source: Tutorials/TOF Sequential Single Peak Fit/TOF Sequential Single Peak Fit.htm @ 3547

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414  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
415  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
416  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
417  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
418  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
419  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
420  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
421  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
422  <w:LsdException Locked="false" Priority="34" QFormat="true"
423   Name="List Paragraph"/>
424  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
425  <w:LsdException Locked="false" Priority="30" QFormat="true"
426   Name="Intense Quote"/>
427  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
428  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
429  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
430  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
431  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
432  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
433  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
434  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
435  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
436  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
437  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
438  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
439  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
440  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
441  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
442  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
443  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
444  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
445  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
446  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
447  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
448  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
449  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
450  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
451  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
452  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
453  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
454  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
455  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
456  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
457  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
458  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
459  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
460  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
461  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
462  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
463  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
464  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
465  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
466  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
467  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
468  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
469  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
470  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
471  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
472  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
473  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
474  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
475  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
476  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
477  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
478  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
479  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
480  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
481  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
482  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
483  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
484  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
485  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
486  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
487  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
488  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
489  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
490  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
491  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
492  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
493  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
494  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
495  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
496  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
497  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
498  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
499  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
500  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
501  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
502  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
503  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
504  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
505  <w:LsdException Locked="false" Priority="19" QFormat="true"
506   Name="Subtle Emphasis"/>
507  <w:LsdException Locked="false" Priority="21" QFormat="true"
508   Name="Intense Emphasis"/>
509  <w:LsdException Locked="false" Priority="31" QFormat="true"
510   Name="Subtle Reference"/>
511  <w:LsdException Locked="false" Priority="32" QFormat="true"
512   Name="Intense Reference"/>
513  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
514  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
515   UnhideWhenUsed="true" Name="Bibliography"/>
516  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
517   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
518  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
519  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
520  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
521  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
522  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
523  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
524  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
525  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
526  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
527  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
528  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
529  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
530  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
531  <w:LsdException Locked="false" Priority="46"
532   Name="Grid Table 1 Light Accent 1"/>
533  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
534  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
535  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
536  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
537  <w:LsdException Locked="false" Priority="51"
538   Name="Grid Table 6 Colorful Accent 1"/>
539  <w:LsdException Locked="false" Priority="52"
540   Name="Grid Table 7 Colorful Accent 1"/>
541  <w:LsdException Locked="false" Priority="46"
542   Name="Grid Table 1 Light Accent 2"/>
543  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
544  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
545  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
546  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
547  <w:LsdException Locked="false" Priority="51"
548   Name="Grid Table 6 Colorful Accent 2"/>
549  <w:LsdException Locked="false" Priority="52"
550   Name="Grid Table 7 Colorful Accent 2"/>
551  <w:LsdException Locked="false" Priority="46"
552   Name="Grid Table 1 Light Accent 3"/>
553  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
554  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
555  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
556  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
557  <w:LsdException Locked="false" Priority="51"
558   Name="Grid Table 6 Colorful Accent 3"/>
559  <w:LsdException Locked="false" Priority="52"
560   Name="Grid Table 7 Colorful Accent 3"/>
561  <w:LsdException Locked="false" Priority="46"
562   Name="Grid Table 1 Light Accent 4"/>
563  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
564  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
565  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
566  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
567  <w:LsdException Locked="false" Priority="51"
568   Name="Grid Table 6 Colorful Accent 4"/>
569  <w:LsdException Locked="false" Priority="52"
570   Name="Grid Table 7 Colorful Accent 4"/>
571  <w:LsdException Locked="false" Priority="46"
572   Name="Grid Table 1 Light Accent 5"/>
573  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
574  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
575  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
576  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
577  <w:LsdException Locked="false" Priority="51"
578   Name="Grid Table 6 Colorful Accent 5"/>
579  <w:LsdException Locked="false" Priority="52"
580   Name="Grid Table 7 Colorful Accent 5"/>
581  <w:LsdException Locked="false" Priority="46"
582   Name="Grid Table 1 Light Accent 6"/>
583  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
584  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
585  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
586  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
587  <w:LsdException Locked="false" Priority="51"
588   Name="Grid Table 6 Colorful Accent 6"/>
589  <w:LsdException Locked="false" Priority="52"
590   Name="Grid Table 7 Colorful Accent 6"/>
591  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
592  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
593  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
594  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
595  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
596  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
597  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
598  <w:LsdException Locked="false" Priority="46"
599   Name="List Table 1 Light Accent 1"/>
600  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
601  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
602  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
603  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
604  <w:LsdException Locked="false" Priority="51"
605   Name="List Table 6 Colorful Accent 1"/>
606  <w:LsdException Locked="false" Priority="52"
607   Name="List Table 7 Colorful Accent 1"/>
608  <w:LsdException Locked="false" Priority="46"
609   Name="List Table 1 Light Accent 2"/>
610  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
611  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
612  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
613  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
614  <w:LsdException Locked="false" Priority="51"
615   Name="List Table 6 Colorful Accent 2"/>
616  <w:LsdException Locked="false" Priority="52"
617   Name="List Table 7 Colorful Accent 2"/>
618  <w:LsdException Locked="false" Priority="46"
619   Name="List Table 1 Light Accent 3"/>
620  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
621  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
622  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
623  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
624  <w:LsdException Locked="false" Priority="51"
625   Name="List Table 6 Colorful Accent 3"/>
626  <w:LsdException Locked="false" Priority="52"
627   Name="List Table 7 Colorful Accent 3"/>
628  <w:LsdException Locked="false" Priority="46"
629   Name="List Table 1 Light Accent 4"/>
630  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
631  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
632  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
633  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
634  <w:LsdException Locked="false" Priority="51"
635   Name="List Table 6 Colorful Accent 4"/>
636  <w:LsdException Locked="false" Priority="52"
637   Name="List Table 7 Colorful Accent 4"/>
638  <w:LsdException Locked="false" Priority="46"
639   Name="List Table 1 Light Accent 5"/>
640  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
641  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
642  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
643  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
644  <w:LsdException Locked="false" Priority="51"
645   Name="List Table 6 Colorful Accent 5"/>
646  <w:LsdException Locked="false" Priority="52"
647   Name="List Table 7 Colorful Accent 5"/>
648  <w:LsdException Locked="false" Priority="46"
649   Name="List Table 1 Light Accent 6"/>
650  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
651  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
652  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
653  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
654  <w:LsdException Locked="false" Priority="51"
655   Name="List Table 6 Colorful Accent 6"/>
656  <w:LsdException Locked="false" Priority="52"
657   Name="List Table 7 Colorful Accent 6"/>
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1153-->
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1188</head>
1189
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1192<div class=WordSection1>
1193
1194<h1>TOF Sequential Single Peak Fits and loading curve</h1>
1195
1196<p class=MsoNormal>A common analysis of diffraction data obtained from a
1197polycrystalline sample subjected to a changing uniaxial load is to follow the behavior
1198of fitted single peaks. The data sets considered here were obtained on the
1199Vulcan diffractometer at SNS, Oak Ridge National Laboratory. The layout of the
1200instrument</p>
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1650
1651<p class=MsoNormal><span class=GramE>has</span> panels of detectors on both
1652sides of the sample (in this case a Œ” stainless steel rod) oriented so that
1653the loading axis is 45° to the incident neutron beam. Thus one detector “Bank
16541” only views crystallites with diffraction vectors parallel to the loading
1655direction while the other “Bank 2” only views crystallites with diffraction
1656vectors perpendicular to the load. In such an experiment, as the load is
1657increased (as a tension) we would expect that the reflections would shift to
1658higher d-<span class=SpellE>spacings</span> in Bank 1 and those seen in Bank 2
1659would shift to smaller d-<span class=SpellE>spacings</span>. If the load is a
1660compression, then the responses in the reflection positions would be reversed.
1661The shift records the response “strain” of the crystal lattice to the load
1662“stress”. The particular experiment done here was to subject the steel rod to
1663ten tension/compression cycles over 13 hours recording a diffraction pattern
1664from the two detectors each minute yielding ~800 data sets. The 1<sup>st</sup>
1665loading cycle was done slowly over ~4.5hrs and the remaining ones done ~1hr
1666each; we will focus on just the 1<sup>st</sup> cycle for this tutorial
1667comprising 61 powder patterns. Note that menu entries and user input are shown
1668in bold face below as <b style='mso-bidi-font-weight:normal'><span
1669style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1670mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Help/About
1671GSAS-II</span></b>, which lists first the name of the menu (here <b
1672style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1673mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1674minor-latin'>Help</span></b>) and second the name of the entry in the menu
1675(here <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1676mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1677minor-latin'>About GSAS-II</span></b>).</p>
1678
1679<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
1680href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
1681text-underline:none'>start GSAS-II</span></a></span></u>.</p>
1682
1683<h2>Step 1. Import the powder data for sequential fitting</h2>
1684
1685<p class=MsoNormal>Use the <b style='mso-bidi-font-weight:normal'>Import/Powder
1686data/from GSAS powder data file</b> menu item to read the data file into the
1687current GSAS-II project. </p>
1688
1689<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
1690
1691<p class=MsoNormal>A file selection dialog will be shown; its appearance will
1692depend on your OS. Change the search directory to <b style='mso-bidi-font-weight:
1693normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1694minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>TOF
1695Sequential Single Peak Fit/data</span></b> and then select all the *.<span
1696class=SpellE>gsa</span> files (435.gda-495.gda) and press <b style='mso-bidi-font-weight:
1697normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1698minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Open</span></b>.
1699A small popup window will appear</p>
1700
1701<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1702 id="Picture_x0020_14" o:spid="_x0000_i1059" type="#_x0000_t75" style='width:176.25pt;
1703 height:227.25pt;visibility:visible;mso-wrap-style:square'>
1704 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image002.png"
1705  o:title=""/>
1706</v:shape><![endif]--><![if !vml]><img border=0 width=235 height=303
1707src="TOF%20Sequential%20Single%20Peak%20Fit_files/image003.gif" v:shapes="Picture_x0020_14"><![endif]></span></p>
1708
1709<p class=MsoNormal>Select just <b style='mso-bidi-font-weight:normal'><span
1710style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1711mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>435.gda BANK
17121</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1713style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1714mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
1715After a pause while the data is read the main window will highlight the last
1716entry (PWDR 495.gda Bank1)</p>
1717
1718<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1719 id="Picture_x0020_15" o:spid="_x0000_i1058" type="#_x0000_t75" style='width:466.5pt;
1720 height:174pt;visibility:visible;mso-wrap-style:square'>
1721 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image004.png"
1722  o:title=""/>
1723</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=232
1724src="TOF%20Sequential%20Single%20Peak%20Fit_files/image005.gif" v:shapes="Picture_x0020_15"><![endif]></span></p>
1725
1726<p class=MsoNormal><span class=GramE>and</span> show the powder pattern</p>
1727
1728<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1729 id="Picture_x0020_16" o:spid="_x0000_i1057" type="#_x0000_t75" style='width:466.5pt;
1730 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1731 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image006.png"
1732  o:title=""/>
1733</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1734src="TOF%20Sequential%20Single%20Peak%20Fit_files/image007.gif" v:shapes="Picture_x0020_16"><![endif]></span></p>
1735
1736<p class=MsoNormal>You may start here but it is slightly better to start with
1737the 1<sup>st</sup> data set; select <b style='mso-bidi-font-weight:normal'><span
1738style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1739mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PWDR 435.gda
1740BANK 1</span></b> from the tree (press the ‘<b style='mso-bidi-font-weight:
1741normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1742minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>+</span></b>’
1743to expand it) and select <b style='mso-bidi-font-weight:normal'><span
1744style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1745mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Limits</span></b></p>
1746
1747<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1748 id="Picture_x0020_17" o:spid="_x0000_i1056" type="#_x0000_t75" style='width:467.25pt;
1749 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1750 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image008.png"
1751  o:title=""/>
1752</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
1753src="TOF%20Sequential%20Single%20Peak%20Fit_files/image009.gif" v:shapes="Picture_x0020_17"><![endif]></span></p>
1754
1755<p class=MsoNormal>The plot shows the current limits as vertical green &amp;
1756red dashed lines.</p>
1757
1758<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1759 id="Picture_x0020_18" o:spid="_x0000_i1055" type="#_x0000_t75" style='width:467.25pt;
1760 height:333pt;visibility:visible;mso-wrap-style:square'>
1761 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image010.png"
1762  o:title=""/>
1763</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=444
1764src="TOF%20Sequential%20Single%20Peak%20Fit_files/image011.gif" v:shapes="Picture_x0020_18"><![endif]></span></p>
1765
1766<p class=MsoNormal>Set the <span class=SpellE><b style='mso-bidi-font-weight:
1767normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1768minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmax</span></b></span>
1769value to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1770mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1771minor-latin'>37000</span></b> and the <span class=SpellE><b style='mso-bidi-font-weight:
1772normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1773minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmin</span></b></span>
1774to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1775mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1776minor-latin'>11000</span></b>; this will encompass the 1<sup>st</sup> 10 peaks
1777of the powder pattern.</p>
1778
1779<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1780 id="Picture_x0020_19" o:spid="_x0000_i1054" type="#_x0000_t75" style='width:467.25pt;
1781 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1782 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image012.png"
1783  o:title=""/>
1784</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
1785src="TOF%20Sequential%20Single%20Peak%20Fit_files/image013.gif" v:shapes="Picture_x0020_19"><![endif]></span></p>
1786
1787<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1788 id="Picture_x0020_20" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:466.5pt;
1789 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1790 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image014.png"
1791  o:title=""/>
1792</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1793src="TOF%20Sequential%20Single%20Peak%20Fit_files/image015.gif" v:shapes="Picture_x0020_20"><![endif]></span></p>
1794
1795<p class=MsoNormal>Next copy these limits to the other PWDR data sets; do <b
1796style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1797mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1798minor-latin'>Edit Limits/Copy</span></b>. A selection dialog box will appear</p>
1799
1800<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1801 id="Picture_x0020_21" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:189.75pt;
1802 height:316.5pt;visibility:visible;mso-wrap-style:square'>
1803 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image016.png"
1804  o:title=""/>
1805</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=422
1806src="TOF%20Sequential%20Single%20Peak%20Fit_files/image017.gif" v:shapes="Picture_x0020_21"><![endif]></span></p>
1807
1808<p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span
1809style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1810mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set All</span></b>
1811and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1812mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1813minor-latin'>OK</span></b>; the limits will be copied to the other histograms.</p>
1814
1815<h2>Step 2. Peak fitting for 1<sup>st</sup> data set.</h2>
1816
1817<p class=MsoNormal>In this step we will select the 10 reflections for single
1818peak fits and fit them. Select <b style='mso-bidi-font-weight:normal'><span
1819style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1820mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak List</span></b>
1821for the 1<sup>st</sup> PWDR data set; it will be empty. To populate it do <b
1822style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1823mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1824minor-latin'>Peak Fitting/Auto Search</span></b>; this will find the 10 peaks
1825and put them in the list and mark them on the plot with vertical blue lines.</p>
1826
1827<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1828 id="Picture_x0020_23" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:466.5pt;
1829 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1830 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image018.png"
1831  o:title=""/>
1832</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=339
1833src="TOF%20Sequential%20Single%20Peak%20Fit_files/image019.gif" v:shapes="Picture_x0020_23"><![endif]></span></p>
1834
1835<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1836 id="Picture_x0020_24" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:466.5pt;
1837 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1838 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image020.png"
1839  o:title=""/>
1840</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1841src="TOF%20Sequential%20Single%20Peak%20Fit_files/image021.gif" v:shapes="Picture_x0020_24"><![endif]></span></p>
1842
1843<p class=MsoNormal>Next do <b style='mso-bidi-font-weight:normal'><span
1844style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1845mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak Fitting/<span
1846class=SpellE>Peakfit</span></span></b> from the menu; a file dialog will appear
1847asking for a file name (I used “<b style='mso-bidi-font-weight:normal'><span
1848style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1849mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>steel</span></b>”)
1850to create a new project. The refinement will then do the initial fit to the 10
1851peaks varying only intensity and background (default of 3 term <span
1852class=SpellE>Chebyschev</span> <span class=SpellE>polynominal</span>). The
1853result is </p>
1854
1855<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1856 id="Picture_x0020_25" o:spid="_x0000_i1049" type="#_x0000_t75" style='width:466.5pt;
1857 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1858 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image022.png"
1859  o:title=""/>
1860</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1861src="TOF%20Sequential%20Single%20Peak%20Fit_files/image023.gif" v:shapes="Picture_x0020_25"><![endif]></span></p>
1862
1863<p class=MsoNormal><span class=GramE>and</span> shows the need for further
1864refinement for both position &amp; peak width. To do this double click on the <b
1865style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1866mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1867minor-latin'>refine</span></b> column heading for <b style='mso-bidi-font-weight:
1868normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1869minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>position</span></b>
1870and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1871mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1872minor-latin'>sigma</span></b> selecting ‘<b style='mso-bidi-font-weight:normal'><span
1873style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1874mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Y</span></b>’
1875from the popup in each case. When done the Peak List should look like</p>
1876
1877<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1878 id="Picture_x0020_26" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:466.5pt;
1879 height:168pt;visibility:visible;mso-wrap-style:square'>
1880 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image024.png"
1881  o:title=""/>
1882</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=224
1883src="TOF%20Sequential%20Single%20Peak%20Fit_files/image025.gif" v:shapes="Picture_x0020_26"><![endif]></span></p>
1884
1885<p class=MsoNormal><span class=GramE>with</span> check marks in three columns.
1886Then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1887mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1888minor-latin'>Peak Fitting/<span class=SpellE>Peakfit</span></span></b>; the fit
1889will be much improved</p>
1890
1891<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1892 id="Picture_x0020_28" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:466.5pt;
1893 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1894 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image026.png"
1895  o:title=""/>
1896</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1897src="TOF%20Sequential%20Single%20Peak%20Fit_files/image027.gif" v:shapes="Picture_x0020_28"><![endif]></span></p>
1898
1899<p class=MsoNormal>I’ve pressed both ‘<b style='mso-bidi-font-weight:normal'><span
1900style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1901mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>W</span></b>’
1902to get the <span style='font-family:Symbol'>D</span>I/<span style='font-family:
1903Symbol'>s</span>(I) curve and ‘<b style='mso-bidi-font-weight:normal'><span
1904style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1905mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>S</span></b>’
1906to see <span class=SpellE>sqrt</span>(intensity) on the plot. The residual for
1907the fit (see console for this) is ~14%; it perhaps could be improved by more
1908background terms but this will not have much effect on the peak parameters.</p>
1909
1910<h2>Step 3. Sequential peak fit</h2>
1911
1912<p class=MsoNormal>To prepare for the sequential peak fitting we need to copy
1913the results from fitting 10 peaks to the other PWDR histograms. Do <b
1914style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1915mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1916minor-latin'>Peak Fitting/Peak copy</span></b>; a selection dialog will appear.
1917Do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1918mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1919minor-latin'>Set All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1920style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1921mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
1922the peak fit data will be copied to the other PWDR histograms. Next do <b
1923style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1924mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1925minor-latin'>Peak Fitting/<span class=SpellE>Seq</span> <span class=SpellE>Peakfit</span></span></b>;
1926again a selection dialog will appear</p>
1927
1928<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1929 id="Picture_x0020_29" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:189.75pt;
1930 height:339pt;visibility:visible;mso-wrap-style:square'>
1931 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image028.png"
1932  o:title=""/>
1933</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=452
1934src="TOF%20Sequential%20Single%20Peak%20Fit_files/image029.gif" v:shapes="Picture_x0020_29"><![endif]></span></p>
1935
1936<p class=MsoNormal>Notice this one does offer the possibility of doing the fit
1937in reverse (i.e. start from the last PWDR entry) and also to copy the result
1938from one fit to the next one in sequence as possibly better starting values for
1939its refinement. We’ll not bother with either here. Do <b style='mso-bidi-font-weight:
1940normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1941minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set
1942All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1943style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1944mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
1945GSAS-II will rapidly do the 10 peak fitting on all 61 PWDR histograms. The
1946final sequential result is displayed</p>
1947
1948<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1949 id="Picture_x0020_30" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:472.5pt;
1950 height:166.5pt;visibility:visible;mso-wrap-style:square'>
1951 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image030.png"
1952  o:title=""/>
1953</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=222
1954src="TOF%20Sequential%20Single%20Peak%20Fit_files/image031.gif" v:shapes="Picture_x0020_30"><![endif]></span></p>
1955
1956<p class=MsoNormal>The table is quite large with &gt;30 columns and 61 rows so
1957I’ve shown only a bit of it. If you select a row, the plot will show the
1958corresponding PWDR plot and fit; this is the same as selecting a PWDR entry in
1959the main data tree (this will respond to arrow keys to step from one PWDR entry
1960to the next and show the corresponding plot). For your first view of the sequential
1961result double click on the <b style='mso-bidi-font-weight:normal'><span
1962style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1963mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
1964column heading; the variation in this value across the sequence will be
1965plotted; each point has the error bar obtained in the refinement</p>
1966
1967<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1968 id="Picture_x0020_31" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:471.75pt;
1969 height:336pt;visibility:visible;mso-wrap-style:square'>
1970 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image032.png"
1971  o:title=""/>
1972</v:shape><![endif]--><![if !vml]><img border=0 width=629 height=448
1973src="TOF%20Sequential%20Single%20Peak%20Fit_files/image033.gif" v:shapes="Picture_x0020_31"><![endif]></span></p>
1974
1975<p class=MsoNormal>This shows the result of a loading/unloading cycle
1976essentially in time (data collection sequence number). More interesting would
1977be to show the dependence on load; we need to set the applied load used for
1978each data set.</p>
1979
1980<h2>Step 4. Import applied load table</h2>
1981
1982<p class=MsoNormal>A hard way to enter the loads is to do each one by hand;
1983they are entered in the <b style='mso-bidi-font-weight:normal'><span
1984style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1985mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sample
1986Parameters</span></b> tree item for each PWDR entry. Select that now for the 1<sup>st</sup>
1987PWDR entry</p>
1988
1989<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1990 id="Picture_x0020_33" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:445.5pt;
1991 height:395.25pt;visibility:visible;mso-wrap-style:square'>
1992 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image034.png"
1993  o:title=""/>
1994</v:shape><![endif]--><![if !vml]><img border=0 width=594 height=527
1995src="TOF%20Sequential%20Single%20Peak%20Fit_files/image035.gif" v:shapes="Picture_x0020_33"><![endif]></span></p>
1996
1997<p class=MsoNormal>Notice there is an entry at the bottom of the table for <b
1998style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1999mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2000minor-latin'>Applied load (MN)</span></b>; you’d have to fill that in for every
2001PWDR data set. However, there is an easier way since a metadata file with this
2002information was provided by the Vulcan Instrument Scientist. To access it do <b
2003style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2004mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2005minor-latin'>Command/Load all</span></b>; a file selection dialog will appear.
2006Choose <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2007mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2008minor-latin'>28902sampleenv_chopped_mean.txt</span></b> and open it; a Select
2009columns dialog box will appear</p>
2010
2011<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2012 id="Picture_x0020_34" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:469.5pt;
2013 height:321.75pt;visibility:visible;mso-wrap-style:square'>
2014 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image036.png"
2015  o:title=""/>
2016</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=429
2017src="TOF%20Sequential%20Single%20Peak%20Fit_files/image037.gif" v:shapes="Picture_x0020_34"><![endif]></span></p>
2018
2019<p class=MsoNormal>Looking over the column headings, one is marked “stress” and
2020another is marked “force”. Their ratio is presumably the cross-section area of
2021the steel rod (in mm<sup>2</sup>). So (counting from zero) the column we want for
2022<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2023mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2024minor-latin'>Applied loa</span></b>d is Column #6 (1<sup>st</sup> value
2025~169.45); select <b style='mso-bidi-font-weight:normal'><span style='font-family:
2026"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2027minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b> from the
2028pulldown under the heading. The table should show</p>
2029
2030<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2031 id="Picture_x0020_35" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:427.5pt;
2032 height:293.25pt;visibility:visible;mso-wrap-style:square'>
2033 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image038.png"
2034  o:title=""/>
2035</v:shape><![endif]--><![if !vml]><img border=0 width=570 height=391
2036src="TOF%20Sequential%20Single%20Peak%20Fit_files/image039.gif" v:shapes="Picture_x0020_35"><![endif]></span></p>
2037
2038<p class=MsoNormal>Notice you can apply conversion factors to the column of
2039values if desired; just enter it in the <b style='mso-bidi-font-weight:normal'><span
2040style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2041mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Modify by</span></b>
2042box.</p>
2043
2044<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
2045style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2046mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2047all the Sample Parameters tables will be updated filling in the appropriate
2048values for <span class=GramE>Applied</span> load.</p>
2049
2050<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2051style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2052mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sequential
2053peak fit results</span></b> from the data tree</p>
2054
2055<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2056 id="Picture_x0020_36" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:426.75pt;
2057 height:198.75pt;visibility:visible;mso-wrap-style:square'>
2058 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image040.png"
2059  o:title=""/>
2060</v:shape><![endif]--><![if !vml]><img border=0 width=569 height=265
2061src="TOF%20Sequential%20Single%20Peak%20Fit_files/image041.gif" v:shapes="Picture_x0020_36"><![endif]></span></p>
2062
2063<p class=MsoNormal>Applied load is a new column entry in the table; double
2064click the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2065mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2066minor-latin'>pos0</span></b> column heading. A new plot will appear</p>
2067
2068<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2069 id="Picture_x0020_37" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:471pt;
2070 height:335.25pt;visibility:visible;mso-wrap-style:square'>
2071 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image032.png"
2072  o:title=""/>
2073</v:shape><![endif]--><![if !vml]><img border=0 width=628 height=447
2074src="TOF%20Sequential%20Single%20Peak%20Fit_files/image042.gif" v:shapes="Picture_x0020_37"><![endif]></span></p>
2075
2076<p class=MsoNormal><span class=GramE>which</span> is unchanged from before. Place
2077the cursor anywhere on the plot (i.e. select it) and press <span class=GramE>the
2078‘<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2079mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2080minor-latin'>s</span></b>’</span> key; a popup dialog will appear.</p>
2081
2082<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2083 id="Picture_x0020_39" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:240pt;
2084 height:232.5pt;visibility:visible;mso-wrap-style:square'>
2085 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image043.png"
2086  o:title=""/>
2087</v:shape><![endif]--><![if !vml]><img border=0 width=320 height=310
2088src="TOF%20Sequential%20Single%20Peak%20Fit_files/image044.gif" v:shapes="Picture_x0020_39"><![endif]></span></p>
2089
2090<p class=MsoNormal>Select <span class=GramE><b style='mso-bidi-font-weight:
2091normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2092minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied</span></b></span><b
2093style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2094mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2095minor-latin'> load</span></b> and press <b style='mso-bidi-font-weight:normal'><span
2096style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2097mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
2098The plot will change (you may have to select ‘<b style='mso-bidi-font-weight:
2099normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2100minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>’
2101again)</p>
2102
2103<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2104 id="Picture_x0020_40" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:466.5pt;
2105 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2106 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image045.png"
2107  o:title=""/>
2108</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2109src="TOF%20Sequential%20Single%20Peak%20Fit_files/image046.gif" v:shapes="Picture_x0020_40"><![endif]><!--[if gte vml 1]><v:shape
2110 id="Picture_x0020_41" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:464.25pt;
2111 height:330pt;visibility:visible;mso-wrap-style:square'>
2112 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image047.png"
2113  o:title=""/>
2114</v:shape><![endif]--><![if !vml]><img border=0 width=619 height=440
2115src="TOF%20Sequential%20Single%20Peak%20Fit_files/image048.gif" v:shapes="Picture_x0020_41"><![endif]></span></p>
2116
2117<p class=MsoNormal>This shows the perfectly linear response of peak position
2118with applied load. Select another <span class=SpellE><b style='mso-bidi-font-weight:
2119normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2120minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos</span></b></span>
2121parameter; the plot will change</p>
2122
2123<p class=MsoNormal><o:p>&nbsp;</o:p></p>
2124
2125<p class=MsoNormal>Pos1 shows hysteresis in a load/unload cycle; some of other
2126peaks will be similar while others will resemble pos0. This would be a good
2127place to do <b style='mso-bidi-font-weight:normal'><span style='font-family:
2128"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2129minor-latin;mso-bidi-theme-font:minor-latin'>File/Save project</span></b>.</p>
2130
2131<h2>Step 5. Sequential data fitting</h2>
2132
2133<p class=MsoNormal>Since pos0 gives a nice straight line response to load, we
2134can try to extract the <span class=SpellE>Hookes</span> Law elastic coefficient
2135for that reflection. To do this we must find the strain from the peak position
2136shift from the zero load value. First select <b style='mso-bidi-font-weight:
2137normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2138minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2139from the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2140mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2141minor-latin'>Sequential results</span></b> table.</p>
2142
2143<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
2144style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_42"
2145 o:spid="_x0000_i1035" type="#_x0000_t75" style='width:466.5pt;height:331.5pt;
2146 visibility:visible;mso-wrap-style:square'>
2147 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image045.png"
2148  o:title=""/>
2149</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2150src="TOF%20Sequential%20Single%20Peak%20Fit_files/image049.gif" v:shapes="Picture_x0020_42"><![endif]></span></p>
2151
2152<p class=MsoNormal>Using the cursor, find the zero load point on the curve and
2153note value for pos0; it will show up in a tool tip displayed as the cursor is
2154positioned. I found pos0=33937 at load=0. We will use this to compute the
2155strain0 = (pos0-33937)/33937; we want this as a new column in the table. To do
2156this do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2157mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2158minor-latin'>Pseudo <span class=SpellE>Vars</span>/Add Formula</span></b>; a
2159new window “Expression Editor” will appear</p>
2160
2161<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2162 id="Picture_x0020_46" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:465pt;
2163 height:255pt;visibility:visible;mso-wrap-style:square'>
2164 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image050.png"
2165  o:title=""/>
2166</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2167src="TOF%20Sequential%20Single%20Peak%20Fit_files/image051.gif" v:shapes="Picture_x0020_46"><![endif]></span></p>
2168
2169<p class=MsoNormal>Enter <b style='mso-bidi-font-weight:normal'><span
2170style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2171mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2172in the box after the + sign; the window will be redrawn</p>
2173
2174<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2175 id="Picture_x0020_47" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:465pt;
2176 height:255pt;visibility:visible;mso-wrap-style:square'>
2177 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image052.png"
2178  o:title=""/>
2179</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2180src="TOF%20Sequential%20Single%20Peak%20Fit_files/image053.gif" v:shapes="Picture_x0020_47"><![endif]></span></p>
2181
2182<p class=MsoNormal>Select ‘<b style='mso-bidi-font-weight:normal'><span
2183style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2184mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>’
2185from the pulldown next to the ‘x’ (your variable name in the equation); a new
2186selection box will appear. Choose <b style='mso-bidi-font-weight:normal'><span
2187style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2188mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2189(<span class=SpellE>pos</span> for the filter can help reduce the choices) from
2190the list and press <b style='mso-bidi-font-weight:normal'><span
2191style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2192mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
2193The window is again redrawn</p>
2194
2195<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2196 id="Picture_x0020_48" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:465pt;
2197 height:255pt;visibility:visible;mso-wrap-style:square'>
2198 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image054.png"
2199  o:title=""/>
2200</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2201src="TOF%20Sequential%20Single%20Peak%20Fit_files/image055.gif" v:shapes="Picture_x0020_48"><![endif]></span></p>
2202
2203<p class=MsoNormal>All looks properly filled in so press <b style='mso-bidi-font-weight:
2204normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2205minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2206the sequential table will now have a new column at the end with the entered
2207equation as its name</p>
2208
2209<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2210 id="Picture_x0020_49" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:466.5pt;
2211 height:192.75pt;visibility:visible;mso-wrap-style:square'>
2212 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image056.png"
2213  o:title=""/>
2214</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=257
2215src="TOF%20Sequential%20Single%20Peak%20Fit_files/image057.gif" v:shapes="Picture_x0020_49"><![endif]></span></p>
2216
2217<p class=MsoNormal>Click on that column heading to see its plot vs load</p>
2218
2219<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2220 id="Picture_x0020_50" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:466.5pt;
2221 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2222 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image058.png"
2223  o:title=""/>
2224</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2225src="TOF%20Sequential%20Single%20Peak%20Fit_files/image059.gif" v:shapes="Picture_x0020_50"><![endif]></span></p>
2226
2227<p class=MsoNormal>This is what we want to fit to get the <span class=SpellE>Hookes</span>
2228Law coefficient. Do <b style='mso-bidi-font-weight:normal'><span
2229style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2230mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Parametric
2231Fit/Add equation</span></b>; the Expression Editor window will appear</p>
2232
2233<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2234 id="Picture_x0020_51" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;
2235 height:255pt;visibility:visible;mso-wrap-style:square'>
2236 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image060.png"
2237  o:title=""/>
2238</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2239src="TOF%20Sequential%20Single%20Peak%20Fit_files/image061.gif" v:shapes="Picture_x0020_51"><![endif]></span></p>
2240
2241<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2242style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2243mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>
2244from the pull down on the left of the = sign and pick <b style='mso-bidi-font-weight:
2245normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2246minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2247from the list. Then enter <b style='mso-bidi-font-weight:normal'><span
2248style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2249mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m*<span
2250class=SpellE>y+b</span></span></b> in the box to the right of the = sign. NB: x
2251was used earlier so we can’t use it here. That establishes the equation you are
2252trying to fit to the data. The window will change to give</p>
2253
2254<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2255 id="Picture_x0020_52" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:465pt;
2256 height:255pt;visibility:visible;mso-wrap-style:square'>
2257 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image062.png"
2258  o:title=""/>
2259</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2260src="TOF%20Sequential%20Single%20Peak%20Fit_files/image063.gif" v:shapes="Picture_x0020_52"><![endif]></span></p>
2261
2262<p class=MsoNormal>For the three pull downs, <b style='mso-bidi-font-weight:
2263normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2264minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>b</span></b>
2265is <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2266mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2267minor-latin'>Free</span></b>, <b style='mso-bidi-font-weight:normal'><span
2268style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2269mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m</span></b>
2270is also <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2271mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2272minor-latin'>Free</span></b> (the fitting variables) and <b style='mso-bidi-font-weight:
2273normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2274minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>y</span></b>
2275is a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2276mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2277minor-latin'>Global</span></b>; select <b style='mso-bidi-font-weight:normal'><span
2278style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2279mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b>
2280for it. The Editor will change again</p>
2281
2282<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2283 id="Picture_x0020_53" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt;
2284 height:255pt;visibility:visible;mso-wrap-style:square'>
2285 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image064.png"
2286  o:title=""/>
2287</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2288src="TOF%20Sequential%20Single%20Peak%20Fit_files/image065.gif" v:shapes="Picture_x0020_53"><![endif]></span></p>
2289
2290<p class=MsoNormal>Press <span class=GramE><b style='mso-bidi-font-weight:normal'><span
2291style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2292mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Fit</span></b></span>
2293or even just <b style='mso-bidi-font-weight:normal'><span style='font-family:
2294"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2295minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>. The console will
2296show the fitting result</p>
2297
2298<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2299 id="Picture_x0020_54" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:243.75pt;
2300 height:120.75pt;visibility:visible;mso-wrap-style:square'>
2301 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image066.png"
2302  o:title=""/>
2303</v:shape><![endif]--><![if !vml]><img border=0 width=325 height=161
2304src="TOF%20Sequential%20Single%20Peak%20Fit_files/image067.gif" v:shapes="Picture_x0020_54"><![endif]></span></p>
2305
2306<p class=MsoNormal>And the plot will show the best fit line in red; it nicely
2307matches the data.</p>
2308
2309<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2310 id="Picture_x0020_55" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:469.5pt;
2311 height:334.5pt;visibility:visible;mso-wrap-style:square'>
2312 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image068.png"
2313  o:title=""/>
2314</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=446
2315src="TOF%20Sequential%20Single%20Peak%20Fit_files/image069.gif" v:shapes="Picture_x0020_55"><![endif]></span></p>
2316
2317<p class=MsoNormal>The resulting <span class=SpellE>Hookes</span> Law
2318coefficient is 40.38(13<span class=GramE>)x10</span><sup>-6 </sup>MN<sup>-1</sup>
2319for this reflection (austenite 111).<span style='mso-spacerun:yes'> 
2320</span>This end the tutorial; save the project if desired. You can further
2321explore the sequential results and perhaps extract <span class=SpellE>Hookes</span>
2322Law coefficients for the other reflections that show no hysteresis. If you want
2323the look at Bank 2 data (the opposite detector) you should start with a fresh
2324GSAS-II project file and follow this tutorial for it. The ratio of the
2325corresponding slope for the austenite 111 reflection with what we found here
2326should be the Poisson ratio.</p>
2327
2328</div>
2329
2330</body>
2331
2332</html>
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