source: Tutorials/TOF Sequential Single Peak Fit/TOF Sequential Single Peak Fit.htm @ 5000

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add data link to tutorials

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413  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
414  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
415  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
416  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
417  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
418  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
419  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
420  <w:LsdException Locked="false" Priority="34" QFormat="true"
421   Name="List Paragraph"/>
422  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
423  <w:LsdException Locked="false" Priority="30" QFormat="true"
424   Name="Intense Quote"/>
425  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
426  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
427  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
428  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
429  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
430  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
431  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
432  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
433  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
434  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
435  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
436  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
437  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
438  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
439  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
440  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
441  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
442  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
443  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
444  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
445  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
446  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
447  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
448  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
449  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
450  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
451  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
452  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
453  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
454  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
455  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
456  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
457  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
458  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
459  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
460  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
461  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
462  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
463  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
464  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
465  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
466  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
467  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
468  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
469  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
470  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
471  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
472  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
473  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
474  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
475  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
476  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
477  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
478  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
479  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
480  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
481  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
482  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
483  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
484  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
485  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
486  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
487  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
488  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
489  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
490  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
491  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
492  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
493  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
494  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
495  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
496  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
497  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
498  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
499  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
500  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
501  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
502  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
503  <w:LsdException Locked="false" Priority="19" QFormat="true"
504   Name="Subtle Emphasis"/>
505  <w:LsdException Locked="false" Priority="21" QFormat="true"
506   Name="Intense Emphasis"/>
507  <w:LsdException Locked="false" Priority="31" QFormat="true"
508   Name="Subtle Reference"/>
509  <w:LsdException Locked="false" Priority="32" QFormat="true"
510   Name="Intense Reference"/>
511  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
512  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
513   UnhideWhenUsed="true" Name="Bibliography"/>
514  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
515   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
516  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
517  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
518  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
519  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
520  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
521  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
522  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
523  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
524  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
525  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
526  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
527  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
528  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
529  <w:LsdException Locked="false" Priority="46"
530   Name="Grid Table 1 Light Accent 1"/>
531  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
532  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
533  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
534  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
535  <w:LsdException Locked="false" Priority="51"
536   Name="Grid Table 6 Colorful Accent 1"/>
537  <w:LsdException Locked="false" Priority="52"
538   Name="Grid Table 7 Colorful Accent 1"/>
539  <w:LsdException Locked="false" Priority="46"
540   Name="Grid Table 1 Light Accent 2"/>
541  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
542  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
543  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
544  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
545  <w:LsdException Locked="false" Priority="51"
546   Name="Grid Table 6 Colorful Accent 2"/>
547  <w:LsdException Locked="false" Priority="52"
548   Name="Grid Table 7 Colorful Accent 2"/>
549  <w:LsdException Locked="false" Priority="46"
550   Name="Grid Table 1 Light Accent 3"/>
551  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
552  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
553  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
554  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
555  <w:LsdException Locked="false" Priority="51"
556   Name="Grid Table 6 Colorful Accent 3"/>
557  <w:LsdException Locked="false" Priority="52"
558   Name="Grid Table 7 Colorful Accent 3"/>
559  <w:LsdException Locked="false" Priority="46"
560   Name="Grid Table 1 Light Accent 4"/>
561  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
562  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
563  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
564  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
565  <w:LsdException Locked="false" Priority="51"
566   Name="Grid Table 6 Colorful Accent 4"/>
567  <w:LsdException Locked="false" Priority="52"
568   Name="Grid Table 7 Colorful Accent 4"/>
569  <w:LsdException Locked="false" Priority="46"
570   Name="Grid Table 1 Light Accent 5"/>
571  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
572  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
573  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
574  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
575  <w:LsdException Locked="false" Priority="51"
576   Name="Grid Table 6 Colorful Accent 5"/>
577  <w:LsdException Locked="false" Priority="52"
578   Name="Grid Table 7 Colorful Accent 5"/>
579  <w:LsdException Locked="false" Priority="46"
580   Name="Grid Table 1 Light Accent 6"/>
581  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
582  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
583  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
584  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
585  <w:LsdException Locked="false" Priority="51"
586   Name="Grid Table 6 Colorful Accent 6"/>
587  <w:LsdException Locked="false" Priority="52"
588   Name="Grid Table 7 Colorful Accent 6"/>
589  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
590  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
591  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
592  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
593  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
594  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
595  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
596  <w:LsdException Locked="false" Priority="46"
597   Name="List Table 1 Light Accent 1"/>
598  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
599  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
600  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
601  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
602  <w:LsdException Locked="false" Priority="51"
603   Name="List Table 6 Colorful Accent 1"/>
604  <w:LsdException Locked="false" Priority="52"
605   Name="List Table 7 Colorful Accent 1"/>
606  <w:LsdException Locked="false" Priority="46"
607   Name="List Table 1 Light Accent 2"/>
608  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
609  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
610  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
611  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
612  <w:LsdException Locked="false" Priority="51"
613   Name="List Table 6 Colorful Accent 2"/>
614  <w:LsdException Locked="false" Priority="52"
615   Name="List Table 7 Colorful Accent 2"/>
616  <w:LsdException Locked="false" Priority="46"
617   Name="List Table 1 Light Accent 3"/>
618  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
619  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
620  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
621  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
622  <w:LsdException Locked="false" Priority="51"
623   Name="List Table 6 Colorful Accent 3"/>
624  <w:LsdException Locked="false" Priority="52"
625   Name="List Table 7 Colorful Accent 3"/>
626  <w:LsdException Locked="false" Priority="46"
627   Name="List Table 1 Light Accent 4"/>
628  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
629  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
630  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
631  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
632  <w:LsdException Locked="false" Priority="51"
633   Name="List Table 6 Colorful Accent 4"/>
634  <w:LsdException Locked="false" Priority="52"
635   Name="List Table 7 Colorful Accent 4"/>
636  <w:LsdException Locked="false" Priority="46"
637   Name="List Table 1 Light Accent 5"/>
638  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
639  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
640  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
641  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
642  <w:LsdException Locked="false" Priority="51"
643   Name="List Table 6 Colorful Accent 5"/>
644  <w:LsdException Locked="false" Priority="52"
645   Name="List Table 7 Colorful Accent 5"/>
646  <w:LsdException Locked="false" Priority="46"
647   Name="List Table 1 Light Accent 6"/>
648  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
649  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
650  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
651  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
652  <w:LsdException Locked="false" Priority="51"
653   Name="List Table 6 Colorful Accent 6"/>
654  <w:LsdException Locked="false" Priority="52"
655   Name="List Table 7 Colorful Accent 6"/>
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1186<h1>TOF Sequential Single Peak Fits and loading curve</h1>
1187
1188<P><BL>
1189  <LI><B>A video version of this tutorial is available at
1190<A href="https://anl.box.com/v/TOFSequentialSinglePeakFit" target="_blank">
1191https://anl.box.com/v/TOFSequentialSinglePeakFit</A></B>
1192  <LI>Exercise files are found <A href="./data/" target="_blank">here</a>
1193</BL></P><P></P>
1194
1195 <p class=MsoNormal><B>Introduction:</B> A common analysis of diffraction data obtained from a
1196polycrystalline sample subjected to a changing uniaxial load is to follow the
1197behavior of fitted single peaks. The data sets considered here were obtained on
1198the Vulcan diffractometer at SNS, Oak Ridge National Laboratory. The layout of
1199the instrument</p>
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1384     mso-bidi-theme-font:minor-bidi;color:black;mso-themecolor:text1;
1385     mso-font-kerning:12.0pt'>°</span><span style='font-size:18.0pt;font-family:
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1387     "Times New Roman";mso-bidi-theme-font:minor-bidi;color:black;mso-themecolor:
1388     text1;mso-font-kerning:12.0pt'> Detector<span
1389     style='mso-spacerun:yes'>                </span>parallel planes “Bank 2”</span></p>
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1420     <div>
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1423     mso-bidi-font-family:"Times New Roman";mso-bidi-theme-font:minor-bidi;
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1649
1650<p class=MsoNormal>has panels of detectors on both sides of the sample (in this
1651case a Œ” stainless steel rod) oriented so that the loading axis is 45° to the
1652incident neutron beam. Thus one detector “Bank 1” only views crystallites with
1653diffraction vectors parallel to the loading direction while the other “Bank 2”
1654only views crystallites with diffraction vectors perpendicular to the load. In
1655such an experiment, as the load is increased (as a tension) we would expect
1656that the reflections would shift to higher d-spacings in Bank 1 and those seen
1657in Bank 2 would shift to smaller d-spacings. If the load is a compression, then
1658the responses in the reflection positions would be reversed. The shift records
1659the response “strain” of the crystal lattice to the load “stress”. The
1660particular experiment done here was to subject the steel rod to ten
1661tension/compression cycles over 13 hours recording a diffraction pattern from
1662the two detectors each minute yielding ~800 data sets. The 1<sup>st</sup>
1663loading cycle was done slowly over ~4.5hrs and the remaining ones done ~1hr
1664each; we will focus on just the 1<sup>st</sup> cycle for this tutorial
1665comprising 61 powder patterns. Note that menu entries and user input are shown
1666in bold face below as <b style='mso-bidi-font-weight:normal'><span
1667style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1668mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Help/About
1669GSAS-II</span></b>, which lists first the name of the menu (here <b
1670style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1671mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1672minor-latin'>Help</span></b>) and second the name of the entry in the menu
1673(here <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1674mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1675minor-latin'>About GSAS-II</span></b>).</p>
1676
1677<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
1678href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
1679text-underline:none'>start GSAS-II</span></a></span></u>.</p>
1680
1681<h2>Step 1. Import the powder data for sequential fitting</h2>
1682
1683<p class=MsoNormal>Use the <b style='mso-bidi-font-weight:normal'>Import/Powder
1684data/from GSAS powder data file</b> menu item to read the data file into the
1685current GSAS-II project. </p>
1686
1687<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
1688
1689<p class=MsoNormal>A file selection dialog will be shown; its appearance will
1690depend on your OS. Change the search directory to <b style='mso-bidi-font-weight:
1691normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1692minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>TOF
1693Sequential Single Peak Fit/data</span></b> and then select all the *.gsa files
1694(435.gda-495.gda) and press <b style='mso-bidi-font-weight:normal'><span
1695style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1696mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Open</span></b>.
1697A small popup window will appear</p>
1698
1699<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1700 id="Picture_x0020_14" o:spid="_x0000_i1059" type="#_x0000_t75" style='width:176.25pt;
1701 height:227.25pt;visibility:visible;mso-wrap-style:square'>
1702 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image002.png"
1703  o:title=""/>
1704</v:shape><![endif]--><![if !vml]><img border=0 width=235 height=303
1705src="TOF%20Sequential%20Single%20Peak%20Fit_files/image071.gif" v:shapes="Picture_x0020_14"><![endif]></span></p>
1706
1707<p class=MsoNormal>Select just <b style='mso-bidi-font-weight:normal'><span
1708style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1709mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>435.gda BANK
17101</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1711style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1712mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
1713After a pause while the data is read the main window will highlight the last
1714entry (PWDR 495.gda Bank1)</p>
1715
1716<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1717 id="Picture_x0020_15" o:spid="_x0000_i1058" type="#_x0000_t75" style='width:466.5pt;
1718 height:174pt;visibility:visible;mso-wrap-style:square'>
1719 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image004.png"
1720  o:title=""/>
1721</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=232
1722src="TOF%20Sequential%20Single%20Peak%20Fit_files/image072.gif" v:shapes="Picture_x0020_15"><![endif]></span></p>
1723
1724<p class=MsoNormal>and show the powder pattern</p>
1725
1726<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1727 id="Picture_x0020_16" o:spid="_x0000_i1057" type="#_x0000_t75" style='width:466.5pt;
1728 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1729 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image006.png"
1730  o:title=""/>
1731</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1732src="TOF%20Sequential%20Single%20Peak%20Fit_files/image073.gif" v:shapes="Picture_x0020_16"><![endif]></span></p>
1733
1734<p class=MsoNormal>You may start here but it is slightly better to start with
1735the 1<sup>st</sup> data set; select <b style='mso-bidi-font-weight:normal'><span
1736style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1737mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PWDR 435.gda
1738BANK 1</span></b> from the tree (press the ‘<b style='mso-bidi-font-weight:
1739normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1740minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>+</span></b>’
1741to expand it) and select <b style='mso-bidi-font-weight:normal'><span
1742style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1743mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Limits</span></b></p>
1744
1745<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1746 id="Picture_x0020_17" o:spid="_x0000_i1056" type="#_x0000_t75" style='width:467.25pt;
1747 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1748 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image008.png"
1749  o:title=""/>
1750</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
1751src="TOF%20Sequential%20Single%20Peak%20Fit_files/image074.gif" v:shapes="Picture_x0020_17"><![endif]></span></p>
1752
1753<p class=MsoNormal>The plot shows the current limits as vertical green &amp;
1754red dashed lines.</p>
1755
1756<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1757 id="Picture_x0020_18" o:spid="_x0000_i1055" type="#_x0000_t75" style='width:467.25pt;
1758 height:333pt;visibility:visible;mso-wrap-style:square'>
1759 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image010.png"
1760  o:title=""/>
1761</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=444
1762src="TOF%20Sequential%20Single%20Peak%20Fit_files/image075.gif" v:shapes="Picture_x0020_18"><![endif]></span></p>
1763
1764<p class=MsoNormal>Set the <b style='mso-bidi-font-weight:normal'><span
1765style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1766mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmax</span></b>
1767value to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1768mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1769minor-latin'>37000</span></b> and the <b style='mso-bidi-font-weight:normal'><span
1770style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1771mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmin</span></b>
1772to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1773mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1774minor-latin'>11000</span></b>; this will encompass the 1<sup>st</sup> 10 peaks
1775of the powder pattern.</p>
1776
1777<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1778 id="Picture_x0020_19" o:spid="_x0000_i1054" type="#_x0000_t75" style='width:467.25pt;
1779 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1780 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image012.png"
1781  o:title=""/>
1782</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
1783src="TOF%20Sequential%20Single%20Peak%20Fit_files/image076.gif" v:shapes="Picture_x0020_19"><![endif]></span></p>
1784
1785<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1786 id="Picture_x0020_20" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:466.5pt;
1787 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1788 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image014.png"
1789  o:title=""/>
1790</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1791src="TOF%20Sequential%20Single%20Peak%20Fit_files/image077.gif" v:shapes="Picture_x0020_20"><![endif]></span></p>
1792
1793<p class=MsoNormal>Next copy these limits to the other PWDR data sets; do <b
1794style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1795mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1796minor-latin'>Edit Limits/Copy</span></b>. A selection dialog box will appear</p>
1797
1798<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1799 id="Picture_x0020_21" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:189.75pt;
1800 height:316.5pt;visibility:visible;mso-wrap-style:square'>
1801 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image016.png"
1802  o:title=""/>
1803</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=422
1804src="TOF%20Sequential%20Single%20Peak%20Fit_files/image078.gif" v:shapes="Picture_x0020_21"><![endif]></span></p>
1805
1806<p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span
1807style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1808mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set All</span></b>
1809and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1810mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1811minor-latin'>OK</span></b>; the limits will be copied to the other histograms.</p>
1812
1813<h2>Step 2. Peak fitting for 1<sup>st</sup> data set.</h2>
1814
1815<p class=MsoNormal>In this step we will select the 10 reflections for single
1816peak fits and fit them. Select <b style='mso-bidi-font-weight:normal'><span
1817style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1818mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak List</span></b>
1819for the 1<sup>st</sup> PWDR data set; it will be empty. To populate it do <b
1820style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1821mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1822minor-latin'>Peak Fitting/Auto Search</span></b>; this will find the 10 peaks
1823and put them in the list and mark them on the plot with vertical blue lines.</p>
1824
1825<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1826 id="Picture_x0020_23" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:466.5pt;
1827 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1828 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image018.png"
1829  o:title=""/>
1830</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=339
1831src="TOF%20Sequential%20Single%20Peak%20Fit_files/image079.gif" v:shapes="Picture_x0020_23"><![endif]></span></p>
1832
1833<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1834 id="Picture_x0020_24" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:466.5pt;
1835 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1836 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image020.png"
1837  o:title=""/>
1838</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1839src="TOF%20Sequential%20Single%20Peak%20Fit_files/image080.gif" v:shapes="Picture_x0020_24"><![endif]></span></p>
1840
1841<p class=MsoNormal>Next do <b style='mso-bidi-font-weight:normal'><span
1842style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1843mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak
1844Fitting/Peakfit</span></b> from the menu; a file dialog will appear asking for
1845a file name (I used “<b style='mso-bidi-font-weight:normal'><span
1846style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1847mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>steel</span></b>”)
1848to create a new project. The refinement will then do the initial fit to the 10
1849peaks varying only intensity and background (default of 3 term Chebyschev
1850polynominal). The result is </p>
1851
1852<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1853 id="Picture_x0020_25" o:spid="_x0000_i1049" type="#_x0000_t75" style='width:466.5pt;
1854 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1855 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image022.png"
1856  o:title=""/>
1857</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1858src="TOF%20Sequential%20Single%20Peak%20Fit_files/image081.gif" v:shapes="Picture_x0020_25"><![endif]></span></p>
1859
1860<p class=MsoNormal>and shows the need for further refinement for both position
1861&amp; peak width. To do this double click on the <b style='mso-bidi-font-weight:
1862normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1863minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>refine</span></b>
1864column heading for <b style='mso-bidi-font-weight:normal'><span
1865style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1866mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>position</span></b>
1867and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1868mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1869minor-latin'>sigma</span></b> selecting ‘<b style='mso-bidi-font-weight:normal'><span
1870style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1871mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Y</span></b>’
1872from the popup in each case. When done the Peak List should look like</p>
1873
1874<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1875 id="Picture_x0020_26" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:466.5pt;
1876 height:168pt;visibility:visible;mso-wrap-style:square'>
1877 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image024.png"
1878  o:title=""/>
1879</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=224
1880src="TOF%20Sequential%20Single%20Peak%20Fit_files/image082.gif" v:shapes="Picture_x0020_26"><![endif]></span></p>
1881
1882<p class=MsoNormal>with check marks in three columns. Then do <b
1883style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1884mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1885minor-latin'>Peak Fitting/Peakfit</span></b>; the fit will be much improved</p>
1886
1887<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1888 id="Picture_x0020_28" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:466.5pt;
1889 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1890 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image026.png"
1891  o:title=""/>
1892</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1893src="TOF%20Sequential%20Single%20Peak%20Fit_files/image083.gif" v:shapes="Picture_x0020_28"><![endif]></span></p>
1894
1895<p class=MsoNormal>I’ve pressed both ‘<b style='mso-bidi-font-weight:normal'><span
1896style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1897mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>W</span></b>’
1898to get the <span style='font-family:Symbol'>D</span>I/<span style='font-family:
1899Symbol'>s</span>(I) curve and ‘<b style='mso-bidi-font-weight:normal'><span
1900style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1901mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>S</span></b>’
1902to see sqrt(intensity) on the plot. The residual for the fit (see console for
1903this) is ~14%; it perhaps could be improved by more background terms but this
1904will not have much effect on the peak parameters.</p>
1905
1906<h2>Step 3. Sequential peak fit</h2>
1907
1908<p class=MsoNormal>To prepare for the sequential peak fitting we need to copy
1909the results from fitting 10 peaks to the other PWDR histograms. Do <b
1910style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1911mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1912minor-latin'>Peak Fitting/Peak copy</span></b>; a selection dialog will appear.
1913Do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1914mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1915minor-latin'>Set All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1916style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1917mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
1918the peak fit data will be copied to the other PWDR histograms. Next do <b
1919style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1920mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1921minor-latin'>Peak Fitting/Seq Peakfit</span></b>; again a selection dialog will
1922appear</p>
1923
1924<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1925 id="Picture_x0020_29" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:189.75pt;
1926 height:339pt;visibility:visible;mso-wrap-style:square'>
1927 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image028.png"
1928  o:title=""/>
1929</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=452
1930src="TOF%20Sequential%20Single%20Peak%20Fit_files/image084.gif" v:shapes="Picture_x0020_29"><![endif]></span></p>
1931
1932<p class=MsoNormal>Notice this one does offer the possibility of doing the fit
1933in reverse (i.e. start from the last PWDR entry) and also to copy the result
1934from one fit to the next one in sequence as possibly better starting values for
1935its refinement. We’ll not bother with either here. Do <b style='mso-bidi-font-weight:
1936normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1937minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set
1938All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1939style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1940mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
1941GSAS-II will rapidly do the 10 peak fitting on all 61 PWDR histograms. The
1942final sequential result is displayed</p>
1943
1944<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1945 id="Picture_x0020_30" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:472.5pt;
1946 height:166.5pt;visibility:visible;mso-wrap-style:square'>
1947 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image030.png"
1948  o:title=""/>
1949</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=222
1950src="TOF%20Sequential%20Single%20Peak%20Fit_files/image085.gif" v:shapes="Picture_x0020_30"><![endif]></span></p>
1951
1952<p class=MsoNormal>The table is quite large with &gt;30 columns and 61 rows so
1953I’ve shown only a bit of it. If you select a row, the plot will show the
1954corresponding PWDR plot and fit; this is the same as selecting a PWDR entry in
1955the main data tree (this will respond to arrow keys to step from one PWDR entry
1956to the next and show the corresponding plot). For your first view of the sequential
1957result double click on the <b style='mso-bidi-font-weight:normal'><span
1958style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1959mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
1960column heading; the variation in this value across the sequence will be
1961plotted; each point has the error bar obtained in the refinement</p>
1962
1963<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1964 id="Picture_x0020_31" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:471.75pt;
1965 height:336pt;visibility:visible;mso-wrap-style:square'>
1966 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image032.png"
1967  o:title=""/>
1968</v:shape><![endif]--><![if !vml]><img border=0 width=629 height=448
1969src="TOF%20Sequential%20Single%20Peak%20Fit_files/image086.gif" v:shapes="Picture_x0020_31"><![endif]></span></p>
1970
1971<p class=MsoNormal>This shows the result of a loading/unloading cycle
1972essentially in time (data collection sequence number). More interesting would
1973be to show the dependence on load; we need to set the applied load used for
1974each data set.</p>
1975
1976<h2>Step 4. Import applied load table</h2>
1977
1978<p class=MsoNormal>A hard way to enter the loads is to do each one by hand;
1979they are entered in the <b style='mso-bidi-font-weight:normal'><span
1980style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1981mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sample
1982Parameters</span></b> tree item for each PWDR entry. Select that now for the 1<sup>st</sup>
1983PWDR entry</p>
1984
1985<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1986 id="Picture_x0020_33" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:445.5pt;
1987 height:395.25pt;visibility:visible;mso-wrap-style:square'>
1988 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image034.png"
1989  o:title=""/>
1990</v:shape><![endif]--><![if !vml]><img border=0 width=594 height=527
1991src="TOF%20Sequential%20Single%20Peak%20Fit_files/image087.gif" v:shapes="Picture_x0020_33"><![endif]></span></p>
1992
1993<p class=MsoNormal>Notice there is an entry at the bottom of the table for <b
1994style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1995mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1996minor-latin'>Applied load (MN)</span></b>; you’d have to fill that in for every
1997PWDR data set. However, there is an easier way since a metadata file with this
1998information was provided by the Vulcan Instrument Scientist. To access it do <b
1999style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2000mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2001minor-latin'>Command/Load all</span></b>; a file selection dialog will appear.
2002Choose <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2003mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2004minor-latin'>28902sampleenv_chopped_mean.txt</span></b> and open it; a Select
2005columns dialog box will appear</p>
2006
2007<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2008 id="Picture_x0020_34" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:469.5pt;
2009 height:321.75pt;visibility:visible;mso-wrap-style:square'>
2010 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image036.png"
2011  o:title=""/>
2012</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=429
2013src="TOF%20Sequential%20Single%20Peak%20Fit_files/image088.gif" v:shapes="Picture_x0020_34"><![endif]></span></p>
2014
2015<p class=MsoNormal>Looking over the column headings, one is marked “stress” and
2016another is marked “force”. Their ratio is presumably the cross-section area of
2017the steel rod (in mm<sup>2</sup>). So (counting from zero) the column we want for
2018<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2019mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2020minor-latin'>Applied loa</span></b>d is Column #6 (1<sup>st</sup> value
2021~169.45); select <b style='mso-bidi-font-weight:normal'><span style='font-family:
2022"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2023minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b> from the
2024pulldown under the heading. The table should show</p>
2025
2026<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2027 id="Picture_x0020_35" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:427.5pt;
2028 height:293.25pt;visibility:visible;mso-wrap-style:square'>
2029 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image038.png"
2030  o:title=""/>
2031</v:shape><![endif]--><![if !vml]><img border=0 width=570 height=391
2032src="TOF%20Sequential%20Single%20Peak%20Fit_files/image089.gif" v:shapes="Picture_x0020_35"><![endif]></span></p>
2033
2034<p class=MsoNormal>Notice you can apply conversion factors to the column of
2035values if desired; just enter it in the <b style='mso-bidi-font-weight:normal'><span
2036style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2037mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Modify by</span></b>
2038box.</p>
2039
2040<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
2041style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2042mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2043all the Sample Parameters tables will be updated filling in the appropriate
2044values for Applied load.</p>
2045
2046<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2047style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2048mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sequential
2049peak fit results</span></b> from the data tree</p>
2050
2051<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2052 id="Picture_x0020_36" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:426.75pt;
2053 height:198.75pt;visibility:visible;mso-wrap-style:square'>
2054 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image040.png"
2055  o:title=""/>
2056</v:shape><![endif]--><![if !vml]><img border=0 width=569 height=265
2057src="TOF%20Sequential%20Single%20Peak%20Fit_files/image090.gif" v:shapes="Picture_x0020_36"><![endif]></span></p>
2058
2059<p class=MsoNormal>Applied load is a new column entry in the table; double
2060click the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2061mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2062minor-latin'>pos0</span></b> column heading. A new plot will appear</p>
2063
2064<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2065 id="Picture_x0020_37" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:471pt;
2066 height:335.25pt;visibility:visible;mso-wrap-style:square'>
2067 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image032.png"
2068  o:title=""/>
2069</v:shape><![endif]--><![if !vml]><img border=0 width=628 height=447
2070src="TOF%20Sequential%20Single%20Peak%20Fit_files/image091.gif" v:shapes="Picture_x0020_37"><![endif]></span></p>
2071
2072<p class=MsoNormal>which is unchanged from before. Place the cursor anywhere on
2073the plot (i.e. select it) and press the ‘<b style='mso-bidi-font-weight:normal'><span
2074style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2075mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>s</span></b>’
2076key; a popup dialog will appear.</p>
2077
2078<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2079 id="Picture_x0020_39" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:240pt;
2080 height:232.5pt;visibility:visible;mso-wrap-style:square'>
2081 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image043.png"
2082  o:title=""/>
2083</v:shape><![endif]--><![if !vml]><img border=0 width=320 height=310
2084src="TOF%20Sequential%20Single%20Peak%20Fit_files/image092.gif" v:shapes="Picture_x0020_39"><![endif]></span></p>
2085
2086<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2087style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2088mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b>
2089and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2090mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2091minor-latin'>OK</span></b>. The plot will change (you may have to select ‘<b
2092style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2093mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2094minor-latin'>pos0</span></b>’ again)</p>
2095
2096<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2097 id="Picture_x0020_40" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:466.5pt;
2098 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2099 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image045.png"
2100  o:title=""/>
2101</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2102src="TOF%20Sequential%20Single%20Peak%20Fit_files/image093.gif" v:shapes="Picture_x0020_40"><![endif]></span></p>
2103
2104<p class=MsoNormal>This shows the perfectly linear response of peak position
2105with applied load. Select another <b style='mso-bidi-font-weight:normal'><span
2106style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2107mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos</span></b>
2108parameter; the plot will change</p>
2109
2110<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2111 id="Picture_x0020_41" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:464.25pt;
2112 height:330pt;visibility:visible;mso-wrap-style:square'>
2113 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image047.png"
2114  o:title=""/>
2115</v:shape><![endif]--><![if !vml]><img border=0 width=619 height=440
2116src="TOF%20Sequential%20Single%20Peak%20Fit_files/image094.gif" v:shapes="Picture_x0020_41"><![endif]></span></p>
2117
2118<p class=MsoNormal>Pos1 shows hysteresis in a load/unload cycle; some of other
2119peaks will be similar while others will resemble pos0. This would be a good
2120place to do <b style='mso-bidi-font-weight:normal'><span style='font-family:
2121"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2122minor-latin;mso-bidi-theme-font:minor-latin'>File/Save project</span></b>.</p>
2123
2124<h2>Step 5. Sequential data fitting</h2>
2125
2126<p class=MsoNormal>Since pos0 gives a nice straight line response to load, we
2127can try to extract the Hookes Law elastic coefficient for that reflection. To
2128do this we must find the strain from the peak position shift from the zero load
2129value. First select <b style='mso-bidi-font-weight:normal'><span
2130style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2131mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2132from the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2133mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2134minor-latin'>Sequential results</span></b> table.</p>
2135
2136<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
2137style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_42"
2138 o:spid="_x0000_i1035" type="#_x0000_t75" style='width:466.5pt;height:331.5pt;
2139 visibility:visible;mso-wrap-style:square'>
2140 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image045.png"
2141  o:title=""/>
2142</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2143src="TOF%20Sequential%20Single%20Peak%20Fit_files/image095.gif" v:shapes="Picture_x0020_42"><![endif]></span></p>
2144
2145<p class=MsoNormal>Using the cursor, find the zero load point on the curve and
2146note value for pos0; it will show up in a tool tip displayed as the cursor is
2147positioned. I found pos0=33937 at load=0. We will use this to compute the
2148strain0 = (pos0-33937)/33937; we want this as a new column in the table. To do
2149this do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2150mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2151minor-latin'>Pseudo Vars/Add Formula</span></b>; a new window “Expression
2152Editor” will appear</p>
2153
2154<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2155 id="Picture_x0020_46" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:465pt;
2156 height:255pt;visibility:visible;mso-wrap-style:square'>
2157 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image050.png"
2158  o:title=""/>
2159</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2160src="TOF%20Sequential%20Single%20Peak%20Fit_files/image096.gif" v:shapes="Picture_x0020_46"><![endif]></span></p>
2161
2162<p class=MsoNormal>Enter <b style='mso-bidi-font-weight:normal'><span
2163style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2164mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2165in the box after the + sign; the window will be redrawn</p>
2166
2167<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2168 id="Picture_x0020_47" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:465pt;
2169 height:255pt;visibility:visible;mso-wrap-style:square'>
2170 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image052.png"
2171  o:title=""/>
2172</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2173src="TOF%20Sequential%20Single%20Peak%20Fit_files/image097.gif" v:shapes="Picture_x0020_47"><![endif]></span></p>
2174
2175<p class=MsoNormal>Select ‘<b style='mso-bidi-font-weight:normal'><span
2176style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2177mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>’
2178from the pulldown next to the ‘x’ (your variable name in the equation); a new
2179selection box will appear. Choose <b style='mso-bidi-font-weight:normal'><span
2180style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2181mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2182(pos for the filter can help reduce the choices) from the list and press <b
2183style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2184mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2185minor-latin'>OK</span></b>. The window is again redrawn</p>
2186
2187<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2188 id="Picture_x0020_48" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:465pt;
2189 height:255pt;visibility:visible;mso-wrap-style:square'>
2190 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image054.png"
2191  o:title=""/>
2192</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2193src="TOF%20Sequential%20Single%20Peak%20Fit_files/image098.gif" v:shapes="Picture_x0020_48"><![endif]></span></p>
2194
2195<p class=MsoNormal>All looks properly filled in so press <b style='mso-bidi-font-weight:
2196normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2197minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2198the sequential table will now have a new column at the end with the entered
2199equation as its name</p>
2200
2201<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2202 id="Picture_x0020_49" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:466.5pt;
2203 height:192.75pt;visibility:visible;mso-wrap-style:square'>
2204 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image056.png"
2205  o:title=""/>
2206</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=257
2207src="TOF%20Sequential%20Single%20Peak%20Fit_files/image099.gif" v:shapes="Picture_x0020_49"><![endif]></span></p>
2208
2209<p class=MsoNormal>Click on that column heading to see its plot vs load</p>
2210
2211<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2212 id="Picture_x0020_50" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:466.5pt;
2213 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2214 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image058.png"
2215  o:title=""/>
2216</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2217src="TOF%20Sequential%20Single%20Peak%20Fit_files/image100.gif" v:shapes="Picture_x0020_50"><![endif]></span></p>
2218
2219<p class=MsoNormal>This is what we want to fit to get the Hookes Law
2220coefficient. Do <b style='mso-bidi-font-weight:normal'><span style='font-family:
2221"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2222minor-latin;mso-bidi-theme-font:minor-latin'>Parametric Fit/Add equation</span></b>;
2223the Expression Editor window will appear</p>
2224
2225<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2226 id="Picture_x0020_51" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;
2227 height:255pt;visibility:visible;mso-wrap-style:square'>
2228 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image060.png"
2229  o:title=""/>
2230</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2231src="TOF%20Sequential%20Single%20Peak%20Fit_files/image101.gif" v:shapes="Picture_x0020_51"><![endif]></span></p>
2232
2233<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2234style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2235mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>
2236from the pull down on the left of the = sign and pick <b style='mso-bidi-font-weight:
2237normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2238minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2239from the list. Then enter <b style='mso-bidi-font-weight:normal'><span
2240style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2241mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m*y+b</span></b>
2242in the box to the right of the = sign. NB: x was used earlier so we can’t use
2243it here. That establishes the equation you are trying to fit to the data. The
2244window will change to give</p>
2245
2246<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2247 id="Picture_x0020_52" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:465pt;
2248 height:255pt;visibility:visible;mso-wrap-style:square'>
2249 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image062.png"
2250  o:title=""/>
2251</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2252src="TOF%20Sequential%20Single%20Peak%20Fit_files/image102.gif" v:shapes="Picture_x0020_52"><![endif]></span></p>
2253
2254<p class=MsoNormal>For the three pull downs, <b style='mso-bidi-font-weight:
2255normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2256minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>b</span></b>
2257is <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2258mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2259minor-latin'>Free</span></b>, <b style='mso-bidi-font-weight:normal'><span
2260style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2261mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m</span></b>
2262is also <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2263mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2264minor-latin'>Free</span></b> (the fitting variables) and <b style='mso-bidi-font-weight:
2265normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2266minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>y</span></b>
2267is a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2268mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2269minor-latin'>Global</span></b>; select <b style='mso-bidi-font-weight:normal'><span
2270style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2271mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b>
2272for it. The Editor will change again</p>
2273
2274<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2275 id="Picture_x0020_53" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt;
2276 height:255pt;visibility:visible;mso-wrap-style:square'>
2277 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image064.png"
2278  o:title=""/>
2279</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2280src="TOF%20Sequential%20Single%20Peak%20Fit_files/image103.gif" v:shapes="Picture_x0020_53"><![endif]></span></p>
2281
2282<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
2283style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2284mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Fit</span></b>
2285or even just <b style='mso-bidi-font-weight:normal'><span style='font-family:
2286"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2287minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>. The console will
2288show the fitting result</p>
2289
2290<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2291 id="Picture_x0020_54" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:243.75pt;
2292 height:120.75pt;visibility:visible;mso-wrap-style:square'>
2293 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image066.png"
2294  o:title=""/>
2295</v:shape><![endif]--><![if !vml]><img border=0 width=325 height=161
2296src="TOF%20Sequential%20Single%20Peak%20Fit_files/image104.gif" v:shapes="Picture_x0020_54"><![endif]></span></p>
2297
2298<p class=MsoNormal>And the plot will show the best fit line in red; it nicely
2299matches the data.</p>
2300
2301<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2302 id="Picture_x0020_55" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:469.5pt;
2303 height:334.5pt;visibility:visible;mso-wrap-style:square'>
2304 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image068.png"
2305  o:title=""/>
2306</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=446
2307src="TOF%20Sequential%20Single%20Peak%20Fit_files/image105.gif" v:shapes="Picture_x0020_55"><![endif]></span></p>
2308
2309<p class=MsoNormal>The resulting Hookes Law coefficient is 40.38(13)x10<sup>-6 </sup>MN<sup>-1</sup>
2310for this reflection (austenite 111).<span style='mso-spacerun:yes'> 
2311</span>This end the tutorial; save the project if desired. You can further
2312explore the sequential results and perhaps extract Hookes Law coefficients for
2313the other reflections that show no hysteresis. If you want the look at Bank 2
2314data (the opposite detector) you should start with a fresh GSAS-II project file
2315and follow this tutorial for it. The ratio of the corresponding slope for the
2316austenite 111 reflection with what we found here should be the Poisson ratio.</p>
2317
2318</div>
2319
2320</body>
2321
2322</html>
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