| 1 | VERSION 6 Mon Feb 14 10:36:18 2005 |
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| 2 | DESCR sucrose |
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| 3 | HSTRY 1 EXPEDT Win32 Feb 14 10:42:08 2005 P PH |
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| 4 | HSTRY 2 POWPREF Win32 Feb 14 10:42:24 2005 |
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| 5 | HSTRY 3 POWPREF Win32 Oct 03 10:14:31 2006 |
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| 6 | HSTRY 4 GENLES Win32 Oct 03 10:14:39 2006 Sdsq= 0.307E+04 S/E= 0.794 |
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| 7 | HSTRY 5 EXPEDT Win32 Oct 03 11:09:30 2006 P H |
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| 8 | HSTRY 6 POWPREF Win32 Oct 03 11:09:39 2006 |
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| 9 | HSTRY 7 GENLES Win32 Oct 03 11:09:43 2006 Sdsq= 0.683E+07 S/E= 0.436E-04 |
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| 10 | HSTRY 8 EXPEDT Win32 Oct 03 13:13:47 2006 L O |
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| 11 | HSTRY 9 EXPEDT Win32 Oct 03 13:16:56 2006 L LO |
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| 12 | HSTRY 10 GENLES Win32 Oct 03 13:17:01 2006 Sdsq= 0.323E+07 S/E= 313. |
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| 13 | HSTRY 11 EXPEDT Win32 Oct 03 13:18:07 2006 L O |
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| 14 | HSTRY 12 GENLES Win32 Oct 03 13:18:12 2006 Sdsq= 0.830E+06 S/E= 139. |
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| 15 | HSTRY 13 EXPEDT Win32 Oct 03 13:20:58 2006 L O |
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| 16 | HSTRY 14 GENLES Win32 Oct 03 13:21:07 2006 Sdsq= 0.713E+06 S/E= 40.3 |
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| 17 | HSTRY 15 EXPEDT Win32 Oct 03 13:23:46 2006 P H |
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| 18 | HSTRY 16 POWPREF Win32 Oct 03 13:23:50 2006 |
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| 19 | HSTRY 17 GENLES Win32 Oct 03 13:23:56 2006 Sdsq= 0.338E+06 S/E= 33.6 |
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| 20 | HSTRY 18 GENLES Win32 Oct 03 13:24:03 2006 Sdsq= 0.331E+06 S/E= 22.4 |
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| 21 | HSTRY 19 EXPEDT Win32 Oct 03 13:24:33 2006 File cleanup only |
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| 22 | HSTRY 20 GENLES Win32 Oct 03 13:25:03 2006 Sdsq= 0.328E+06 S/E= 16.3 |
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| 23 | HSTRY 21 EXPEDT Win32 Oct 03 13:26:21 2006 L O |
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| 24 | HSTRY 22 GENLES Win32 Oct 03 13:26:25 2006 Sdsq= 0.327E+06 S/E= 11.0 |
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| 25 | HSTRY 23 EXPTOOL Win32 Oct 03 13:48:10 2006 P P |
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| 26 | HSTRY 24 EXPEDT Win32 Oct 03 13:49:19 2006 P P |
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| 27 | HSTRY 25 EXPEDT Win32 Oct 03 13:50:19 2006 P P |
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| 28 | HSTRY 26 EXPGUI 1.75 1.42 (46 changes) -- 10/03/06 13:50:56 |
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| 29 | HSTRY 27 EXPTOOL Win32 Oct 03 13:50:56 2006 P A |
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| 30 | HSTRY 28 EXPGUI 1.75 1.42 (3 changes) -- 10/03/06 13:51:45 |
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| 31 | HSTRY 29 POWPREF Win32 Oct 03 13:51:46 2006 |
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| 32 | HSTRY 30 GENLES Win32 Oct 03 13:51:53 2006 Sdsq= 0.451E+06 S/E= 0.131 |
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| 33 | HSTRY 31 EXPGUI 1.75 1.42 (4 changes) -- 10/03/06 13:53:03 |
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| 34 | HSTRY 32 GENLES Win32 Oct 03 13:53:04 2006 Sdsq= 0.202E+06 S/E= 6.49 |
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| 35 | HSTRY 33 EXPGUI 1.75 1.42 (8 changes) -- 10/03/06 13:54:39 |
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| 36 | HSTRY 34 GENLES Win32 Oct 03 13:54:41 2006 Sdsq= 0.147E+06 S/E= 0.117 |
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| 37 | HSTRY 35 EXPGUI 1.75 1.42 (2 changes) -- 10/03/06 13:55:13 |
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| 38 | HSTRY 36 GENLES Win32 Oct 03 13:55:14 2006 Sdsq= 0.146E+06 S/E= 0.539 |
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| 39 | HSTRY 37 EXPGUI 1.75 1.42 (2 changes) -- 10/03/06 13:55:27 |
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| 40 | HSTRY 38 GENLES Win32 Oct 03 13:55:30 2006 Sdsq= 0.145E+06 S/E= 0.603 |
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| 41 | HSTRY 39 EXPGUI 1.75 1.42 (1 changes) -- 10/03/06 13:55:43 |
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| 42 | HSTRY 40 GENLES Win32 Oct 03 13:55:45 2006 Sdsq= 0.543E+05 S/E= 3.48 |
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| 43 | HSTRY 41 EXPGUI 1.75 1.42 (1 changes) -- 10/03/06 13:56:58 |
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| 44 | HSTRY 42 GENLES Win32 Oct 03 13:57:01 2006 Sdsq= 0.275E+05 S/E= 11.9 |
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| 45 | HSTRY 43 EXPEDT Win32 Apr 04 13:47:35 2007 L L |
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| 46 | HSTRY 44 GENLES Win32 Apr 04 13:47:40 2007 Sdsq= 0.272E+05 S/E= 9.33 |
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| 47 | HSTRY 45 GENLES Win32 Apr 04 13:49:29 2007 Sdsq= 0.264E+05 S/E= 7.42 |
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| 48 | HSTRY 46 EXPEDT Win32 Apr 04 13:49:56 2007 L O |
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| 49 | HSTRY 47 GENLES Win32 Apr 04 13:50:00 2007 Sdsq= 0.249E+05 S/E= 1.13 |
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| 50 | HSTRY 48 GENLES Win32 Apr 04 14:35:43 2007 Sdsq= 0.249E+05 S/E= 0.682 |
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| 51 | HSTRY 49 EXPEDT Win32 May 28 09:08:34 2007 LA |
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| 52 | HSTRY 50 EXPEDT Win32 Sep 30 16:22:17 2007 L O |
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| 53 | HSTRY 51 EXPEDT Win32 Sep 30 16:25:23 2007 L O |
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| 54 | HSTRY 52 EXPEDT Win32 Oct 19 09:36:53 2011 LA |
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| 55 | DSGL CDAT1 DRAD ARAD NOFO |
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| 56 | DSGL CDAT2 DRAD ARAD NOFO |
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| 57 | GNLS RUN on Apr 04 14:35:43 2007 Total cycles run 167 24879. |
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| 58 | GNLS CDAT1 MXCY 9 MARQ1.02PRNT1024 |
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| 59 | GNLS SHFTS 0.32 0.04 |
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| 60 | AFAC C 2.310020.8439 1.020010.2075 1.5886 .5687 .865051.6512 .2156 RHF |
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| 61 | AFAC C_ 12.011 .6648 .0035 |
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| 62 | AFAC C_SIZ 1.12 0.92 1.65 3 |
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| 63 | AFAC C_XAB 288.3 170.4 84.13 10.67 7.054 52.30 141.0 |
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| 64 | AFAC C_XF1 0.036 0.027 0.018 0.003 0.002 0.049 0.024-0.001-0.001-0.001 |
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| 65 | AFAC C_XF2 0.021 0.015 0.009 0.002 0.001 0.031 0.012 0.000 0.000 0.000 |
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| 66 | AFAC H .49300210.5109.32291226.1257.1401913.14236.04081057.7997.003038 SDS |
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| 67 | AFAC H_ 1.008-.3741 20.6 19.2 |
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| 68 | AFAC H_SIZ 0.98 0.78 1.20 118 |
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| 69 | AFAC H_XAB .6888 .6700 .6548 .6238 .6131 .7240 .6640 |
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| 70 | AFAC H_XF1 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. |
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| 71 | AFAC H_XF2 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. |
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| 72 | AFAC O 3.048513.2771 2.2868 5.7011 1.5463 .3239 .867032.9089 .2508 RHF |
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| 73 | AFAC O_ 15.999 .5805 .00019 |
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| 74 | AFAC O_SIZ 1.09 0.89 1.45 96 1.40 |
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| 75 | AFAC O_XAB 988.0 590.6 293.1 30.48 17.21 1730. 478.0 |
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| 76 | AFAC O_XF1 0.093 0.072 0.049 0.011 0.006 0.121 0.063-0.002-0.003-0.003 |
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| 77 | AFAC O_XF2 0.073 0.052 0.032 0.006 0.004 0.106 0.044 0.000 0.000 0.000 |
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| 78 | EXPR HTYP1 PXC |
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| 79 | EXPR NATYP 3 |
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| 80 | EXPR NHST 1 |
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| 81 | EXPR ATYP 1 O 11 1.09 0.89 1.45 96 1.40 |
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| 82 | EXPR ATYP 2 C 12 1.12 0.92 1.65 3 |
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| 83 | EXPR ATYP 3 H 22 0.98 0.78 1.20 118 |
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| 84 | EXPR NPHAS 1 0 0 0 0 0 0 0 0 |
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| 85 | REFN GDNFT Reduced CHI**2 = 7.133 for 125 variables |
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| 86 | REFN RPOWD 0.0234 0.0196 3613 24879. |
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| 87 | REFN STATS Cycle 167 There were 3613 observations. Total CHI**2 = 2.4879E+04 |
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| 88 | CRS1 PNAM SUCROSE |
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| 89 | CRS1 NATOM 45 |
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| 90 | CRS1 ABC 10.863168 8.703946 7.757701 Y 0 |
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| 91 | CRS1 ABCSIG 0.000153 0.000120 0.000107 |
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| 92 | CRS1 ANGLES 90.0000 102.9426 90.0000 |
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| 93 | CRS1 ANGSIG 0.0000 0.0005 0.0000 |
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| 94 | CRS1 AT 1A O -0.164254 -0.157852 0.607290 1.000000O1 2 000 |
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| 95 | CRS1 AT 1B 0.040561 I XU |
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| 96 | CRS1 AT 2A O -0.231485 -0.061788 0.265443 1.000000O2 2 000 |
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| 97 | CRS1 AT 2B 0.057560 I XU |
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| 98 | CRS1 AT 3A O -0.295166 0.245759 0.317444 1.000000O3 2 000 |
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| 99 | CRS1 AT 3B 0.109726 I XU |
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| 100 | CRS1 AT 4A O -0.340114 0.326551 0.654647 1.000000O4 2 000 |
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| 101 | CRS1 AT 4B 0.138454 I XU |
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| 102 | CRS1 AT 5A O -0.392465 -0.103270 0.623136 1.000000O5 2 000 |
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| 103 | CRS1 AT 5B 0.028472 I XU |
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| 104 | CRS1 AT 6A O -0.576481 0.051765 0.726621 1.000000O6 2 000 |
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| 105 | CRS1 AT 6B 0.047865 I XU |
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| 106 | CRS1 AT 7A O -0.026064 -0.269992 0.384540 1.000000O11 2 000 |
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| 107 | CRS1 AT 7B 0.067787 I XU |
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| 108 | CRS1 AT 8A O -0.219269 -0.443970 0.672126 1.000000O21 2 000 |
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| 109 | CRS1 AT 8B 0.053494 I XU |
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| 110 | CRS1 AT 9A O 0.067388 -0.191789 0.783754 1.000000O31 2 000 |
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| 111 | CRS1 AT 9B 0.061425 I XU |
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| 112 | CRS1 AT 10A O 0.018320 -0.397973 1.080663 1.000000O41 2 000 |
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| 113 | CRS1 AT 10B 0.111212 I XU |
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| 114 | CRS1 AT 11A O -0.328317 -0.287414 0.964056 1.000000O61 2 000 |
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| 115 | CRS1 AT 11B 0.096466 I XU |
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| 116 | CRS1 AT 12A C -0.299305 -0.166713 0.523976 1.000000C1 2 000 |
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| 117 | CRS1 AT 12B 0.021275 I XU |
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| 118 | CRS1 AT 13A C -0.333469 -0.017226 0.345055 1.000000C2 2 000 |
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| 119 | CRS1 AT 13B 0.019679 I XU |
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| 120 | CRS1 AT 14A C -0.267194 0.121736 0.461451 1.000000C3 2 000 |
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| 121 | CRS1 AT 14B 0.018025 I XU |
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| 122 | CRS1 AT 15A C -0.374575 0.172912 0.565194 1.000000C4 2 000 |
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| 123 | CRS1 AT 15B 0.000268 I XU |
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| 124 | CRS1 AT 16A C -0.349910 0.106966 0.716598 1.000000C5 2 000 |
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| 125 | CRS1 AT 16B 0.032578 I XU |
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| 126 | CRS1 AT 17A C -0.446764 0.038868 0.802935 1.000000C6 2 000 |
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| 127 | CRS1 AT 17B 0.022298 I XU |
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| 128 | CRS1 AT 18A C -0.102176 -0.408149 0.454657 1.000000C11 2 000 |
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| 129 | CRS1 AT 18B 0.002823 I XU |
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| 130 | CRS1 AT 19A C -0.117978 -0.322890 0.643846 1.000000C21 2 000 |
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| 131 | CRS1 AT 19B -0.019107 I XU |
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| 132 | CRS1 AT 20A C -0.014363 -0.345739 0.794304 1.000000C31 2 000 |
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| 133 | CRS1 AT 20B 0.095309 I XU |
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| 134 | CRS1 AT 21A C -0.076372 -0.348567 0.921647 1.000000C41 2 000 |
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| 135 | CRS1 AT 21B 0.001039 I XU |
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| 136 | CRS1 AT 22A C -0.197330 -0.436359 0.845452 1.000000C51 2 000 |
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| 137 | CRS1 AT 22B 0.047428 I XU |
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| 138 | CRS1 AT 23A C -0.285790 -0.475785 0.972198 1.000000C61 2 000 |
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| 139 | CRS1 AT 23B 0.002722 I XU |
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| 140 | CRS1 AT 24A H -0.334700 -0.254900 0.461200 1.000000H1 2 000 |
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| 141 | CRS1 AT 24B 0.029000 I |
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| 142 | CRS1 AT 25A H -0.411600 -0.030700 0.288300 1.000000H2 2 000 |
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| 143 | CRS1 AT 25B 0.035000 I |
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| 144 | CRS1 AT 26A H -0.187100 0.144800 0.510300 1.000000H3 2 000 |
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| 145 | CRS1 AT 26B 0.037200 I |
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| 146 | CRS1 AT 27A H -0.471700 0.168100 0.478200 1.000000H4 2 000 |
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| 147 | CRS1 AT 27B 0.037700 I |
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| 148 | CRS1 AT 28A H -0.263800 0.061300 0.790700 1.000000H5 2 000 |
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| 149 | CRS1 AT 28B 0.038200 I |
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| 150 | CRS1 AT 29A H -0.453100 0.187300 0.865600 1.000000H6 2 000 |
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| 151 | CRS1 AT 29B 0.053800 I |
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| 152 | CRS1 AT 30A H -0.052000 -0.477600 0.478400 1.000000H11 2 000 |
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| 153 | CRS1 AT 30B 0.044400 I |
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| 154 | CRS1 AT 31A H -0.194700 -0.390900 0.367000 1.000000H12 2 000 |
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| 155 | CRS1 AT 31B 0.041000 I |
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| 156 | CRS1 AT 32A H -0.271900 -0.127700 0.153400 1.000000H23 2 000 |
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| 157 | CRS1 AT 32B 0.041600 I |
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| 158 | CRS1 AT 33A H 0.049500 -0.411600 0.771000 1.000000H31 2 000 |
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| 159 | CRS1 AT 33B 0.030400 I |
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| 160 | CRS1 AT 34A H -0.231800 0.266000 0.257500 1.000000H33 2 000 |
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| 161 | CRS1 AT 34B 0.048500 I |
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| 162 | CRS1 AT 35A H -0.098400 -0.222800 0.984500 1.000000H41 2 000 |
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| 163 | CRS1 AT 35B 0.031700 I |
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| 164 | CRS1 AT 36A H -0.340700 0.391300 0.567500 1.000000H43 2 000 |
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| 165 | CRS1 AT 36B 0.088000 I |
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| 166 | CRS1 AT 37A H -0.146500 -0.559900 0.886800 1.000000H51 2 000 |
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| 167 | CRS1 AT 37B 0.035200 I |
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| 168 | CRS1 AT 38A H -0.437200 -0.007400 0.928100 1.000000H61 2 000 |
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| 169 | CRS1 AT 38B 0.055100 I |
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| 170 | CRS1 AT 39A H -0.265100 -0.460100 1.088700 1.000000H62 2 000 |
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| 171 | CRS1 AT 39B 0.049600 I |
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| 172 | CRS1 AT 40A H -0.601500 -0.061700 0.713400 1.000000H63 2 000 |
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| 173 | CRS1 AT 40B 0.050600 I |
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| 174 | CRS1 AT 41A H -0.084500 -0.175300 0.345800 1.000000H101 2 000 |
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| 175 | CRS1 AT 41B 0.040700 I |
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| 176 | CRS1 AT 42A H 0.031000 -0.091100 0.823900 1.000000H301 2 000 |
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| 177 | CRS1 AT 42B 0.037000 I |
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| 178 | CRS1 AT 43A H 0.016700 -0.346200 1.196100 1.000000H401 2 000 |
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| 179 | CRS1 AT 43B 0.038200 I |
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| 180 | CRS1 AT 44A H -0.347700 -0.222000 0.839700 1.000000H601 2 000 |
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| 181 | CRS1 AT 44B 0.045000 I |
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| 182 | CRS1 AT 45A H -0.367200 -0.488100 0.880500 1.000000H611 2 000 |
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| 183 | CRS1 AT 45B 0.054800 I |
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| 184 | CRS1 CELVOL 714.875 0.027 |
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| 185 | CRS1 CHMF 1 O 11.00 |
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| 186 | CRS1 CHMF 2 C 12.00 |
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| 187 | CRS1 CHMF 3 H 22.00 |
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| 188 | CRS1 SG SYM P 1 21 1 |
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| 189 | CRS1 SPAXIS 0 0 1 |
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| 190 | HAP1 1 ZONE 0 0 0 0 |
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| 191 | HAP1 1EXTPOW 0.00000E+00 N 0 |
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| 192 | HAP1 1NAXIS 1 |
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| 193 | HAP1 1PHSFR 1.0000 N 0 |
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| 194 | HAP1 1PRCF 5 17 0.005 YY YY Y YY |
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| 195 | HAP1 1PRCF 1 0.000000E+00 -0.998165E+00 0.202298E+01 0.000000E+00 |
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| 196 | HAP1 1PRCF 2 0.985688E+00 0.209294E+01 0.100000E-02 0.100000E-02 |
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| 197 | HAP1 1PRCF 3 -0.429964E+01 0.000000E+00 0.697807E+01 -0.726388E+00 |
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| 198 | HAP1 1PRCF 4 0.000000E+00 0.000000E+00 0.000000E+00 0.000000E+00 |
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| 199 | HAP1 1PRCF 5 0.000000E+00 |
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| 200 | HAP1 1PREFO1 1.000000 1.000000 0.000000 0.000000 1.000000 NN 0 0 |
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| 201 | HAP1 1RADDAM 0.00000E+00 N 0 0.00 |
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| 202 | HST 1 HFIL C:\RBVD\sucrose\sucrose_1sec_A_0.GSA |
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| 203 | HST 1 HNAM F:\Oct_2003\disk1\sucrose_std_745mm_0.mar3450: Azimuth/2-theta |
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| 204 | HST 1 IFIL C:\RBVD\sucrose\inst_xry.prm |
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| 205 | HST 1 BANK 1 |
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| 206 | HST 1 BIGFO 0.166072E+06 |
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| 207 | HST 1 CHANS 1386 1 3613 30744340 5000 |
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| 208 | HST 1 EPHAS 0 0 0 0 0 0 0 0 0 Y |
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| 209 | HST 1 ICONR 0.6194280 0.0000000 -0.13099 Z 0 0.95000 0 0.50000 |
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| 210 | HST 1 ICONS 0.6194280 0.0000000 -1.84763 Z 0 0.95000 0 0.50000 |
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| 211 | HST 1 IRAD 0 |
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| 212 | HST 1 MAXRF 8 |
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| 213 | HST 1 NEXC 2 |
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| 214 | HST 1 NPHAS 1 0 0 0 0 0 0 0 0 |
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| 215 | HST 1 NREF 133 1.8765 Y Y |
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| 216 | HST 1 R-FAC 123 0.01160 5.233365E+04 |
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| 217 | HST 1 RPOWD 0.0234 0.0196 3613 24879. |
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| 218 | HST 1 TRNGE 7.00092 18.91080 |
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| 219 | HST 1 WREXP 0.0089 |
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| 220 | HST 1ABSCOR 0.000000E+00 0.000000E+00 N 0 |
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| 221 | HST 1BAKGD 7 20 Y 0 Y |
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| 222 | HST 1BAKGD1 0.422923E+04 0.425598E+04 0.378613E+04 0.304949E+04 |
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| 223 | HST 1BAKGD2 0.280152E+04 0.260038E+04 0.221872E+04 0.194238E+04 |
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| 224 | HST 1BAKGD3 0.176586E+04 0.165544E+04 0.148281E+04 0.143475E+04 |
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| 225 | HST 1BAKGD4 0.137137E+04 0.133823E+04 0.130461E+04 0.116757E+04 |
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| 226 | HST 1BAKGD5 0.112117E+04 0.104554E+04 0.102951E+04 0.102649E+04 |
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| 227 | HST 1CHI 0.00 |
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| 228 | HST 1EXC 1 0.000 7.000 |
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| 229 | HST 1EXC 2 19.000 1000.000 |
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| 230 | HST 1EXMNMX 1.00000 1.00000 |
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| 231 | HST 1FFANS1 O 0.000 0.000 NN 0 |
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| 232 | HST 1FFANS2 C 0.000 0.000 NN 0 |
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| 233 | HST 1FFANS3 H 0.000 0.000 NN 0 |
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| 234 | HST 1HSCALE 54.989 Y 0 |
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| 235 | HST 1I HEAD DUMMY INCIDENT SPECTRUM FOR X-RAY DIFFRACTOMETER |
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| 236 | HST 1I ITYP 0 0.0000 180.0000 1 |
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| 237 | HST 1MNREF 0 1.9792 |
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| 238 | HST 1ODMNMX 1.00000 1.00000 |
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| 239 | HST 1PRCF1 5 8 0.005 |
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| 240 | HST 1PRCF11 0.000000E+00 0.418369E+01 0.162835E+01 0.000000E+00 |
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| 241 | HST 1PRCF12 0.000000E+00 0.000000E+00 0.010000E-01 0.010000E-01 |
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| 242 | HST 1RSP 0.0308 0.0199 0.0274 0.0097 0.0113 0.0094 0.0119 0.0086 0.0106 |
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| 243 | HST 1RSPA 0.0455 0.0310 0.0354 0.0146 0.0124 0.0091 0.0123 0.0092 0.0102 |
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| 244 | HST 1RSPTT 7.00 8.32 9.65 10.97 12.29 13.62 14.94 16.26 17.59 18.91 |
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| 245 | HST 1RSPW 0.0463 0.0259 0.0352 0.0137 0.0144 0.0125 0.0149 0.0110 0.0138 |
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| 246 | HST 1RSPWA 0.0629 0.0390 0.0449 0.0176 0.0146 0.0112 0.0153 0.0105 0.0116 |
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| 247 | HST 1TRMNMX 1.00000 1.00000 |
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| 248 | ZZZZZZZZZZZZ Last EXP file record |
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