source: trunk/help/Calibration of an area detector in GSAS.htm @ 1114

Last change on this file since 1114 was 1114, checked in by toby, 9 years ago

fix help error by reverting and editing html by hand

  • Property svn:keywords set to Author
  • Property svn:mime-type set to text/html
File size: 51.3 KB
Line 
1<html xmlns:v="urn:schemas-microsoft-com:vml"
2xmlns:o="urn:schemas-microsoft-com:office:office"
3xmlns:w="urn:schemas-microsoft-com:office:word"
4xmlns:m="http://schemas.microsoft.com/office/2004/12/omml"
5xmlns="http://www.w3.org/TR/REC-html40">
6
7<head>
8<meta http-equiv=Content-Type content="text/html; charset=windows-1252">
9<meta name=ProgId content=Word.Document>
10<meta name=Generator content="Microsoft Word 14">
11<meta name=Originator content="Microsoft Word 14">
12<link rel=File-List
13href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/filelist.xml">
14<link rel=Edit-Time-Data
15href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/editdata.mso">
16<!--[if !mso]>
17<style>
18v\:* {behavior:url(#default#VML);}
19o\:* {behavior:url(#default#VML);}
20w\:* {behavior:url(#default#VML);}
21.shape {behavior:url(#default#VML);}
22</style>
23<![endif]--><!--[if gte mso 9]><xml>
24 <o:DocumentProperties>
25  <o:Author>Von Dreele</o:Author>
26  <o:LastAuthor>Von Dreele</o:LastAuthor>
27  <o:Revision>14</o:Revision>
28  <o:TotalTime>137</o:TotalTime>
29  <o:Created>2012-05-04T19:00:00Z</o:Created>
30  <o:LastSaved>2013-04-30T17:13:00Z</o:LastSaved>
31  <o:Pages>4</o:Pages>
32  <o:Words>695</o:Words>
33  <o:Characters>3966</o:Characters>
34  <o:Company>Argonne National Laboratory</o:Company>
35  <o:Lines>33</o:Lines>
36  <o:Paragraphs>9</o:Paragraphs>
37  <o:CharactersWithSpaces>4652</o:CharactersWithSpaces>
38  <o:Version>14.00</o:Version>
39 </o:DocumentProperties>
40 <o:OfficeDocumentSettings>
41  <o:AllowPNG/>
42 </o:OfficeDocumentSettings>
43</xml><![endif]-->
44<link rel=themeData
45href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/themedata.thmx">
46<link rel=colorSchemeMapping
47href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/colorschememapping.xml">
48<!--[if gte mso 9]><xml>
49 <w:WordDocument>
50  <w:Zoom>156</w:Zoom>
51  <w:SpellingState>Clean</w:SpellingState>
52  <w:GrammarState>Clean</w:GrammarState>
53  <w:TrackMoves>false</w:TrackMoves>
54  <w:TrackFormatting/>
55  <w:PunctuationKerning/>
56  <w:ValidateAgainstSchemas/>
57  <w:SaveIfXMLInvalid>false</w:SaveIfXMLInvalid>
58  <w:IgnoreMixedContent>false</w:IgnoreMixedContent>
59  <w:AlwaysShowPlaceholderText>false</w:AlwaysShowPlaceholderText>
60  <w:DoNotPromoteQF/>
61  <w:LidThemeOther>EN-US</w:LidThemeOther>
62  <w:LidThemeAsian>X-NONE</w:LidThemeAsian>
63  <w:LidThemeComplexScript>X-NONE</w:LidThemeComplexScript>
64  <w:Compatibility>
65   <w:BreakWrappedTables/>
66   <w:SnapToGridInCell/>
67   <w:WrapTextWithPunct/>
68   <w:UseAsianBreakRules/>
69   <w:DontGrowAutofit/>
70   <w:SplitPgBreakAndParaMark/>
71   <w:EnableOpenTypeKerning/>
72   <w:DontFlipMirrorIndents/>
73   <w:OverrideTableStyleHps/>
74  </w:Compatibility>
75  <w:BrowserLevel>MicrosoftInternetExplorer4</w:BrowserLevel>
76  <m:mathPr>
77   <m:mathFont m:val="Cambria Math"/>
78   <m:brkBin m:val="before"/>
79   <m:brkBinSub m:val="&#45;-"/>
80   <m:smallFrac m:val="off"/>
81   <m:dispDef/>
82   <m:lMargin m:val="0"/>
83   <m:rMargin m:val="0"/>
84   <m:defJc m:val="centerGroup"/>
85   <m:wrapIndent m:val="1440"/>
86   <m:intLim m:val="subSup"/>
87   <m:naryLim m:val="undOvr"/>
88  </m:mathPr></w:WordDocument>
89</xml><![endif]--><!--[if gte mso 9]><xml>
90 <w:LatentStyles DefLockedState="false" DefUnhideWhenUsed="true"
91  DefSemiHidden="true" DefQFormat="false" DefPriority="99"
92  LatentStyleCount="267">
93  <w:LsdException Locked="false" Priority="0" SemiHidden="false"
94   UnhideWhenUsed="false" QFormat="true" Name="Normal"/>
95  <w:LsdException Locked="false" Priority="9" SemiHidden="false"
96   UnhideWhenUsed="false" QFormat="true" Name="heading 1"/>
97  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 2"/>
98  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 3"/>
99  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 4"/>
100  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 5"/>
101  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 6"/>
102  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 7"/>
103  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 8"/>
104  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 9"/>
105  <w:LsdException Locked="false" Priority="39" Name="toc 1"/>
106  <w:LsdException Locked="false" Priority="39" Name="toc 2"/>
107  <w:LsdException Locked="false" Priority="39" Name="toc 3"/>
108  <w:LsdException Locked="false" Priority="39" Name="toc 4"/>
109  <w:LsdException Locked="false" Priority="39" Name="toc 5"/>
110  <w:LsdException Locked="false" Priority="39" Name="toc 6"/>
111  <w:LsdException Locked="false" Priority="39" Name="toc 7"/>
112  <w:LsdException Locked="false" Priority="39" Name="toc 8"/>
113  <w:LsdException Locked="false" Priority="39" Name="toc 9"/>
114  <w:LsdException Locked="false" Priority="35" QFormat="true" Name="caption"/>
115  <w:LsdException Locked="false" Priority="10" SemiHidden="false"
116   UnhideWhenUsed="false" QFormat="true" Name="Title"/>
117  <w:LsdException Locked="false" Priority="1" Name="Default Paragraph Font"/>
118  <w:LsdException Locked="false" Priority="11" SemiHidden="false"
119   UnhideWhenUsed="false" QFormat="true" Name="Subtitle"/>
120  <w:LsdException Locked="false" Priority="22" SemiHidden="false"
121   UnhideWhenUsed="false" QFormat="true" Name="Strong"/>
122  <w:LsdException Locked="false" Priority="20" SemiHidden="false"
123   UnhideWhenUsed="false" QFormat="true" Name="Emphasis"/>
124  <w:LsdException Locked="false" Priority="59" SemiHidden="false"
125   UnhideWhenUsed="false" Name="Table Grid"/>
126  <w:LsdException Locked="false" UnhideWhenUsed="false" Name="Placeholder Text"/>
127  <w:LsdException Locked="false" Priority="1" SemiHidden="false"
128   UnhideWhenUsed="false" QFormat="true" Name="No Spacing"/>
129  <w:LsdException Locked="false" Priority="60" SemiHidden="false"
130   UnhideWhenUsed="false" Name="Light Shading"/>
131  <w:LsdException Locked="false" Priority="61" SemiHidden="false"
132   UnhideWhenUsed="false" Name="Light List"/>
133  <w:LsdException Locked="false" Priority="62" SemiHidden="false"
134   UnhideWhenUsed="false" Name="Light Grid"/>
135  <w:LsdException Locked="false" Priority="63" SemiHidden="false"
136   UnhideWhenUsed="false" Name="Medium Shading 1"/>
137  <w:LsdException Locked="false" Priority="64" SemiHidden="false"
138   UnhideWhenUsed="false" Name="Medium Shading 2"/>
139  <w:LsdException Locked="false" Priority="65" SemiHidden="false"
140   UnhideWhenUsed="false" Name="Medium List 1"/>
141  <w:LsdException Locked="false" Priority="66" SemiHidden="false"
142   UnhideWhenUsed="false" Name="Medium List 2"/>
143  <w:LsdException Locked="false" Priority="67" SemiHidden="false"
144   UnhideWhenUsed="false" Name="Medium Grid 1"/>
145  <w:LsdException Locked="false" Priority="68" SemiHidden="false"
146   UnhideWhenUsed="false" Name="Medium Grid 2"/>
147  <w:LsdException Locked="false" Priority="69" SemiHidden="false"
148   UnhideWhenUsed="false" Name="Medium Grid 3"/>
149  <w:LsdException Locked="false" Priority="70" SemiHidden="false"
150   UnhideWhenUsed="false" Name="Dark List"/>
151  <w:LsdException Locked="false" Priority="71" SemiHidden="false"
152   UnhideWhenUsed="false" Name="Colorful Shading"/>
153  <w:LsdException Locked="false" Priority="72" SemiHidden="false"
154   UnhideWhenUsed="false" Name="Colorful List"/>
155  <w:LsdException Locked="false" Priority="73" SemiHidden="false"
156   UnhideWhenUsed="false" Name="Colorful Grid"/>
157  <w:LsdException Locked="false" Priority="60" SemiHidden="false"
158   UnhideWhenUsed="false" Name="Light Shading Accent 1"/>
159  <w:LsdException Locked="false" Priority="61" SemiHidden="false"
160   UnhideWhenUsed="false" Name="Light List Accent 1"/>
161  <w:LsdException Locked="false" Priority="62" SemiHidden="false"
162   UnhideWhenUsed="false" Name="Light Grid Accent 1"/>
163  <w:LsdException Locked="false" Priority="63" SemiHidden="false"
164   UnhideWhenUsed="false" Name="Medium Shading 1 Accent 1"/>
165  <w:LsdException Locked="false" Priority="64" SemiHidden="false"
166   UnhideWhenUsed="false" Name="Medium Shading 2 Accent 1"/>
167  <w:LsdException Locked="false" Priority="65" SemiHidden="false"
168   UnhideWhenUsed="false" Name="Medium List 1 Accent 1"/>
169  <w:LsdException Locked="false" UnhideWhenUsed="false" Name="Revision"/>
170  <w:LsdException Locked="false" Priority="34" SemiHidden="false"
171   UnhideWhenUsed="false" QFormat="true" Name="List Paragraph"/>
172  <w:LsdException Locked="false" Priority="29" SemiHidden="false"
173   UnhideWhenUsed="false" QFormat="true" Name="Quote"/>
174  <w:LsdException Locked="false" Priority="30" SemiHidden="false"
175   UnhideWhenUsed="false" QFormat="true" Name="Intense Quote"/>
176  <w:LsdException Locked="false" Priority="66" SemiHidden="false"
177   UnhideWhenUsed="false" Name="Medium List 2 Accent 1"/>
178  <w:LsdException Locked="false" Priority="67" SemiHidden="false"
179   UnhideWhenUsed="false" Name="Medium Grid 1 Accent 1"/>
180  <w:LsdException Locked="false" Priority="68" SemiHidden="false"
181   UnhideWhenUsed="false" Name="Medium Grid 2 Accent 1"/>
182  <w:LsdException Locked="false" Priority="69" SemiHidden="false"
183   UnhideWhenUsed="false" Name="Medium Grid 3 Accent 1"/>
184  <w:LsdException Locked="false" Priority="70" SemiHidden="false"
185   UnhideWhenUsed="false" Name="Dark List Accent 1"/>
186  <w:LsdException Locked="false" Priority="71" SemiHidden="false"
187   UnhideWhenUsed="false" Name="Colorful Shading Accent 1"/>
188  <w:LsdException Locked="false" Priority="72" SemiHidden="false"
189   UnhideWhenUsed="false" Name="Colorful List Accent 1"/>
190  <w:LsdException Locked="false" Priority="73" SemiHidden="false"
191   UnhideWhenUsed="false" Name="Colorful Grid Accent 1"/>
192  <w:LsdException Locked="false" Priority="60" SemiHidden="false"
193   UnhideWhenUsed="false" Name="Light Shading Accent 2"/>
194  <w:LsdException Locked="false" Priority="61" SemiHidden="false"
195   UnhideWhenUsed="false" Name="Light List Accent 2"/>
196  <w:LsdException Locked="false" Priority="62" SemiHidden="false"
197   UnhideWhenUsed="false" Name="Light Grid Accent 2"/>
198  <w:LsdException Locked="false" Priority="63" SemiHidden="false"
199   UnhideWhenUsed="false" Name="Medium Shading 1 Accent 2"/>
200  <w:LsdException Locked="false" Priority="64" SemiHidden="false"
201   UnhideWhenUsed="false" Name="Medium Shading 2 Accent 2"/>
202  <w:LsdException Locked="false" Priority="65" SemiHidden="false"
203   UnhideWhenUsed="false" Name="Medium List 1 Accent 2"/>
204  <w:LsdException Locked="false" Priority="66" SemiHidden="false"
205   UnhideWhenUsed="false" Name="Medium List 2 Accent 2"/>
206  <w:LsdException Locked="false" Priority="67" SemiHidden="false"
207   UnhideWhenUsed="false" Name="Medium Grid 1 Accent 2"/>
208  <w:LsdException Locked="false" Priority="68" SemiHidden="false"
209   UnhideWhenUsed="false" Name="Medium Grid 2 Accent 2"/>
210  <w:LsdException Locked="false" Priority="69" SemiHidden="false"
211   UnhideWhenUsed="false" Name="Medium Grid 3 Accent 2"/>
212  <w:LsdException Locked="false" Priority="70" SemiHidden="false"
213   UnhideWhenUsed="false" Name="Dark List Accent 2"/>
214  <w:LsdException Locked="false" Priority="71" SemiHidden="false"
215   UnhideWhenUsed="false" Name="Colorful Shading Accent 2"/>
216  <w:LsdException Locked="false" Priority="72" SemiHidden="false"
217   UnhideWhenUsed="false" Name="Colorful List Accent 2"/>
218  <w:LsdException Locked="false" Priority="73" SemiHidden="false"
219   UnhideWhenUsed="false" Name="Colorful Grid Accent 2"/>
220  <w:LsdException Locked="false" Priority="60" SemiHidden="false"
221   UnhideWhenUsed="false" Name="Light Shading Accent 3"/>
222  <w:LsdException Locked="false" Priority="61" SemiHidden="false"
223   UnhideWhenUsed="false" Name="Light List Accent 3"/>
224  <w:LsdException Locked="false" Priority="62" SemiHidden="false"
225   UnhideWhenUsed="false" Name="Light Grid Accent 3"/>
226  <w:LsdException Locked="false" Priority="63" SemiHidden="false"
227   UnhideWhenUsed="false" Name="Medium Shading 1 Accent 3"/>
228  <w:LsdException Locked="false" Priority="64" SemiHidden="false"
229   UnhideWhenUsed="false" Name="Medium Shading 2 Accent 3"/>
230  <w:LsdException Locked="false" Priority="65" SemiHidden="false"
231   UnhideWhenUsed="false" Name="Medium List 1 Accent 3"/>
232  <w:LsdException Locked="false" Priority="66" SemiHidden="false"
233   UnhideWhenUsed="false" Name="Medium List 2 Accent 3"/>
234  <w:LsdException Locked="false" Priority="67" SemiHidden="false"
235   UnhideWhenUsed="false" Name="Medium Grid 1 Accent 3"/>
236  <w:LsdException Locked="false" Priority="68" SemiHidden="false"
237   UnhideWhenUsed="false" Name="Medium Grid 2 Accent 3"/>
238  <w:LsdException Locked="false" Priority="69" SemiHidden="false"
239   UnhideWhenUsed="false" Name="Medium Grid 3 Accent 3"/>
240  <w:LsdException Locked="false" Priority="70" SemiHidden="false"
241   UnhideWhenUsed="false" Name="Dark List Accent 3"/>
242  <w:LsdException Locked="false" Priority="71" SemiHidden="false"
243   UnhideWhenUsed="false" Name="Colorful Shading Accent 3"/>
244  <w:LsdException Locked="false" Priority="72" SemiHidden="false"
245   UnhideWhenUsed="false" Name="Colorful List Accent 3"/>
246  <w:LsdException Locked="false" Priority="73" SemiHidden="false"
247   UnhideWhenUsed="false" Name="Colorful Grid Accent 3"/>
248  <w:LsdException Locked="false" Priority="60" SemiHidden="false"
249   UnhideWhenUsed="false" Name="Light Shading Accent 4"/>
250  <w:LsdException Locked="false" Priority="61" SemiHidden="false"
251   UnhideWhenUsed="false" Name="Light List Accent 4"/>
252  <w:LsdException Locked="false" Priority="62" SemiHidden="false"
253   UnhideWhenUsed="false" Name="Light Grid Accent 4"/>
254  <w:LsdException Locked="false" Priority="63" SemiHidden="false"
255   UnhideWhenUsed="false" Name="Medium Shading 1 Accent 4"/>
256  <w:LsdException Locked="false" Priority="64" SemiHidden="false"
257   UnhideWhenUsed="false" Name="Medium Shading 2 Accent 4"/>
258  <w:LsdException Locked="false" Priority="65" SemiHidden="false"
259   UnhideWhenUsed="false" Name="Medium List 1 Accent 4"/>
260  <w:LsdException Locked="false" Priority="66" SemiHidden="false"
261   UnhideWhenUsed="false" Name="Medium List 2 Accent 4"/>
262  <w:LsdException Locked="false" Priority="67" SemiHidden="false"
263   UnhideWhenUsed="false" Name="Medium Grid 1 Accent 4"/>
264  <w:LsdException Locked="false" Priority="68" SemiHidden="false"
265   UnhideWhenUsed="false" Name="Medium Grid 2 Accent 4"/>
266  <w:LsdException Locked="false" Priority="69" SemiHidden="false"
267   UnhideWhenUsed="false" Name="Medium Grid 3 Accent 4"/>
268  <w:LsdException Locked="false" Priority="70" SemiHidden="false"
269   UnhideWhenUsed="false" Name="Dark List Accent 4"/>
270  <w:LsdException Locked="false" Priority="71" SemiHidden="false"
271   UnhideWhenUsed="false" Name="Colorful Shading Accent 4"/>
272  <w:LsdException Locked="false" Priority="72" SemiHidden="false"
273   UnhideWhenUsed="false" Name="Colorful List Accent 4"/>
274  <w:LsdException Locked="false" Priority="73" SemiHidden="false"
275   UnhideWhenUsed="false" Name="Colorful Grid Accent 4"/>
276  <w:LsdException Locked="false" Priority="60" SemiHidden="false"
277   UnhideWhenUsed="false" Name="Light Shading Accent 5"/>
278  <w:LsdException Locked="false" Priority="61" SemiHidden="false"
279   UnhideWhenUsed="false" Name="Light List Accent 5"/>
280  <w:LsdException Locked="false" Priority="62" SemiHidden="false"
281   UnhideWhenUsed="false" Name="Light Grid Accent 5"/>
282  <w:LsdException Locked="false" Priority="63" SemiHidden="false"
283   UnhideWhenUsed="false" Name="Medium Shading 1 Accent 5"/>
284  <w:LsdException Locked="false" Priority="64" SemiHidden="false"
285   UnhideWhenUsed="false" Name="Medium Shading 2 Accent 5"/>
286  <w:LsdException Locked="false" Priority="65" SemiHidden="false"
287   UnhideWhenUsed="false" Name="Medium List 1 Accent 5"/>
288  <w:LsdException Locked="false" Priority="66" SemiHidden="false"
289   UnhideWhenUsed="false" Name="Medium List 2 Accent 5"/>
290  <w:LsdException Locked="false" Priority="67" SemiHidden="false"
291   UnhideWhenUsed="false" Name="Medium Grid 1 Accent 5"/>
292  <w:LsdException Locked="false" Priority="68" SemiHidden="false"
293   UnhideWhenUsed="false" Name="Medium Grid 2 Accent 5"/>
294  <w:LsdException Locked="false" Priority="69" SemiHidden="false"
295   UnhideWhenUsed="false" Name="Medium Grid 3 Accent 5"/>
296  <w:LsdException Locked="false" Priority="70" SemiHidden="false"
297   UnhideWhenUsed="false" Name="Dark List Accent 5"/>
298  <w:LsdException Locked="false" Priority="71" SemiHidden="false"
299   UnhideWhenUsed="false" Name="Colorful Shading Accent 5"/>
300  <w:LsdException Locked="false" Priority="72" SemiHidden="false"
301   UnhideWhenUsed="false" Name="Colorful List Accent 5"/>
302  <w:LsdException Locked="false" Priority="73" SemiHidden="false"
303   UnhideWhenUsed="false" Name="Colorful Grid Accent 5"/>
304  <w:LsdException Locked="false" Priority="60" SemiHidden="false"
305   UnhideWhenUsed="false" Name="Light Shading Accent 6"/>
306  <w:LsdException Locked="false" Priority="61" SemiHidden="false"
307   UnhideWhenUsed="false" Name="Light List Accent 6"/>
308  <w:LsdException Locked="false" Priority="62" SemiHidden="false"
309   UnhideWhenUsed="false" Name="Light Grid Accent 6"/>
310  <w:LsdException Locked="false" Priority="63" SemiHidden="false"
311   UnhideWhenUsed="false" Name="Medium Shading 1 Accent 6"/>
312  <w:LsdException Locked="false" Priority="64" SemiHidden="false"
313   UnhideWhenUsed="false" Name="Medium Shading 2 Accent 6"/>
314  <w:LsdException Locked="false" Priority="65" SemiHidden="false"
315   UnhideWhenUsed="false" Name="Medium List 1 Accent 6"/>
316  <w:LsdException Locked="false" Priority="66" SemiHidden="false"
317   UnhideWhenUsed="false" Name="Medium List 2 Accent 6"/>
318  <w:LsdException Locked="false" Priority="67" SemiHidden="false"
319   UnhideWhenUsed="false" Name="Medium Grid 1 Accent 6"/>
320  <w:LsdException Locked="false" Priority="68" SemiHidden="false"
321   UnhideWhenUsed="false" Name="Medium Grid 2 Accent 6"/>
322  <w:LsdException Locked="false" Priority="69" SemiHidden="false"
323   UnhideWhenUsed="false" Name="Medium Grid 3 Accent 6"/>
324  <w:LsdException Locked="false" Priority="70" SemiHidden="false"
325   UnhideWhenUsed="false" Name="Dark List Accent 6"/>
326  <w:LsdException Locked="false" Priority="71" SemiHidden="false"
327   UnhideWhenUsed="false" Name="Colorful Shading Accent 6"/>
328  <w:LsdException Locked="false" Priority="72" SemiHidden="false"
329   UnhideWhenUsed="false" Name="Colorful List Accent 6"/>
330  <w:LsdException Locked="false" Priority="73" SemiHidden="false"
331   UnhideWhenUsed="false" Name="Colorful Grid Accent 6"/>
332  <w:LsdException Locked="false" Priority="19" SemiHidden="false"
333   UnhideWhenUsed="false" QFormat="true" Name="Subtle Emphasis"/>
334  <w:LsdException Locked="false" Priority="21" SemiHidden="false"
335   UnhideWhenUsed="false" QFormat="true" Name="Intense Emphasis"/>
336  <w:LsdException Locked="false" Priority="31" SemiHidden="false"
337   UnhideWhenUsed="false" QFormat="true" Name="Subtle Reference"/>
338  <w:LsdException Locked="false" Priority="32" SemiHidden="false"
339   UnhideWhenUsed="false" QFormat="true" Name="Intense Reference"/>
340  <w:LsdException Locked="false" Priority="33" SemiHidden="false"
341   UnhideWhenUsed="false" QFormat="true" Name="Book Title"/>
342  <w:LsdException Locked="false" Priority="37" Name="Bibliography"/>
343  <w:LsdException Locked="false" Priority="39" QFormat="true" Name="TOC Heading"/>
344 </w:LatentStyles>
345</xml><![endif]-->
346<style>
347<!--
348 /* Font Definitions */
349 @font-face
350        {font-family:"Cambria Math";
351        panose-1:2 4 5 3 5 4 6 3 2 4;
352        mso-font-charset:0;
353        mso-generic-font-family:roman;
354        mso-font-pitch:variable;
355        mso-font-signature:-536870145 1107305727 0 0 415 0;}
356@font-face
357        {font-family:Calibri;
358        panose-1:2 15 5 2 2 2 4 3 2 4;
359        mso-font-charset:0;
360        mso-generic-font-family:swiss;
361        mso-font-pitch:variable;
362        mso-font-signature:-536870145 1073786111 1 0 415 0;}
363@font-face
364        {font-family:Tahoma;
365        panose-1:2 11 6 4 3 5 4 4 2 4;
366        mso-font-charset:0;
367        mso-generic-font-family:swiss;
368        mso-font-pitch:variable;
369        mso-font-signature:-520081665 -1073717157 41 0 66047 0;}
370 /* Style Definitions */
371 p.MsoNormal, li.MsoNormal, div.MsoNormal
372        {mso-style-unhide:no;
373        mso-style-qformat:yes;
374        mso-style-parent:"";
375        margin:0in;
376        margin-bottom:.0001pt;
377        mso-pagination:widow-orphan;
378        font-size:12.0pt;
379        font-family:"Times New Roman","serif";
380        mso-fareast-font-family:"Times New Roman";
381        mso-fareast-theme-font:minor-fareast;}
382h1
383        {mso-style-priority:9;
384        mso-style-unhide:no;
385        mso-style-qformat:yes;
386        mso-style-link:"Heading 1 Char";
387        mso-margin-top-alt:auto;
388        margin-right:0in;
389        mso-margin-bottom-alt:auto;
390        margin-left:0in;
391        mso-pagination:widow-orphan;
392        mso-outline-level:1;
393        font-size:24.0pt;
394        font-family:"Times New Roman","serif";
395        mso-fareast-font-family:"Times New Roman";
396        mso-fareast-theme-font:minor-fareast;
397        font-weight:bold;}
398h2
399        {mso-style-noshow:yes;
400        mso-style-priority:9;
401        mso-style-qformat:yes;
402        mso-style-link:"Heading 2 Char";
403        mso-margin-top-alt:auto;
404        margin-right:0in;
405        mso-margin-bottom-alt:auto;
406        margin-left:0in;
407        mso-pagination:widow-orphan;
408        mso-outline-level:2;
409        font-size:18.0pt;
410        font-family:"Times New Roman","serif";
411        mso-fareast-font-family:"Times New Roman";
412        mso-fareast-theme-font:minor-fareast;
413        font-weight:bold;}
414h3
415        {mso-style-noshow:yes;
416        mso-style-priority:9;
417        mso-style-qformat:yes;
418        mso-style-link:"Heading 3 Char";
419        mso-margin-top-alt:auto;
420        margin-right:0in;
421        mso-margin-bottom-alt:auto;
422        margin-left:0in;
423        mso-pagination:widow-orphan;
424        mso-outline-level:3;
425        font-size:13.5pt;
426        font-family:"Times New Roman","serif";
427        mso-fareast-font-family:"Times New Roman";
428        mso-fareast-theme-font:minor-fareast;
429        font-weight:bold;}
430h4
431        {mso-style-noshow:yes;
432        mso-style-priority:9;
433        mso-style-qformat:yes;
434        mso-style-link:"Heading 4 Char";
435        mso-style-next:Normal;
436        margin-top:10.0pt;
437        margin-right:0in;
438        margin-bottom:0in;
439        margin-left:0in;
440        margin-bottom:.0001pt;
441        mso-pagination:widow-orphan lines-together;
442        page-break-after:avoid;
443        mso-outline-level:4;
444        font-size:13.0pt;
445        font-family:"Cambria","serif";
446        mso-ascii-font-family:Cambria;
447        mso-ascii-theme-font:major-latin;
448        mso-fareast-font-family:"Times New Roman";
449        mso-fareast-theme-font:major-fareast;
450        mso-hansi-font-family:Cambria;
451        mso-hansi-theme-font:major-latin;
452        mso-bidi-font-family:"Times New Roman";
453        mso-bidi-theme-font:major-bidi;
454        color:#4F81BD;
455        mso-themecolor:accent1;
456        font-weight:bold;
457        font-style:italic;}
458h5
459        {mso-style-noshow:yes;
460        mso-style-priority:9;
461        mso-style-qformat:yes;
462        mso-style-link:"Heading 5 Char";
463        mso-margin-top-alt:auto;
464        margin-right:0in;
465        mso-margin-bottom-alt:auto;
466        margin-left:0in;
467        mso-pagination:widow-orphan;
468        mso-outline-level:5;
469        font-size:12.0pt;
470        font-family:"Times New Roman","serif";
471        mso-fareast-font-family:"Times New Roman";
472        mso-fareast-theme-font:minor-fareast;
473        color:#4F4FFF;
474        font-weight:bold;}
475a:visited, span.MsoHyperlinkFollowed
476        {mso-style-noshow:yes;
477        mso-style-priority:99;
478        color:purple;
479        text-decoration:underline;
480        text-underline:single;}
481p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap
482        {mso-style-noshow:yes;
483        mso-style-priority:99;
484        mso-style-link:"Document Map Char";
485        margin:0in;
486        margin-bottom:.0001pt;
487        mso-pagination:widow-orphan;
488        font-size:8.0pt;
489        font-family:"Tahoma","sans-serif";
490        mso-fareast-font-family:"Times New Roman";
491        mso-fareast-theme-font:minor-fareast;}
492p
493        {mso-style-noshow:yes;
494        mso-style-priority:99;
495        mso-margin-top-alt:auto;
496        margin-right:0in;
497        mso-margin-bottom-alt:auto;
498        margin-left:0in;
499        mso-pagination:widow-orphan;
500        font-size:12.0pt;
501        font-family:"Times New Roman","serif";
502        mso-fareast-font-family:"Times New Roman";
503        mso-fareast-theme-font:minor-fareast;}
504pre
505        {mso-style-noshow:yes;
506        mso-style-priority:99;
507        mso-style-link:"HTML Preformatted Char";
508        margin:0in;
509        margin-bottom:.0001pt;
510        mso-pagination:widow-orphan;
511        tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt;
512        font-size:10.0pt;
513        font-family:"Courier New";
514        mso-fareast-font-family:"Times New Roman";}
515p.MsoAcetate, li.MsoAcetate, div.MsoAcetate
516        {mso-style-noshow:yes;
517        mso-style-priority:99;
518        mso-style-link:"Balloon Text Char";
519        margin:0in;
520        margin-bottom:.0001pt;
521        mso-pagination:widow-orphan;
522        font-size:8.0pt;
523        font-family:"Tahoma","sans-serif";
524        mso-fareast-font-family:"Times New Roman";
525        mso-fareast-theme-font:minor-fareast;}
526span.MsoPlaceholderText
527        {mso-style-noshow:yes;
528        mso-style-priority:99;
529        mso-style-unhide:no;
530        color:gray;}
531p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing
532        {mso-style-noshow:yes;
533        mso-style-priority:1;
534        mso-style-unhide:no;
535        mso-style-qformat:yes;
536        mso-style-parent:"";
537        margin:0in;
538        margin-bottom:.0001pt;
539        mso-pagination:widow-orphan;
540        font-size:12.0pt;
541        font-family:"Times New Roman","serif";
542        mso-fareast-font-family:"Times New Roman";
543        mso-fareast-theme-font:minor-fareast;}
544p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph
545        {mso-style-noshow:yes;
546        mso-style-priority:34;
547        mso-style-unhide:no;
548        mso-style-qformat:yes;
549        margin-top:0in;
550        margin-right:0in;
551        margin-bottom:0in;
552        margin-left:.5in;
553        margin-bottom:.0001pt;
554        mso-add-space:auto;
555        mso-pagination:widow-orphan;
556        font-size:12.0pt;
557        font-family:"Times New Roman","serif";
558        mso-fareast-font-family:"Times New Roman";
559        mso-fareast-theme-font:minor-fareast;}
560p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst
561        {mso-style-noshow:yes;
562        mso-style-priority:34;
563        mso-style-unhide:no;
564        mso-style-qformat:yes;
565        mso-style-type:export-only;
566        margin-top:0in;
567        margin-right:0in;
568        margin-bottom:0in;
569        margin-left:.5in;
570        margin-bottom:.0001pt;
571        mso-add-space:auto;
572        mso-pagination:widow-orphan;
573        font-size:12.0pt;
574        font-family:"Times New Roman","serif";
575        mso-fareast-font-family:"Times New Roman";
576        mso-fareast-theme-font:minor-fareast;}
577p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle
578        {mso-style-noshow:yes;
579        mso-style-priority:34;
580        mso-style-unhide:no;
581        mso-style-qformat:yes;
582        mso-style-type:export-only;
583        margin-top:0in;
584        margin-right:0in;
585        margin-bottom:0in;
586        margin-left:.5in;
587        margin-bottom:.0001pt;
588        mso-add-space:auto;
589        mso-pagination:widow-orphan;
590        font-size:12.0pt;
591        font-family:"Times New Roman","serif";
592        mso-fareast-font-family:"Times New Roman";
593        mso-fareast-theme-font:minor-fareast;}
594p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast
595        {mso-style-noshow:yes;
596        mso-style-priority:34;
597        mso-style-unhide:no;
598        mso-style-qformat:yes;
599        mso-style-type:export-only;
600        margin-top:0in;
601        margin-right:0in;
602        margin-bottom:0in;
603        margin-left:.5in;
604        margin-bottom:.0001pt;
605        mso-add-space:auto;
606        mso-pagination:widow-orphan;
607        font-size:12.0pt;
608        font-family:"Times New Roman","serif";
609        mso-fareast-font-family:"Times New Roman";
610        mso-fareast-theme-font:minor-fareast;}
611span.MsoIntenseReference
612        {mso-style-priority:32;
613        mso-style-unhide:no;
614        mso-style-qformat:yes;
615        font-variant:small-caps;
616        color:#C0504D;
617        mso-themecolor:accent2;
618        letter-spacing:.25pt;
619        font-weight:bold;
620        text-decoration:underline;
621        text-underline:single;}
622span.Heading1Char
623        {mso-style-name:"Heading 1 Char";
624        mso-style-priority:9;
625        mso-style-unhide:no;
626        mso-style-locked:yes;
627        mso-style-link:"Heading 1";
628        mso-ansi-font-size:24.0pt;
629        mso-bidi-font-size:24.0pt;
630        font-family:"Times New Roman","serif";
631        mso-ascii-font-family:"Times New Roman";
632        mso-fareast-font-family:"Times New Roman";
633        mso-fareast-theme-font:minor-fareast;
634        mso-hansi-font-family:"Times New Roman";
635        mso-bidi-font-family:"Times New Roman";
636        mso-font-kerning:18.0pt;
637        font-weight:bold;}
638span.Heading2Char
639        {mso-style-name:"Heading 2 Char";
640        mso-style-noshow:yes;
641        mso-style-priority:9;
642        mso-style-unhide:no;
643        mso-style-locked:yes;
644        mso-style-link:"Heading 2";
645        mso-ansi-font-size:18.0pt;
646        mso-bidi-font-size:18.0pt;
647        font-family:"Times New Roman","serif";
648        mso-ascii-font-family:"Times New Roman";
649        mso-fareast-font-family:"Times New Roman";
650        mso-fareast-theme-font:minor-fareast;
651        mso-hansi-font-family:"Times New Roman";
652        mso-bidi-font-family:"Times New Roman";
653        font-weight:bold;}
654span.Heading3Char
655        {mso-style-name:"Heading 3 Char";
656        mso-style-noshow:yes;
657        mso-style-priority:9;
658        mso-style-unhide:no;
659        mso-style-locked:yes;
660        mso-style-link:"Heading 3";
661        mso-ansi-font-size:13.5pt;
662        mso-bidi-font-size:13.5pt;
663        font-family:"Times New Roman","serif";
664        mso-ascii-font-family:"Times New Roman";
665        mso-fareast-font-family:"Times New Roman";
666        mso-fareast-theme-font:minor-fareast;
667        mso-hansi-font-family:"Times New Roman";
668        mso-bidi-font-family:"Times New Roman";
669        font-weight:bold;}
670span.Heading4Char
671        {mso-style-name:"Heading 4 Char";
672        mso-style-noshow:yes;
673        mso-style-priority:9;
674        mso-style-unhide:no;
675        mso-style-locked:yes;
676        mso-style-link:"Heading 4";
677        mso-ansi-font-size:13.0pt;
678        mso-bidi-font-size:13.0pt;
679        font-family:"Cambria","serif";
680        mso-ascii-font-family:Cambria;
681        mso-ascii-theme-font:major-latin;
682        mso-fareast-font-family:"Times New Roman";
683        mso-fareast-theme-font:major-fareast;
684        mso-hansi-font-family:Cambria;
685        mso-hansi-theme-font:major-latin;
686        mso-bidi-font-family:"Times New Roman";
687        mso-bidi-theme-font:major-bidi;
688        color:#4F81BD;
689        mso-themecolor:accent1;
690        font-weight:bold;
691        font-style:italic;}
692span.Heading5Char
693        {mso-style-name:"Heading 5 Char";
694        mso-style-noshow:yes;
695        mso-style-priority:9;
696        mso-style-unhide:no;
697        mso-style-locked:yes;
698        mso-style-link:"Heading 5";
699        mso-ansi-font-size:12.0pt;
700        mso-bidi-font-size:12.0pt;
701        font-family:"Times New Roman","serif";
702        mso-ascii-font-family:"Times New Roman";
703        mso-fareast-font-family:"Times New Roman";
704        mso-fareast-theme-font:minor-fareast;
705        mso-hansi-font-family:"Times New Roman";
706        mso-bidi-font-family:"Times New Roman";
707        color:#4F4FFF;
708        font-weight:bold;}
709span.HTMLPreformattedChar
710        {mso-style-name:"HTML Preformatted Char";
711        mso-style-noshow:yes;
712        mso-style-priority:99;
713        mso-style-unhide:no;
714        mso-style-locked:yes;
715        mso-style-link:"HTML Preformatted";
716        font-family:"Courier New";
717        mso-ascii-font-family:"Courier New";
718        mso-fareast-font-family:"Times New Roman";
719        mso-hansi-font-family:"Courier New";
720        mso-bidi-font-family:"Courier New";}
721span.DocumentMapChar
722        {mso-style-name:"Document Map Char";
723        mso-style-noshow:yes;
724        mso-style-priority:99;
725        mso-style-unhide:no;
726        mso-style-locked:yes;
727        mso-style-link:"Document Map";
728        mso-ansi-font-size:8.0pt;
729        mso-bidi-font-size:8.0pt;
730        font-family:"Tahoma","sans-serif";
731        mso-ascii-font-family:Tahoma;
732        mso-fareast-font-family:"Times New Roman";
733        mso-fareast-theme-font:minor-fareast;
734        mso-hansi-font-family:Tahoma;
735        mso-bidi-font-family:Tahoma;}
736span.BalloonTextChar
737        {mso-style-name:"Balloon Text Char";
738        mso-style-noshow:yes;
739        mso-style-priority:99;
740        mso-style-unhide:no;
741        mso-style-locked:yes;
742        mso-style-link:"Balloon Text";
743        mso-ansi-font-size:8.0pt;
744        mso-bidi-font-size:8.0pt;
745        font-family:"Tahoma","sans-serif";
746        mso-ascii-font-family:Tahoma;
747        mso-fareast-font-family:"Times New Roman";
748        mso-fareast-theme-font:minor-fareast;
749        mso-hansi-font-family:Tahoma;
750        mso-bidi-font-family:Tahoma;}
751span.SpellE
752        {mso-style-name:"";
753        mso-spl-e:yes;}
754span.GramE
755        {mso-style-name:"";
756        mso-gram-e:yes;}
757.MsoChpDefault
758        {mso-style-type:export-only;
759        mso-default-props:yes;
760        font-size:10.0pt;
761        mso-ansi-font-size:10.0pt;
762        mso-bidi-font-size:10.0pt;
763        font-family:"Calibri","sans-serif";
764        mso-ascii-font-family:Calibri;
765        mso-ascii-theme-font:minor-latin;
766        mso-fareast-font-family:Calibri;
767        mso-fareast-theme-font:minor-latin;
768        mso-hansi-font-family:Calibri;
769        mso-hansi-theme-font:minor-latin;
770        mso-bidi-font-family:"Times New Roman";
771        mso-bidi-theme-font:minor-bidi;}
772@page WordSection1
773        {size:8.5in 11.0in;
774        margin:1.0in 1.0in 1.0in 1.0in;
775        mso-header-margin:.5in;
776        mso-footer-margin:.5in;
777        mso-paper-source:0;}
778div.WordSection1
779        {page:WordSection1;}
780-->
781</style>
782<!--[if gte mso 10]>
783<style>
784 /* Style Definitions */
785 table.MsoNormalTable
786        {mso-style-name:"Table Normal";
787        mso-tstyle-rowband-size:0;
788        mso-tstyle-colband-size:0;
789        mso-style-noshow:yes;
790        mso-style-priority:99;
791        mso-style-parent:"";
792        mso-padding-alt:0in 5.4pt 0in 5.4pt;
793        mso-para-margin:0in;
794        mso-para-margin-bottom:.0001pt;
795        mso-pagination:widow-orphan;
796        font-size:10.0pt;
797        font-family:"Calibri","sans-serif";
798        mso-ascii-font-family:Calibri;
799        mso-ascii-theme-font:minor-latin;
800        mso-hansi-font-family:Calibri;
801        mso-hansi-theme-font:minor-latin;}
802</style>
803<![endif]--><!--[if gte mso 9]><xml>
804 <o:shapedefaults v:ext="edit" spidmax="1026"/>
805</xml><![endif]--><!--[if gte mso 9]><xml>
806 <o:shapelayout v:ext="edit">
807  <o:idmap v:ext="edit" data="1"/>
808 </o:shapelayout></xml><![endif]-->
809</head>
810
811<body lang=EN-US link="#000000" vlink=purple style='tab-interval:.5in'>
812
813<div class=WordSection1>
814
815<p class=MsoNormal><span class=Heading1Char><span style='font-size:24.0pt'>Calibration
816of an area detector in GSAS-II</span></span><b><span style='font-size:14.0pt;
817color:#365F91;mso-themecolor:accent1;mso-themeshade:191'><o:p></o:p></span></b></p>
818
819<p class=MsoNormal>In this tutorial, data collected with a Perkin-Elmer area
820detector at APS 11-ID-C with a wavelength 0.10798 A, where the detector was
821intentionally tilted at 45 degrees, are used. Note that menu entries are listed
822in bold face below as <b style='mso-bidi-font-weight:normal'><span
823style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
824mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
825minor-latin'>Help/About GSAS-II</span></b>, which lists first the name of the
826menu (here <b style='mso-bidi-font-weight:normal'><span style='font-family:
827"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
828minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Help</span></b>)
829and second the name of the entry in the menu (here <b style='mso-bidi-font-weight:
830normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
831minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
832mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).</p>
833
834<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
835href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
836text-underline:none'>start GSAS-II</span></a></span></u>.</p>
837
838<h1>Step 1: read in the data file</h1>
839
840<p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the <b
841style='mso-bidi-font-weight:normal'>Data/Read image data</b> menu item to read
842the data file into the current GSAS-II project. </p>
843
844<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
845
846<p class=MsoNormal>A file selection dialog will be shown; its appearance will
847depend on your OS. Change the search directory to <b style='mso-bidi-font-weight:
848normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
849minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
850mso-bidi-theme-font:minor-latin'>/Exercises/images</span></b> and then select
851the file </p>
852
853<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
854style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
855mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
856minor-latin'>La_hex_+45deg-00015.tif</span></b> and press <b style='mso-bidi-font-weight:
857normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
858minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
859mso-bidi-theme-font:minor-latin'>Open</span></b>.<span style='mso-no-proof:
860yes'> <o:p></o:p></span></p>
861
862<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype
863 id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t"
864 path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f">
865 <v:stroke joinstyle="miter"/>
866 <v:formulas>
867  <v:f eqn="if lineDrawn pixelLineWidth 0"/>
868  <v:f eqn="sum @0 1 0"/>
869  <v:f eqn="sum 0 0 @1"/>
870  <v:f eqn="prod @2 1 2"/>
871  <v:f eqn="prod @3 21600 pixelWidth"/>
872  <v:f eqn="prod @3 21600 pixelHeight"/>
873  <v:f eqn="sum @0 0 1"/>
874  <v:f eqn="prod @6 1 2"/>
875  <v:f eqn="prod @7 21600 pixelWidth"/>
876  <v:f eqn="sum @8 21600 0"/>
877  <v:f eqn="prod @7 21600 pixelHeight"/>
878  <v:f eqn="sum @10 21600 0"/>
879 </v:formulas>
880 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
881 <o:lock v:ext="edit" aspectratio="t"/>
882</v:shapetype><v:shape id="_x0000_i1032" type="#_x0000_t75" style='width:300pt;
883 height:187.5pt;visibility:visible;mso-wrap-style:square'>
884 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png"
885  o:title=""/>
886</v:shape><![endif]--><![if !vml]><img border=0 width=400 height=250
887src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png"
888v:shapes="_x0000_i1032"><![endif]></span></p>
889
890<p class=MsoNormal>At this point the data tree window will have several
891entries; the highlighted one specifies the contents of the data window as <b
892style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
893mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
894Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span><o:p></o:p></b></p>
895
896<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
897 id="Picture_x0020_10" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:472.5pt;
898 height:342pt;visibility:visible;mso-wrap-style:square'>
899 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png"
900  o:title=""/>
901</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=456
902src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png"
903v:shapes="Picture_x0020_10"><![endif]></span></p>
904
905<p class=MsoNormal><span style='mso-spacerun:yes'> </span>The plot window shows
906the image; notice the elliptical shape of the powder diffraction rings
907due to the 45 degree detector tilt. The
908blue <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
909mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
910Calibri;mso-bidi-theme-font:minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span></b>
911marks the beam location (which defaults to the image center); the
912calibration you will perform here will find the correct
913placement for it. Also note that as the mouse is moved across the plot
914the plot window status bar (at bottom of plot window) shows the
915cursor position, as computed from the default (incorrect)
916calibration values. These constants will be correctly determined after you finish the calibration.</p>
917
918<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
919style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_11"
920 o:spid="_x0000_i1030" type="#_x0000_t75" style='width:525pt;height:450pt;
921 visibility:visible;mso-wrap-style:square'>
922 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
923  o:title=""/>
924</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
925src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
926v:shapes="Picture_x0020_11"><![endif]></span></p>
927
928<h1><span style='mso-spacerun:yes'> </span>Step 2: Edit image parameters</h1>
929
930<p class=MsoNormal><span style='mso-spacerun:yes'> </span>Note that, alas, very
931few image formats contain all of the important metadata about the image, so it
932needs to be added manually. In this case set the <b style='mso-bidi-font-weight:
933normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
934minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
935mso-bidi-theme-font:minor-latin'>wavelength</span></b> to <b style='mso-bidi-font-weight:
936normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
937minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
938mso-bidi-theme-font:minor-latin'>0.10798</span></b>. It is also helpful to
939change the display of the image so that it is easier to see the diffraction
940rings. Lowering the maximum intensity to 10,000 to 20,000 counts will help
941(note that this can be done by moving the <span class=GramE>slider,</span> or
942by typing a value in the box and then clicking on another control or pressing
943the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
944mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
945Calibri;mso-bidi-theme-font:minor-latin'>Enter</span></b> or <b
946style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
947mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
948Calibri;mso-bidi-theme-font:minor-latin'>Tab</span></b> key). You may also wish
949to select another color scheme using the <b style='mso-bidi-font-weight:normal'><span
950style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
951mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
952minor-latin'>Color bar</span></b> selector. </p>
953
954<h1><span style='mso-spacerun:yes'> </span>Step 3: Calibrate</h1>
955
956<h3><span style='mso-spacerun:yes'> </span>First: </h3>
957
958<p class=MsoNormal><span style='mso-spacerun:yes'>   </span>Set the material
959used as a sample in the box labeled <span class=SpellE><b style='mso-bidi-font-weight:
960normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
961minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
962mso-bidi-theme-font:minor-latin'>Calibrant</span></b></span>; select <b
963style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
964mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
965Calibri;mso-bidi-theme-font:minor-latin'>LaB6 SRM660a</span></b></p>
966
967<h3><span style='mso-spacerun:yes'> </span>Second: </h3>
968
969<p class=MsoNormal><span style='mso-spacerun:yes'>   </span>Use the <b
970style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
971mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
972Calibri;mso-bidi-theme-font:minor-latin'>Operations/Calibrate</span></b> menu
973item (note this menu is on the <b style='mso-bidi-font-weight:normal'><span
974style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
975mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
976minor-latin'>Image Controls</span></b> window or for the Mac, the <span
977class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family:
978"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
979minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Image<span
980style='mso-spacerun:yes'>  </span>Controls</span></b></span> window must be
981active to place this into the system menu bar). At this point the status line
982on the bottom of the <b style='mso-bidi-font-weight:normal'><span
983style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
984mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
985minor-latin'>Image Controls</span></b> window changes with a prompt to select
986points for calibration.</p>
987
988<h3>Third: </h3>
989
990<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>Use the left mouse
991button to click on at least five locations on the innermost ring. As each point
992is defined, a red &quot;<b style='mso-bidi-font-weight:normal'><span
993style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
994mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
995minor-latin;color:red'>+</span></b>&quot; is added to the plot. You need not
996hit the ring exactly as the code will search for the locally highest
997point. (On the Mac with a two or three button mouse, also use the left
998mouse button, or with a standard Mac single-button mouse, use the
999regular mouse button.)</p>
1000
1001<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1002 id="Picture_x0020_8" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt;
1003 height:450pt;visibility:visible;mso-wrap-style:square'>
1004 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
1005  o:title=""/>
1006</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1007src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
1008v:shapes="Picture_x0020_8"><![endif]></span></p>
1009
1010<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>To remove a point
1011added in error click on that point with the right mouse button
1012(on the Mac, if you have a single-button mouse, hold the control key
1013down and click).
1014</p>
1015
1016<h3><span style='mso-spacerun:yes'> </span>Fourth:</h3>
1017
1018<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>When done, press the
1019right mouse button well away from any points that have been added
1020(on the Mac, if you have a single-button mouse, hold the control key
1021down and click).
1022</p>
1023
1024<p class=MsoNormal>The calibration is then performed. First the rings are
1025located and an ellipse is optimized for each ring. The indexed rings are first
1026shown in red as the calibration proceeds and center of each ellipse is noted
1027with a blue &quot;<b style='mso-bidi-font-weight:normal'><span
1028style='color:#4F81BD;mso-themecolor:accent1'>+</span></b>&quot;. When all rings
1029have been fitted, the entire ensemble of rings is refitted to the detector
1030parameters and the rings are then shown in blue. The beam position (blue “<span
1031style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
1032mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1033minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span>”) is now correctly
1034positioned.</p>
1035
1036<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
1037style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_9"
1038 o:spid="_x0000_i1028" type="#_x0000_t75" style='width:525pt;height:450pt;
1039 visibility:visible;mso-wrap-style:square'>
1040 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
1041  o:title=""/>
1042</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1043src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
1044v:shapes="Picture_x0020_9"><![endif]></span><span
1045style='mso-spacerun:yes'> </span></p>
1046
1047<p class=MsoNormal>The derived calibration results are shown in the <b
1048style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
1049mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1050Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window.</p>
1051
1052<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1053 id="Picture_x0020_13" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:472.5pt;
1054 height:342pt;visibility:visible;mso-wrap-style:square'>
1055 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png"
1056  o:title=""/>
1057</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=456
1058src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png"
1059v:shapes="Picture_x0020_13"><![endif]></span><span
1060style='mso-spacerun:yes'> </span></p>
1061
1062<p class=MsoNormal><span class=GramE>and</span> the console window shows
1063details of the fit.</p>
1064
1065<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1066 id="Picture_x0020_14" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:396.75pt;
1067 height:134.25pt;visibility:visible;mso-wrap-style:square'>
1068 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
1069  o:title=""/>
1070</v:shape><![endif]--><![if !vml]><img border=0 width=529 height=179
1071src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
1072v:shapes="Picture_x0020_14"><![endif]></span></p>
1073
1074<p class=MsoNormal><span style='mso-spacerun:yes'> </span>To see the actual
1075points selected by the program, click on the <b style='mso-bidi-font-weight:
1076normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
1077minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1078mso-bidi-theme-font:minor-latin'>show ring picks?</span></b> <span class=GramE>check</span>
1079box </p>
1080
1081<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1082 id="Picture_x0020_15" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt;
1083 height:450pt;visibility:visible;mso-wrap-style:square'>
1084 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
1085  o:title=""/>
1086</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1087src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
1088v:shapes="Picture_x0020_15"><![endif]></span><span
1089style='mso-spacerun:yes'> </span><span style='color:#1F497D;mso-themecolor:
1090text2'><o:p></o:p></span></p>
1091
1092<p class=MsoNormal>When this is done, it sometimes occurs that the points
1093selected for the outermost rings are scattered between that and the next ring.
1094This can be repaired by changing the pixel search range to 10 and using the <b
1095style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
1096mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1097Calibri;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b> menu
1098item.</p>
1099
1100<p class=MsoNormal>Assuming that these calibration results will be applied to
1101other images in the same GSAS-II project, click on <b style='mso-bidi-font-weight:
1102normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
1103minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1104mso-bidi-theme-font:minor-latin'>Use as default for all images</span></b>. You
1105may also save a copy of the calibration values to a file <span
1106style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
1107mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1108minor-latin'>(<span class=SpellE><i style='mso-bidi-font-style:normal'>name</i><b
1109style='mso-bidi-font-weight:normal'>.imctrl</b></span></span>) with the <b
1110style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
1111mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1112Calibri;mso-bidi-theme-font:minor-latin'>Operations/Save Controls</span></b>
1113menu item. To save the project, including the now-derived calibration information,
1114use the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
1115mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1116Calibri;mso-bidi-theme-font:minor-latin'>File/Save</span> </b><b
1117style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri","sans-serif";
1118mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1119Calibri;mso-bidi-theme-font:minor-latin'>Project</span></b><span
1120style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:minor-latin;
1121mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1122minor-latin'> </span>menu item associated with the data tree window; as this
1123project has not been saved before the file save dialog will need a file name.
1124Don’t enter the extension; it will be set to “<b style='mso-bidi-font-weight:
1125normal'><span style='font-family:"Calibri","sans-serif";mso-ascii-theme-font:
1126minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1127mso-bidi-theme-font:minor-latin'>.<span class=SpellE>gpx</span></span></b>”.</p>
1128
1129<h2>Next step: <span class=MsoHyperlink><span style='color:#0070C0'><a
1130href="Integration%20of%20area%20detector%20data%20in%20GSAS.htm"><u><span
1131style='color:black'>Integrate the Data</span></u></a></span></span></h2>
1132
1133</div>
1134
1135</body>
1136
1137</html>
Note: See TracBrowser for help on using the repository browser.