source: Tutorials/TOF Sequential Single Peak Fit/TOF Sequential Single Peak Fit.htm @ 3553

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finish web tutorials for now

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414  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
415  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
416  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
417  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
418  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
419  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
420  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
421  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
422  <w:LsdException Locked="false" Priority="34" QFormat="true"
423   Name="List Paragraph"/>
424  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
425  <w:LsdException Locked="false" Priority="30" QFormat="true"
426   Name="Intense Quote"/>
427  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
428  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
429  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
430  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
431  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
432  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
433  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
434  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
435  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
436  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
437  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
438  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
439  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
440  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
441  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
442  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
443  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
444  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
445  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
446  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
447  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
448  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
449  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
450  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
451  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
452  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
453  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
454  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
455  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
456  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
457  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
458  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
459  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
460  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
461  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
462  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
463  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
464  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
465  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
466  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
467  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
468  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
469  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
470  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
471  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
472  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
473  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
474  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
475  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
476  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
477  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
478  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
479  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
480  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
481  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
482  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
483  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
484  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
485  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
486  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
487  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
488  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
489  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
490  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
491  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
492  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
493  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
494  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
495  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
496  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
497  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
498  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
499  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
500  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
501  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
502  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
503  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
504  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
505  <w:LsdException Locked="false" Priority="19" QFormat="true"
506   Name="Subtle Emphasis"/>
507  <w:LsdException Locked="false" Priority="21" QFormat="true"
508   Name="Intense Emphasis"/>
509  <w:LsdException Locked="false" Priority="31" QFormat="true"
510   Name="Subtle Reference"/>
511  <w:LsdException Locked="false" Priority="32" QFormat="true"
512   Name="Intense Reference"/>
513  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
514  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
515   UnhideWhenUsed="true" Name="Bibliography"/>
516  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
517   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
518  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
519  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
520  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
521  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
522  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
523  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
524  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
525  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
526  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
527  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
528  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
529  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
530  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
531  <w:LsdException Locked="false" Priority="46"
532   Name="Grid Table 1 Light Accent 1"/>
533  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
534  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
535  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
536  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
537  <w:LsdException Locked="false" Priority="51"
538   Name="Grid Table 6 Colorful Accent 1"/>
539  <w:LsdException Locked="false" Priority="52"
540   Name="Grid Table 7 Colorful Accent 1"/>
541  <w:LsdException Locked="false" Priority="46"
542   Name="Grid Table 1 Light Accent 2"/>
543  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
544  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
545  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
546  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
547  <w:LsdException Locked="false" Priority="51"
548   Name="Grid Table 6 Colorful Accent 2"/>
549  <w:LsdException Locked="false" Priority="52"
550   Name="Grid Table 7 Colorful Accent 2"/>
551  <w:LsdException Locked="false" Priority="46"
552   Name="Grid Table 1 Light Accent 3"/>
553  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
554  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
555  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
556  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
557  <w:LsdException Locked="false" Priority="51"
558   Name="Grid Table 6 Colorful Accent 3"/>
559  <w:LsdException Locked="false" Priority="52"
560   Name="Grid Table 7 Colorful Accent 3"/>
561  <w:LsdException Locked="false" Priority="46"
562   Name="Grid Table 1 Light Accent 4"/>
563  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
564  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
565  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
566  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
567  <w:LsdException Locked="false" Priority="51"
568   Name="Grid Table 6 Colorful Accent 4"/>
569  <w:LsdException Locked="false" Priority="52"
570   Name="Grid Table 7 Colorful Accent 4"/>
571  <w:LsdException Locked="false" Priority="46"
572   Name="Grid Table 1 Light Accent 5"/>
573  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
574  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
575  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
576  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
577  <w:LsdException Locked="false" Priority="51"
578   Name="Grid Table 6 Colorful Accent 5"/>
579  <w:LsdException Locked="false" Priority="52"
580   Name="Grid Table 7 Colorful Accent 5"/>
581  <w:LsdException Locked="false" Priority="46"
582   Name="Grid Table 1 Light Accent 6"/>
583  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
584  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
585  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
586  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
587  <w:LsdException Locked="false" Priority="51"
588   Name="Grid Table 6 Colorful Accent 6"/>
589  <w:LsdException Locked="false" Priority="52"
590   Name="Grid Table 7 Colorful Accent 6"/>
591  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
592  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
593  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
594  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
595  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
596  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
597  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
598  <w:LsdException Locked="false" Priority="46"
599   Name="List Table 1 Light Accent 1"/>
600  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
601  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
602  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
603  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
604  <w:LsdException Locked="false" Priority="51"
605   Name="List Table 6 Colorful Accent 1"/>
606  <w:LsdException Locked="false" Priority="52"
607   Name="List Table 7 Colorful Accent 1"/>
608  <w:LsdException Locked="false" Priority="46"
609   Name="List Table 1 Light Accent 2"/>
610  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
611  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
612  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
613  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
614  <w:LsdException Locked="false" Priority="51"
615   Name="List Table 6 Colorful Accent 2"/>
616  <w:LsdException Locked="false" Priority="52"
617   Name="List Table 7 Colorful Accent 2"/>
618  <w:LsdException Locked="false" Priority="46"
619   Name="List Table 1 Light Accent 3"/>
620  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
621  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
622  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
623  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
624  <w:LsdException Locked="false" Priority="51"
625   Name="List Table 6 Colorful Accent 3"/>
626  <w:LsdException Locked="false" Priority="52"
627   Name="List Table 7 Colorful Accent 3"/>
628  <w:LsdException Locked="false" Priority="46"
629   Name="List Table 1 Light Accent 4"/>
630  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
631  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
632  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
633  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
634  <w:LsdException Locked="false" Priority="51"
635   Name="List Table 6 Colorful Accent 4"/>
636  <w:LsdException Locked="false" Priority="52"
637   Name="List Table 7 Colorful Accent 4"/>
638  <w:LsdException Locked="false" Priority="46"
639   Name="List Table 1 Light Accent 5"/>
640  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
641  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
642  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
643  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
644  <w:LsdException Locked="false" Priority="51"
645   Name="List Table 6 Colorful Accent 5"/>
646  <w:LsdException Locked="false" Priority="52"
647   Name="List Table 7 Colorful Accent 5"/>
648  <w:LsdException Locked="false" Priority="46"
649   Name="List Table 1 Light Accent 6"/>
650  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
651  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
652  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
653  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
654  <w:LsdException Locked="false" Priority="51"
655   Name="List Table 6 Colorful Accent 6"/>
656  <w:LsdException Locked="false" Priority="52"
657   Name="List Table 7 Colorful Accent 6"/>
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1193
1194<h1>TOF Sequential Single Peak Fits and loading curve</h1>
1195
1196<P><B>A video version of this tutorial is available at
1197<A href="https://anl.box.com/v/TOFSequentialSinglePeakFit" target="_blank">
1198https://anl.box.com/v/TOFSequentialSinglePeakFit</A></B></P>
1199
1200 <p class=MsoNormal>A common analysis of diffraction data obtained from a
1201polycrystalline sample subjected to a changing uniaxial load is to follow the behavior
1202of fitted single peaks. The data sets considered here were obtained on the
1203Vulcan diffractometer at SNS, Oak Ridge National Laboratory. The layout of the
1204instrument</p>
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1389     mso-bidi-theme-font:minor-bidi;color:black;mso-themecolor:text1;
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1392     "Times New Roman";mso-bidi-theme-font:minor-bidi;color:black;mso-themecolor:
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1423    <tr>
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1654
1655<p class=MsoNormal><span class=GramE>has</span> panels of detectors on both
1656sides of the sample (in this case a Œ” stainless steel rod) oriented so that
1657the loading axis is 45° to the incident neutron beam. Thus one detector “Bank
16581” only views crystallites with diffraction vectors parallel to the loading
1659direction while the other “Bank 2” only views crystallites with diffraction
1660vectors perpendicular to the load. In such an experiment, as the load is
1661increased (as a tension) we would expect that the reflections would shift to
1662higher d-<span class=SpellE>spacings</span> in Bank 1 and those seen in Bank 2
1663would shift to smaller d-<span class=SpellE>spacings</span>. If the load is a
1664compression, then the responses in the reflection positions would be reversed.
1665The shift records the response “strain” of the crystal lattice to the load
1666“stress”. The particular experiment done here was to subject the steel rod to
1667ten tension/compression cycles over 13 hours recording a diffraction pattern
1668from the two detectors each minute yielding ~800 data sets. The 1<sup>st</sup>
1669loading cycle was done slowly over ~4.5hrs and the remaining ones done ~1hr
1670each; we will focus on just the 1<sup>st</sup> cycle for this tutorial
1671comprising 61 powder patterns. Note that menu entries and user input are shown
1672in bold face below as <b style='mso-bidi-font-weight:normal'><span
1673style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1674mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Help/About
1675GSAS-II</span></b>, which lists first the name of the menu (here <b
1676style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1677mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1678minor-latin'>Help</span></b>) and second the name of the entry in the menu
1679(here <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1680mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1681minor-latin'>About GSAS-II</span></b>).</p>
1682
1683<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
1684href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
1685text-underline:none'>start GSAS-II</span></a></span></u>.</p>
1686
1687<h2>Step 1. Import the powder data for sequential fitting</h2>
1688
1689<p class=MsoNormal>Use the <b style='mso-bidi-font-weight:normal'>Import/Powder
1690data/from GSAS powder data file</b> menu item to read the data file into the
1691current GSAS-II project. </p>
1692
1693<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
1694
1695<p class=MsoNormal>A file selection dialog will be shown; its appearance will
1696depend on your OS. Change the search directory to <b style='mso-bidi-font-weight:
1697normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1698minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>TOF
1699Sequential Single Peak Fit/data</span></b> and then select all the *.<span
1700class=SpellE>gsa</span> files (435.gda-495.gda) and press <b style='mso-bidi-font-weight:
1701normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1702minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Open</span></b>.
1703A small popup window will appear</p>
1704
1705<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1706 id="Picture_x0020_14" o:spid="_x0000_i1059" type="#_x0000_t75" style='width:176.25pt;
1707 height:227.25pt;visibility:visible;mso-wrap-style:square'>
1708 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image002.png"
1709  o:title=""/>
1710</v:shape><![endif]--><![if !vml]><img border=0 width=235 height=303
1711src="TOF%20Sequential%20Single%20Peak%20Fit_files/image003.gif" v:shapes="Picture_x0020_14"><![endif]></span></p>
1712
1713<p class=MsoNormal>Select just <b style='mso-bidi-font-weight:normal'><span
1714style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1715mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>435.gda BANK
17161</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1717style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1718mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
1719After a pause while the data is read the main window will highlight the last
1720entry (PWDR 495.gda Bank1)</p>
1721
1722<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1723 id="Picture_x0020_15" o:spid="_x0000_i1058" type="#_x0000_t75" style='width:466.5pt;
1724 height:174pt;visibility:visible;mso-wrap-style:square'>
1725 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image004.png"
1726  o:title=""/>
1727</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=232
1728src="TOF%20Sequential%20Single%20Peak%20Fit_files/image005.gif" v:shapes="Picture_x0020_15"><![endif]></span></p>
1729
1730<p class=MsoNormal><span class=GramE>and</span> show the powder pattern</p>
1731
1732<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1733 id="Picture_x0020_16" o:spid="_x0000_i1057" type="#_x0000_t75" style='width:466.5pt;
1734 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1735 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image006.png"
1736  o:title=""/>
1737</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1738src="TOF%20Sequential%20Single%20Peak%20Fit_files/image007.gif" v:shapes="Picture_x0020_16"><![endif]></span></p>
1739
1740<p class=MsoNormal>You may start here but it is slightly better to start with
1741the 1<sup>st</sup> data set; select <b style='mso-bidi-font-weight:normal'><span
1742style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1743mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PWDR 435.gda
1744BANK 1</span></b> from the tree (press the ‘<b style='mso-bidi-font-weight:
1745normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1746minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>+</span></b>’
1747to expand it) and select <b style='mso-bidi-font-weight:normal'><span
1748style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1749mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Limits</span></b></p>
1750
1751<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1752 id="Picture_x0020_17" o:spid="_x0000_i1056" type="#_x0000_t75" style='width:467.25pt;
1753 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1754 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image008.png"
1755  o:title=""/>
1756</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
1757src="TOF%20Sequential%20Single%20Peak%20Fit_files/image009.gif" v:shapes="Picture_x0020_17"><![endif]></span></p>
1758
1759<p class=MsoNormal>The plot shows the current limits as vertical green &amp;
1760red dashed lines.</p>
1761
1762<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1763 id="Picture_x0020_18" o:spid="_x0000_i1055" type="#_x0000_t75" style='width:467.25pt;
1764 height:333pt;visibility:visible;mso-wrap-style:square'>
1765 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image010.png"
1766  o:title=""/>
1767</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=444
1768src="TOF%20Sequential%20Single%20Peak%20Fit_files/image011.gif" v:shapes="Picture_x0020_18"><![endif]></span></p>
1769
1770<p class=MsoNormal>Set the <span class=SpellE><b style='mso-bidi-font-weight:
1771normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1772minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmax</span></b></span>
1773value to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1774mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1775minor-latin'>37000</span></b> and the <span class=SpellE><b style='mso-bidi-font-weight:
1776normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1777minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmin</span></b></span>
1778to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1779mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1780minor-latin'>11000</span></b>; this will encompass the 1<sup>st</sup> 10 peaks
1781of the powder pattern.</p>
1782
1783<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1784 id="Picture_x0020_19" o:spid="_x0000_i1054" type="#_x0000_t75" style='width:467.25pt;
1785 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1786 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image012.png"
1787  o:title=""/>
1788</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
1789src="TOF%20Sequential%20Single%20Peak%20Fit_files/image013.gif" v:shapes="Picture_x0020_19"><![endif]></span></p>
1790
1791<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1792 id="Picture_x0020_20" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:466.5pt;
1793 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1794 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image014.png"
1795  o:title=""/>
1796</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1797src="TOF%20Sequential%20Single%20Peak%20Fit_files/image015.gif" v:shapes="Picture_x0020_20"><![endif]></span></p>
1798
1799<p class=MsoNormal>Next copy these limits to the other PWDR data sets; do <b
1800style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1801mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1802minor-latin'>Edit Limits/Copy</span></b>. A selection dialog box will appear</p>
1803
1804<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1805 id="Picture_x0020_21" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:189.75pt;
1806 height:316.5pt;visibility:visible;mso-wrap-style:square'>
1807 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image016.png"
1808  o:title=""/>
1809</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=422
1810src="TOF%20Sequential%20Single%20Peak%20Fit_files/image017.gif" v:shapes="Picture_x0020_21"><![endif]></span></p>
1811
1812<p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span
1813style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1814mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set All</span></b>
1815and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1816mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1817minor-latin'>OK</span></b>; the limits will be copied to the other histograms.</p>
1818
1819<h2>Step 2. Peak fitting for 1<sup>st</sup> data set.</h2>
1820
1821<p class=MsoNormal>In this step we will select the 10 reflections for single
1822peak fits and fit them. Select <b style='mso-bidi-font-weight:normal'><span
1823style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1824mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak List</span></b>
1825for the 1<sup>st</sup> PWDR data set; it will be empty. To populate it do <b
1826style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1827mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1828minor-latin'>Peak Fitting/Auto Search</span></b>; this will find the 10 peaks
1829and put them in the list and mark them on the plot with vertical blue lines.</p>
1830
1831<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1832 id="Picture_x0020_23" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:466.5pt;
1833 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1834 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image018.png"
1835  o:title=""/>
1836</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=339
1837src="TOF%20Sequential%20Single%20Peak%20Fit_files/image019.gif" v:shapes="Picture_x0020_23"><![endif]></span></p>
1838
1839<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1840 id="Picture_x0020_24" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:466.5pt;
1841 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1842 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image020.png"
1843  o:title=""/>
1844</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1845src="TOF%20Sequential%20Single%20Peak%20Fit_files/image021.gif" v:shapes="Picture_x0020_24"><![endif]></span></p>
1846
1847<p class=MsoNormal>Next do <b style='mso-bidi-font-weight:normal'><span
1848style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1849mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak Fitting/<span
1850class=SpellE>Peakfit</span></span></b> from the menu; a file dialog will appear
1851asking for a file name (I used “<b style='mso-bidi-font-weight:normal'><span
1852style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1853mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>steel</span></b>”)
1854to create a new project. The refinement will then do the initial fit to the 10
1855peaks varying only intensity and background (default of 3 term <span
1856class=SpellE>Chebyschev</span> <span class=SpellE>polynominal</span>). The
1857result is </p>
1858
1859<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1860 id="Picture_x0020_25" o:spid="_x0000_i1049" type="#_x0000_t75" style='width:466.5pt;
1861 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1862 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image022.png"
1863  o:title=""/>
1864</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1865src="TOF%20Sequential%20Single%20Peak%20Fit_files/image023.gif" v:shapes="Picture_x0020_25"><![endif]></span></p>
1866
1867<p class=MsoNormal><span class=GramE>and</span> shows the need for further
1868refinement for both position &amp; peak width. To do this double click on the <b
1869style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1870mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1871minor-latin'>refine</span></b> column heading for <b style='mso-bidi-font-weight:
1872normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1873minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>position</span></b>
1874and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1875mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1876minor-latin'>sigma</span></b> selecting ‘<b style='mso-bidi-font-weight:normal'><span
1877style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1878mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Y</span></b>’
1879from the popup in each case. When done the Peak List should look like</p>
1880
1881<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1882 id="Picture_x0020_26" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:466.5pt;
1883 height:168pt;visibility:visible;mso-wrap-style:square'>
1884 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image024.png"
1885  o:title=""/>
1886</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=224
1887src="TOF%20Sequential%20Single%20Peak%20Fit_files/image025.gif" v:shapes="Picture_x0020_26"><![endif]></span></p>
1888
1889<p class=MsoNormal><span class=GramE>with</span> check marks in three columns.
1890Then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1891mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1892minor-latin'>Peak Fitting/<span class=SpellE>Peakfit</span></span></b>; the fit
1893will be much improved</p>
1894
1895<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1896 id="Picture_x0020_28" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:466.5pt;
1897 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1898 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image026.png"
1899  o:title=""/>
1900</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1901src="TOF%20Sequential%20Single%20Peak%20Fit_files/image027.gif" v:shapes="Picture_x0020_28"><![endif]></span></p>
1902
1903<p class=MsoNormal>I’ve pressed both ‘<b style='mso-bidi-font-weight:normal'><span
1904style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1905mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>W</span></b>’
1906to get the <span style='font-family:Symbol'>D</span>I/<span style='font-family:
1907Symbol'>s</span>(I) curve and ‘<b style='mso-bidi-font-weight:normal'><span
1908style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1909mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>S</span></b>’
1910to see <span class=SpellE>sqrt</span>(intensity) on the plot. The residual for
1911the fit (see console for this) is ~14%; it perhaps could be improved by more
1912background terms but this will not have much effect on the peak parameters.</p>
1913
1914<h2>Step 3. Sequential peak fit</h2>
1915
1916<p class=MsoNormal>To prepare for the sequential peak fitting we need to copy
1917the results from fitting 10 peaks to the other PWDR histograms. Do <b
1918style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1919mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1920minor-latin'>Peak Fitting/Peak copy</span></b>; a selection dialog will appear.
1921Do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1922mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1923minor-latin'>Set All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1924style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1925mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
1926the peak fit data will be copied to the other PWDR histograms. Next do <b
1927style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1928mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1929minor-latin'>Peak Fitting/<span class=SpellE>Seq</span> <span class=SpellE>Peakfit</span></span></b>;
1930again a selection dialog will appear</p>
1931
1932<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1933 id="Picture_x0020_29" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:189.75pt;
1934 height:339pt;visibility:visible;mso-wrap-style:square'>
1935 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image028.png"
1936  o:title=""/>
1937</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=452
1938src="TOF%20Sequential%20Single%20Peak%20Fit_files/image029.gif" v:shapes="Picture_x0020_29"><![endif]></span></p>
1939
1940<p class=MsoNormal>Notice this one does offer the possibility of doing the fit
1941in reverse (i.e. start from the last PWDR entry) and also to copy the result
1942from one fit to the next one in sequence as possibly better starting values for
1943its refinement. We’ll not bother with either here. Do <b style='mso-bidi-font-weight:
1944normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1945minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set
1946All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1947style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1948mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
1949GSAS-II will rapidly do the 10 peak fitting on all 61 PWDR histograms. The
1950final sequential result is displayed</p>
1951
1952<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1953 id="Picture_x0020_30" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:472.5pt;
1954 height:166.5pt;visibility:visible;mso-wrap-style:square'>
1955 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image030.png"
1956  o:title=""/>
1957</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=222
1958src="TOF%20Sequential%20Single%20Peak%20Fit_files/image031.gif" v:shapes="Picture_x0020_30"><![endif]></span></p>
1959
1960<p class=MsoNormal>The table is quite large with &gt;30 columns and 61 rows so
1961I’ve shown only a bit of it. If you select a row, the plot will show the
1962corresponding PWDR plot and fit; this is the same as selecting a PWDR entry in
1963the main data tree (this will respond to arrow keys to step from one PWDR entry
1964to the next and show the corresponding plot). For your first view of the sequential
1965result double click on the <b style='mso-bidi-font-weight:normal'><span
1966style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1967mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
1968column heading; the variation in this value across the sequence will be
1969plotted; each point has the error bar obtained in the refinement</p>
1970
1971<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1972 id="Picture_x0020_31" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:471.75pt;
1973 height:336pt;visibility:visible;mso-wrap-style:square'>
1974 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image032.png"
1975  o:title=""/>
1976</v:shape><![endif]--><![if !vml]><img border=0 width=629 height=448
1977src="TOF%20Sequential%20Single%20Peak%20Fit_files/image033.gif" v:shapes="Picture_x0020_31"><![endif]></span></p>
1978
1979<p class=MsoNormal>This shows the result of a loading/unloading cycle
1980essentially in time (data collection sequence number). More interesting would
1981be to show the dependence on load; we need to set the applied load used for
1982each data set.</p>
1983
1984<h2>Step 4. Import applied load table</h2>
1985
1986<p class=MsoNormal>A hard way to enter the loads is to do each one by hand;
1987they are entered in the <b style='mso-bidi-font-weight:normal'><span
1988style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1989mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sample
1990Parameters</span></b> tree item for each PWDR entry. Select that now for the 1<sup>st</sup>
1991PWDR entry</p>
1992
1993<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1994 id="Picture_x0020_33" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:445.5pt;
1995 height:395.25pt;visibility:visible;mso-wrap-style:square'>
1996 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image034.png"
1997  o:title=""/>
1998</v:shape><![endif]--><![if !vml]><img border=0 width=594 height=527
1999src="TOF%20Sequential%20Single%20Peak%20Fit_files/image035.gif" v:shapes="Picture_x0020_33"><![endif]></span></p>
2000
2001<p class=MsoNormal>Notice there is an entry at the bottom of the table for <b
2002style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2003mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2004minor-latin'>Applied load (MN)</span></b>; you’d have to fill that in for every
2005PWDR data set. However, there is an easier way since a metadata file with this
2006information was provided by the Vulcan Instrument Scientist. To access it do <b
2007style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2008mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2009minor-latin'>Command/Load all</span></b>; a file selection dialog will appear.
2010Choose <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2011mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2012minor-latin'>28902sampleenv_chopped_mean.txt</span></b> and open it; a Select
2013columns dialog box will appear</p>
2014
2015<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2016 id="Picture_x0020_34" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:469.5pt;
2017 height:321.75pt;visibility:visible;mso-wrap-style:square'>
2018 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image036.png"
2019  o:title=""/>
2020</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=429
2021src="TOF%20Sequential%20Single%20Peak%20Fit_files/image037.gif" v:shapes="Picture_x0020_34"><![endif]></span></p>
2022
2023<p class=MsoNormal>Looking over the column headings, one is marked “stress” and
2024another is marked “force”. Their ratio is presumably the cross-section area of
2025the steel rod (in mm<sup>2</sup>). So (counting from zero) the column we want for
2026<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2027mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2028minor-latin'>Applied loa</span></b>d is Column #6 (1<sup>st</sup> value
2029~169.45); select <b style='mso-bidi-font-weight:normal'><span style='font-family:
2030"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2031minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b> from the
2032pulldown under the heading. The table should show</p>
2033
2034<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2035 id="Picture_x0020_35" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:427.5pt;
2036 height:293.25pt;visibility:visible;mso-wrap-style:square'>
2037 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image038.png"
2038  o:title=""/>
2039</v:shape><![endif]--><![if !vml]><img border=0 width=570 height=391
2040src="TOF%20Sequential%20Single%20Peak%20Fit_files/image039.gif" v:shapes="Picture_x0020_35"><![endif]></span></p>
2041
2042<p class=MsoNormal>Notice you can apply conversion factors to the column of
2043values if desired; just enter it in the <b style='mso-bidi-font-weight:normal'><span
2044style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2045mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Modify by</span></b>
2046box.</p>
2047
2048<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
2049style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2050mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2051all the Sample Parameters tables will be updated filling in the appropriate
2052values for <span class=GramE>Applied</span> load.</p>
2053
2054<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2055style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2056mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sequential
2057peak fit results</span></b> from the data tree</p>
2058
2059<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2060 id="Picture_x0020_36" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:426.75pt;
2061 height:198.75pt;visibility:visible;mso-wrap-style:square'>
2062 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image040.png"
2063  o:title=""/>
2064</v:shape><![endif]--><![if !vml]><img border=0 width=569 height=265
2065src="TOF%20Sequential%20Single%20Peak%20Fit_files/image041.gif" v:shapes="Picture_x0020_36"><![endif]></span></p>
2066
2067<p class=MsoNormal>Applied load is a new column entry in the table; double
2068click the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2069mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2070minor-latin'>pos0</span></b> column heading. A new plot will appear</p>
2071
2072<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2073 id="Picture_x0020_37" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:471pt;
2074 height:335.25pt;visibility:visible;mso-wrap-style:square'>
2075 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image032.png"
2076  o:title=""/>
2077</v:shape><![endif]--><![if !vml]><img border=0 width=628 height=447
2078src="TOF%20Sequential%20Single%20Peak%20Fit_files/image042.gif" v:shapes="Picture_x0020_37"><![endif]></span></p>
2079
2080<p class=MsoNormal><span class=GramE>which</span> is unchanged from before. Place
2081the cursor anywhere on the plot (i.e. select it) and press <span class=GramE>the
2082‘<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2083mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2084minor-latin'>s</span></b>’</span> key; a popup dialog will appear.</p>
2085
2086<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2087 id="Picture_x0020_39" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:240pt;
2088 height:232.5pt;visibility:visible;mso-wrap-style:square'>
2089 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image043.png"
2090  o:title=""/>
2091</v:shape><![endif]--><![if !vml]><img border=0 width=320 height=310
2092src="TOF%20Sequential%20Single%20Peak%20Fit_files/image044.gif" v:shapes="Picture_x0020_39"><![endif]></span></p>
2093
2094<p class=MsoNormal>Select <span class=GramE><b style='mso-bidi-font-weight:
2095normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2096minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied</span></b></span><b
2097style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2098mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2099minor-latin'> load</span></b> and press <b style='mso-bidi-font-weight:normal'><span
2100style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2101mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
2102The plot will change (you may have to select ‘<b style='mso-bidi-font-weight:
2103normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2104minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>’
2105again)</p>
2106
2107<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2108 id="Picture_x0020_40" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:466.5pt;
2109 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2110 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image045.png"
2111  o:title=""/>
2112</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2113src="TOF%20Sequential%20Single%20Peak%20Fit_files/image046.gif" v:shapes="Picture_x0020_40"><![endif]><!--[if gte vml 1]><v:shape
2114 id="Picture_x0020_41" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:464.25pt;
2115 height:330pt;visibility:visible;mso-wrap-style:square'>
2116 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image047.png"
2117  o:title=""/>
2118</v:shape><![endif]--><![if !vml]><img border=0 width=619 height=440
2119src="TOF%20Sequential%20Single%20Peak%20Fit_files/image048.gif" v:shapes="Picture_x0020_41"><![endif]></span></p>
2120
2121<p class=MsoNormal>This shows the perfectly linear response of peak position
2122with applied load. Select another <span class=SpellE><b style='mso-bidi-font-weight:
2123normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2124minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos</span></b></span>
2125parameter; the plot will change</p>
2126
2127<p class=MsoNormal><o:p>&nbsp;</o:p></p>
2128
2129<p class=MsoNormal>Pos1 shows hysteresis in a load/unload cycle; some of other
2130peaks will be similar while others will resemble pos0. This would be a good
2131place to do <b style='mso-bidi-font-weight:normal'><span style='font-family:
2132"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2133minor-latin;mso-bidi-theme-font:minor-latin'>File/Save project</span></b>.</p>
2134
2135<h2>Step 5. Sequential data fitting</h2>
2136
2137<p class=MsoNormal>Since pos0 gives a nice straight line response to load, we
2138can try to extract the <span class=SpellE>Hookes</span> Law elastic coefficient
2139for that reflection. To do this we must find the strain from the peak position
2140shift from the zero load value. First select <b style='mso-bidi-font-weight:
2141normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2142minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2143from the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2144mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2145minor-latin'>Sequential results</span></b> table.</p>
2146
2147<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
2148style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_42"
2149 o:spid="_x0000_i1035" type="#_x0000_t75" style='width:466.5pt;height:331.5pt;
2150 visibility:visible;mso-wrap-style:square'>
2151 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image045.png"
2152  o:title=""/>
2153</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2154src="TOF%20Sequential%20Single%20Peak%20Fit_files/image049.gif" v:shapes="Picture_x0020_42"><![endif]></span></p>
2155
2156<p class=MsoNormal>Using the cursor, find the zero load point on the curve and
2157note value for pos0; it will show up in a tool tip displayed as the cursor is
2158positioned. I found pos0=33937 at load=0. We will use this to compute the
2159strain0 = (pos0-33937)/33937; we want this as a new column in the table. To do
2160this do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2161mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2162minor-latin'>Pseudo <span class=SpellE>Vars</span>/Add Formula</span></b>; a
2163new window “Expression Editor” will appear</p>
2164
2165<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2166 id="Picture_x0020_46" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:465pt;
2167 height:255pt;visibility:visible;mso-wrap-style:square'>
2168 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image050.png"
2169  o:title=""/>
2170</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2171src="TOF%20Sequential%20Single%20Peak%20Fit_files/image051.gif" v:shapes="Picture_x0020_46"><![endif]></span></p>
2172
2173<p class=MsoNormal>Enter <b style='mso-bidi-font-weight:normal'><span
2174style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2175mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2176in the box after the + sign; the window will be redrawn</p>
2177
2178<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2179 id="Picture_x0020_47" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:465pt;
2180 height:255pt;visibility:visible;mso-wrap-style:square'>
2181 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image052.png"
2182  o:title=""/>
2183</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2184src="TOF%20Sequential%20Single%20Peak%20Fit_files/image053.gif" v:shapes="Picture_x0020_47"><![endif]></span></p>
2185
2186<p class=MsoNormal>Select ‘<b style='mso-bidi-font-weight:normal'><span
2187style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2188mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>’
2189from the pulldown next to the ‘x’ (your variable name in the equation); a new
2190selection box will appear. Choose <b style='mso-bidi-font-weight:normal'><span
2191style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2192mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2193(<span class=SpellE>pos</span> for the filter can help reduce the choices) from
2194the list and press <b style='mso-bidi-font-weight:normal'><span
2195style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2196mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
2197The window is again redrawn</p>
2198
2199<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2200 id="Picture_x0020_48" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:465pt;
2201 height:255pt;visibility:visible;mso-wrap-style:square'>
2202 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image054.png"
2203  o:title=""/>
2204</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2205src="TOF%20Sequential%20Single%20Peak%20Fit_files/image055.gif" v:shapes="Picture_x0020_48"><![endif]></span></p>
2206
2207<p class=MsoNormal>All looks properly filled in so press <b style='mso-bidi-font-weight:
2208normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2209minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2210the sequential table will now have a new column at the end with the entered
2211equation as its name</p>
2212
2213<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2214 id="Picture_x0020_49" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:466.5pt;
2215 height:192.75pt;visibility:visible;mso-wrap-style:square'>
2216 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image056.png"
2217  o:title=""/>
2218</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=257
2219src="TOF%20Sequential%20Single%20Peak%20Fit_files/image057.gif" v:shapes="Picture_x0020_49"><![endif]></span></p>
2220
2221<p class=MsoNormal>Click on that column heading to see its plot vs load</p>
2222
2223<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2224 id="Picture_x0020_50" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:466.5pt;
2225 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2226 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image058.png"
2227  o:title=""/>
2228</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2229src="TOF%20Sequential%20Single%20Peak%20Fit_files/image059.gif" v:shapes="Picture_x0020_50"><![endif]></span></p>
2230
2231<p class=MsoNormal>This is what we want to fit to get the <span class=SpellE>Hookes</span>
2232Law coefficient. Do <b style='mso-bidi-font-weight:normal'><span
2233style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2234mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Parametric
2235Fit/Add equation</span></b>; the Expression Editor window will appear</p>
2236
2237<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2238 id="Picture_x0020_51" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;
2239 height:255pt;visibility:visible;mso-wrap-style:square'>
2240 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image060.png"
2241  o:title=""/>
2242</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2243src="TOF%20Sequential%20Single%20Peak%20Fit_files/image061.gif" v:shapes="Picture_x0020_51"><![endif]></span></p>
2244
2245<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2246style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2247mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>
2248from the pull down on the left of the = sign and pick <b style='mso-bidi-font-weight:
2249normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2250minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2251from the list. Then enter <b style='mso-bidi-font-weight:normal'><span
2252style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2253mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m*<span
2254class=SpellE>y+b</span></span></b> in the box to the right of the = sign. NB: x
2255was used earlier so we can’t use it here. That establishes the equation you are
2256trying to fit to the data. The window will change to give</p>
2257
2258<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2259 id="Picture_x0020_52" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:465pt;
2260 height:255pt;visibility:visible;mso-wrap-style:square'>
2261 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image062.png"
2262  o:title=""/>
2263</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2264src="TOF%20Sequential%20Single%20Peak%20Fit_files/image063.gif" v:shapes="Picture_x0020_52"><![endif]></span></p>
2265
2266<p class=MsoNormal>For the three pull downs, <b style='mso-bidi-font-weight:
2267normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2268minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>b</span></b>
2269is <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2270mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2271minor-latin'>Free</span></b>, <b style='mso-bidi-font-weight:normal'><span
2272style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2273mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m</span></b>
2274is also <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2275mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2276minor-latin'>Free</span></b> (the fitting variables) and <b style='mso-bidi-font-weight:
2277normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2278minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>y</span></b>
2279is a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2280mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2281minor-latin'>Global</span></b>; select <b style='mso-bidi-font-weight:normal'><span
2282style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2283mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b>
2284for it. The Editor will change again</p>
2285
2286<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2287 id="Picture_x0020_53" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt;
2288 height:255pt;visibility:visible;mso-wrap-style:square'>
2289 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image064.png"
2290  o:title=""/>
2291</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2292src="TOF%20Sequential%20Single%20Peak%20Fit_files/image065.gif" v:shapes="Picture_x0020_53"><![endif]></span></p>
2293
2294<p class=MsoNormal>Press <span class=GramE><b style='mso-bidi-font-weight:normal'><span
2295style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2296mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Fit</span></b></span>
2297or even just <b style='mso-bidi-font-weight:normal'><span style='font-family:
2298"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2299minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>. The console will
2300show the fitting result</p>
2301
2302<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2303 id="Picture_x0020_54" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:243.75pt;
2304 height:120.75pt;visibility:visible;mso-wrap-style:square'>
2305 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image066.png"
2306  o:title=""/>
2307</v:shape><![endif]--><![if !vml]><img border=0 width=325 height=161
2308src="TOF%20Sequential%20Single%20Peak%20Fit_files/image067.gif" v:shapes="Picture_x0020_54"><![endif]></span></p>
2309
2310<p class=MsoNormal>And the plot will show the best fit line in red; it nicely
2311matches the data.</p>
2312
2313<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2314 id="Picture_x0020_55" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:469.5pt;
2315 height:334.5pt;visibility:visible;mso-wrap-style:square'>
2316 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image068.png"
2317  o:title=""/>
2318</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=446
2319src="TOF%20Sequential%20Single%20Peak%20Fit_files/image069.gif" v:shapes="Picture_x0020_55"><![endif]></span></p>
2320
2321<p class=MsoNormal>The resulting <span class=SpellE>Hookes</span> Law
2322coefficient is 40.38(13<span class=GramE>)x10</span><sup>-6 </sup>MN<sup>-1</sup>
2323for this reflection (austenite 111).<span style='mso-spacerun:yes'> 
2324</span>This end the tutorial; save the project if desired. You can further
2325explore the sequential results and perhaps extract <span class=SpellE>Hookes</span>
2326Law coefficients for the other reflections that show no hysteresis. If you want
2327the look at Bank 2 data (the opposite detector) you should start with a fresh
2328GSAS-II project file and follow this tutorial for it. The ratio of the
2329corresponding slope for the austenite 111 reflection with what we found here
2330should be the Poisson ratio.</p>
2331
2332</div>
2333
2334</body>
2335
2336</html>
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