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| 23 | <o:Author>Von Dreele</o:Author> |
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| 25 | <o:Revision>19</o:Revision> |
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| 307 | <w:LsdException Locked="false" Priority="61" SemiHidden="false" |
|---|
| 308 | UnhideWhenUsed="false" Name="Light List Accent 6"/> |
|---|
| 309 | <w:LsdException Locked="false" Priority="62" SemiHidden="false" |
|---|
| 310 | UnhideWhenUsed="false" Name="Light Grid Accent 6"/> |
|---|
| 311 | <w:LsdException Locked="false" Priority="63" SemiHidden="false" |
|---|
| 312 | UnhideWhenUsed="false" Name="Medium Shading 1 Accent 6"/> |
|---|
| 313 | <w:LsdException Locked="false" Priority="64" SemiHidden="false" |
|---|
| 314 | UnhideWhenUsed="false" Name="Medium Shading 2 Accent 6"/> |
|---|
| 315 | <w:LsdException Locked="false" Priority="65" SemiHidden="false" |
|---|
| 316 | UnhideWhenUsed="false" Name="Medium List 1 Accent 6"/> |
|---|
| 317 | <w:LsdException Locked="false" Priority="66" SemiHidden="false" |
|---|
| 318 | UnhideWhenUsed="false" Name="Medium List 2 Accent 6"/> |
|---|
| 319 | <w:LsdException Locked="false" Priority="67" SemiHidden="false" |
|---|
| 320 | UnhideWhenUsed="false" Name="Medium Grid 1 Accent 6"/> |
|---|
| 321 | <w:LsdException Locked="false" Priority="68" SemiHidden="false" |
|---|
| 322 | UnhideWhenUsed="false" Name="Medium Grid 2 Accent 6"/> |
|---|
| 323 | <w:LsdException Locked="false" Priority="69" SemiHidden="false" |
|---|
| 324 | UnhideWhenUsed="false" Name="Medium Grid 3 Accent 6"/> |
|---|
| 325 | <w:LsdException Locked="false" Priority="70" SemiHidden="false" |
|---|
| 326 | UnhideWhenUsed="false" Name="Dark List Accent 6"/> |
|---|
| 327 | <w:LsdException Locked="false" Priority="71" SemiHidden="false" |
|---|
| 328 | UnhideWhenUsed="false" Name="Colorful Shading Accent 6"/> |
|---|
| 329 | <w:LsdException Locked="false" Priority="72" SemiHidden="false" |
|---|
| 330 | UnhideWhenUsed="false" Name="Colorful List Accent 6"/> |
|---|
| 331 | <w:LsdException Locked="false" Priority="73" SemiHidden="false" |
|---|
| 332 | UnhideWhenUsed="false" Name="Colorful Grid Accent 6"/> |
|---|
| 333 | <w:LsdException Locked="false" Priority="19" SemiHidden="false" |
|---|
| 334 | UnhideWhenUsed="false" QFormat="true" Name="Subtle Emphasis"/> |
|---|
| 335 | <w:LsdException Locked="false" Priority="21" SemiHidden="false" |
|---|
| 336 | UnhideWhenUsed="false" QFormat="true" Name="Intense Emphasis"/> |
|---|
| 337 | <w:LsdException Locked="false" Priority="31" SemiHidden="false" |
|---|
| 338 | UnhideWhenUsed="false" QFormat="true" Name="Subtle Reference"/> |
|---|
| 339 | <w:LsdException Locked="false" Priority="32" SemiHidden="false" |
|---|
| 340 | UnhideWhenUsed="false" QFormat="true" Name="Intense Reference"/> |
|---|
| 341 | <w:LsdException Locked="false" Priority="33" SemiHidden="false" |
|---|
| 342 | UnhideWhenUsed="false" QFormat="true" Name="Book Title"/> |
|---|
| 343 | <w:LsdException Locked="false" Priority="37" Name="Bibliography"/> |
|---|
| 344 | <w:LsdException Locked="false" Priority="39" QFormat="true" Name="TOC Heading"/> |
|---|
| 345 | </w:LatentStyles> |
|---|
| 346 | </xml><![endif]--> |
|---|
| 347 | <style> |
|---|
| 348 | <!-- |
|---|
| 349 | /* Font Definitions */ |
|---|
| 350 | @font-face |
|---|
| 351 | {font-family:Calibri; |
|---|
| 352 | panose-1:2 15 5 2 2 2 4 3 2 4; |
|---|
| 353 | mso-font-charset:0; |
|---|
| 354 | mso-generic-font-family:swiss; |
|---|
| 355 | mso-font-pitch:variable; |
|---|
| 356 | mso-font-signature:-520092929 1073786111 9 0 415 0;} |
|---|
| 357 | @font-face |
|---|
| 358 | {font-family:Tahoma; |
|---|
| 359 | panose-1:2 11 6 4 3 5 4 4 2 4; |
|---|
| 360 | mso-font-charset:0; |
|---|
| 361 | mso-generic-font-family:swiss; |
|---|
| 362 | mso-font-pitch:variable; |
|---|
| 363 | mso-font-signature:-520081665 -1073717157 41 0 66047 0;} |
|---|
| 364 | /* Style Definitions */ |
|---|
| 365 | p.MsoNormal, li.MsoNormal, div.MsoNormal |
|---|
| 366 | {mso-style-unhide:no; |
|---|
| 367 | mso-style-qformat:yes; |
|---|
| 368 | mso-style-parent:""; |
|---|
| 369 | margin:0in; |
|---|
| 370 | margin-bottom:.0001pt; |
|---|
| 371 | mso-pagination:widow-orphan; |
|---|
| 372 | font-size:12.0pt; |
|---|
| 373 | font-family:"Times New Roman","serif"; |
|---|
| 374 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 375 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 376 | h1 |
|---|
| 377 | {mso-style-priority:9; |
|---|
| 378 | mso-style-unhide:no; |
|---|
| 379 | mso-style-qformat:yes; |
|---|
| 380 | mso-style-link:"Heading 1 Char"; |
|---|
| 381 | mso-margin-top-alt:auto; |
|---|
| 382 | margin-right:0in; |
|---|
| 383 | mso-margin-bottom-alt:auto; |
|---|
| 384 | margin-left:0in; |
|---|
| 385 | mso-pagination:widow-orphan; |
|---|
| 386 | mso-outline-level:1; |
|---|
| 387 | font-size:24.0pt; |
|---|
| 388 | font-family:"Times New Roman","serif"; |
|---|
| 389 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 390 | mso-fareast-theme-font:minor-fareast; |
|---|
| 391 | font-weight:bold;} |
|---|
| 392 | h2 |
|---|
| 393 | {mso-style-noshow:yes; |
|---|
| 394 | mso-style-priority:9; |
|---|
| 395 | mso-style-qformat:yes; |
|---|
| 396 | mso-style-link:"Heading 2 Char"; |
|---|
| 397 | mso-margin-top-alt:auto; |
|---|
| 398 | margin-right:0in; |
|---|
| 399 | mso-margin-bottom-alt:auto; |
|---|
| 400 | margin-left:0in; |
|---|
| 401 | mso-pagination:widow-orphan; |
|---|
| 402 | mso-outline-level:2; |
|---|
| 403 | font-size:18.0pt; |
|---|
| 404 | font-family:"Times New Roman","serif"; |
|---|
| 405 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 406 | mso-fareast-theme-font:minor-fareast; |
|---|
| 407 | font-weight:bold;} |
|---|
| 408 | h3 |
|---|
| 409 | {mso-style-noshow:yes; |
|---|
| 410 | mso-style-priority:9; |
|---|
| 411 | mso-style-qformat:yes; |
|---|
| 412 | mso-style-link:"Heading 3 Char"; |
|---|
| 413 | mso-margin-top-alt:auto; |
|---|
| 414 | margin-right:0in; |
|---|
| 415 | mso-margin-bottom-alt:auto; |
|---|
| 416 | margin-left:0in; |
|---|
| 417 | mso-pagination:widow-orphan; |
|---|
| 418 | mso-outline-level:3; |
|---|
| 419 | font-size:13.5pt; |
|---|
| 420 | font-family:"Times New Roman","serif"; |
|---|
| 421 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 422 | mso-fareast-theme-font:minor-fareast; |
|---|
| 423 | font-weight:bold;} |
|---|
| 424 | h4 |
|---|
| 425 | {mso-style-noshow:yes; |
|---|
| 426 | mso-style-priority:9; |
|---|
| 427 | mso-style-qformat:yes; |
|---|
| 428 | mso-style-link:"Heading 4 Char"; |
|---|
| 429 | mso-style-next:Normal; |
|---|
| 430 | margin-top:10.0pt; |
|---|
| 431 | margin-right:0in; |
|---|
| 432 | margin-bottom:0in; |
|---|
| 433 | margin-left:0in; |
|---|
| 434 | margin-bottom:.0001pt; |
|---|
| 435 | mso-pagination:widow-orphan lines-together; |
|---|
| 436 | page-break-after:avoid; |
|---|
| 437 | mso-outline-level:4; |
|---|
| 438 | font-size:13.0pt; |
|---|
| 439 | font-family:"Cambria","serif"; |
|---|
| 440 | mso-ascii-font-family:Cambria; |
|---|
| 441 | mso-ascii-theme-font:major-latin; |
|---|
| 442 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 443 | mso-fareast-theme-font:major-fareast; |
|---|
| 444 | mso-hansi-font-family:Cambria; |
|---|
| 445 | mso-hansi-theme-font:major-latin; |
|---|
| 446 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 447 | mso-bidi-theme-font:major-bidi; |
|---|
| 448 | color:#4F81BD; |
|---|
| 449 | mso-themecolor:accent1; |
|---|
| 450 | font-weight:bold; |
|---|
| 451 | font-style:italic;} |
|---|
| 452 | h5 |
|---|
| 453 | {mso-style-noshow:yes; |
|---|
| 454 | mso-style-priority:9; |
|---|
| 455 | mso-style-qformat:yes; |
|---|
| 456 | mso-style-link:"Heading 5 Char"; |
|---|
| 457 | mso-margin-top-alt:auto; |
|---|
| 458 | margin-right:0in; |
|---|
| 459 | mso-margin-bottom-alt:auto; |
|---|
| 460 | margin-left:0in; |
|---|
| 461 | mso-pagination:widow-orphan; |
|---|
| 462 | mso-outline-level:5; |
|---|
| 463 | font-size:12.0pt; |
|---|
| 464 | font-family:"Times New Roman","serif"; |
|---|
| 465 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 466 | mso-fareast-theme-font:minor-fareast; |
|---|
| 467 | color:#4F4FFF; |
|---|
| 468 | font-weight:bold;} |
|---|
| 469 | p.MsoTitle, li.MsoTitle, div.MsoTitle |
|---|
| 470 | {mso-style-noshow:yes; |
|---|
| 471 | mso-style-priority:10; |
|---|
| 472 | mso-style-unhide:no; |
|---|
| 473 | mso-style-qformat:yes; |
|---|
| 474 | mso-style-link:"Title Char"; |
|---|
| 475 | mso-style-next:Normal; |
|---|
| 476 | margin-top:0in; |
|---|
| 477 | margin-right:0in; |
|---|
| 478 | margin-bottom:15.0pt; |
|---|
| 479 | margin-left:0in; |
|---|
| 480 | mso-add-space:auto; |
|---|
| 481 | mso-pagination:widow-orphan; |
|---|
| 482 | border:none; |
|---|
| 483 | mso-border-bottom-alt:solid #4F81BD 1.0pt; |
|---|
| 484 | mso-border-bottom-themecolor:accent1; |
|---|
| 485 | padding:0in; |
|---|
| 486 | mso-padding-alt:0in 0in 4.0pt 0in; |
|---|
| 487 | font-size:26.0pt; |
|---|
| 488 | font-family:"Cambria","serif"; |
|---|
| 489 | mso-ascii-font-family:Cambria; |
|---|
| 490 | mso-ascii-theme-font:major-latin; |
|---|
| 491 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 492 | mso-fareast-theme-font:major-fareast; |
|---|
| 493 | mso-hansi-font-family:Cambria; |
|---|
| 494 | mso-hansi-theme-font:major-latin; |
|---|
| 495 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 496 | mso-bidi-theme-font:major-bidi; |
|---|
| 497 | color:#17365D; |
|---|
| 498 | mso-themecolor:text2; |
|---|
| 499 | mso-themeshade:191; |
|---|
| 500 | letter-spacing:.25pt; |
|---|
| 501 | mso-font-kerning:14.0pt;} |
|---|
| 502 | p.MsoTitleCxSpFirst, li.MsoTitleCxSpFirst, div.MsoTitleCxSpFirst |
|---|
| 503 | {mso-style-noshow:yes; |
|---|
| 504 | mso-style-priority:10; |
|---|
| 505 | mso-style-unhide:no; |
|---|
| 506 | mso-style-qformat:yes; |
|---|
| 507 | mso-style-link:"Title Char"; |
|---|
| 508 | mso-style-next:Normal; |
|---|
| 509 | mso-style-type:export-only; |
|---|
| 510 | margin:0in; |
|---|
| 511 | margin-bottom:.0001pt; |
|---|
| 512 | mso-add-space:auto; |
|---|
| 513 | mso-pagination:widow-orphan; |
|---|
| 514 | border:none; |
|---|
| 515 | mso-border-bottom-alt:solid #4F81BD 1.0pt; |
|---|
| 516 | mso-border-bottom-themecolor:accent1; |
|---|
| 517 | padding:0in; |
|---|
| 518 | mso-padding-alt:0in 0in 4.0pt 0in; |
|---|
| 519 | font-size:26.0pt; |
|---|
| 520 | font-family:"Cambria","serif"; |
|---|
| 521 | mso-ascii-font-family:Cambria; |
|---|
| 522 | mso-ascii-theme-font:major-latin; |
|---|
| 523 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 524 | mso-fareast-theme-font:major-fareast; |
|---|
| 525 | mso-hansi-font-family:Cambria; |
|---|
| 526 | mso-hansi-theme-font:major-latin; |
|---|
| 527 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 528 | mso-bidi-theme-font:major-bidi; |
|---|
| 529 | color:#17365D; |
|---|
| 530 | mso-themecolor:text2; |
|---|
| 531 | mso-themeshade:191; |
|---|
| 532 | letter-spacing:.25pt; |
|---|
| 533 | mso-font-kerning:14.0pt;} |
|---|
| 534 | p.MsoTitleCxSpMiddle, li.MsoTitleCxSpMiddle, div.MsoTitleCxSpMiddle |
|---|
| 535 | {mso-style-noshow:yes; |
|---|
| 536 | mso-style-priority:10; |
|---|
| 537 | mso-style-unhide:no; |
|---|
| 538 | mso-style-qformat:yes; |
|---|
| 539 | mso-style-link:"Title Char"; |
|---|
| 540 | mso-style-next:Normal; |
|---|
| 541 | mso-style-type:export-only; |
|---|
| 542 | margin:0in; |
|---|
| 543 | margin-bottom:.0001pt; |
|---|
| 544 | mso-add-space:auto; |
|---|
| 545 | mso-pagination:widow-orphan; |
|---|
| 546 | border:none; |
|---|
| 547 | mso-border-bottom-alt:solid #4F81BD 1.0pt; |
|---|
| 548 | mso-border-bottom-themecolor:accent1; |
|---|
| 549 | padding:0in; |
|---|
| 550 | mso-padding-alt:0in 0in 4.0pt 0in; |
|---|
| 551 | font-size:26.0pt; |
|---|
| 552 | font-family:"Cambria","serif"; |
|---|
| 553 | mso-ascii-font-family:Cambria; |
|---|
| 554 | mso-ascii-theme-font:major-latin; |
|---|
| 555 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 556 | mso-fareast-theme-font:major-fareast; |
|---|
| 557 | mso-hansi-font-family:Cambria; |
|---|
| 558 | mso-hansi-theme-font:major-latin; |
|---|
| 559 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 560 | mso-bidi-theme-font:major-bidi; |
|---|
| 561 | color:#17365D; |
|---|
| 562 | mso-themecolor:text2; |
|---|
| 563 | mso-themeshade:191; |
|---|
| 564 | letter-spacing:.25pt; |
|---|
| 565 | mso-font-kerning:14.0pt;} |
|---|
| 566 | p.MsoTitleCxSpLast, li.MsoTitleCxSpLast, div.MsoTitleCxSpLast |
|---|
| 567 | {mso-style-noshow:yes; |
|---|
| 568 | mso-style-priority:10; |
|---|
| 569 | mso-style-unhide:no; |
|---|
| 570 | mso-style-qformat:yes; |
|---|
| 571 | mso-style-link:"Title Char"; |
|---|
| 572 | mso-style-next:Normal; |
|---|
| 573 | mso-style-type:export-only; |
|---|
| 574 | margin-top:0in; |
|---|
| 575 | margin-right:0in; |
|---|
| 576 | margin-bottom:15.0pt; |
|---|
| 577 | margin-left:0in; |
|---|
| 578 | mso-add-space:auto; |
|---|
| 579 | mso-pagination:widow-orphan; |
|---|
| 580 | border:none; |
|---|
| 581 | mso-border-bottom-alt:solid #4F81BD 1.0pt; |
|---|
| 582 | mso-border-bottom-themecolor:accent1; |
|---|
| 583 | padding:0in; |
|---|
| 584 | mso-padding-alt:0in 0in 4.0pt 0in; |
|---|
| 585 | font-size:26.0pt; |
|---|
| 586 | font-family:"Cambria","serif"; |
|---|
| 587 | mso-ascii-font-family:Cambria; |
|---|
| 588 | mso-ascii-theme-font:major-latin; |
|---|
| 589 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 590 | mso-fareast-theme-font:major-fareast; |
|---|
| 591 | mso-hansi-font-family:Cambria; |
|---|
| 592 | mso-hansi-theme-font:major-latin; |
|---|
| 593 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 594 | mso-bidi-theme-font:major-bidi; |
|---|
| 595 | color:#17365D; |
|---|
| 596 | mso-themecolor:text2; |
|---|
| 597 | mso-themeshade:191; |
|---|
| 598 | letter-spacing:.25pt; |
|---|
| 599 | mso-font-kerning:14.0pt;} |
|---|
| 600 | a:link, span.MsoHyperlink |
|---|
| 601 | {mso-style-priority:99; |
|---|
| 602 | color:blue; |
|---|
| 603 | text-decoration:underline; |
|---|
| 604 | text-underline:single;} |
|---|
| 605 | a:visited, span.MsoHyperlinkFollowed |
|---|
| 606 | {mso-style-noshow:yes; |
|---|
| 607 | mso-style-priority:99; |
|---|
| 608 | color:purple; |
|---|
| 609 | text-decoration:underline; |
|---|
| 610 | text-underline:single;} |
|---|
| 611 | p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap |
|---|
| 612 | {mso-style-noshow:yes; |
|---|
| 613 | mso-style-priority:99; |
|---|
| 614 | mso-style-link:"Document Map Char"; |
|---|
| 615 | margin:0in; |
|---|
| 616 | margin-bottom:.0001pt; |
|---|
| 617 | mso-pagination:widow-orphan; |
|---|
| 618 | font-size:8.0pt; |
|---|
| 619 | font-family:"Tahoma","sans-serif"; |
|---|
| 620 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 621 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 622 | p |
|---|
| 623 | {mso-style-noshow:yes; |
|---|
| 624 | mso-style-priority:99; |
|---|
| 625 | mso-margin-top-alt:auto; |
|---|
| 626 | margin-right:0in; |
|---|
| 627 | mso-margin-bottom-alt:auto; |
|---|
| 628 | margin-left:0in; |
|---|
| 629 | mso-pagination:widow-orphan; |
|---|
| 630 | font-size:12.0pt; |
|---|
| 631 | font-family:"Times New Roman","serif"; |
|---|
| 632 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 633 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 634 | pre |
|---|
| 635 | {mso-style-noshow:yes; |
|---|
| 636 | mso-style-priority:99; |
|---|
| 637 | mso-style-link:"HTML Preformatted Char"; |
|---|
| 638 | margin:0in; |
|---|
| 639 | margin-bottom:.0001pt; |
|---|
| 640 | mso-pagination:widow-orphan; |
|---|
| 641 | tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt; |
|---|
| 642 | font-size:10.0pt; |
|---|
| 643 | font-family:"Courier New"; |
|---|
| 644 | mso-fareast-font-family:"Times New Roman";} |
|---|
| 645 | p.MsoAcetate, li.MsoAcetate, div.MsoAcetate |
|---|
| 646 | {mso-style-noshow:yes; |
|---|
| 647 | mso-style-priority:99; |
|---|
| 648 | mso-style-link:"Balloon Text Char"; |
|---|
| 649 | margin:0in; |
|---|
| 650 | margin-bottom:.0001pt; |
|---|
| 651 | mso-pagination:widow-orphan; |
|---|
| 652 | font-size:8.0pt; |
|---|
| 653 | font-family:"Tahoma","sans-serif"; |
|---|
| 654 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 655 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 656 | span.MsoPlaceholderText |
|---|
| 657 | {mso-style-noshow:yes; |
|---|
| 658 | mso-style-priority:99; |
|---|
| 659 | mso-style-unhide:no; |
|---|
| 660 | color:gray;} |
|---|
| 661 | p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing |
|---|
| 662 | {mso-style-noshow:yes; |
|---|
| 663 | mso-style-priority:1; |
|---|
| 664 | mso-style-unhide:no; |
|---|
| 665 | mso-style-qformat:yes; |
|---|
| 666 | mso-style-parent:""; |
|---|
| 667 | margin:0in; |
|---|
| 668 | margin-bottom:.0001pt; |
|---|
| 669 | mso-pagination:widow-orphan; |
|---|
| 670 | font-size:12.0pt; |
|---|
| 671 | font-family:"Times New Roman","serif"; |
|---|
| 672 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 673 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 674 | p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph |
|---|
| 675 | {mso-style-noshow:yes; |
|---|
| 676 | mso-style-priority:34; |
|---|
| 677 | mso-style-unhide:no; |
|---|
| 678 | mso-style-qformat:yes; |
|---|
| 679 | margin-top:0in; |
|---|
| 680 | margin-right:0in; |
|---|
| 681 | margin-bottom:0in; |
|---|
| 682 | margin-left:.5in; |
|---|
| 683 | margin-bottom:.0001pt; |
|---|
| 684 | mso-add-space:auto; |
|---|
| 685 | mso-pagination:widow-orphan; |
|---|
| 686 | font-size:12.0pt; |
|---|
| 687 | font-family:"Times New Roman","serif"; |
|---|
| 688 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 689 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 690 | p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst |
|---|
| 691 | {mso-style-noshow:yes; |
|---|
| 692 | mso-style-priority:34; |
|---|
| 693 | mso-style-unhide:no; |
|---|
| 694 | mso-style-qformat:yes; |
|---|
| 695 | mso-style-type:export-only; |
|---|
| 696 | margin-top:0in; |
|---|
| 697 | margin-right:0in; |
|---|
| 698 | margin-bottom:0in; |
|---|
| 699 | margin-left:.5in; |
|---|
| 700 | margin-bottom:.0001pt; |
|---|
| 701 | mso-add-space:auto; |
|---|
| 702 | mso-pagination:widow-orphan; |
|---|
| 703 | font-size:12.0pt; |
|---|
| 704 | font-family:"Times New Roman","serif"; |
|---|
| 705 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 706 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 707 | p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle |
|---|
| 708 | {mso-style-noshow:yes; |
|---|
| 709 | mso-style-priority:34; |
|---|
| 710 | mso-style-unhide:no; |
|---|
| 711 | mso-style-qformat:yes; |
|---|
| 712 | mso-style-type:export-only; |
|---|
| 713 | margin-top:0in; |
|---|
| 714 | margin-right:0in; |
|---|
| 715 | margin-bottom:0in; |
|---|
| 716 | margin-left:.5in; |
|---|
| 717 | margin-bottom:.0001pt; |
|---|
| 718 | mso-add-space:auto; |
|---|
| 719 | mso-pagination:widow-orphan; |
|---|
| 720 | font-size:12.0pt; |
|---|
| 721 | font-family:"Times New Roman","serif"; |
|---|
| 722 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 723 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 724 | p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast |
|---|
| 725 | {mso-style-noshow:yes; |
|---|
| 726 | mso-style-priority:34; |
|---|
| 727 | mso-style-unhide:no; |
|---|
| 728 | mso-style-qformat:yes; |
|---|
| 729 | mso-style-type:export-only; |
|---|
| 730 | margin-top:0in; |
|---|
| 731 | margin-right:0in; |
|---|
| 732 | margin-bottom:0in; |
|---|
| 733 | margin-left:.5in; |
|---|
| 734 | margin-bottom:.0001pt; |
|---|
| 735 | mso-add-space:auto; |
|---|
| 736 | mso-pagination:widow-orphan; |
|---|
| 737 | font-size:12.0pt; |
|---|
| 738 | font-family:"Times New Roman","serif"; |
|---|
| 739 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 740 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 741 | span.MsoIntenseReference |
|---|
| 742 | {mso-style-priority:32; |
|---|
| 743 | mso-style-unhide:no; |
|---|
| 744 | mso-style-qformat:yes; |
|---|
| 745 | font-variant:small-caps; |
|---|
| 746 | color:#C0504D; |
|---|
| 747 | mso-themecolor:accent2; |
|---|
| 748 | letter-spacing:.25pt; |
|---|
| 749 | font-weight:bold; |
|---|
| 750 | text-decoration:underline; |
|---|
| 751 | text-underline:single;} |
|---|
| 752 | span.Heading1Char |
|---|
| 753 | {mso-style-name:"Heading 1 Char"; |
|---|
| 754 | mso-style-priority:9; |
|---|
| 755 | mso-style-unhide:no; |
|---|
| 756 | mso-style-locked:yes; |
|---|
| 757 | mso-style-link:"Heading 1"; |
|---|
| 758 | mso-ansi-font-size:24.0pt; |
|---|
| 759 | mso-bidi-font-size:24.0pt; |
|---|
| 760 | font-family:"Times New Roman","serif"; |
|---|
| 761 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 762 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 763 | mso-fareast-theme-font:minor-fareast; |
|---|
| 764 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 765 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 766 | mso-font-kerning:18.0pt; |
|---|
| 767 | font-weight:bold;} |
|---|
| 768 | span.Heading2Char |
|---|
| 769 | {mso-style-name:"Heading 2 Char"; |
|---|
| 770 | mso-style-noshow:yes; |
|---|
| 771 | mso-style-priority:9; |
|---|
| 772 | mso-style-unhide:no; |
|---|
| 773 | mso-style-locked:yes; |
|---|
| 774 | mso-style-link:"Heading 2"; |
|---|
| 775 | mso-ansi-font-size:18.0pt; |
|---|
| 776 | mso-bidi-font-size:18.0pt; |
|---|
| 777 | font-family:"Times New Roman","serif"; |
|---|
| 778 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 779 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 780 | mso-fareast-theme-font:minor-fareast; |
|---|
| 781 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 782 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 783 | font-weight:bold;} |
|---|
| 784 | span.Heading3Char |
|---|
| 785 | {mso-style-name:"Heading 3 Char"; |
|---|
| 786 | mso-style-noshow:yes; |
|---|
| 787 | mso-style-priority:9; |
|---|
| 788 | mso-style-unhide:no; |
|---|
| 789 | mso-style-locked:yes; |
|---|
| 790 | mso-style-link:"Heading 3"; |
|---|
| 791 | mso-ansi-font-size:13.5pt; |
|---|
| 792 | mso-bidi-font-size:13.5pt; |
|---|
| 793 | font-family:"Times New Roman","serif"; |
|---|
| 794 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 795 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 796 | mso-fareast-theme-font:minor-fareast; |
|---|
| 797 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 798 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 799 | font-weight:bold;} |
|---|
| 800 | span.Heading4Char |
|---|
| 801 | {mso-style-name:"Heading 4 Char"; |
|---|
| 802 | mso-style-noshow:yes; |
|---|
| 803 | mso-style-priority:9; |
|---|
| 804 | mso-style-unhide:no; |
|---|
| 805 | mso-style-locked:yes; |
|---|
| 806 | mso-style-link:"Heading 4"; |
|---|
| 807 | mso-ansi-font-size:13.0pt; |
|---|
| 808 | mso-bidi-font-size:13.0pt; |
|---|
| 809 | font-family:"Cambria","serif"; |
|---|
| 810 | mso-ascii-font-family:Cambria; |
|---|
| 811 | mso-ascii-theme-font:major-latin; |
|---|
| 812 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 813 | mso-fareast-theme-font:major-fareast; |
|---|
| 814 | mso-hansi-font-family:Cambria; |
|---|
| 815 | mso-hansi-theme-font:major-latin; |
|---|
| 816 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 817 | mso-bidi-theme-font:major-bidi; |
|---|
| 818 | color:#4F81BD; |
|---|
| 819 | mso-themecolor:accent1; |
|---|
| 820 | font-weight:bold; |
|---|
| 821 | font-style:italic;} |
|---|
| 822 | span.Heading5Char |
|---|
| 823 | {mso-style-name:"Heading 5 Char"; |
|---|
| 824 | mso-style-noshow:yes; |
|---|
| 825 | mso-style-priority:9; |
|---|
| 826 | mso-style-unhide:no; |
|---|
| 827 | mso-style-locked:yes; |
|---|
| 828 | mso-style-link:"Heading 5"; |
|---|
| 829 | mso-ansi-font-size:12.0pt; |
|---|
| 830 | mso-bidi-font-size:12.0pt; |
|---|
| 831 | font-family:"Times New Roman","serif"; |
|---|
| 832 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 833 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 834 | mso-fareast-theme-font:minor-fareast; |
|---|
| 835 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 836 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 837 | color:#4F4FFF; |
|---|
| 838 | font-weight:bold;} |
|---|
| 839 | span.HTMLPreformattedChar |
|---|
| 840 | {mso-style-name:"HTML Preformatted Char"; |
|---|
| 841 | mso-style-noshow:yes; |
|---|
| 842 | mso-style-priority:99; |
|---|
| 843 | mso-style-unhide:no; |
|---|
| 844 | mso-style-locked:yes; |
|---|
| 845 | mso-style-link:"HTML Preformatted"; |
|---|
| 846 | font-family:"Courier New"; |
|---|
| 847 | mso-ascii-font-family:"Courier New"; |
|---|
| 848 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 849 | mso-hansi-font-family:"Courier New"; |
|---|
| 850 | mso-bidi-font-family:"Courier New";} |
|---|
| 851 | span.TitleChar |
|---|
| 852 | {mso-style-name:"Title Char"; |
|---|
| 853 | mso-style-priority:10; |
|---|
| 854 | mso-style-unhide:no; |
|---|
| 855 | mso-style-locked:yes; |
|---|
| 856 | mso-style-link:Title; |
|---|
| 857 | mso-ansi-font-size:26.0pt; |
|---|
| 858 | mso-bidi-font-size:26.0pt; |
|---|
| 859 | font-family:"Cambria","serif"; |
|---|
| 860 | mso-ascii-font-family:Cambria; |
|---|
| 861 | mso-ascii-theme-font:major-latin; |
|---|
| 862 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 863 | mso-fareast-theme-font:major-fareast; |
|---|
| 864 | mso-hansi-font-family:Cambria; |
|---|
| 865 | mso-hansi-theme-font:major-latin; |
|---|
| 866 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 867 | mso-bidi-theme-font:major-bidi; |
|---|
| 868 | color:#17365D; |
|---|
| 869 | mso-themecolor:text2; |
|---|
| 870 | mso-themeshade:191; |
|---|
| 871 | letter-spacing:.25pt; |
|---|
| 872 | mso-font-kerning:14.0pt;} |
|---|
| 873 | span.DocumentMapChar |
|---|
| 874 | {mso-style-name:"Document Map Char"; |
|---|
| 875 | mso-style-noshow:yes; |
|---|
| 876 | mso-style-priority:99; |
|---|
| 877 | mso-style-unhide:no; |
|---|
| 878 | mso-style-locked:yes; |
|---|
| 879 | mso-style-link:"Document Map"; |
|---|
| 880 | mso-ansi-font-size:8.0pt; |
|---|
| 881 | mso-bidi-font-size:8.0pt; |
|---|
| 882 | font-family:"Tahoma","sans-serif"; |
|---|
| 883 | mso-ascii-font-family:Tahoma; |
|---|
| 884 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 885 | mso-fareast-theme-font:minor-fareast; |
|---|
| 886 | mso-hansi-font-family:Tahoma; |
|---|
| 887 | mso-bidi-font-family:Tahoma;} |
|---|
| 888 | span.BalloonTextChar |
|---|
| 889 | {mso-style-name:"Balloon Text Char"; |
|---|
| 890 | mso-style-noshow:yes; |
|---|
| 891 | mso-style-priority:99; |
|---|
| 892 | mso-style-unhide:no; |
|---|
| 893 | mso-style-locked:yes; |
|---|
| 894 | mso-style-link:"Balloon Text"; |
|---|
| 895 | mso-ansi-font-size:8.0pt; |
|---|
| 896 | mso-bidi-font-size:8.0pt; |
|---|
| 897 | font-family:"Tahoma","sans-serif"; |
|---|
| 898 | mso-ascii-font-family:Tahoma; |
|---|
| 899 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 900 | mso-fareast-theme-font:minor-fareast; |
|---|
| 901 | mso-hansi-font-family:Tahoma; |
|---|
| 902 | mso-bidi-font-family:Tahoma;} |
|---|
| 903 | span.SpellE |
|---|
| 904 | {mso-style-name:""; |
|---|
| 905 | mso-spl-e:yes;} |
|---|
| 906 | span.GramE |
|---|
| 907 | {mso-style-name:""; |
|---|
| 908 | mso-gram-e:yes;} |
|---|
| 909 | .MsoChpDefault |
|---|
| 910 | {mso-style-type:export-only; |
|---|
| 911 | mso-default-props:yes; |
|---|
| 912 | font-size:10.0pt; |
|---|
| 913 | mso-ansi-font-size:10.0pt; |
|---|
| 914 | mso-bidi-font-size:10.0pt; |
|---|
| 915 | font-family:"Calibri","sans-serif"; |
|---|
| 916 | mso-ascii-font-family:Calibri; |
|---|
| 917 | mso-ascii-theme-font:minor-latin; |
|---|
| 918 | mso-fareast-font-family:Calibri; |
|---|
| 919 | mso-fareast-theme-font:minor-latin; |
|---|
| 920 | mso-hansi-font-family:Calibri; |
|---|
| 921 | mso-hansi-theme-font:minor-latin; |
|---|
| 922 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 923 | mso-bidi-theme-font:minor-bidi;} |
|---|
| 924 | @page WordSection1 |
|---|
| 925 | {size:8.5in 11.0in; |
|---|
| 926 | margin:1.0in 1.0in 1.0in 1.0in; |
|---|
| 927 | mso-header-margin:.5in; |
|---|
| 928 | mso-footer-margin:.5in; |
|---|
| 929 | mso-paper-source:0;} |
|---|
| 930 | div.WordSection1 |
|---|
| 931 | {page:WordSection1;} |
|---|
| 932 | /* List Definitions */ |
|---|
| 933 | @list l0 |
|---|
| 934 | {mso-list-id:608973138; |
|---|
| 935 | mso-list-type:hybrid; |
|---|
| 936 | mso-list-template-ids:-1449999034 67698703 67698713 67698715 67698703 67698713 67698715 67698703 67698713 67698715;} |
|---|
| 937 | @list l0:level1 |
|---|
| 938 | {mso-level-tab-stop:none; |
|---|
| 939 | mso-level-number-position:left; |
|---|
| 940 | text-indent:-.25in;} |
|---|
| 941 | @list l0:level2 |
|---|
| 942 | {mso-level-number-format:alpha-lower; |
|---|
| 943 | mso-level-tab-stop:none; |
|---|
| 944 | mso-level-number-position:left; |
|---|
| 945 | text-indent:-.25in;} |
|---|
| 946 | @list l0:level3 |
|---|
| 947 | {mso-level-number-format:roman-lower; |
|---|
| 948 | mso-level-tab-stop:none; |
|---|
| 949 | mso-level-number-position:right; |
|---|
| 950 | text-indent:-9.0pt;} |
|---|
| 951 | @list l0:level4 |
|---|
| 952 | {mso-level-tab-stop:none; |
|---|
| 953 | mso-level-number-position:left; |
|---|
| 954 | text-indent:-.25in;} |
|---|
| 955 | @list l0:level5 |
|---|
| 956 | {mso-level-number-format:alpha-lower; |
|---|
| 957 | mso-level-tab-stop:none; |
|---|
| 958 | mso-level-number-position:left; |
|---|
| 959 | text-indent:-.25in;} |
|---|
| 960 | @list l0:level6 |
|---|
| 961 | {mso-level-number-format:roman-lower; |
|---|
| 962 | mso-level-tab-stop:none; |
|---|
| 963 | mso-level-number-position:right; |
|---|
| 964 | text-indent:-9.0pt;} |
|---|
| 965 | @list l0:level7 |
|---|
| 966 | {mso-level-tab-stop:none; |
|---|
| 967 | mso-level-number-position:left; |
|---|
| 968 | text-indent:-.25in;} |
|---|
| 969 | @list l0:level8 |
|---|
| 970 | {mso-level-number-format:alpha-lower; |
|---|
| 971 | mso-level-tab-stop:none; |
|---|
| 972 | mso-level-number-position:left; |
|---|
| 973 | text-indent:-.25in;} |
|---|
| 974 | @list l0:level9 |
|---|
| 975 | {mso-level-number-format:roman-lower; |
|---|
| 976 | mso-level-tab-stop:none; |
|---|
| 977 | mso-level-number-position:right; |
|---|
| 978 | text-indent:-9.0pt;} |
|---|
| 979 | @list l1 |
|---|
| 980 | {mso-list-id:894583186; |
|---|
| 981 | mso-list-type:hybrid; |
|---|
| 982 | mso-list-template-ids:1821937756 67698703 67698713 67698715 67698703 67698713 67698715 67698703 67698713 67698715;} |
|---|
| 983 | @list l1:level1 |
|---|
| 984 | {mso-level-tab-stop:none; |
|---|
| 985 | mso-level-number-position:left; |
|---|
| 986 | margin-left:39.0pt; |
|---|
| 987 | text-indent:-.25in;} |
|---|
| 988 | @list l1:level2 |
|---|
| 989 | {mso-level-number-format:alpha-lower; |
|---|
| 990 | mso-level-tab-stop:none; |
|---|
| 991 | mso-level-number-position:left; |
|---|
| 992 | margin-left:75.0pt; |
|---|
| 993 | text-indent:-.25in;} |
|---|
| 994 | @list l1:level3 |
|---|
| 995 | {mso-level-number-format:roman-lower; |
|---|
| 996 | mso-level-tab-stop:none; |
|---|
| 997 | mso-level-number-position:right; |
|---|
| 998 | margin-left:111.0pt; |
|---|
| 999 | text-indent:-9.0pt;} |
|---|
| 1000 | @list l1:level4 |
|---|
| 1001 | {mso-level-tab-stop:none; |
|---|
| 1002 | mso-level-number-position:left; |
|---|
| 1003 | margin-left:147.0pt; |
|---|
| 1004 | text-indent:-.25in;} |
|---|
| 1005 | @list l1:level5 |
|---|
| 1006 | {mso-level-number-format:alpha-lower; |
|---|
| 1007 | mso-level-tab-stop:none; |
|---|
| 1008 | mso-level-number-position:left; |
|---|
| 1009 | margin-left:183.0pt; |
|---|
| 1010 | text-indent:-.25in;} |
|---|
| 1011 | @list l1:level6 |
|---|
| 1012 | {mso-level-number-format:roman-lower; |
|---|
| 1013 | mso-level-tab-stop:none; |
|---|
| 1014 | mso-level-number-position:right; |
|---|
| 1015 | margin-left:219.0pt; |
|---|
| 1016 | text-indent:-9.0pt;} |
|---|
| 1017 | @list l1:level7 |
|---|
| 1018 | {mso-level-tab-stop:none; |
|---|
| 1019 | mso-level-number-position:left; |
|---|
| 1020 | margin-left:255.0pt; |
|---|
| 1021 | text-indent:-.25in;} |
|---|
| 1022 | @list l1:level8 |
|---|
| 1023 | {mso-level-number-format:alpha-lower; |
|---|
| 1024 | mso-level-tab-stop:none; |
|---|
| 1025 | mso-level-number-position:left; |
|---|
| 1026 | margin-left:291.0pt; |
|---|
| 1027 | text-indent:-.25in;} |
|---|
| 1028 | @list l1:level9 |
|---|
| 1029 | {mso-level-number-format:roman-lower; |
|---|
| 1030 | mso-level-tab-stop:none; |
|---|
| 1031 | mso-level-number-position:right; |
|---|
| 1032 | margin-left:327.0pt; |
|---|
| 1033 | text-indent:-9.0pt;} |
|---|
| 1034 | @list l2 |
|---|
| 1035 | {mso-list-id:983856491; |
|---|
| 1036 | mso-list-type:hybrid; |
|---|
| 1037 | mso-list-template-ids:-44896332 67698703 67698713 461011134 67698703 67698713 67698715 67698703 67698713 67698715;} |
|---|
| 1038 | @list l2:level1 |
|---|
| 1039 | {mso-level-tab-stop:none; |
|---|
| 1040 | mso-level-number-position:left; |
|---|
| 1041 | text-indent:-.25in;} |
|---|
| 1042 | @list l2:level2 |
|---|
| 1043 | {mso-level-number-format:alpha-lower; |
|---|
| 1044 | mso-level-tab-stop:none; |
|---|
| 1045 | mso-level-number-position:left; |
|---|
| 1046 | text-indent:-.25in;} |
|---|
| 1047 | @list l2:level3 |
|---|
| 1048 | {mso-level-start-at:0; |
|---|
| 1049 | mso-level-number-format:bullet; |
|---|
| 1050 | mso-level-text:\F0B7; |
|---|
| 1051 | mso-level-tab-stop:none; |
|---|
| 1052 | mso-level-number-position:left; |
|---|
| 1053 | margin-left:117.0pt; |
|---|
| 1054 | text-indent:-.25in; |
|---|
| 1055 | font-family:Symbol; |
|---|
| 1056 | mso-fareast-font-family:"Times New Roman"; |
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| 1057 | mso-fareast-theme-font:minor-fareast; |
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| 1058 | mso-bidi-font-family:"Times New Roman";} |
|---|
| 1059 | @list l2:level4 |
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| 1060 | {mso-level-tab-stop:none; |
|---|
| 1061 | mso-level-number-position:left; |
|---|
| 1062 | text-indent:-.25in;} |
|---|
| 1063 | @list l2:level5 |
|---|
| 1064 | {mso-level-number-format:alpha-lower; |
|---|
| 1065 | mso-level-tab-stop:none; |
|---|
| 1066 | mso-level-number-position:left; |
|---|
| 1067 | text-indent:-.25in;} |
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| 1068 | @list l2:level6 |
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| 1069 | {mso-level-number-format:roman-lower; |
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| 1070 | mso-level-tab-stop:none; |
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| 1071 | mso-level-number-position:right; |
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| 1072 | text-indent:-9.0pt;} |
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| 1073 | @list l2:level7 |
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| 1074 | {mso-level-tab-stop:none; |
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| 1075 | mso-level-number-position:left; |
|---|
| 1076 | text-indent:-.25in;} |
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| 1077 | @list l2:level8 |
|---|
| 1078 | {mso-level-number-format:alpha-lower; |
|---|
| 1079 | mso-level-tab-stop:none; |
|---|
| 1080 | mso-level-number-position:left; |
|---|
| 1081 | text-indent:-.25in;} |
|---|
| 1082 | @list l2:level9 |
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| 1083 | {mso-level-number-format:roman-lower; |
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| 1084 | mso-level-tab-stop:none; |
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| 1085 | mso-level-number-position:right; |
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| 1086 | text-indent:-9.0pt;} |
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| 1087 | ol |
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| 1088 | {margin-bottom:0in;} |
|---|
| 1089 | ul |
|---|
| 1090 | {margin-bottom:0in;} |
|---|
| 1091 | --> |
|---|
| 1092 | </style> |
|---|
| 1093 | <!--[if gte mso 10]> |
|---|
| 1094 | <style> |
|---|
| 1095 | /* Style Definitions */ |
|---|
| 1096 | table.MsoNormalTable |
|---|
| 1097 | {mso-style-name:"Table Normal"; |
|---|
| 1098 | mso-tstyle-rowband-size:0; |
|---|
| 1099 | mso-tstyle-colband-size:0; |
|---|
| 1100 | mso-style-noshow:yes; |
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| 1101 | mso-style-priority:99; |
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| 1102 | mso-style-parent:""; |
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| 1103 | mso-padding-alt:0in 5.4pt 0in 5.4pt; |
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| 1107 | font-size:10.0pt; |
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| 1108 | font-family:"Calibri","sans-serif"; |
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| 1109 | mso-ascii-font-family:Calibri; |
|---|
| 1110 | mso-ascii-theme-font:minor-latin; |
|---|
| 1111 | mso-hansi-font-family:Calibri; |
|---|
| 1112 | mso-hansi-theme-font:minor-latin; |
|---|
| 1113 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 1114 | mso-bidi-theme-font:minor-bidi;} |
|---|
| 1115 | </style> |
|---|
| 1116 | <![endif]--><!--[if gte mso 9]><xml> |
|---|
| 1117 | <o:shapedefaults v:ext="edit" spidmax="1027"/> |
|---|
| 1118 | </xml><![endif]--><!--[if gte mso 9]><xml> |
|---|
| 1119 | <o:shapelayout v:ext="edit"> |
|---|
| 1120 | <o:idmap v:ext="edit" data="1"/> |
|---|
| 1121 | </o:shapelayout></xml><![endif]--> |
|---|
| 1122 | </head> |
|---|
| 1123 | |
|---|
| 1124 | <body lang=EN-US link=blue vlink=purple style='tab-interval:.5in'> |
|---|
| 1125 | |
|---|
| 1126 | <div class=WordSection1> |
|---|
| 1127 | |
|---|
| 1128 | <h1>Fit Peaks/<span class=SpellE>Autoindexing</span> in GSAS-II </h1> |
|---|
| 1129 | |
|---|
| 1130 | <p class=MsoNormal>In this exercise you will use GSAS-II to search for a unit |
|---|
| 1131 | cell that matches a set of diffraction peaks -- a process known as |
|---|
| 1132 | auto-indexing. First peaks must be located and optimized and then indexing can |
|---|
| 1133 | be done.</p> |
|---|
| 1134 | |
|---|
| 1135 | <p class=MsoNormal>If you have not done so already, <a |
|---|
| 1136 | href="Starting%20GSAS.htm">start GSAS-II</a>.</p> |
|---|
| 1137 | |
|---|
| 1138 | <h2>Step 1: read in the data file</h2> |
|---|
| 1139 | |
|---|
| 1140 | <p class=MsoListParagraphCxSpFirst style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span |
|---|
| 1141 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span |
|---|
| 1142 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Use |
|---|
| 1143 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1144 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1145 | minor-latin'>Import/Powder Data/from GSAS file</span></b> menu item to read the |
|---|
| 1146 | data file into the current GSAS-II project. This read option is set to read any |
|---|
| 1147 | of the powder data formats (except neutron TOF time map files) defined for GSAS |
|---|
| 1148 | (angles in <span class=SpellE>centidegrees</span>). Other submenu items will |
|---|
| 1149 | read the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
|---|
| 1150 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1151 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>cif</span></b></span> |
|---|
| 1152 | format or the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
|---|
| 1153 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1154 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>xye</span></b></span> |
|---|
| 1155 | format (angles in degrees) used by <span class=SpellE>Topas</span>, etc.<span |
|---|
| 1156 | style='mso-spacerun:yes'> </span>Change the file directory to <b |
|---|
| 1157 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1158 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1159 | minor-latin'>Exercises/LaB6</span></b><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1160 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1161 | minor-latin'> to find the file; you may need to change the file type to <b |
|---|
| 1162 | style='mso-bidi-font-weight:normal'>All files (*.*)</b> to find the desired |
|---|
| 1163 | file.</span></p> |
|---|
| 1164 | |
|---|
| 1165 | <p class=MsoListParagraphCxSpMiddle style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span |
|---|
| 1166 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span |
|---|
| 1167 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Select |
|---|
| 1168 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1169 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1170 | minor-latin'>11bmb_3844.fxye</span></b><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1171 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1172 | minor-latin'> data</span> file in the first dialog and press <b |
|---|
| 1173 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1174 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1175 | minor-latin'>Open</span></b>. There will be a Dialog box asking <span |
|---|
| 1176 | class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1177 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1178 | minor-latin;mso-bidi-theme-font:minor-latin'>Is</span></b></span><b |
|---|
| 1179 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1180 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1181 | minor-latin'> this the file you want?</span></b> Press <span class=GramE><b |
|---|
| 1182 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1183 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1184 | minor-latin'>Yes</span></b></span> button to proceed.</p> |
|---|
| 1185 | |
|---|
| 1186 | <p class=MsoListParagraphCxSpLast style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span |
|---|
| 1187 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>3.<span |
|---|
| 1188 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>The |
|---|
| 1189 | file <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1190 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1191 | minor-latin'>11bmb_3844.prm</span></b> instrument parameter file is |
|---|
| 1192 | automatically selected; it was produced by 11BM-B instrument processing |
|---|
| 1193 | software when the corresponding <span class=SpellE><b style='mso-bidi-font-weight: |
|---|
| 1194 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1195 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>fxye</span></b></span> |
|---|
| 1196 | file was created from the 12 detector raw data. If absent or the name doesnt |
|---|
| 1197 | match the data file name, a file dialog will appear for you to select the |
|---|
| 1198 | correct instrument parameter file.</p> |
|---|
| 1199 | |
|---|
| 1200 | <p class=MsoNormal>At this point the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1201 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1202 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data |
|---|
| 1203 | tree</span></b> window will have several entries </p> |
|---|
| 1204 | |
|---|
| 1205 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype |
|---|
| 1206 | id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t" |
|---|
| 1207 | path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f"> |
|---|
| 1208 | <v:stroke joinstyle="miter"/> |
|---|
| 1209 | <v:formulas> |
|---|
| 1210 | <v:f eqn="if lineDrawn pixelLineWidth 0"/> |
|---|
| 1211 | <v:f eqn="sum @0 1 0"/> |
|---|
| 1212 | <v:f eqn="sum 0 0 @1"/> |
|---|
| 1213 | <v:f eqn="prod @2 1 2"/> |
|---|
| 1214 | <v:f eqn="prod @3 21600 pixelWidth"/> |
|---|
| 1215 | <v:f eqn="prod @3 21600 pixelHeight"/> |
|---|
| 1216 | <v:f eqn="sum @0 0 1"/> |
|---|
| 1217 | <v:f eqn="prod @6 1 2"/> |
|---|
| 1218 | <v:f eqn="prod @7 21600 pixelWidth"/> |
|---|
| 1219 | <v:f eqn="sum @8 21600 0"/> |
|---|
| 1220 | <v:f eqn="prod @7 21600 pixelHeight"/> |
|---|
| 1221 | <v:f eqn="sum @10 21600 0"/> |
|---|
| 1222 | </v:formulas> |
|---|
| 1223 | <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> |
|---|
| 1224 | <o:lock v:ext="edit" aspectratio="t"/> |
|---|
| 1225 | </v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1046" type="#_x0000_t75" |
|---|
| 1226 | style='width:225pt;height:187.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1227 | <v:imagedata src="Fit%20Peaks_files/image001.png" o:title=""/> |
|---|
| 1228 | </v:shape><![endif]--><![if !vml]><img border=0 width=300 height=250 |
|---|
| 1229 | src="Fit%20Peaks_files/image001.png" v:shapes="Picture_x0020_1"><![endif]></span></p> |
|---|
| 1230 | |
|---|
| 1231 | <p class=MsoNormal><span class=GramE>and</span> the plot window will show the |
|---|
| 1232 | powder pattern</p> |
|---|
| 1233 | |
|---|
| 1234 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1235 | id="Picture_x0020_2" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:525pt; |
|---|
| 1236 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1237 | <v:imagedata src="Fit%20Peaks_files/image002.png" o:title=""/> |
|---|
| 1238 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1239 | src="Fit%20Peaks_files/image002.png" v:shapes="Picture_x0020_2"><![endif]></span></p> |
|---|
| 1240 | |
|---|
| 1241 | <h2>Step 2: Select Limits </h2> |
|---|
| 1242 | |
|---|
| 1243 | <p class=MsoNormal><span style='mso-spacerun:yes'> </span>This pattern has much |
|---|
| 1244 | more data than we need, so it is helpful to cut down the range. Click on the <b |
|---|
| 1245 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1246 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1247 | minor-latin'>Limits</span></b> item in the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1248 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1249 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data |
|---|
| 1250 | tree</span></b>. The small window is repainted. Use the <b style='mso-bidi-font-weight: |
|---|
| 1251 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1252 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>changed</span></b> |
|---|
| 1253 | row of entry boxes to set <span class=SpellE><b style='mso-bidi-font-weight: |
|---|
| 1254 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1255 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmin</span></b></span> |
|---|
| 1256 | and <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
|---|
| 1257 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1258 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmax</span></b></span> |
|---|
| 1259 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1260 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1261 | minor-latin'>4</span></b> and <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1262 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1263 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>27.5</span></b>. |
|---|
| 1264 | Notice on the plot that the limit lines have moved to these positions; the |
|---|
| 1265 | green lower limit is just below the 1<sup>st</sup> peak and the red upper limit |
|---|
| 1266 | is in a wide gap between peaks. You may also drag the limit lines to the |
|---|
| 1267 | desired location or place them by a left mouse click on a data point for the |
|---|
| 1268 | lower limit or a right click on a data point for the upper limit.</p> |
|---|
| 1269 | |
|---|
| 1270 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1271 | id="Picture_x0020_3" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:225pt; |
|---|
| 1272 | height:120pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1273 | <v:imagedata src="Fit%20Peaks_files/image003.png" o:title=""/> |
|---|
| 1274 | </v:shape><![endif]--><![if !vml]><img border=0 width=300 height=160 |
|---|
| 1275 | src="Fit%20Peaks_files/image003.png" v:shapes="Picture_x0020_3"><![endif]></span></p> |
|---|
| 1276 | |
|---|
| 1277 | <h2>Step 3: Determine Peak Positions</h2> |
|---|
| 1278 | |
|---|
| 1279 | <p class=MsoListParagraphCxSpFirst style='margin-left:39.0pt;mso-add-space: |
|---|
| 1280 | auto;text-indent:-.25in;mso-list:l1 level1 lfo4'><![if !supportLists]><span |
|---|
| 1281 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span |
|---|
| 1282 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Click |
|---|
| 1283 | on the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1284 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1285 | minor-latin'>Peak List</span></b> item in the <b style='mso-bidi-font-weight: |
|---|
| 1286 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1287 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II |
|---|
| 1288 | data tree</span></b>. This creates an empty window of peak positions (the <b |
|---|
| 1289 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1290 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1291 | minor-latin'>Limits</span></b> window is erased). At this point it is wise <span |
|---|
| 1292 | class=GramE>to<span style='mso-spacerun:yes'> </span>zoom</span> in on the |
|---|
| 1293 | data that will be used for indexing. </p> |
|---|
| 1294 | |
|---|
| 1295 | <p class=MsoListParagraphCxSpMiddle style='margin-left:39.0pt;mso-add-space: |
|---|
| 1296 | auto;text-indent:-.25in;mso-list:l1 level1 lfo4'><![if !supportLists]><span |
|---|
| 1297 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span |
|---|
| 1298 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Click |
|---|
| 1299 | on the Zoom button, <span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1300 | id="Picture_x0020_4" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:21.75pt; |
|---|
| 1301 | height:18.75pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1302 | <v:imagedata src="Fit%20Peaks_files/image004.jpg" o:title="" croptop="1f" |
|---|
| 1303 | cropbottom="-1f" cropleft="35827f" cropright="19224f"/> |
|---|
| 1304 | </v:shape><![endif]--><![if !vml]><img border=0 width=29 height=25 |
|---|
| 1305 | src="Fit%20Peaks_files/image005.jpg" v:shapes="Picture_x0020_4"><![endif]></span>, |
|---|
| 1306 | then press the left mouse in one corner of the region to be used; holding the |
|---|
| 1307 | mouse button down, drag over the region to the opposite corner; a box will be |
|---|
| 1308 | drawn over the region to be zoomed. </p> |
|---|
| 1309 | |
|---|
| 1310 | <p class=MsoListParagraphCxSpMiddle style='margin-left:39.0pt;mso-add-space: |
|---|
| 1311 | auto;text-indent:-.25in;mso-list:l1 level1 lfo4'><![if !supportLists]><span |
|---|
| 1312 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>3.<span |
|---|
| 1313 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]><b |
|---|
| 1314 | style='mso-bidi-font-weight:normal'>Important</b>: Click on the Zoom <span |
|---|
| 1315 | style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_5" |
|---|
| 1316 | o:spid="_x0000_i1042" type="#_x0000_t75" style='width:23.25pt;height:20.25pt; |
|---|
| 1317 | visibility:visible;mso-wrap-style:square'> |
|---|
| 1318 | <v:imagedata src="Fit%20Peaks_files/image004.jpg" o:title="" croptop="1f" |
|---|
| 1319 | cropbottom="-1f" cropleft="35827f" cropright="19224f"/> |
|---|
| 1320 | </v:shape><![endif]--><![if !vml]><img border=0 width=31 height=27 |
|---|
| 1321 | src="Fit%20Peaks_files/image006.jpg" v:shapes="Picture_x0020_5"><![endif]></span><span |
|---|
| 1322 | style='mso-spacerun:yes'> </span>button again to turn off the zoom mode. </p> |
|---|
| 1323 | |
|---|
| 1324 | <p class=MsoListParagraphCxSpMiddle style='margin-left:39.0pt;mso-add-space: |
|---|
| 1325 | auto;text-indent:-.25in;mso-list:l1 level1 lfo4'><![if !supportLists]><span |
|---|
| 1326 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>4.<span |
|---|
| 1327 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Using |
|---|
| 1328 | the left mouse button, click on a data point near the top of each peak to be |
|---|
| 1329 | added to the peak list. It is usually best to start at the upper end of the |
|---|
| 1330 | pattern as the next peak to pick isnt obscured by the tool tip. As this is |
|---|
| 1331 | done, a vertical blue line is drawn in the plot window<span |
|---|
| 1332 | style='mso-spacerun:yes'> </span>for each peak selected</p> |
|---|
| 1333 | |
|---|
| 1334 | <p class=MsoListParagraphCxSpMiddle style='margin-left:39.0pt;mso-add-space: |
|---|
| 1335 | auto'><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_6" |
|---|
| 1336 | o:spid="_x0000_i1041" type="#_x0000_t75" style='width:525pt;height:450pt; |
|---|
| 1337 | visibility:visible;mso-wrap-style:square'> |
|---|
| 1338 | <v:imagedata src="Fit%20Peaks_files/image007.png" o:title=""/> |
|---|
| 1339 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1340 | src="Fit%20Peaks_files/image007.png" v:shapes="Picture_x0020_6"><![endif]></span></p> |
|---|
| 1341 | |
|---|
| 1342 | <p class=MsoListParagraphCxSpMiddle style='margin-left:39.0pt;mso-add-space: |
|---|
| 1343 | auto'><span class=GramE>and</span> peaks are added to the <b style='mso-bidi-font-weight: |
|---|
| 1344 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1345 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak |
|---|
| 1346 | List</span></b> window in order of increasing 2<span style='font-family:Symbol'>Q</span>.</p> |
|---|
| 1347 | |
|---|
| 1348 | <p class=MsoListParagraphCxSpMiddle style='margin-left:39.0pt;mso-add-space: |
|---|
| 1349 | auto'><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_7" |
|---|
| 1350 | o:spid="_x0000_i1040" type="#_x0000_t75" style='width:401.25pt;height:262.5pt; |
|---|
| 1351 | visibility:visible;mso-wrap-style:square'> |
|---|
| 1352 | <v:imagedata src="Fit%20Peaks_files/image008.png" o:title=""/> |
|---|
| 1353 | </v:shape><![endif]--><![if !vml]><img border=0 width=535 height=350 |
|---|
| 1354 | src="Fit%20Peaks_files/image008.png" v:shapes="Picture_x0020_7"><![endif]></span></p> |
|---|
| 1355 | |
|---|
| 1356 | <p class=MsoListParagraphCxSpMiddle style='margin-left:39.0pt;mso-add-space: |
|---|
| 1357 | auto'>Note that if peaks are not being added, you probably have not exited zoom |
|---|
| 1358 | mode.</p> |
|---|
| 1359 | |
|---|
| 1360 | <p class=MsoListParagraphCxSpLast style='margin-left:39.0pt;mso-add-space:auto'>Add |
|---|
| 1361 | approximately 20-25 peaks total to the peak list (there will be 20 in this |
|---|
| 1362 | example). Be sure to add the lowest angle peaks that are visible in the plot. |
|---|
| 1363 | You may drag a peak position as needed; be sure the zoom/shift buttons are off. |
|---|
| 1364 | A position may be deleted with a right click with the mouse on the blue line.</p> |
|---|
| 1365 | |
|---|
| 1366 | <h2>Step 4: Refine Peak Positions</h2> |
|---|
| 1367 | |
|---|
| 1368 | <p class=MsoNormal>This refinement proceeds stepwise; first doing the default |
|---|
| 1369 | refinement and then adding <span class=GramE>a parameters</span> to complete |
|---|
| 1370 | the fitting,</p> |
|---|
| 1371 | |
|---|
| 1372 | <p class=MsoListParagraphCxSpFirst style='text-indent:-.25in;mso-list:l2 level1 lfo6'><![if !supportLists]><span |
|---|
| 1373 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span |
|---|
| 1374 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Refine |
|---|
| 1375 | the peak intensities and the background. These parameters have their refinement |
|---|
| 1376 | flags turned on by default. Use the menu item <b style='mso-bidi-font-weight: |
|---|
| 1377 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1378 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak |
|---|
| 1379 | Fitting/LSQ <span class=SpellE>PeakFit</span> </span></b>on the<b |
|---|
| 1380 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1381 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1382 | minor-latin'> Peak List </span></b>window. Do <b style='mso-bidi-font-weight: |
|---|
| 1383 | normal'>NOT</b> use the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1384 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1385 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Calculate/Refine</span></b> |
|---|
| 1386 | menu item in the <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1387 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1388 | minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data tree</span></b> |
|---|
| 1389 | window; that it to be used for Rietveld/Pawley refinements. You will be asked |
|---|
| 1390 | to save the current project before the fit will proceed; change directory if |
|---|
| 1391 | desired and provide a suitable name (we assume <b style='mso-bidi-font-weight: |
|---|
| 1392 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1393 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>LaB6</span></b>). |
|---|
| 1394 | A window will show the progress of the refinement and will close when the |
|---|
| 1395 | least-squares fit <span class=GramE>is</span> complete (usually very fast). The |
|---|
| 1396 | plot is updated with the fit, the peak list window is updated with the new peak |
|---|
| 1397 | values and a summary of the refinement is shown on the console window as well.</p> |
|---|
| 1398 | |
|---|
| 1399 | <p class=MsoListParagraphCxSpMiddle><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1400 | id="Picture_x0020_8" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:525pt; |
|---|
| 1401 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1402 | <v:imagedata src="Fit%20Peaks_files/image009.png" o:title=""/> |
|---|
| 1403 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1404 | src="Fit%20Peaks_files/image009.png" v:shapes="Picture_x0020_8"><![endif]></span></p> |
|---|
| 1405 | |
|---|
| 1406 | <p class=MsoListParagraphCxSpMiddle><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1407 | id="Picture_x0020_9" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:401.25pt; |
|---|
| 1408 | height:262.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1409 | <v:imagedata src="Fit%20Peaks_files/image010.png" o:title=""/> |
|---|
| 1410 | </v:shape><![endif]--><![if !vml]><img border=0 width=535 height=350 |
|---|
| 1411 | src="Fit%20Peaks_files/image010.png" v:shapes="Picture_x0020_9"><![endif]></span></p> |
|---|
| 1412 | |
|---|
| 1413 | <p class=MsoListParagraphCxSpMiddle style='text-indent:-.25in;mso-list:l2 level1 lfo6'><![if !supportLists]><span |
|---|
| 1414 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span |
|---|
| 1415 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Now |
|---|
| 1416 | add refinement of the peak positions. This can be done by clicking on all the |
|---|
| 1417 | refinement flags for the individual peaks or it is possible to set them all at |
|---|
| 1418 | the same time using this recipe: </p> |
|---|
| 1419 | |
|---|
| 1420 | <p class=MsoListParagraphCxSpMiddle style='margin-left:1.0in;mso-add-space: |
|---|
| 1421 | auto;text-indent:-.25in;mso-list:l2 level2 lfo6'><![if !supportLists]><span |
|---|
| 1422 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>a.<span |
|---|
| 1423 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]><span |
|---|
| 1424 | class=GramE>single-click</span> on any value in the table to select it, for |
|---|
| 1425 | example the first peak position. A black box appears around the value. </p> |
|---|
| 1426 | |
|---|
| 1427 | <p class=MsoListParagraphCxSpLast style='margin-left:1.0in;mso-add-space:auto; |
|---|
| 1428 | text-indent:-.25in;mso-list:l2 level2 lfo6'><![if !supportLists]><span |
|---|
| 1429 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>b.<span |
|---|
| 1430 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]><span |
|---|
| 1431 | class=GramE>single-click</span> on the refine label above the peak position |
|---|
| 1432 | check-boxes. The entire column of checkboxes is highlighted in blue. Press the <b |
|---|
| 1433 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1434 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1435 | minor-latin'>y</span></b> key to turn on all refinement flags (<b |
|---|
| 1436 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1437 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1438 | minor-latin'>n</span></b> would turn them off).</p> |
|---|
| 1439 | |
|---|
| 1440 | <p class=MsoNormal style='margin-left:.5in'>Next, repeat the refinement using |
|---|
| 1441 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1442 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1443 | minor-latin'>Peak Fitting/LSQ <span class=SpellE>PeakFit</span></span></b> menu |
|---|
| 1444 | item in the <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1445 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1446 | minor-latin;mso-bidi-theme-font:minor-latin'>Peak List</span></b> window.</p> |
|---|
| 1447 | |
|---|
| 1448 | <p class=MsoNormal style='margin-left:.5in'><span |
|---|
| 1449 | style='mso-spacerun:yes'> </span>Now, select peak widths for refinement. <span |
|---|
| 1450 | style='mso-fareast-font-family:"Times New Roman"'>This can be performed in 2 |
|---|
| 1451 | different ways. Method 1: refine sigma (Gaussian width) and/or |
|---|
| 1452 | gamma (Lorentzian width) for individual peaks. To do this, click the |
|---|
| 1453 | refinement flags for sigma and/or gamma in the Peak List window. |
|---|
| 1454 | Method 2: preferably, the LS refinement of peak |
|---|
| 1455 | widths can be constrained to follow an instrumental broadening |
|---|
| 1456 | equation as described below. Note - one cannot refine ALL peak widths |
|---|
| 1457 | using both individual sigma & gamma values AND instrumental |
|---|
| 1458 | broadening terms at the same time.<b style='mso-bidi-font-weight:normal'> </b><o:p></o:p></span></p> |
|---|
| 1459 | |
|---|
| 1460 | <p class=MsoNormal style='margin-left:.5in'><span style='mso-fareast-font-family: |
|---|
| 1461 | "Times New Roman";mso-bidi-font-weight:bold'>To constrain refined peak widths |
|---|
| 1462 | to an instrumental broadening equation, first<b> s</b></span>elect the <b |
|---|
| 1463 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1464 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1465 | minor-latin'>Instrumental Parameters</span></b> item in the data tree. <span |
|---|
| 1466 | class=GramE>This opens a window for peak profile terms<b> </b><span |
|---|
| 1467 | style='mso-bidi-font-weight:bold'>and also create</span></span><span |
|---|
| 1468 | style='mso-bidi-font-weight:bold'> a new plot window showing the |
|---|
| 1469 | instrument profile resolution curve.</span></p> |
|---|
| 1470 | |
|---|
| 1471 | <p class=MsoNormal style='margin-left:.5in'><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1472 | id="Picture_x0020_10" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:422.25pt; |
|---|
| 1473 | height:154.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1474 | <v:imagedata src="Fit%20Peaks_files/image011.png" o:title=""/> |
|---|
| 1475 | </v:shape><![endif]--><![if !vml]><img border=0 width=563 height=206 |
|---|
| 1476 | src="Fit%20Peaks_files/image011.png" v:shapes="Picture_x0020_10"><![endif]></span></p> |
|---|
| 1477 | |
|---|
| 1478 | <p class=MsoListParagraphCxSpFirst>The plot window shows the resolution curves |
|---|
| 1479 | corresponding to the values of the Gaussian U, V, W, Lorentzian X & Y |
|---|
| 1480 | coefficients; + marks show the individual values based on the sig & gam |
|---|
| 1481 | values for the peaks in Peak List. Select the refine flag checkbox for Gaussian |
|---|
| 1482 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1483 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1484 | minor-latin'>U</span></b>, <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1485 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1486 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>V</span></b>, |
|---|
| 1487 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1488 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1489 | minor-latin'>W</span></b>, and Lorentzian <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1490 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1491 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>X</span></b>, |
|---|
| 1492 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1493 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1494 | minor-latin'>Y</span></b>. </p> |
|---|
| 1495 | |
|---|
| 1496 | <p class=MsoListParagraphCxSpMiddle style='text-indent:-.25in;mso-list:l2 level1 lfo6'><![if !supportLists]><span |
|---|
| 1497 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>3.<span |
|---|
| 1498 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Then, |
|---|
| 1499 | repeat the refinement. First click on the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1500 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1501 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak List</span></b> |
|---|
| 1502 | item in the data tree and then refine using the <b style='mso-bidi-font-weight: |
|---|
| 1503 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1504 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak |
|---|
| 1505 | Fitting/LSQ <span class=SpellE>PeakFit</span></span></b> menu item. At this |
|---|
| 1506 | point a good fit should be seen by zooming in on individual peaks. (For example |
|---|
| 1507 | see </p> |
|---|
| 1508 | |
|---|
| 1509 | <p class=MsoListParagraphCxSpMiddle><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1510 | id="Picture_x0020_11" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt; |
|---|
| 1511 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1512 | <v:imagedata src="Fit%20Peaks_files/image012.png" o:title=""/> |
|---|
| 1513 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1514 | src="Fit%20Peaks_files/image012.png" v:shapes="Picture_x0020_11"><![endif]></span></p> |
|---|
| 1515 | |
|---|
| 1516 | <p class=MsoListParagraphCxSpLast>The <span class=SpellE>Rwp</span> is ~6% as |
|---|
| 1517 | shown on the console window. Again the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1518 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1519 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak List</span></b> |
|---|
| 1520 | entries are all updated with new values and those in <b style='mso-bidi-font-weight: |
|---|
| 1521 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1522 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Instrument |
|---|
| 1523 | Parameters</span></b> are also updated.</p> |
|---|
| 1524 | |
|---|
| 1525 | <h2><span class=GramE>Step 5.</span> Prepare Indexing Peak List</h2> |
|---|
| 1526 | |
|---|
| 1527 | <p class=MsoNormal>A separate list of peaks is kept for use in <span |
|---|
| 1528 | class=SpellE>autoindexing</span>. It is found in the <b style='mso-bidi-font-weight: |
|---|
| 1529 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1530 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Index |
|---|
| 1531 | Peak List</span></b> item in the data tree. In the initially empty window |
|---|
| 1532 | created by this action, use menu item <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1533 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1534 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Index Peaks |
|---|
| 1535 | Operations/Load</span></b> to copy the fitted peaks from the <b |
|---|
| 1536 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1537 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1538 | minor-latin'>Peak List</span></b>.</p> |
|---|
| 1539 | |
|---|
| 1540 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1541 | id="Picture_x0020_12" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:367.5pt; |
|---|
| 1542 | height:225pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1543 | <v:imagedata src="Fit%20Peaks_files/image013.png" o:title=""/> |
|---|
| 1544 | </v:shape><![endif]--><![if !vml]><img border=0 width=490 height=300 |
|---|
| 1545 | src="Fit%20Peaks_files/image013.png" v:shapes="Picture_x0020_12"><![endif]></span></p> |
|---|
| 1546 | |
|---|
| 1547 | <p class=MsoNormal>Note that by default all peaks are selected to be used. You |
|---|
| 1548 | may choose to not use a fitted peak (e.g. if suspected it is from a |
|---|
| 1549 | contaminant).</p> |
|---|
| 1550 | |
|---|
| 1551 | <h2><span class=GramE>Step 6.</span> Run <span class=SpellE>Autoindexing</span></h2> |
|---|
| 1552 | |
|---|
| 1553 | <p class=MsoNormal>Select the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1554 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1555 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Unit Cells |
|---|
| 1556 | List</span></b> data item. This brings up a window for indexing and cell refinement |
|---|
| 1557 | options</p> |
|---|
| 1558 | |
|---|
| 1559 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1560 | id="Picture_x0020_13" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:527.25pt; |
|---|
| 1561 | height:204pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1562 | <v:imagedata src="Fit%20Peaks_files/image014.png" o:title=""/> |
|---|
| 1563 | </v:shape><![endif]--><![if !vml]><img border=0 width=703 height=272 |
|---|
| 1564 | src="Fit%20Peaks_files/image014.png" v:shapes="Picture_x0020_13"><![endif]></span></p> |
|---|
| 1565 | |
|---|
| 1566 | <p class=MsoNormal>For the most rapid search (since we know the right answer), |
|---|
| 1567 | select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1568 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1569 | minor-latin'>Cubic-P</span></b> and launch the search using menu item <b |
|---|
| 1570 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1571 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1572 | minor-latin'>Cell Index/Index Cell</span></b>. The search then runs and the console |
|---|
| 1573 | shows a running list of possible cells as they are found; the sorted by M20 |
|---|
| 1574 | list of possible matching cells is shown in the <b style='mso-bidi-font-weight: |
|---|
| 1575 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1576 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Unit |
|---|
| 1577 | Cells List</span></b> window</p> |
|---|
| 1578 | |
|---|
| 1579 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1580 | id="Picture_x0020_14" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:527.25pt; |
|---|
| 1581 | height:376.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1582 | <v:imagedata src="Fit%20Peaks_files/image015.png" o:title=""/> |
|---|
| 1583 | </v:shape><![endif]--><![if !vml]><img border=0 width=703 height=502 |
|---|
| 1584 | src="Fit%20Peaks_files/image015.png" v:shapes="Picture_x0020_14"><![endif]></span></p> |
|---|
| 1585 | |
|---|
| 1586 | <h2><span class=GramE>Step 7.</span> Review Cell Choices</h2> |
|---|
| 1587 | |
|---|
| 1588 | <p class=MsoNormal>Review the list of cells associated with the <b |
|---|
| 1589 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1590 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1591 | minor-latin'>Unit Cells List</span></b> data item. Note that as one selects a |
|---|
| 1592 | unit cell, the generated reflections for that cell are shown in the plot with |
|---|
| 1593 | dashed red lines. Sliding the cursor over these lines shows a small popup |
|---|
| 1594 | window with the indexed <span class=SpellE>hkl</span> for them. Note how the |
|---|
| 1595 | first cell in the list (M20~3000) with a=5.87864 Å generates very many lines |
|---|
| 1596 | with no corresponding peaks (NB: this solution might not always show up!)</p> |
|---|
| 1597 | |
|---|
| 1598 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1599 | id="Picture_x0020_15" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt; |
|---|
| 1600 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1601 | <v:imagedata src="Fit%20Peaks_files/image016.png" o:title=""/> |
|---|
| 1602 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1603 | src="Fit%20Peaks_files/image016.png" v:shapes="Picture_x0020_15"><![endif]></span><span |
|---|
| 1604 | style='mso-spacerun:yes'> </span></p> |
|---|
| 1605 | |
|---|
| 1606 | <p class=MsoNormal><span class=GramE>while</span> the (M20~600) cell with |
|---|
| 1607 | a=2.93932 Å generates not enough lines to match all the peaks</p> |
|---|
| 1608 | |
|---|
| 1609 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1610 | id="Picture_x0020_16" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt; |
|---|
| 1611 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1612 | <v:imagedata src="Fit%20Peaks_files/image017.png" o:title=""/> |
|---|
| 1613 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1614 | src="Fit%20Peaks_files/image017.png" v:shapes="Picture_x0020_16"><![endif]></span></p> |
|---|
| 1615 | |
|---|
| 1616 | <h2><span class=GramE>Step 8.</span> Select/Refine Cell</h2> |
|---|
| 1617 | |
|---|
| 1618 | <p class=MsoNormal>Select the cell with M20 ~ 2900 with a = 4.1568 Å. This |
|---|
| 1619 | indexes all peaks with almost a perfect fit to the peak positions (compare |
|---|
| 1620 | dashed red lines to solid blue ones). Import the cell information using the <b |
|---|
| 1621 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1622 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1623 | minor-latin'>Cell Index/Copy Cell</span></b> menu option. Then optimize the |
|---|
| 1624 | cell by refining the lattice parameters and the two-theta zero: click on the |
|---|
| 1625 | refine checkbox next to the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1626 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1627 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Zero offset</span></b> |
|---|
| 1628 | value and then the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1629 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1630 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Cell |
|---|
| 1631 | Index/Refine Cell</span></b> menu option. <span class=GramE>The a</span> cell |
|---|
| 1632 | parameter value shifts from 4.15679 to 4.15684 when zero is refined. Press the <b |
|---|
| 1633 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1634 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1635 | minor-latin'>Show refined <span class=SpellE>hkl</span> positions + Zero offset</span></b> |
|---|
| 1636 | button to update the plot including the refined <b style='mso-bidi-font-weight: |
|---|
| 1637 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1638 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Zero |
|---|
| 1639 | offset</span></b> (in this case hardly anything happens!) </p> |
|---|
| 1640 | |
|---|
| 1641 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1642 | id="Picture_x0020_17" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:527.25pt; |
|---|
| 1643 | height:334.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1644 | <v:imagedata src="Fit%20Peaks_files/image018.png" o:title=""/> |
|---|
| 1645 | </v:shape><![endif]--><![if !vml]><img border=0 width=703 height=446 |
|---|
| 1646 | src="Fit%20Peaks_files/image018.png" v:shapes="Picture_x0020_17"><![endif]></span></p> |
|---|
| 1647 | |
|---|
| 1648 | <p class=MsoNormal>Notice that a new entry heads the list in the <b |
|---|
| 1649 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1650 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1651 | minor-latin'>Indexing Result</span></b> section of the <b style='mso-bidi-font-weight: |
|---|
| 1652 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1653 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Cell |
|---|
| 1654 | Index/Refine</span></b> window with an improved M20(=3614.66) and a new value |
|---|
| 1655 | for <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1656 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1657 | minor-latin'>Zero offset</span></b> is shown.</p> |
|---|
| 1658 | |
|---|
| 1659 | <p class=MsoNormal>(Optional) Finally, use of the <b style='mso-bidi-font-weight: |
|---|
| 1660 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1661 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Cell |
|---|
| 1662 | Index/New phase</span></b> menu option allows one to create a phase with these |
|---|
| 1663 | lattice parameters in the data tree under <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1664 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1665 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Phases</span></b>.<span |
|---|
| 1666 | style='mso-spacerun:yes'> </span>A name for the new phase is requested. This |
|---|
| 1667 | creates the tree item <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1668 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1669 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Phases</span></b> |
|---|
| 1670 | (if it wasnt already present). This new phase can be used in future analysis |
|---|
| 1671 | (e.g. Rietveld or Pawley refinement).</p> |
|---|
| 1672 | |
|---|
| 1673 | <p class=MsoNormal>To continue with the second part of this exercise, <span |
|---|
| 1674 | class=GramE>do the menu item</span> <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1675 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1676 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>File/Close |
|---|
| 1677 | project</span></b> in the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1678 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1679 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data |
|---|
| 1680 | tree </span></b>window. You will be asked if you want it saved; if <span |
|---|
| 1681 | class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1682 | "Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1683 | minor-latin;mso-bidi-theme-font:minor-latin'>Yes</span></b></span> then all the |
|---|
| 1684 | peak fitting/indexing & cell refinement results will be saved to the <b |
|---|
| 1685 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1686 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1687 | minor-latin'>LaB6.gpx</span></b> file. If <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1688 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1689 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>No</span></b> |
|---|
| 1690 | then the file will remain as it was when created at Step 4 above.</p> |
|---|
| 1691 | |
|---|
| 1692 | <h1>2<sup>nd</sup> Fit Peaks/<span class=SpellE>Autoindexing</span> in GSAS-II </h1> |
|---|
| 1693 | |
|---|
| 1694 | <p class=MsoNormal>In this exercise we will fit peaks and index them for the |
|---|
| 1695 | new mineral <a href="http://en.wikipedia.org/wiki/Jadarite"><span class=SpellE>jadarite</span></a> |
|---|
| 1696 | (aka <a href="http://en.wikipedia.org/wiki/Kryptonite">kryptonite</a>). The |
|---|
| 1697 | data was also collected on 11BM-B at APS. The unit cell is monoclinic so is a |
|---|
| 1698 | more substantial test of the indexing capability of GSAS-II.</p> |
|---|
| 1699 | |
|---|
| 1700 | <h2><span class=GramE>Step 1.</span> Read in the data. </h2> |
|---|
| 1701 | |
|---|
| 1702 | <p class=MsoNormal>The file is <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1703 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1704 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>\Exercises\<span |
|---|
| 1705 | class=SpellE>krptonite</span>\11bmb_6231.fxye</span></b>; it has a |
|---|
| 1706 | corresponding <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
|---|
| 1707 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1708 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>prm</span></b></span> |
|---|
| 1709 | file. Load them in & the plot is</p> |
|---|
| 1710 | |
|---|
| 1711 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1712 | id="Picture_x0020_18" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt; |
|---|
| 1713 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1714 | <v:imagedata src="Fit%20Peaks_files/image019.png" o:title=""/> |
|---|
| 1715 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1716 | src="Fit%20Peaks_files/image019.png" v:shapes="Picture_x0020_18"><![endif]></span></p> |
|---|
| 1717 | |
|---|
| 1718 | <p class=MsoNormal>Ive zoomed in & shifted the plot some to highlight the |
|---|
| 1719 | lower part of the pattern.</p> |
|---|
| 1720 | |
|---|
| 1721 | <h2>Step 2 Set limits</h2> |
|---|
| 1722 | |
|---|
| 1723 | <p class=MsoNormal>Set the limits as <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1724 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1725 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>3</span></b> |
|---|
| 1726 | and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1727 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1728 | minor-latin'>10</span></b>.</p> |
|---|
| 1729 | |
|---|
| 1730 | <h2>Step 3 Pick peaks</h2> |
|---|
| 1731 | |
|---|
| 1732 | <p class=MsoNormal>Pick all peaks you can see between the limits (including the |
|---|
| 1733 | small ones). Note some peaks have shoulders most notably at 5.07, 6.04, |
|---|
| 1734 | 7.81deg. I found 28 peaks (there were a few very weak ones I skipped they |
|---|
| 1735 | might be from a second phase? Well see later).</p> |
|---|
| 1736 | |
|---|
| 1737 | <p class=MsoNormal><!--[if gte vml 1]><v:shape id="Picture_x0020_19" o:spid="_x0000_s1026" |
|---|
| 1738 | type="#_x0000_t75" style='position:absolute;margin-left:0;margin-top:0; |
|---|
| 1739 | width:525pt;height:450pt;z-index:251658240;visibility:visible; |
|---|
| 1740 | mso-wrap-style:square;mso-width-percent:0;mso-height-percent:0; |
|---|
| 1741 | mso-wrap-distance-left:9pt;mso-wrap-distance-top:0;mso-wrap-distance-right:9pt; |
|---|
| 1742 | mso-wrap-distance-bottom:0;mso-position-horizontal:left; |
|---|
| 1743 | mso-position-horizontal-relative:text;mso-position-vertical:top; |
|---|
| 1744 | mso-position-vertical-relative:text;mso-width-percent:0;mso-height-percent:0; |
|---|
| 1745 | mso-width-relative:page;mso-height-relative:page'> |
|---|
| 1746 | <v:imagedata src="Fit%20Peaks_files/image020.png" o:title=""/> |
|---|
| 1747 | <w:wrap type="square"/> |
|---|
| 1748 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
|---|
| 1749 | src="Fit%20Peaks_files/image020.png" align=left hspace=12 v:shapes="Picture_x0020_19"><![endif]><br |
|---|
| 1750 | clear=all style='mso-special-character:line-break'> |
|---|
| 1751 | </p> |
|---|
| 1752 | |
|---|
| 1753 | <h2><span class=GramE>Step 4.</span> Refine peaks</h2> |
|---|
| 1754 | |
|---|
| 1755 | <p class=MsoNormal>Following the steps above, refine the peaks and the profile |
|---|
| 1756 | shape parameters in <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1757 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1758 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Instrument |
|---|
| 1759 | Parameters</span></b>. You will be asked for a project file name at the first |
|---|
| 1760 | refinement (I used <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
|---|
| 1761 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1762 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>jadarite</span></b></span><b |
|---|
| 1763 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1764 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1765 | minor-latin'></span></b>). In the end my refinement converged at <span |
|---|
| 1766 | class=SpellE>Rwp</span>=13.18% and some peaks do show some discrepancy as the |
|---|
| 1767 | sample is more complex than the simple <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1768 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1769 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>U</span></b>, |
|---|
| 1770 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1771 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1772 | minor-latin'>V</span></b>, <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1773 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1774 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>W</span></b>, |
|---|
| 1775 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1776 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1777 | minor-latin'>X</span></b>, <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1778 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1779 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Y</span></b> |
|---|
| 1780 | model can accommodate. However, this is good enough to proceed.</p> |
|---|
| 1781 | |
|---|
| 1782 | <h2><span class=GramE>Step 5.</span> Prepare Indexing Peak List</h2> |
|---|
| 1783 | |
|---|
| 1784 | <p class=MsoNormal>As before do <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1785 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1786 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Operations/Load/Reload</span></b> |
|---|
| 1787 | in the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1788 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1789 | minor-latin'>Index Peak List</span></b> window.</p> |
|---|
| 1790 | |
|---|
| 1791 | <h2><span class=GramE>Step 6.</span> Index the cell</h2> |
|---|
| 1792 | |
|---|
| 1793 | <p class=MsoNormal>Lets assume that we know the cell in primitive monoclinic. |
|---|
| 1794 | In a real world case we wouldnt know this and we would have to try each <span |
|---|
| 1795 | class=SpellE>Bravais</span> lattice. These can be done as a group, but it takes |
|---|
| 1796 | time to go through all the bad cases.</p> |
|---|
| 1797 | |
|---|
| 1798 | <p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1799 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1800 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Monoclinic-P</span></b> |
|---|
| 1801 | and do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1802 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1803 | minor-latin'>Cell Index/Refine/Index cell</span></b> in the <b |
|---|
| 1804 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1805 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1806 | minor-latin'>Unit Cells List</span></b> window. Progress will be much slower |
|---|
| 1807 | and suitable results will be slow in coming so be patient. Watch the console |
|---|
| 1808 | window; the right answer will have an obviously large M20 (~630) and a volume |
|---|
| 1809 | of ~594Å<sup>3</sup> (10<sup>th</sup> column of console display). Once this is |
|---|
| 1810 | seen (it may take more than one try to get this) you can stop the indexing |
|---|
| 1811 | search by pressing <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1812 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1813 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Cancel</span></b> |
|---|
| 1814 | on the progress bar window. It may take more than one press to fully stop it. |
|---|
| 1815 | My result was </p> |
|---|
| 1816 | |
|---|
| 1817 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1818 | id="Picture_x0020_20" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:527.25pt; |
|---|
| 1819 | height:376.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1820 | <v:imagedata src="Fit%20Peaks_files/image021.png" o:title=""/> |
|---|
| 1821 | </v:shape><![endif]--><![if !vml]><img border=0 width=703 height=502 |
|---|
| 1822 | src="Fit%20Peaks_files/image021.png" v:shapes="Picture_x0020_20"><![endif]></span></p> |
|---|
| 1823 | |
|---|
| 1824 | <p class=MsoNormal>Notice an equally good M20 result with twice the volume. The |
|---|
| 1825 | plot shows every peak indexed including a couple of weak peaks not selected for |
|---|
| 1826 | the peak fitting.</p> |
|---|
| 1827 | |
|---|
| 1828 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1829 | id="Picture_x0020_21" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:525pt; |
|---|
| 1830 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1831 | <v:imagedata src="Fit%20Peaks_files/image022.png" o:title=""/> |
|---|
| 1832 | </v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600 |
|---|
| 1833 | src="Fit%20Peaks_files/image022.png" v:shapes="Picture_x0020_21"><![endif]></span></p> |
|---|
| 1834 | |
|---|
| 1835 | <p class=MsoNormal>Although the weak peak at 2<span style='font-family:Symbol; |
|---|
| 1836 | mso-char-type:symbol;mso-symbol-font-family:Symbol'><span style='mso-char-type: |
|---|
| 1837 | symbol;mso-symbol-font-family:Symbol'>Q</span></span>~7.3 has a shoulder that |
|---|
| 1838 | wasnt indexed. I presume that is a contaminant. By sliding the cursor over the |
|---|
| 1839 | index lines without any visible peak you can see that the missing ones are |
|---|
| 1840 | (010, 100, 001, 110, 030, 111, 20-1, 10-2, 041, 050, 21-2, 23-1, 22-2, 141, |
|---|
| 1841 | 201,102, 15-1, 112, & 24-1). Many of these are accidental but the 0k0; k≠2n |
|---|
| 1842 | and h0l; h+l≠2n ones characterize the space group P2<sub>1</sub>/n. Armed |
|---|
| 1843 | with this information you can <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1844 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1845 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Make new |
|---|
| 1846 | phase</span></b> for the indexed cell (I called it <b style='mso-bidi-font-weight: |
|---|
| 1847 | normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font: |
|---|
| 1848 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>kryptonite</span></b>) |
|---|
| 1849 | and set the space group in the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1850 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1851 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Phase Data |
|---|
| 1852 | for kryptonite</span></b> window.</p> |
|---|
| 1853 | |
|---|
| 1854 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1855 | id="Picture_x0020_22" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:597.75pt; |
|---|
| 1856 | height:214.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1857 | <v:imagedata src="Fit%20Peaks_files/image023.png" o:title=""/> |
|---|
| 1858 | </v:shape><![endif]--><![if !vml]><img border=0 width=797 height=286 |
|---|
| 1859 | src="Fit%20Peaks_files/image023.png" v:shapes="Picture_x0020_22"><![endif]></span></p> |
|---|
| 1860 | |
|---|
| 1861 | <p class=MsoNormal>Setting the space group will show a window with some |
|---|
| 1862 | information. Press <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1863 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1864 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b> |
|---|
| 1865 | to close it.</p> |
|---|
| 1866 | |
|---|
| 1867 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1868 | id="Picture_x0020_23" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:333.75pt; |
|---|
| 1869 | height:209.25pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1870 | <v:imagedata src="Fit%20Peaks_files/image024.png" o:title=""/> |
|---|
| 1871 | </v:shape><![endif]--><![if !vml]><img border=0 width=445 height=279 |
|---|
| 1872 | src="Fit%20Peaks_files/image024.png" v:shapes="Picture_x0020_23"><![endif]></span></p> |
|---|
| 1873 | |
|---|
| 1874 | <p class=MsoNormal>This concludes this exercise; <span class=GramE><b |
|---|
| 1875 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1876 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1877 | minor-latin'>Save</span></b></span> the project file as it is needed for the <b |
|---|
| 1878 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif"; |
|---|
| 1879 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1880 | minor-latin'><a href="Charge%20Flipping%20in%20GSAS.htm">Charge Flipping</a></span></b> |
|---|
| 1881 | exercise. The features of the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1882 | style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin; |
|---|
| 1883 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Phase Data</span></b> |
|---|
| 1884 | window will be presented in other exercises.</p> |
|---|
| 1885 | |
|---|
| 1886 | </div> |
|---|
| 1887 | |
|---|
| 1888 | </body> |
|---|
| 1889 | |
|---|
| 1890 | </html> |
|---|
