-size:8.0pt; |
---|
624 | font-family:"Tahoma","sans-serif"; |
---|
625 | mso-fareast-font-family:"Times New Roman"; |
---|
626 | mso-fareast-theme-font:minor-fareast;} |
---|
627 | p |
---|
628 | {mso-style-noshow:yes; |
---|
629 | mso-style-priority:99; |
---|
630 | mso-margin-top-alt:auto; |
---|
631 | margin-right:0in; |
---|
632 | mso-margin-bottom-alt:auto; |
---|
633 | margin-left:0in; |
---|
634 | mso-pagination:widow-orphan; |
---|
635 | font-size:12.0pt; |
---|
636 | font-family:"Times New Roman","serif"; |
---|
637 | mso-fareast-font-family:"Times New Roman"; |
---|
638 | mso-fareast-theme-font:minor-fareast;} |
---|
639 | pre |
---|
640 | {mso-style-noshow:yes; |
---|
641 | mso-style-priority:99; |
---|
642 | mso-style-link:"HTML Preformatted Char"; |
---|
643 | margin:0in; |
---|
644 | margin-bottom:.0001pt; |
---|
645 | mso-pagination:widow-orphan; |
---|
646 | tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt; |
---|
647 | font-size:10.0pt; |
---|
648 | font-family:"Courier New"; |
---|
649 | mso-fareast-font-family:"Times New Roman";} |
---|
650 | p.MsoAcetate, li.MsoAcetate, div.MsoAcetate |
---|
651 | {mso-style-noshow:yes; |
---|
652 | mso-style-priority:99; |
---|
653 | mso-style-link:"Balloon Text Char"; |
---|
654 | margin:0in; |
---|
655 | margin-bottom:.0001pt; |
---|
656 | mso-pagination:widow-orphan; |
---|
657 | font-size:8.0pt; |
---|
658 | font-family:"Tahoma","sans-serif"; |
---|
659 | mso-fareast-font-family:"Times New Roman"; |
---|
660 | mso-fareast-theme-font:minor-fareast;} |
---|
661 | span.MsoPlaceholderText |
---|
662 | {mso-style-noshow:yes; |
---|
663 | mso-style-priority:99; |
---|
664 | mso-style-unhide:no; |
---|
665 | color:gray;} |
---|
666 | p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing |
---|
667 | {mso-style-noshow:yes; |
---|
668 | mso-style-priority:1; |
---|
669 | mso-style-unhide:no; |
---|
670 | mso-style-qformat:yes; |
---|
671 | mso-style-parent:""; |
---|
672 | margin:0in; |
---|
673 | margin-bottom:.0001pt; |
---|
674 | mso-pagination:widow-orphan; |
---|
675 | font-size:12.0pt; |
---|
676 | font-family:"Times New Roman","serif"; |
---|
677 | mso-fareast-font-family:"Times New Roman"; |
---|
678 | mso-fareast-theme-font:minor-fareast;} |
---|
679 | p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph |
---|
680 | {mso-style-noshow:yes; |
---|
681 | mso-style-priority:34; |
---|
682 | mso-style-unhide:no; |
---|
683 | mso-style-qformat:yes; |
---|
684 | margin-top:0in; |
---|
685 | margin-right:0in; |
---|
686 | margin-bottom:0in; |
---|
687 | margin-left:.5in; |
---|
688 | margin-bottom:.0001pt; |
---|
689 | mso-add-space:auto; |
---|
690 | mso-pagination:widow-orphan; |
---|
691 | font-size:12.0pt; |
---|
692 | font-family:"Times New Roman","serif"; |
---|
693 | mso-fareast-font-family:"Times New Roman"; |
---|
694 | mso-fareast-theme-font:minor-fareast;} |
---|
695 | p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst |
---|
696 | {mso-style-noshow:yes; |
---|
697 | mso-style-priority:34; |
---|
698 | mso-style-unhide:no; |
---|
699 | mso-style-qformat:yes; |
---|
700 | mso-style-type:export-only; |
---|
701 | margin-top:0in; |
---|
702 | margin-right:0in; |
---|
703 | margin-bottom:0in; |
---|
704 | margin-left:.5in; |
---|
705 | margin-bottom:.0001pt; |
---|
706 | mso-add-space:auto; |
---|
707 | mso-pagination:widow-orphan; |
---|
708 | font-size:12.0pt; |
---|
709 | font-family:"Times New Roman","serif"; |
---|
710 | mso-fareast-font-family:"Times New Roman"; |
---|
711 | mso-fareast-theme-font:minor-fareast;} |
---|
712 | p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle |
---|
713 | {mso-style-noshow:yes; |
---|
714 | mso-style-priority:34; |
---|
715 | mso-style-unhide:no; |
---|
716 | mso-style-qformat:yes; |
---|
717 | mso-style-type:export-only; |
---|
718 | margin-top:0in; |
---|
719 | margin-right:0in; |
---|
720 | margin-bottom:0in; |
---|
721 | margin-left:.5in; |
---|
722 | margin-bottom:.0001pt; |
---|
723 | mso-add-space:auto; |
---|
724 | mso-pagination:widow-orphan; |
---|
725 | font-size:12.0pt; |
---|
726 | font-family:"Times New Roman","serif"; |
---|
727 | mso-fareast-font-family:"Times New Roman"; |
---|
728 | mso-fareast-theme-font:minor-fareast;} |
---|
729 | p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast |
---|
730 | {mso-style-noshow:yes; |
---|
731 | mso-style-priority:34; |
---|
732 | mso-style-unhide:no; |
---|
733 | mso-style-qformat:yes; |
---|
734 | mso-style-type:export-only; |
---|
735 | margin-top:0in; |
---|
736 | margin-right:0in; |
---|
737 | margin-bottom:0in; |
---|
738 | margin-left:.5in; |
---|
739 | margin-bottom:.0001pt; |
---|
740 | mso-add-space:auto; |
---|
741 | mso-pagination:widow-orphan; |
---|
742 | font-size:12.0pt; |
---|
743 | font-family:"Times New Roman","serif"; |
---|
744 | mso-fareast-font-family:"Times New Roman"; |
---|
745 | mso-fareast-theme-font:minor-fareast;} |
---|
746 | span.MsoIntenseReference |
---|
747 | {mso-style-priority:32; |
---|
748 | mso-style-unhide:no; |
---|
749 | mso-style-qformat:yes; |
---|
750 | font-variant:small-caps; |
---|
751 | color:#C0504D; |
---|
752 | mso-themecolor:accent2; |
---|
753 | letter-spacing:.25pt; |
---|
754 | font-weight:bold; |
---|
755 | text-decoration:underline; |
---|
756 | text-underline:single;} |
---|
757 | span.Heading1Char |
---|
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971 | |
---|
972 | <h1>Integration of area detector data in GSAS-II</h1> |
---|
973 | |
---|
974 | <p class=MsoNormal>In this demo, data collected with a Perkin-Elmer area |
---|
975 | detector at APS 11-ID-C with a wavelength 0.10798 A, where the detector was |
---|
976 | intentionally tilted at 45 degrees, are used. Note that menu entries are listed |
---|
977 | in <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
978 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
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979 | Calibri;mso-bidi-theme-font:minor-latin'>bold face</span></b> below as <b |
---|
980 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
981 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
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982 | Calibri;mso-bidi-theme-font:minor-latin'>Help/About GSAS-II</span></b>, which |
---|
983 | lists first the name of the menu (here <b style='mso-bidi-font-weight:normal'><span |
---|
984 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
985 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
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986 | minor-latin'>Help</span></b>) and second the name of the entry in the menu |
---|
987 | (here <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
988 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
---|
989 | Calibri;mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).</p> |
---|
990 | |
---|
991 | <h2>Prerequisite:<span style='mso-spacerun:yes'> </span><a |
---|
992 | href="Calibration%20of%20an%20area%20detector%20in%20GSAS.htm">Calibration Demo</a></h2> |
---|
993 | |
---|
994 | <p class=MsoNormal>This assumes that an image data set has been read in and |
---|
995 | calibration results have been derived, see the <a |
---|
996 | href="Calibration%20of%20an%20area%20detector%20in%20GSAS.htm">Calibration Demo</a></p> |
---|
997 | |
---|
998 | <h2>Step 1: Clear calibration plot</h2> |
---|
999 | |
---|
1000 | <p class=MsoNormal>Assuming the previous step was calibration, the image plot |
---|
1001 | will show the located rings and possibly all the picked points. These are no |
---|
1002 | longer needed. The <b style='mso-bidi-font-weight:normal'><span |
---|
1003 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1004 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1005 | minor-latin'>Image Controls/Clear Calibration</span></b> menu entry removes |
---|
1006 | these from the plot, but<u> does not clear the calibration results</u>. Use of |
---|
1007 | this menu item is not required, but does speed future display of results. </p> |
---|
1008 | |
---|
1009 | <h2>Step 2: Integration Settings</h2> |
---|
1010 | |
---|
1011 | <p class=MsoNormal>In the simplest case, all that is needed is to click on the <b |
---|
1012 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
1013 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
---|
1014 | Calibri;mso-bidi-theme-font:minor-latin'>Do full integration?</span></b> <span |
---|
1015 | class=GramE>check</span> box and adjust the inner and outer 2-theta values with |
---|
1016 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
1017 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
---|
1018 | Calibri;mso-bidi-theme-font:minor-latin'>Inner 2-theta</span></b> and<b |
---|
1019 | style='mso-bidi-font-weight:normal'> </b><b style='mso-bidi-font-weight:normal'><span |
---|
1020 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1021 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1022 | minor-latin'>Outer 2-theta</span></b> controls. It is helpful to see the |
---|
1023 | two-theta limits on the plot visually, while adjusting the two-theta range. |
---|
1024 | This is done by clicking on the <b style='mso-bidi-font-weight:normal'><span |
---|
1025 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1026 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1027 | minor-latin'>Show integration limits?</span></b> <span class=GramE>check</span> |
---|
1028 | box. Note that inner limit is shown as a green ellipse at 2deg and the outer is |
---|
1029 | shown as a red ellipse at 5deg by default. These limits may also be dragged to |
---|
1030 | the desired values; a small popup window shows the value. <o:p></o:p></p> |
---|
1031 | |
---|
1032 | <p class=MsoNormal>Change the limits to <b style='mso-bidi-font-weight:normal'><span |
---|
1033 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1034 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1035 | minor-latin'>1</span></b> and <b style='mso-bidi-font-weight:normal'><span |
---|
1036 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1037 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1038 | minor-latin'>7</span></b> for this data. Note that changes are displayed when |
---|
1039 | numbers are placed in the boxes only after pressing return or tab key or by |
---|
1040 | clicking on some other item in the window.</p> |
---|
1041 | |
---|
1042 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype |
---|
1043 | id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t" |
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---|
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---|
1057 | <v:f eqn="prod @7 21600 pixelHeight"/> |
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1058 | <v:f eqn="sum @10 21600 0"/> |
---|
1059 | </v:formulas> |
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1060 | <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> |
---|
1061 | <o:lock v:ext="edit" aspectratio="t"/> |
---|
1062 | </v:shapetype><v:shape id="Picture_x0020_6" o:spid="_x0000_i1029" type="#_x0000_t75" |
---|
1063 | style='width:472.5pt;height:342pt;visibility:visible;mso-wrap-style:square'> |
---|
1064 | <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image001.png" |
---|
1065 | o:title=""/> |
---|
1066 | </v:shape><![endif]--><![if !vml]><img border=0 width=630 height=456 |
---|
1067 | src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image001.png" |
---|
1068 | v:shapes="Picture_x0020_6"><![endif]></span></p> |
---|
1069 | |
---|
1070 | <h3>Other useful controls:</h3> |
---|
1071 | |
---|
1072 | <p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span |
---|
1073 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1074 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1075 | minor-latin'>Azimuth offset</span></b>: The image vertical axis (from the beam |
---|
1076 | center, going down) is labeled with the azimuth value placed in the <b |
---|
1077 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
1078 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
---|
1079 | Calibri;mso-bidi-theme-font:minor-latin'>Azimuth offset</span></b> box. This is |
---|
1080 | usually zero unless the image plate has been rotated about its normal axis.</p> |
---|
1081 | |
---|
1082 | <p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span |
---|
1083 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1084 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1085 | minor-latin'>Start/End azimuth</span></b>: The integration is started at the |
---|
1086 | Start azimuth angle in the left box, and when the <b style='mso-bidi-font-weight: |
---|
1087 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
---|
1088 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; |
---|
1089 | mso-bidi-theme-font:minor-latin'>Do full integration?</span></b> <span |
---|
1090 | class=GramE>checkbox</span> is not checked, the integration will be run only to |
---|
1091 | the maximum value specified. When the range is less than 360 degrees, the |
---|
1092 | integration range will be shown (if selected) with the high and low limits |
---|
1093 | plotted and only segments of the max and min ellipses drawn. These limits may |
---|
1094 | also be dragged on the plot to desired locations.</p> |
---|
1095 | |
---|
1096 | <p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span |
---|
1097 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1098 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1099 | minor-latin'>Number of 2-theta bins</span></b>: The resulting 1-D powder |
---|
1100 | pattern after integration will consist of this many points. This number should |
---|
1101 | be on the order of the number of pixels in one direction (since resolution |
---|
1102 | cannot be much better than this) or less, if instrumental resolution and sample |
---|
1103 | broadening does not require that many points. Some trial and error may be |
---|
1104 | needed, but there should more than 6 points across each peak |
---|
1105 | full-width-at-half-maximum (FWHM) in the final pattern to be useful for further |
---|
1106 | analysis. In this case <b style='mso-bidi-font-weight:normal'><span |
---|
1107 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1108 | mso-hansi-theme-font:minor-latin'>5000</span></b> is a better choice than the |
---|
1109 | default.</p> |
---|
1110 | |
---|
1111 | <p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span |
---|
1112 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1113 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1114 | minor-latin'>Number of azimuth bins</span></b>: In cases where the diffraction |
---|
1115 | experiment shows changes as a function of azimuthal angle, the integration can |
---|
1116 | be performed as a function of angle. This number specifies the number of bins |
---|
1117 | to use by azimuthal angle. The process of breaking up the integration in this |
---|
1118 | way is sometimes called "caking" since the integration region grows |
---|
1119 | with distance from the beam-center, with a shape like a slice of cake or pie. |
---|
1120 | When more than one azimuthal bin is used, the regions are shown in the plot |
---|
1121 | with dashed lines, when the Show integration limits?" check box is |
---|
1122 | checked. </p> |
---|
1123 | |
---|
1124 | <p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span |
---|
1125 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1126 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1127 | minor-latin'>Appl. det. absorption</span></b> and <b style='mso-bidi-font-weight: |
---|
1128 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
---|
1129 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; |
---|
1130 | mso-bidi-theme-font:minor-latin'>value</span></b>: The scattered ray beams are |
---|
1131 | partially absorbed by the detector depending on the scattering angle. This |
---|
1132 | reduces the intensity of higher angle data more than low angle data. The value |
---|
1133 | is dependent on the wavelength and the materials used for the front surface of |
---|
1134 | the detector, so some experimentation with a standard is needed to establish an |
---|
1135 | appropriate value.</p> |
---|
1136 | |
---|
1137 | <p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span |
---|
1138 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1139 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1140 | minor-latin'>Background Image</span> </b>and<b style='mso-bidi-font-weight: |
---|
1141 | normal'> </b><b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1142 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1143 | minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Multiplier</span></b>: |
---|
1144 | You can designate a previously read in image as background which will then be |
---|
1145 | used to modify each data image as they are integrated. Note that the <b |
---|
1146 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
1147 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
---|
1148 | Calibri;mso-bidi-theme-font:minor-latin'>Multiplier</span></b> must be negative |
---|
1149 | for it to be subtracted. Note that all images used in this way must be exactly |
---|
1150 | the same format (number of pixels & pixel size).</p> |
---|
1151 | |
---|
1152 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1153 | id="Picture_x0020_7" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:525pt; |
---|
1154 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1155 | <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image002.png" |
---|
1156 | o:title=""/> |
---|
1157 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
---|
1158 | src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image002.png" |
---|
1159 | v:shapes="Picture_x0020_7"><![endif]></span></p> |
---|
1160 | |
---|
1161 | <h2>Step 3: Perform integration </h2> |
---|
1162 | |
---|
1163 | <p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the <b |
---|
1164 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
1165 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
---|
1166 | Calibri;mso-bidi-theme-font:minor-latin'>Image Operations/Integrate</span></b> |
---|
1167 | image data menu item to start the integration. This will take at least a few |
---|
1168 | seconds. If multiple images have been read in, the <b style='mso-bidi-font-weight: |
---|
1169 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
---|
1170 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; |
---|
1171 | mso-bidi-theme-font:minor-latin'>Integrate All</span></b> menu item can be |
---|
1172 | used. This is most useful when the <b style='mso-bidi-font-weight:normal'><span |
---|
1173 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
---|
1174 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1175 | minor-latin'>Use as Default</span></b> option is in use for one image.</p> |
---|
1176 | |
---|
1177 | <p class=MsoNormal><span style='mso-spacerun:yes'> </span>At this point the |
---|
1178 | data tree window will have new entries as each azimuthal "slice" |
---|
1179 | added to the data tree as a powder pattern</p> |
---|
1180 | |
---|
1181 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1182 | id="Picture_x0020_8" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:300pt; |
---|
1183 | height:187.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1184 | <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image003.png" |
---|
1185 | o:title=""/> |
---|
1186 | </v:shape><![endif]--><![if !vml]><img border=0 width=400 height=250 |
---|
1187 | src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image003.png" |
---|
1188 | v:shapes="Picture_x0020_8"><![endif]></span><span |
---|
1189 | style='mso-spacerun:yes'> </span></p> |
---|
1190 | |
---|
1191 | <p class=MsoNormal>Two plots are added to the plot window: One (with tab <b |
---|
1192 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
1193 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
---|
1194 | Calibri;mso-bidi-theme-font:minor-latin'>2D Integration</span></b>) shows the |
---|
1195 | diffraction intensity as a function of both 2-theta and (when there is more |
---|
1196 | than one azimuthal integration region) azimuthal angle.</p> |
---|
1197 | |
---|
1198 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1199 | id="Picture_x0020_9" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:525pt; |
---|
1200 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1201 | <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image004.png" |
---|
1202 | o:title=""/> |
---|
1203 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
---|
1204 | src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image004.png" |
---|
1205 | v:shapes="Picture_x0020_9"><![endif]></span><span |
---|
1206 | style='mso-spacerun:yes'> </span></p> |
---|
1207 | |
---|
1208 | <p class=MsoNormal><span class=GramE>and</span> a conventional 1-D powder |
---|
1209 | pattern(s) for each "slice"</p> |
---|
1210 | |
---|
1211 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1212 | id="Picture_x0020_10" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt; |
---|
1213 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1214 | <v:imagedata src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image005.png" |
---|
1215 | o:title=""/> |
---|
1216 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
---|
1217 | src="Integration%20of%20area%20detector%20data%20in%20GSAS_files/image005.png" |
---|
1218 | v:shapes="Picture_x0020_10"><![endif]></span></p> |
---|
1219 | |
---|
1220 | <p class=MsoNormal>Again you could save the project with <b style='mso-bidi-font-weight: |
---|
1221 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
---|
1222 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; |
---|
1223 | mso-bidi-theme-font:minor-latin'>File/Save project</span></b> on the main <b |
---|
1224 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
---|
1225 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family: |
---|
1226 | Calibri;mso-bidi-theme-font:minor-latin'>GSAS-II data tree</span></b> menu |
---|
1227 | although it is not needed for any further tutorials.</p> |
---|
1228 | |
---|
1229 | <h2>Next demo: <a href="Fit%20Peaks.htm"><span style='color:windowtext; |
---|
1230 | text-decoration:none;text-underline:none'>Fit Peaks and <span class=SpellE>Autoindexing</span></span></a></h2> |
---|
1231 | |
---|
1232 | </div> |
---|
1233 | |
---|
1234 | </body> |
---|
1235 | |
---|
1236 | </html> |
---|