source: Tutorials/TOF Sequential Single Peak Fit/TOF Sequential Single Peak Fit.htm @ 3557

Last change on this file since 3557 was 3556, checked in by vondreele, 5 years ago

small fix (I hope)
  • Property svn:mime-type set to text/html
File size: 124.0 KB
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413  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
414  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
415  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
416  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
417  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
418  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
419  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
420  <w:LsdException Locked="false" Priority="34" QFormat="true"
421   Name="List Paragraph"/>
422  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
423  <w:LsdException Locked="false" Priority="30" QFormat="true"
424   Name="Intense Quote"/>
425  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
426  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
427  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
428  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
429  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
430  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
431  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
432  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
433  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
434  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
435  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
436  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
437  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
438  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
439  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
440  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
441  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
442  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
443  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
444  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
445  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
446  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
447  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
448  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
449  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
450  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
451  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
452  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
453  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
454  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
455  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
456  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
457  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
458  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
459  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
460  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
461  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
462  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
463  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
464  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
465  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
466  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
467  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
468  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
469  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
470  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
471  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
472  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
473  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
474  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
475  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
476  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
477  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
478  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
479  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
480  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
481  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
482  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
483  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
484  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
485  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
486  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
487  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
488  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
489  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
490  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
491  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
492  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
493  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
494  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
495  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
496  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
497  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
498  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
499  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
500  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
501  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
502  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
503  <w:LsdException Locked="false" Priority="19" QFormat="true"
504   Name="Subtle Emphasis"/>
505  <w:LsdException Locked="false" Priority="21" QFormat="true"
506   Name="Intense Emphasis"/>
507  <w:LsdException Locked="false" Priority="31" QFormat="true"
508   Name="Subtle Reference"/>
509  <w:LsdException Locked="false" Priority="32" QFormat="true"
510   Name="Intense Reference"/>
511  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
512  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
513   UnhideWhenUsed="true" Name="Bibliography"/>
514  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
515   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
516  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
517  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
518  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
519  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
520  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
521  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
522  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
523  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
524  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
525  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
526  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
527  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
528  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
529  <w:LsdException Locked="false" Priority="46"
530   Name="Grid Table 1 Light Accent 1"/>
531  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
532  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
533  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
534  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
535  <w:LsdException Locked="false" Priority="51"
536   Name="Grid Table 6 Colorful Accent 1"/>
537  <w:LsdException Locked="false" Priority="52"
538   Name="Grid Table 7 Colorful Accent 1"/>
539  <w:LsdException Locked="false" Priority="46"
540   Name="Grid Table 1 Light Accent 2"/>
541  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
542  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
543  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
544  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
545  <w:LsdException Locked="false" Priority="51"
546   Name="Grid Table 6 Colorful Accent 2"/>
547  <w:LsdException Locked="false" Priority="52"
548   Name="Grid Table 7 Colorful Accent 2"/>
549  <w:LsdException Locked="false" Priority="46"
550   Name="Grid Table 1 Light Accent 3"/>
551  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
552  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
553  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
554  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
555  <w:LsdException Locked="false" Priority="51"
556   Name="Grid Table 6 Colorful Accent 3"/>
557  <w:LsdException Locked="false" Priority="52"
558   Name="Grid Table 7 Colorful Accent 3"/>
559  <w:LsdException Locked="false" Priority="46"
560   Name="Grid Table 1 Light Accent 4"/>
561  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
562  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
563  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
564  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
565  <w:LsdException Locked="false" Priority="51"
566   Name="Grid Table 6 Colorful Accent 4"/>
567  <w:LsdException Locked="false" Priority="52"
568   Name="Grid Table 7 Colorful Accent 4"/>
569  <w:LsdException Locked="false" Priority="46"
570   Name="Grid Table 1 Light Accent 5"/>
571  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
572  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
573  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
574  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
575  <w:LsdException Locked="false" Priority="51"
576   Name="Grid Table 6 Colorful Accent 5"/>
577  <w:LsdException Locked="false" Priority="52"
578   Name="Grid Table 7 Colorful Accent 5"/>
579  <w:LsdException Locked="false" Priority="46"
580   Name="Grid Table 1 Light Accent 6"/>
581  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
582  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
583  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
584  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
585  <w:LsdException Locked="false" Priority="51"
586   Name="Grid Table 6 Colorful Accent 6"/>
587  <w:LsdException Locked="false" Priority="52"
588   Name="Grid Table 7 Colorful Accent 6"/>
589  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
590  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
591  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
592  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
593  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
594  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
595  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
596  <w:LsdException Locked="false" Priority="46"
597   Name="List Table 1 Light Accent 1"/>
598  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
599  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
600  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
601  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
602  <w:LsdException Locked="false" Priority="51"
603   Name="List Table 6 Colorful Accent 1"/>
604  <w:LsdException Locked="false" Priority="52"
605   Name="List Table 7 Colorful Accent 1"/>
606  <w:LsdException Locked="false" Priority="46"
607   Name="List Table 1 Light Accent 2"/>
608  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
609  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
610  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
611  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
612  <w:LsdException Locked="false" Priority="51"
613   Name="List Table 6 Colorful Accent 2"/>
614  <w:LsdException Locked="false" Priority="52"
615   Name="List Table 7 Colorful Accent 2"/>
616  <w:LsdException Locked="false" Priority="46"
617   Name="List Table 1 Light Accent 3"/>
618  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
619  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
620  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
621  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
622  <w:LsdException Locked="false" Priority="51"
623   Name="List Table 6 Colorful Accent 3"/>
624  <w:LsdException Locked="false" Priority="52"
625   Name="List Table 7 Colorful Accent 3"/>
626  <w:LsdException Locked="false" Priority="46"
627   Name="List Table 1 Light Accent 4"/>
628  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
629  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
630  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
631  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
632  <w:LsdException Locked="false" Priority="51"
633   Name="List Table 6 Colorful Accent 4"/>
634  <w:LsdException Locked="false" Priority="52"
635   Name="List Table 7 Colorful Accent 4"/>
636  <w:LsdException Locked="false" Priority="46"
637   Name="List Table 1 Light Accent 5"/>
638  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
639  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
640  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
641  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
642  <w:LsdException Locked="false" Priority="51"
643   Name="List Table 6 Colorful Accent 5"/>
644  <w:LsdException Locked="false" Priority="52"
645   Name="List Table 7 Colorful Accent 5"/>
646  <w:LsdException Locked="false" Priority="46"
647   Name="List Table 1 Light Accent 6"/>
648  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
649  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
650  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
651  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
652  <w:LsdException Locked="false" Priority="51"
653   Name="List Table 6 Colorful Accent 6"/>
654  <w:LsdException Locked="false" Priority="52"
655   Name="List Table 7 Colorful Accent 6"/>
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1186<h1>TOF Sequential Single Peak Fits and loading curve</h1>
1187
1188<P><B>A video version of this tutorial is available at
1189<A href="https://anl.box.com/v/TOFSequentialSinglePeakFit" target="_blank">
1190https://anl.box.com/v/TOFSequentialSinglePeakFit</A></B></P>
1191
1192 <p class=MsoNormal>A common analysis of diffraction data obtained from a
1193polycrystalline sample subjected to a changing uniaxial load is to follow the
1194behavior of fitted single peaks. The data sets considered here were obtained on
1195the Vulcan diffractometer at SNS, Oak Ridge National Laboratory. The layout of
1196the instrument</p>
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1645</v:shape><span style='mso-element:field-end'></span><![endif]--></p>
1646
1647<p class=MsoNormal>has panels of detectors on both sides of the sample (in this
1648case a Œ” stainless steel rod) oriented so that the loading axis is 45° to the
1649incident neutron beam. Thus one detector “Bank 1” only views crystallites with
1650diffraction vectors parallel to the loading direction while the other “Bank 2”
1651only views crystallites with diffraction vectors perpendicular to the load. In
1652such an experiment, as the load is increased (as a tension) we would expect
1653that the reflections would shift to higher d-spacings in Bank 1 and those seen
1654in Bank 2 would shift to smaller d-spacings. If the load is a compression, then
1655the responses in the reflection positions would be reversed. The shift records
1656the response “strain” of the crystal lattice to the load “stress”. The
1657particular experiment done here was to subject the steel rod to ten
1658tension/compression cycles over 13 hours recording a diffraction pattern from
1659the two detectors each minute yielding ~800 data sets. The 1<sup>st</sup>
1660loading cycle was done slowly over ~4.5hrs and the remaining ones done ~1hr
1661each; we will focus on just the 1<sup>st</sup> cycle for this tutorial
1662comprising 61 powder patterns. Note that menu entries and user input are shown
1663in bold face below as <b style='mso-bidi-font-weight:normal'><span
1664style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1665mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Help/About
1666GSAS-II</span></b>, which lists first the name of the menu (here <b
1667style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1668mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1669minor-latin'>Help</span></b>) and second the name of the entry in the menu
1670(here <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1671mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1672minor-latin'>About GSAS-II</span></b>).</p>
1673
1674<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
1675href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
1676text-underline:none'>start GSAS-II</span></a></span></u>.</p>
1677
1678<h2>Step 1. Import the powder data for sequential fitting</h2>
1679
1680<p class=MsoNormal>Use the <b style='mso-bidi-font-weight:normal'>Import/Powder
1681data/from GSAS powder data file</b> menu item to read the data file into the
1682current GSAS-II project. </p>
1683
1684<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
1685
1686<p class=MsoNormal>A file selection dialog will be shown; its appearance will
1687depend on your OS. Change the search directory to <b style='mso-bidi-font-weight:
1688normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1689minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>TOF
1690Sequential Single Peak Fit/data</span></b> and then select all the *.gsa files
1691(435.gda-495.gda) and press <b style='mso-bidi-font-weight:normal'><span
1692style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1693mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Open</span></b>.
1694A small popup window will appear</p>
1695
1696<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1697 id="Picture_x0020_14" o:spid="_x0000_i1059" type="#_x0000_t75" style='width:176.25pt;
1698 height:227.25pt;visibility:visible;mso-wrap-style:square'>
1699 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image002.png"
1700  o:title=""/>
1701</v:shape><![endif]--><![if !vml]><img border=0 width=235 height=303
1702src="TOF%20Sequential%20Single%20Peak%20Fit_files/image071.gif" v:shapes="Picture_x0020_14"><![endif]></span></p>
1703
1704<p class=MsoNormal>Select just <b style='mso-bidi-font-weight:normal'><span
1705style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1706mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>435.gda BANK
17071</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1708style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1709mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
1710After a pause while the data is read the main window will highlight the last
1711entry (PWDR 495.gda Bank1)</p>
1712
1713<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1714 id="Picture_x0020_15" o:spid="_x0000_i1058" type="#_x0000_t75" style='width:466.5pt;
1715 height:174pt;visibility:visible;mso-wrap-style:square'>
1716 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image004.png"
1717  o:title=""/>
1718</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=232
1719src="TOF%20Sequential%20Single%20Peak%20Fit_files/image072.gif" v:shapes="Picture_x0020_15"><![endif]></span></p>
1720
1721<p class=MsoNormal>and show the powder pattern</p>
1722
1723<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1724 id="Picture_x0020_16" o:spid="_x0000_i1057" type="#_x0000_t75" style='width:466.5pt;
1725 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1726 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image006.png"
1727  o:title=""/>
1728</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1729src="TOF%20Sequential%20Single%20Peak%20Fit_files/image073.gif" v:shapes="Picture_x0020_16"><![endif]></span></p>
1730
1731<p class=MsoNormal>You may start here but it is slightly better to start with
1732the 1<sup>st</sup> data set; select <b style='mso-bidi-font-weight:normal'><span
1733style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1734mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PWDR 435.gda
1735BANK 1</span></b> from the tree (press the ‘<b style='mso-bidi-font-weight:
1736normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1737minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>+</span></b>’
1738to expand it) and select <b style='mso-bidi-font-weight:normal'><span
1739style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1740mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Limits</span></b></p>
1741
1742<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1743 id="Picture_x0020_17" o:spid="_x0000_i1056" type="#_x0000_t75" style='width:467.25pt;
1744 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1745 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image008.png"
1746  o:title=""/>
1747</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
1748src="TOF%20Sequential%20Single%20Peak%20Fit_files/image074.gif" v:shapes="Picture_x0020_17"><![endif]></span></p>
1749
1750<p class=MsoNormal>The plot shows the current limits as vertical green &amp;
1751red dashed lines.</p>
1752
1753<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1754 id="Picture_x0020_18" o:spid="_x0000_i1055" type="#_x0000_t75" style='width:467.25pt;
1755 height:333pt;visibility:visible;mso-wrap-style:square'>
1756 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image010.png"
1757  o:title=""/>
1758</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=444
1759src="TOF%20Sequential%20Single%20Peak%20Fit_files/image075.gif" v:shapes="Picture_x0020_18"><![endif]></span></p>
1760
1761<p class=MsoNormal>Set the <b style='mso-bidi-font-weight:normal'><span
1762style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1763mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmax</span></b>
1764value to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1765mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1766minor-latin'>37000</span></b> and the <b style='mso-bidi-font-weight:normal'><span
1767style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1768mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmin</span></b>
1769to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1770mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1771minor-latin'>11000</span></b>; this will encompass the 1<sup>st</sup> 10 peaks
1772of the powder pattern.</p>
1773
1774<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1775 id="Picture_x0020_19" o:spid="_x0000_i1054" type="#_x0000_t75" style='width:467.25pt;
1776 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1777 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image012.png"
1778  o:title=""/>
1779</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
1780src="TOF%20Sequential%20Single%20Peak%20Fit_files/image076.gif" v:shapes="Picture_x0020_19"><![endif]></span></p>
1781
1782<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1783 id="Picture_x0020_20" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:466.5pt;
1784 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1785 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image014.png"
1786  o:title=""/>
1787</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1788src="TOF%20Sequential%20Single%20Peak%20Fit_files/image077.gif" v:shapes="Picture_x0020_20"><![endif]></span></p>
1789
1790<p class=MsoNormal>Next copy these limits to the other PWDR data sets; do <b
1791style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1792mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1793minor-latin'>Edit Limits/Copy</span></b>. A selection dialog box will appear</p>
1794
1795<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1796 id="Picture_x0020_21" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:189.75pt;
1797 height:316.5pt;visibility:visible;mso-wrap-style:square'>
1798 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image016.png"
1799  o:title=""/>
1800</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=422
1801src="TOF%20Sequential%20Single%20Peak%20Fit_files/image078.gif" v:shapes="Picture_x0020_21"><![endif]></span></p>
1802
1803<p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span
1804style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1805mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set All</span></b>
1806and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1807mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1808minor-latin'>OK</span></b>; the limits will be copied to the other histograms.</p>
1809
1810<h2>Step 2. Peak fitting for 1<sup>st</sup> data set.</h2>
1811
1812<p class=MsoNormal>In this step we will select the 10 reflections for single
1813peak fits and fit them. Select <b style='mso-bidi-font-weight:normal'><span
1814style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1815mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak List</span></b>
1816for the 1<sup>st</sup> PWDR data set; it will be empty. To populate it do <b
1817style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1818mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1819minor-latin'>Peak Fitting/Auto Search</span></b>; this will find the 10 peaks
1820and put them in the list and mark them on the plot with vertical blue lines.</p>
1821
1822<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1823 id="Picture_x0020_23" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:466.5pt;
1824 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1825 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image018.png"
1826  o:title=""/>
1827</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=339
1828src="TOF%20Sequential%20Single%20Peak%20Fit_files/image079.gif" v:shapes="Picture_x0020_23"><![endif]></span></p>
1829
1830<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1831 id="Picture_x0020_24" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:466.5pt;
1832 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1833 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image020.png"
1834  o:title=""/>
1835</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1836src="TOF%20Sequential%20Single%20Peak%20Fit_files/image080.gif" v:shapes="Picture_x0020_24"><![endif]></span></p>
1837
1838<p class=MsoNormal>Next do <b style='mso-bidi-font-weight:normal'><span
1839style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1840mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak
1841Fitting/Peakfit</span></b> from the menu; a file dialog will appear asking for
1842a file name (I used “<b style='mso-bidi-font-weight:normal'><span
1843style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1844mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>steel</span></b>”)
1845to create a new project. The refinement will then do the initial fit to the 10
1846peaks varying only intensity and background (default of 3 term Chebyschev
1847polynominal). The result is </p>
1848
1849<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1850 id="Picture_x0020_25" o:spid="_x0000_i1049" type="#_x0000_t75" style='width:466.5pt;
1851 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1852 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image022.png"
1853  o:title=""/>
1854</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1855src="TOF%20Sequential%20Single%20Peak%20Fit_files/image081.gif" v:shapes="Picture_x0020_25"><![endif]></span></p>
1856
1857<p class=MsoNormal>and shows the need for further refinement for both position
1858&amp; peak width. To do this double click on the <b style='mso-bidi-font-weight:
1859normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1860minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>refine</span></b>
1861column heading for <b style='mso-bidi-font-weight:normal'><span
1862style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1863mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>position</span></b>
1864and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1865mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1866minor-latin'>sigma</span></b> selecting ‘<b style='mso-bidi-font-weight:normal'><span
1867style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1868mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Y</span></b>’
1869from the popup in each case. When done the Peak List should look like</p>
1870
1871<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1872 id="Picture_x0020_26" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:466.5pt;
1873 height:168pt;visibility:visible;mso-wrap-style:square'>
1874 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image024.png"
1875  o:title=""/>
1876</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=224
1877src="TOF%20Sequential%20Single%20Peak%20Fit_files/image082.gif" v:shapes="Picture_x0020_26"><![endif]></span></p>
1878
1879<p class=MsoNormal>with check marks in three columns. Then do <b
1880style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1881mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1882minor-latin'>Peak Fitting/Peakfit</span></b>; the fit will be much improved</p>
1883
1884<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1885 id="Picture_x0020_28" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:466.5pt;
1886 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1887 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image026.png"
1888  o:title=""/>
1889</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1890src="TOF%20Sequential%20Single%20Peak%20Fit_files/image083.gif" v:shapes="Picture_x0020_28"><![endif]></span></p>
1891
1892<p class=MsoNormal>I’ve pressed both ‘<b style='mso-bidi-font-weight:normal'><span
1893style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1894mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>W</span></b>’
1895to get the <span style='font-family:Symbol'>D</span>I/<span style='font-family:
1896Symbol'>s</span>(I) curve and ‘<b style='mso-bidi-font-weight:normal'><span
1897style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1898mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>S</span></b>’
1899to see sqrt(intensity) on the plot. The residual for the fit (see console for
1900this) is ~14%; it perhaps could be improved by more background terms but this
1901will not have much effect on the peak parameters.</p>
1902
1903<h2>Step 3. Sequential peak fit</h2>
1904
1905<p class=MsoNormal>To prepare for the sequential peak fitting we need to copy
1906the results from fitting 10 peaks to the other PWDR histograms. Do <b
1907style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1908mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1909minor-latin'>Peak Fitting/Peak copy</span></b>; a selection dialog will appear.
1910Do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1911mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1912minor-latin'>Set All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1913style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1914mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
1915the peak fit data will be copied to the other PWDR histograms. Next do <b
1916style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1917mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1918minor-latin'>Peak Fitting/Seq Peakfit</span></b>; again a selection dialog will
1919appear</p>
1920
1921<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1922 id="Picture_x0020_29" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:189.75pt;
1923 height:339pt;visibility:visible;mso-wrap-style:square'>
1924 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image028.png"
1925  o:title=""/>
1926</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=452
1927src="TOF%20Sequential%20Single%20Peak%20Fit_files/image084.gif" v:shapes="Picture_x0020_29"><![endif]></span></p>
1928
1929<p class=MsoNormal>Notice this one does offer the possibility of doing the fit
1930in reverse (i.e. start from the last PWDR entry) and also to copy the result
1931from one fit to the next one in sequence as possibly better starting values for
1932its refinement. We’ll not bother with either here. Do <b style='mso-bidi-font-weight:
1933normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1934minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set
1935All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1936style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1937mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
1938GSAS-II will rapidly do the 10 peak fitting on all 61 PWDR histograms. The
1939final sequential result is displayed</p>
1940
1941<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1942 id="Picture_x0020_30" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:472.5pt;
1943 height:166.5pt;visibility:visible;mso-wrap-style:square'>
1944 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image030.png"
1945  o:title=""/>
1946</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=222
1947src="TOF%20Sequential%20Single%20Peak%20Fit_files/image085.gif" v:shapes="Picture_x0020_30"><![endif]></span></p>
1948
1949<p class=MsoNormal>The table is quite large with &gt;30 columns and 61 rows so
1950I’ve shown only a bit of it. If you select a row, the plot will show the
1951corresponding PWDR plot and fit; this is the same as selecting a PWDR entry in
1952the main data tree (this will respond to arrow keys to step from one PWDR entry
1953to the next and show the corresponding plot). For your first view of the sequential
1954result double click on the <b style='mso-bidi-font-weight:normal'><span
1955style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1956mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
1957column heading; the variation in this value across the sequence will be
1958plotted; each point has the error bar obtained in the refinement</p>
1959
1960<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1961 id="Picture_x0020_31" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:471.75pt;
1962 height:336pt;visibility:visible;mso-wrap-style:square'>
1963 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image032.png"
1964  o:title=""/>
1965</v:shape><![endif]--><![if !vml]><img border=0 width=629 height=448
1966src="TOF%20Sequential%20Single%20Peak%20Fit_files/image086.gif" v:shapes="Picture_x0020_31"><![endif]></span></p>
1967
1968<p class=MsoNormal>This shows the result of a loading/unloading cycle
1969essentially in time (data collection sequence number). More interesting would
1970be to show the dependence on load; we need to set the applied load used for
1971each data set.</p>
1972
1973<h2>Step 4. Import applied load table</h2>
1974
1975<p class=MsoNormal>A hard way to enter the loads is to do each one by hand;
1976they are entered in the <b style='mso-bidi-font-weight:normal'><span
1977style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1978mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sample
1979Parameters</span></b> tree item for each PWDR entry. Select that now for the 1<sup>st</sup>
1980PWDR entry</p>
1981
1982<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1983 id="Picture_x0020_33" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:445.5pt;
1984 height:395.25pt;visibility:visible;mso-wrap-style:square'>
1985 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image034.png"
1986  o:title=""/>
1987</v:shape><![endif]--><![if !vml]><img border=0 width=594 height=527
1988src="TOF%20Sequential%20Single%20Peak%20Fit_files/image087.gif" v:shapes="Picture_x0020_33"><![endif]></span></p>
1989
1990<p class=MsoNormal>Notice there is an entry at the bottom of the table for <b
1991style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1992mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1993minor-latin'>Applied load (MN)</span></b>; you’d have to fill that in for every
1994PWDR data set. However, there is an easier way since a metadata file with this
1995information was provided by the Vulcan Instrument Scientist. To access it do <b
1996style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1997mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1998minor-latin'>Command/Load all</span></b>; a file selection dialog will appear.
1999Choose <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2000mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2001minor-latin'>28902sampleenv_chopped_mean.txt</span></b> and open it; a Select
2002columns dialog box will appear</p>
2003
2004<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2005 id="Picture_x0020_34" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:469.5pt;
2006 height:321.75pt;visibility:visible;mso-wrap-style:square'>
2007 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image036.png"
2008  o:title=""/>
2009</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=429
2010src="TOF%20Sequential%20Single%20Peak%20Fit_files/image088.gif" v:shapes="Picture_x0020_34"><![endif]></span></p>
2011
2012<p class=MsoNormal>Looking over the column headings, one is marked “stress” and
2013another is marked “force”. Their ratio is presumably the cross-section area of
2014the steel rod (in mm<sup>2</sup>). So (counting from zero) the column we want for
2015<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2016mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2017minor-latin'>Applied loa</span></b>d is Column #6 (1<sup>st</sup> value
2018~169.45); select <b style='mso-bidi-font-weight:normal'><span style='font-family:
2019"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2020minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b> from the
2021pulldown under the heading. The table should show</p>
2022
2023<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2024 id="Picture_x0020_35" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:427.5pt;
2025 height:293.25pt;visibility:visible;mso-wrap-style:square'>
2026 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image038.png"
2027  o:title=""/>
2028</v:shape><![endif]--><![if !vml]><img border=0 width=570 height=391
2029src="TOF%20Sequential%20Single%20Peak%20Fit_files/image089.gif" v:shapes="Picture_x0020_35"><![endif]></span></p>
2030
2031<p class=MsoNormal>Notice you can apply conversion factors to the column of
2032values if desired; just enter it in the <b style='mso-bidi-font-weight:normal'><span
2033style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2034mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Modify by</span></b>
2035box.</p>
2036
2037<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
2038style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2039mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2040all the Sample Parameters tables will be updated filling in the appropriate
2041values for Applied load.</p>
2042
2043<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2044style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2045mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sequential
2046peak fit results</span></b> from the data tree</p>
2047
2048<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2049 id="Picture_x0020_36" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:426.75pt;
2050 height:198.75pt;visibility:visible;mso-wrap-style:square'>
2051 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image040.png"
2052  o:title=""/>
2053</v:shape><![endif]--><![if !vml]><img border=0 width=569 height=265
2054src="TOF%20Sequential%20Single%20Peak%20Fit_files/image090.gif" v:shapes="Picture_x0020_36"><![endif]></span></p>
2055
2056<p class=MsoNormal>Applied load is a new column entry in the table; double
2057click the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2058mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2059minor-latin'>pos0</span></b> column heading. A new plot will appear</p>
2060
2061<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2062 id="Picture_x0020_37" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:471pt;
2063 height:335.25pt;visibility:visible;mso-wrap-style:square'>
2064 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image032.png"
2065  o:title=""/>
2066</v:shape><![endif]--><![if !vml]><img border=0 width=628 height=447
2067src="TOF%20Sequential%20Single%20Peak%20Fit_files/image091.gif" v:shapes="Picture_x0020_37"><![endif]></span></p>
2068
2069<p class=MsoNormal>which is unchanged from before. Place the cursor anywhere on
2070the plot (i.e. select it) and press the ‘<b style='mso-bidi-font-weight:normal'><span
2071style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2072mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>s</span></b>’
2073key; a popup dialog will appear.</p>
2074
2075<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2076 id="Picture_x0020_39" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:240pt;
2077 height:232.5pt;visibility:visible;mso-wrap-style:square'>
2078 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image043.png"
2079  o:title=""/>
2080</v:shape><![endif]--><![if !vml]><img border=0 width=320 height=310
2081src="TOF%20Sequential%20Single%20Peak%20Fit_files/image092.gif" v:shapes="Picture_x0020_39"><![endif]></span></p>
2082
2083<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2084style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2085mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b>
2086and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2087mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2088minor-latin'>OK</span></b>. The plot will change (you may have to select ‘<b
2089style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2090mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2091minor-latin'>pos0</span></b>’ again)</p>
2092
2093<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2094 id="Picture_x0020_40" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:466.5pt;
2095 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2096 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image045.png"
2097  o:title=""/>
2098</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2099src="TOF%20Sequential%20Single%20Peak%20Fit_files/image093.gif" v:shapes="Picture_x0020_40"><![endif]></span></p>
2100
2101<p class=MsoNormal>This shows the perfectly linear response of peak position
2102with applied load. Select another <b style='mso-bidi-font-weight:normal'><span
2103style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2104mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos</span></b>
2105parameter; the plot will change</p>
2106
2107<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2108 id="Picture_x0020_41" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:464.25pt;
2109 height:330pt;visibility:visible;mso-wrap-style:square'>
2110 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image047.png"
2111  o:title=""/>
2112</v:shape><![endif]--><![if !vml]><img border=0 width=619 height=440
2113src="TOF%20Sequential%20Single%20Peak%20Fit_files/image094.gif" v:shapes="Picture_x0020_41"><![endif]></span></p>
2114
2115<p class=MsoNormal>Pos1 shows hysteresis in a load/unload cycle; some of other
2116peaks will be similar while others will resemble pos0. This would be a good
2117place to do <b style='mso-bidi-font-weight:normal'><span style='font-family:
2118"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2119minor-latin;mso-bidi-theme-font:minor-latin'>File/Save project</span></b>.</p>
2120
2121<h2>Step 5. Sequential data fitting</h2>
2122
2123<p class=MsoNormal>Since pos0 gives a nice straight line response to load, we
2124can try to extract the Hookes Law elastic coefficient for that reflection. To
2125do this we must find the strain from the peak position shift from the zero load
2126value. First select <b style='mso-bidi-font-weight:normal'><span
2127style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2128mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2129from the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2130mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2131minor-latin'>Sequential results</span></b> table.</p>
2132
2133<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
2134style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_42"
2135 o:spid="_x0000_i1035" type="#_x0000_t75" style='width:466.5pt;height:331.5pt;
2136 visibility:visible;mso-wrap-style:square'>
2137 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image045.png"
2138  o:title=""/>
2139</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2140src="TOF%20Sequential%20Single%20Peak%20Fit_files/image095.gif" v:shapes="Picture_x0020_42"><![endif]></span></p>
2141
2142<p class=MsoNormal>Using the cursor, find the zero load point on the curve and
2143note value for pos0; it will show up in a tool tip displayed as the cursor is
2144positioned. I found pos0=33937 at load=0. We will use this to compute the
2145strain0 = (pos0-33937)/33937; we want this as a new column in the table. To do
2146this do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2147mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2148minor-latin'>Pseudo Vars/Add Formula</span></b>; a new window “Expression
2149Editor” will appear</p>
2150
2151<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2152 id="Picture_x0020_46" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:465pt;
2153 height:255pt;visibility:visible;mso-wrap-style:square'>
2154 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image050.png"
2155  o:title=""/>
2156</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2157src="TOF%20Sequential%20Single%20Peak%20Fit_files/image096.gif" v:shapes="Picture_x0020_46"><![endif]></span></p>
2158
2159<p class=MsoNormal>Enter <b style='mso-bidi-font-weight:normal'><span
2160style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2161mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2162in the box after the + sign; the window will be redrawn</p>
2163
2164<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2165 id="Picture_x0020_47" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:465pt;
2166 height:255pt;visibility:visible;mso-wrap-style:square'>
2167 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image052.png"
2168  o:title=""/>
2169</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2170src="TOF%20Sequential%20Single%20Peak%20Fit_files/image097.gif" v:shapes="Picture_x0020_47"><![endif]></span></p>
2171
2172<p class=MsoNormal>Select ‘<b style='mso-bidi-font-weight:normal'><span
2173style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2174mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>’
2175from the pulldown next to the ‘x’ (your variable name in the equation); a new
2176selection box will appear. Choose <b style='mso-bidi-font-weight:normal'><span
2177style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2178mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2179(pos for the filter can help reduce the choices) from the list and press <b
2180style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2181mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2182minor-latin'>OK</span></b>. The window is again redrawn</p>
2183
2184<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2185 id="Picture_x0020_48" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:465pt;
2186 height:255pt;visibility:visible;mso-wrap-style:square'>
2187 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image054.png"
2188  o:title=""/>
2189</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2190src="TOF%20Sequential%20Single%20Peak%20Fit_files/image098.gif" v:shapes="Picture_x0020_48"><![endif]></span></p>
2191
2192<p class=MsoNormal>All looks properly filled in so press <b style='mso-bidi-font-weight:
2193normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2194minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2195the sequential table will now have a new column at the end with the entered
2196equation as its name</p>
2197
2198<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2199 id="Picture_x0020_49" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:466.5pt;
2200 height:192.75pt;visibility:visible;mso-wrap-style:square'>
2201 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image056.png"
2202  o:title=""/>
2203</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=257
2204src="TOF%20Sequential%20Single%20Peak%20Fit_files/image099.gif" v:shapes="Picture_x0020_49"><![endif]></span></p>
2205
2206<p class=MsoNormal>Click on that column heading to see its plot vs load</p>
2207
2208<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2209 id="Picture_x0020_50" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:466.5pt;
2210 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2211 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image058.png"
2212  o:title=""/>
2213</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2214src="TOF%20Sequential%20Single%20Peak%20Fit_files/image100.gif" v:shapes="Picture_x0020_50"><![endif]></span></p>
2215
2216<p class=MsoNormal>This is what we want to fit to get the Hookes Law
2217coefficient. Do <b style='mso-bidi-font-weight:normal'><span style='font-family:
2218"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2219minor-latin;mso-bidi-theme-font:minor-latin'>Parametric Fit/Add equation</span></b>;
2220the Expression Editor window will appear</p>
2221
2222<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2223 id="Picture_x0020_51" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;
2224 height:255pt;visibility:visible;mso-wrap-style:square'>
2225 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image060.png"
2226  o:title=""/>
2227</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2228src="TOF%20Sequential%20Single%20Peak%20Fit_files/image101.gif" v:shapes="Picture_x0020_51"><![endif]></span></p>
2229
2230<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2231style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2232mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>
2233from the pull down on the left of the = sign and pick <b style='mso-bidi-font-weight:
2234normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2235minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2236from the list. Then enter <b style='mso-bidi-font-weight:normal'><span
2237style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2238mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m*y+b</span></b>
2239in the box to the right of the = sign. NB: x was used earlier so we can’t use
2240it here. That establishes the equation you are trying to fit to the data. The
2241window will change to give</p>
2242
2243<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2244 id="Picture_x0020_52" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:465pt;
2245 height:255pt;visibility:visible;mso-wrap-style:square'>
2246 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image062.png"
2247  o:title=""/>
2248</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2249src="TOF%20Sequential%20Single%20Peak%20Fit_files/image102.gif" v:shapes="Picture_x0020_52"><![endif]></span></p>
2250
2251<p class=MsoNormal>For the three pull downs, <b style='mso-bidi-font-weight:
2252normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2253minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>b</span></b>
2254is <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2255mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2256minor-latin'>Free</span></b>, <b style='mso-bidi-font-weight:normal'><span
2257style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2258mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m</span></b>
2259is also <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2260mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2261minor-latin'>Free</span></b> (the fitting variables) and <b style='mso-bidi-font-weight:
2262normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2263minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>y</span></b>
2264is a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2265mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2266minor-latin'>Global</span></b>; select <b style='mso-bidi-font-weight:normal'><span
2267style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2268mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b>
2269for it. The Editor will change again</p>
2270
2271<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2272 id="Picture_x0020_53" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt;
2273 height:255pt;visibility:visible;mso-wrap-style:square'>
2274 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image064.png"
2275  o:title=""/>
2276</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2277src="TOF%20Sequential%20Single%20Peak%20Fit_files/image103.gif" v:shapes="Picture_x0020_53"><![endif]></span></p>
2278
2279<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
2280style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2281mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Fit</span></b>
2282or even just <b style='mso-bidi-font-weight:normal'><span style='font-family:
2283"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2284minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>. The console will
2285show the fitting result</p>
2286
2287<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2288 id="Picture_x0020_54" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:243.75pt;
2289 height:120.75pt;visibility:visible;mso-wrap-style:square'>
2290 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image066.png"
2291  o:title=""/>
2292</v:shape><![endif]--><![if !vml]><img border=0 width=325 height=161
2293src="TOF%20Sequential%20Single%20Peak%20Fit_files/image104.gif" v:shapes="Picture_x0020_54"><![endif]></span></p>
2294
2295<p class=MsoNormal>And the plot will show the best fit line in red; it nicely
2296matches the data.</p>
2297
2298<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2299 id="Picture_x0020_55" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:469.5pt;
2300 height:334.5pt;visibility:visible;mso-wrap-style:square'>
2301 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image068.png"
2302  o:title=""/>
2303</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=446
2304src="TOF%20Sequential%20Single%20Peak%20Fit_files/image105.gif" v:shapes="Picture_x0020_55"><![endif]></span></p>
2305
2306<p class=MsoNormal>The resulting Hookes Law coefficient is 40.38(13)x10<sup>-6 </sup>MN<sup>-1</sup>
2307for this reflection (austenite 111).<span style='mso-spacerun:yes'> 
2308</span>This end the tutorial; save the project if desired. You can further
2309explore the sequential results and perhaps extract Hookes Law coefficients for
2310the other reflections that show no hysteresis. If you want the look at Bank 2
2311data (the opposite detector) you should start with a fresh GSAS-II project file
2312and follow this tutorial for it. The ratio of the corresponding slope for the
2313austenite 111 reflection with what we found here should be the Poisson ratio.</p>
2314
2315</div>
2316
2317</body>
2318
2319</html>
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