source: Tutorials/TOF Sequential Single Peak Fit/TOF Sequential Single Peak Fit.htm @ 3476

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414  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
415  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
416  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
417  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
418  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
419  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
420  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
421  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
422  <w:LsdException Locked="false" Priority="34" QFormat="true"
423   Name="List Paragraph"/>
424  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
425  <w:LsdException Locked="false" Priority="30" QFormat="true"
426   Name="Intense Quote"/>
427  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
428  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
429  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
430  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
431  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
432  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
433  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
434  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
435  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
436  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
437  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
438  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
439  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
440  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
441  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
442  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
443  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
444  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
445  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
446  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
447  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
448  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
449  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
450  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
451  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
452  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
453  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
454  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
455  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
456  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
457  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
458  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
459  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
460  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
461  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
462  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
463  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
464  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
465  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
466  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
467  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
468  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
469  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
470  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
471  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
472  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
473  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
474  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
475  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
476  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
477  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
478  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
479  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
480  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
481  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
482  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
483  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
484  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
485  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
486  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
487  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
488  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
489  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
490  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
491  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
492  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
493  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
494  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
495  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
496  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
497  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
498  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
499  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
500  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
501  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
502  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
503  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
504  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
505  <w:LsdException Locked="false" Priority="19" QFormat="true"
506   Name="Subtle Emphasis"/>
507  <w:LsdException Locked="false" Priority="21" QFormat="true"
508   Name="Intense Emphasis"/>
509  <w:LsdException Locked="false" Priority="31" QFormat="true"
510   Name="Subtle Reference"/>
511  <w:LsdException Locked="false" Priority="32" QFormat="true"
512   Name="Intense Reference"/>
513  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
514  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
515   UnhideWhenUsed="true" Name="Bibliography"/>
516  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
517   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
518  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
519  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
520  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
521  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
522  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
523  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
524  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
525  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
526  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
527  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
528  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
529  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
530  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
531  <w:LsdException Locked="false" Priority="46"
532   Name="Grid Table 1 Light Accent 1"/>
533  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
534  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
535  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
536  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
537  <w:LsdException Locked="false" Priority="51"
538   Name="Grid Table 6 Colorful Accent 1"/>
539  <w:LsdException Locked="false" Priority="52"
540   Name="Grid Table 7 Colorful Accent 1"/>
541  <w:LsdException Locked="false" Priority="46"
542   Name="Grid Table 1 Light Accent 2"/>
543  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
544  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
545  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
546  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
547  <w:LsdException Locked="false" Priority="51"
548   Name="Grid Table 6 Colorful Accent 2"/>
549  <w:LsdException Locked="false" Priority="52"
550   Name="Grid Table 7 Colorful Accent 2"/>
551  <w:LsdException Locked="false" Priority="46"
552   Name="Grid Table 1 Light Accent 3"/>
553  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
554  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
555  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
556  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
557  <w:LsdException Locked="false" Priority="51"
558   Name="Grid Table 6 Colorful Accent 3"/>
559  <w:LsdException Locked="false" Priority="52"
560   Name="Grid Table 7 Colorful Accent 3"/>
561  <w:LsdException Locked="false" Priority="46"
562   Name="Grid Table 1 Light Accent 4"/>
563  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
564  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
565  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
566  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
567  <w:LsdException Locked="false" Priority="51"
568   Name="Grid Table 6 Colorful Accent 4"/>
569  <w:LsdException Locked="false" Priority="52"
570   Name="Grid Table 7 Colorful Accent 4"/>
571  <w:LsdException Locked="false" Priority="46"
572   Name="Grid Table 1 Light Accent 5"/>
573  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
574  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
575  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
576  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
577  <w:LsdException Locked="false" Priority="51"
578   Name="Grid Table 6 Colorful Accent 5"/>
579  <w:LsdException Locked="false" Priority="52"
580   Name="Grid Table 7 Colorful Accent 5"/>
581  <w:LsdException Locked="false" Priority="46"
582   Name="Grid Table 1 Light Accent 6"/>
583  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
584  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
585  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
586  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
587  <w:LsdException Locked="false" Priority="51"
588   Name="Grid Table 6 Colorful Accent 6"/>
589  <w:LsdException Locked="false" Priority="52"
590   Name="Grid Table 7 Colorful Accent 6"/>
591  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
592  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
593  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
594  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
595  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
596  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
597  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
598  <w:LsdException Locked="false" Priority="46"
599   Name="List Table 1 Light Accent 1"/>
600  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
601  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
602  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
603  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
604  <w:LsdException Locked="false" Priority="51"
605   Name="List Table 6 Colorful Accent 1"/>
606  <w:LsdException Locked="false" Priority="52"
607   Name="List Table 7 Colorful Accent 1"/>
608  <w:LsdException Locked="false" Priority="46"
609   Name="List Table 1 Light Accent 2"/>
610  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
611  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
612  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
613  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
614  <w:LsdException Locked="false" Priority="51"
615   Name="List Table 6 Colorful Accent 2"/>
616  <w:LsdException Locked="false" Priority="52"
617   Name="List Table 7 Colorful Accent 2"/>
618  <w:LsdException Locked="false" Priority="46"
619   Name="List Table 1 Light Accent 3"/>
620  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
621  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
622  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
623  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
624  <w:LsdException Locked="false" Priority="51"
625   Name="List Table 6 Colorful Accent 3"/>
626  <w:LsdException Locked="false" Priority="52"
627   Name="List Table 7 Colorful Accent 3"/>
628  <w:LsdException Locked="false" Priority="46"
629   Name="List Table 1 Light Accent 4"/>
630  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
631  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
632  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
633  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
634  <w:LsdException Locked="false" Priority="51"
635   Name="List Table 6 Colorful Accent 4"/>
636  <w:LsdException Locked="false" Priority="52"
637   Name="List Table 7 Colorful Accent 4"/>
638  <w:LsdException Locked="false" Priority="46"
639   Name="List Table 1 Light Accent 5"/>
640  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
641  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
642  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
643  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
644  <w:LsdException Locked="false" Priority="51"
645   Name="List Table 6 Colorful Accent 5"/>
646  <w:LsdException Locked="false" Priority="52"
647   Name="List Table 7 Colorful Accent 5"/>
648  <w:LsdException Locked="false" Priority="46"
649   Name="List Table 1 Light Accent 6"/>
650  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
651  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
652  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
653  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
654  <w:LsdException Locked="false" Priority="51"
655   Name="List Table 6 Colorful Accent 6"/>
656  <w:LsdException Locked="false" Priority="52"
657   Name="List Table 7 Colorful Accent 6"/>
658 </w:LatentStyles>
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783        mso-margin-top-alt:auto;
784        margin-right:0in;
785        mso-margin-bottom-alt:auto;
786        margin-left:0in;
787        mso-pagination:widow-orphan;
788        mso-outline-level:5;
789        font-size:12.0pt;
790        font-family:"Times New Roman",serif;
791        mso-fareast-font-family:"Times New Roman";
792        mso-fareast-theme-font:minor-fareast;
793        color:#4F4FFF;
794        font-weight:bold;}
795a:link, span.MsoHyperlink
796        {mso-style-noshow:yes;
797        mso-style-priority:99;
798        color:blue;
799        text-decoration:underline;
800        text-underline:single;}
801a:visited, span.MsoHyperlinkFollowed
802        {mso-style-noshow:yes;
803        mso-style-priority:99;
804        color:purple;
805        text-decoration:underline;
806        text-underline:single;}
807p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap
808        {mso-style-noshow:yes;
809        mso-style-priority:99;
810        mso-style-link:"Document Map Char";
811        margin:0in;
812        margin-bottom:.0001pt;
813        mso-pagination:widow-orphan;
814        font-size:8.0pt;
815        font-family:"Tahoma",sans-serif;
816        mso-fareast-font-family:"Times New Roman";
817        mso-fareast-theme-font:minor-fareast;}
818p
819        {mso-style-noshow:yes;
820        mso-style-priority:99;
821        mso-margin-top-alt:auto;
822        margin-right:0in;
823        mso-margin-bottom-alt:auto;
824        margin-left:0in;
825        mso-pagination:widow-orphan;
826        font-size:12.0pt;
827        font-family:"Times New Roman",serif;
828        mso-fareast-font-family:"Times New Roman";
829        mso-fareast-theme-font:minor-fareast;}
830pre
831        {mso-style-noshow:yes;
832        mso-style-priority:99;
833        mso-style-link:"HTML Preformatted Char";
834        margin:0in;
835        margin-bottom:.0001pt;
836        mso-pagination:widow-orphan;
837        tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt;
838        font-size:10.0pt;
839        font-family:"Courier New";
840        mso-fareast-font-family:"Times New Roman";}
841p.MsoAcetate, li.MsoAcetate, div.MsoAcetate
842        {mso-style-noshow:yes;
843        mso-style-priority:99;
844        mso-style-link:"Balloon Text Char";
845        margin:0in;
846        margin-bottom:.0001pt;
847        mso-pagination:widow-orphan;
848        font-size:8.0pt;
849        font-family:"Tahoma",sans-serif;
850        mso-fareast-font-family:"Times New Roman";
851        mso-fareast-theme-font:minor-fareast;}
852span.MsoPlaceholderText
853        {mso-style-noshow:yes;
854        mso-style-priority:99;
855        mso-style-unhide:no;
856        color:gray;}
857p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing
858        {mso-style-noshow:yes;
859        mso-style-priority:1;
860        mso-style-unhide:no;
861        mso-style-qformat:yes;
862        mso-style-parent:"";
863        margin:0in;
864        margin-bottom:.0001pt;
865        mso-pagination:widow-orphan;
866        font-size:12.0pt;
867        font-family:"Times New Roman",serif;
868        mso-fareast-font-family:"Times New Roman";
869        mso-fareast-theme-font:minor-fareast;}
870p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph
871        {mso-style-noshow:yes;
872        mso-style-priority:34;
873        mso-style-unhide:no;
874        mso-style-qformat:yes;
875        margin-top:0in;
876        margin-right:0in;
877        margin-bottom:0in;
878        margin-left:.5in;
879        margin-bottom:.0001pt;
880        mso-add-space:auto;
881        mso-pagination:widow-orphan;
882        font-size:12.0pt;
883        font-family:"Times New Roman",serif;
884        mso-fareast-font-family:"Times New Roman";
885        mso-fareast-theme-font:minor-fareast;}
886p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst
887        {mso-style-noshow:yes;
888        mso-style-priority:34;
889        mso-style-unhide:no;
890        mso-style-qformat:yes;
891        mso-style-type:export-only;
892        margin-top:0in;
893        margin-right:0in;
894        margin-bottom:0in;
895        margin-left:.5in;
896        margin-bottom:.0001pt;
897        mso-add-space:auto;
898        mso-pagination:widow-orphan;
899        font-size:12.0pt;
900        font-family:"Times New Roman",serif;
901        mso-fareast-font-family:"Times New Roman";
902        mso-fareast-theme-font:minor-fareast;}
903p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle
904        {mso-style-noshow:yes;
905        mso-style-priority:34;
906        mso-style-unhide:no;
907        mso-style-qformat:yes;
908        mso-style-type:export-only;
909        margin-top:0in;
910        margin-right:0in;
911        margin-bottom:0in;
912        margin-left:.5in;
913        margin-bottom:.0001pt;
914        mso-add-space:auto;
915        mso-pagination:widow-orphan;
916        font-size:12.0pt;
917        font-family:"Times New Roman",serif;
918        mso-fareast-font-family:"Times New Roman";
919        mso-fareast-theme-font:minor-fareast;}
920p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast
921        {mso-style-noshow:yes;
922        mso-style-priority:34;
923        mso-style-unhide:no;
924        mso-style-qformat:yes;
925        mso-style-type:export-only;
926        margin-top:0in;
927        margin-right:0in;
928        margin-bottom:0in;
929        margin-left:.5in;
930        margin-bottom:.0001pt;
931        mso-add-space:auto;
932        mso-pagination:widow-orphan;
933        font-size:12.0pt;
934        font-family:"Times New Roman",serif;
935        mso-fareast-font-family:"Times New Roman";
936        mso-fareast-theme-font:minor-fareast;}
937span.MsoIntenseReference
938        {mso-style-priority:32;
939        mso-style-unhide:no;
940        mso-style-qformat:yes;
941        font-variant:small-caps;
942        color:#C0504D;
943        mso-themecolor:accent2;
944        letter-spacing:.25pt;
945        font-weight:bold;
946        text-decoration:underline;
947        text-underline:single;}
948span.Heading1Char
949        {mso-style-name:"Heading 1 Char";
950        mso-style-priority:9;
951        mso-style-unhide:no;
952        mso-style-locked:yes;
953        mso-style-link:"Heading 1";
954        mso-ansi-font-size:24.0pt;
955        mso-bidi-font-size:24.0pt;
956        font-family:"Times New Roman",serif;
957        mso-ascii-font-family:"Times New Roman";
958        mso-fareast-font-family:"Times New Roman";
959        mso-fareast-theme-font:minor-fareast;
960        mso-hansi-font-family:"Times New Roman";
961        mso-bidi-font-family:"Times New Roman";
962        mso-font-kerning:18.0pt;
963        font-weight:bold;}
964span.Heading2Char
965        {mso-style-name:"Heading 2 Char";
966        mso-style-priority:9;
967        mso-style-unhide:no;
968        mso-style-locked:yes;
969        mso-style-link:"Heading 2";
970        mso-ansi-font-size:18.0pt;
971        mso-bidi-font-size:18.0pt;
972        font-family:"Times New Roman",serif;
973        mso-ascii-font-family:"Times New Roman";
974        mso-fareast-font-family:"Times New Roman";
975        mso-fareast-theme-font:minor-fareast;
976        mso-hansi-font-family:"Times New Roman";
977        mso-bidi-font-family:"Times New Roman";
978        font-weight:bold;}
979span.Heading3Char
980        {mso-style-name:"Heading 3 Char";
981        mso-style-noshow:yes;
982        mso-style-priority:9;
983        mso-style-unhide:no;
984        mso-style-locked:yes;
985        mso-style-link:"Heading 3";
986        mso-ansi-font-size:13.5pt;
987        mso-bidi-font-size:13.5pt;
988        font-family:"Times New Roman",serif;
989        mso-ascii-font-family:"Times New Roman";
990        mso-fareast-font-family:"Times New Roman";
991        mso-fareast-theme-font:minor-fareast;
992        mso-hansi-font-family:"Times New Roman";
993        mso-bidi-font-family:"Times New Roman";
994        font-weight:bold;}
995span.Heading4Char
996        {mso-style-name:"Heading 4 Char";
997        mso-style-noshow:yes;
998        mso-style-priority:9;
999        mso-style-unhide:no;
1000        mso-style-locked:yes;
1001        mso-style-link:"Heading 4";
1002        mso-ansi-font-size:13.0pt;
1003        mso-bidi-font-size:13.0pt;
1004        font-family:"Cambria",serif;
1005        mso-ascii-font-family:Cambria;
1006        mso-ascii-theme-font:major-latin;
1007        mso-fareast-font-family:"Times New Roman";
1008        mso-fareast-theme-font:major-fareast;
1009        mso-hansi-font-family:Cambria;
1010        mso-hansi-theme-font:major-latin;
1011        mso-bidi-font-family:"Times New Roman";
1012        mso-bidi-theme-font:major-bidi;
1013        color:#4F81BD;
1014        mso-themecolor:accent1;
1015        font-weight:bold;
1016        font-style:italic;}
1017span.Heading5Char
1018        {mso-style-name:"Heading 5 Char";
1019        mso-style-noshow:yes;
1020        mso-style-priority:9;
1021        mso-style-unhide:no;
1022        mso-style-locked:yes;
1023        mso-style-link:"Heading 5";
1024        mso-ansi-font-size:12.0pt;
1025        mso-bidi-font-size:12.0pt;
1026        font-family:"Times New Roman",serif;
1027        mso-ascii-font-family:"Times New Roman";
1028        mso-fareast-font-family:"Times New Roman";
1029        mso-fareast-theme-font:minor-fareast;
1030        mso-hansi-font-family:"Times New Roman";
1031        mso-bidi-font-family:"Times New Roman";
1032        color:#4F4FFF;
1033        font-weight:bold;}
1034span.HTMLPreformattedChar
1035        {mso-style-name:"HTML Preformatted Char";
1036        mso-style-noshow:yes;
1037        mso-style-priority:99;
1038        mso-style-unhide:no;
1039        mso-style-locked:yes;
1040        mso-style-link:"HTML Preformatted";
1041        mso-ansi-font-size:10.0pt;
1042        mso-bidi-font-size:10.0pt;
1043        font-family:"Courier New";
1044        mso-ascii-font-family:"Courier New";
1045        mso-fareast-font-family:"Times New Roman";
1046        mso-hansi-font-family:"Courier New";
1047        mso-bidi-font-family:"Courier New";}
1048p.msonormal0, li.msonormal0, div.msonormal0
1049        {mso-style-name:msonormal;
1050        mso-style-noshow:yes;
1051        mso-style-priority:99;
1052        mso-style-unhide:no;
1053        mso-margin-top-alt:auto;
1054        margin-right:0in;
1055        mso-margin-bottom-alt:auto;
1056        margin-left:0in;
1057        mso-pagination:widow-orphan;
1058        font-size:12.0pt;
1059        font-family:"Times New Roman",serif;
1060        mso-fareast-font-family:"Times New Roman";
1061        mso-fareast-theme-font:minor-fareast;}
1062span.DocumentMapChar
1063        {mso-style-name:"Document Map Char";
1064        mso-style-noshow:yes;
1065        mso-style-priority:99;
1066        mso-style-unhide:no;
1067        mso-style-locked:yes;
1068        mso-style-link:"Document Map";
1069        mso-ansi-font-size:8.0pt;
1070        mso-bidi-font-size:8.0pt;
1071        font-family:"Tahoma",sans-serif;
1072        mso-ascii-font-family:Tahoma;
1073        mso-fareast-font-family:"Times New Roman";
1074        mso-fareast-theme-font:minor-fareast;
1075        mso-hansi-font-family:Tahoma;
1076        mso-bidi-font-family:Tahoma;}
1077span.BalloonTextChar
1078        {mso-style-name:"Balloon Text Char";
1079        mso-style-noshow:yes;
1080        mso-style-priority:99;
1081        mso-style-unhide:no;
1082        mso-style-locked:yes;
1083        mso-style-link:"Balloon Text";
1084        mso-ansi-font-size:8.0pt;
1085        mso-bidi-font-size:8.0pt;
1086        font-family:"Tahoma",sans-serif;
1087        mso-ascii-font-family:Tahoma;
1088        mso-fareast-font-family:"Times New Roman";
1089        mso-fareast-theme-font:minor-fareast;
1090        mso-hansi-font-family:Tahoma;
1091        mso-bidi-font-family:Tahoma;}
1092span.GSAS-IItextChar
1093        {mso-style-name:"GSAS-II text Char";
1094        mso-style-unhide:no;
1095        mso-style-locked:yes;
1096        mso-style-link:"GSAS-II text";
1097        mso-ansi-font-size:12.0pt;
1098        mso-bidi-font-size:12.0pt;
1099        font-family:"Times New Roman",serif;
1100        mso-ascii-font-family:"Times New Roman";
1101        mso-fareast-font-family:"Times New Roman";
1102        mso-fareast-theme-font:minor-fareast;
1103        mso-hansi-font-family:"Times New Roman";
1104        mso-bidi-font-family:Calibri;
1105        mso-bidi-theme-font:minor-latin;
1106        font-weight:bold;
1107        mso-bidi-font-weight:normal;}
1108p.GSAS-IItext, li.GSAS-IItext, div.GSAS-IItext
1109        {mso-style-name:"GSAS-II text";
1110        mso-style-noshow:yes;
1111        mso-style-priority:99;
1112        mso-style-unhide:no;
1113        mso-style-link:"GSAS-II text Char";
1114        margin:0in;
1115        margin-bottom:.0001pt;
1116        mso-pagination:widow-orphan;
1117        font-size:12.0pt;
1118        font-family:"Calibri",sans-serif;
1119        mso-ascii-font-family:Calibri;
1120        mso-ascii-theme-font:minor-latin;
1121        mso-fareast-font-family:"Times New Roman";
1122        mso-fareast-theme-font:minor-fareast;
1123        mso-hansi-font-family:Calibri;
1124        mso-hansi-theme-font:minor-latin;
1125        mso-bidi-font-family:Calibri;
1126        mso-bidi-theme-font:minor-latin;
1127        font-weight:bold;
1128        mso-bidi-font-weight:normal;}
1129span.SpellE
1130        {mso-style-name:"";
1131        mso-spl-e:yes;}
1132span.GramE
1133        {mso-style-name:"";
1134        mso-gram-e:yes;}
1135.MsoChpDefault
1136        {mso-style-type:export-only;
1137        mso-default-props:yes;
1138        font-size:10.0pt;
1139        mso-ansi-font-size:10.0pt;
1140        mso-bidi-font-size:10.0pt;
1141        font-family:"Calibri",sans-serif;
1142        mso-ascii-font-family:Calibri;
1143        mso-ascii-theme-font:minor-latin;
1144        mso-fareast-font-family:Calibri;
1145        mso-fareast-theme-font:minor-latin;
1146        mso-hansi-font-family:Calibri;
1147        mso-hansi-theme-font:minor-latin;
1148        mso-bidi-font-family:"Times New Roman";
1149        mso-bidi-theme-font:minor-bidi;}
1150@page WordSection1
1151        {size:8.5in 11.0in;
1152        margin:1.0in 1.0in 1.0in 1.0in;
1153        mso-header-margin:.5in;
1154        mso-footer-margin:.5in;
1155        mso-paper-source:0;}
1156div.WordSection1
1157        {page:WordSection1;}
1158 /* List Definitions */
1159 @list l0
1160        {mso-list-id:1325084593;
1161        mso-list-type:hybrid;
1162        mso-list-template-ids:-1895027428 67698689 67698691 67698693 67698689 67698691 67698693 67698689 67698691 67698693;}
1163@list l0:level1
1164        {mso-level-number-format:bullet;
1165        mso-level-text:\F0B7;
1166        mso-level-tab-stop:none;
1167        mso-level-number-position:left;
1168        text-indent:-.25in;
1169        font-family:Symbol;}
1170@list l0:level2
1171        {mso-level-number-format:bullet;
1172        mso-level-text:o;
1173        mso-level-tab-stop:none;
1174        mso-level-number-position:left;
1175        text-indent:-.25in;
1176        font-family:"Courier New";}
1177@list l0:level3
1178        {mso-level-number-format:bullet;
1179        mso-level-text:\F0A7;
1180        mso-level-tab-stop:none;
1181        mso-level-number-position:left;
1182        text-indent:-.25in;
1183        font-family:Wingdings;}
1184@list l0:level4
1185        {mso-level-number-format:bullet;
1186        mso-level-text:\F0B7;
1187        mso-level-tab-stop:none;
1188        mso-level-number-position:left;
1189        text-indent:-.25in;
1190        font-family:Symbol;}
1191@list l0:level5
1192        {mso-level-number-format:bullet;
1193        mso-level-text:o;
1194        mso-level-tab-stop:none;
1195        mso-level-number-position:left;
1196        text-indent:-.25in;
1197        font-family:"Courier New";}
1198@list l0:level6
1199        {mso-level-number-format:bullet;
1200        mso-level-text:\F0A7;
1201        mso-level-tab-stop:none;
1202        mso-level-number-position:left;
1203        text-indent:-.25in;
1204        font-family:Wingdings;}
1205@list l0:level7
1206        {mso-level-number-format:bullet;
1207        mso-level-text:\F0B7;
1208        mso-level-tab-stop:none;
1209        mso-level-number-position:left;
1210        text-indent:-.25in;
1211        font-family:Symbol;}
1212@list l0:level8
1213        {mso-level-number-format:bullet;
1214        mso-level-text:o;
1215        mso-level-tab-stop:none;
1216        mso-level-number-position:left;
1217        text-indent:-.25in;
1218        font-family:"Courier New";}
1219@list l0:level9
1220        {mso-level-number-format:bullet;
1221        mso-level-text:\F0A7;
1222        mso-level-tab-stop:none;
1223        mso-level-number-position:left;
1224        text-indent:-.25in;
1225        font-family:Wingdings;}
1226ol
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1270
1271<h1>TOF Sequential Single Peak Fits and loading curve</h1>
1272
1273<p class=MsoNormal>A common analysis of diffraction data obtained from a
1274polycrystalline sample subjected to a changing uniaxial load is to follow the
1275behavior of fitted single peaks. The data sets considered here were obtained on
1276the Vulcan diffractometer at SNS, Oak Ridge National Laboratory. The layout of
1277the instrument</p>
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1457     mso-bidi-theme-font:minor-bidi;color:black;mso-themecolor:text1;
1458     mso-font-kerning:12.0pt'>°</span><span style='font-size:18.0pt;font-family:
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1460     "Times New Roman";mso-bidi-theme-font:minor-bidi;color:black;mso-themecolor:
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1462     style='mso-spacerun:yes'>               </span>parallel planes “Bank 2”</span><o:p></o:p></p>
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1500     mso-bidi-theme-font:minor-bidi;color:black;mso-themecolor:text1;
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1577     <![if !mso]></td>
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1612     <![if !mso]></td>
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1721
1722<p class=MsoNormal><span class=GramE>has</span> panels of detectors on both sides
1723of the sample (in this case a Œ” stainless steel rod) oriented so that the
1724loading axis is 45° to the incident neutron beam. Thus one detector “Bank 1” only
1725views crystallites with diffraction vectors parallel to the loading direction
1726while the other “Bank 2” only views crystallites with diffraction vectors perpendicular
1727to the load. In such an experiment, as the load is increased (as a tension) we
1728would expect that the reflections would shift to higher d-<span class=SpellE>spacings</span>
1729in Bank 1 and those seen in Bank 2 would shift to smaller d-<span class=SpellE>spacings</span>.
1730If the load is a compression, then the responses in the reflection positions
1731would be reversed. The shift records the response “strain” of the crystal lattice
1732to the load “stress”. The particular experiment done here was to subject the
1733steel rod to ten tension/compression cycles over 13 hours recording a
1734diffraction pattern from the two detectors each minute yielding ~800 data sets.
1735The 1<sup>st</sup> loading cycle was done slowly over ~4.5hrs and the remaining
1736ones done ~1hr each; we will focus on just the 1<sup>st</sup> cycle for this
1737tutorial comprising 61 powder patterns. Note that menu entries and user input
1738are shown in bold face below as <b style='mso-bidi-font-weight:normal'><span
1739style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1740mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Help/About
1741GSAS-II</span></b>, which lists first the name of the menu (here <b
1742style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1743mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1744minor-latin'>Help</span></b>) and second the name of the entry in the menu
1745(here <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1746mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1747minor-latin'>About GSAS-II</span></b>).<o:p></o:p></p>
1748
1749<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
1750href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
1751text-underline:none'>start GSAS-II</span></a></span></u>.</p>
1752
1753<h2>Step 1. Import the powder data for sequential fitting</h2>
1754
1755<p class=MsoNormal>Use the <b style='mso-bidi-font-weight:normal'>Import/Powder
1756data/from GSAS powder data file</b> menu item to read the data file into the
1757current GSAS-II project. <o:p></o:p></p>
1758
1759<p class=MsoNormal><span style='mso-spacerun:yes'> </span><o:p></o:p></p>
1760
1761<p class=MsoNormal>A file selection dialog will be shown; its appearance will
1762depend on your OS. Change the search directory to <b style='mso-bidi-font-weight:
1763normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1764minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>TOF
1765Sequential Single Peak Fit/data</span></b> and then select all the *.<span
1766class=SpellE>gsa</span> files (435.gda-495.gda) and press <b style='mso-bidi-font-weight:
1767normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1768minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Open</span></b>.
1769A small popup window will appear</p>
1770
1771<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1772 id="Picture_x0020_14" o:spid="_x0000_i1059" type="#_x0000_t75" style='width:176.25pt;
1773 height:227.25pt;visibility:visible;mso-wrap-style:square'>
1774 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image003.png"
1775  o:title=""/>
1776</v:shape><![endif]--><![if !vml]><img border=0 width=235 height=303
1777src="TOF%20Sequential%20Single%20Peak%20Fit_files/image029.gif" v:shapes="Picture_x0020_14"><![endif]></span></p>
1778
1779<p class=MsoNormal>Select just <b style='mso-bidi-font-weight:normal'><span
1780style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1781mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>435.gda BANK
17821</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1783style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1784mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
1785After a pause while the data is read the main window will highlight the last
1786entry (PWDR 495.gda Bank1)</p>
1787
1788<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1789 id="Picture_x0020_15" o:spid="_x0000_i1058" type="#_x0000_t75" style='width:466.5pt;
1790 height:174pt;visibility:visible;mso-wrap-style:square'>
1791 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image005.png"
1792  o:title=""/>
1793</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=232
1794src="TOF%20Sequential%20Single%20Peak%20Fit_files/image030.gif" v:shapes="Picture_x0020_15"><![endif]></span></p>
1795
1796<p class=MsoNormal><span class=GramE>and</span> show the powder pattern</p>
1797
1798<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1799 id="Picture_x0020_16" o:spid="_x0000_i1057" type="#_x0000_t75" style='width:466.5pt;
1800 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1801 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image007.png"
1802  o:title=""/>
1803</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1804src="TOF%20Sequential%20Single%20Peak%20Fit_files/image031.gif" v:shapes="Picture_x0020_16"><![endif]></span></p>
1805
1806<p class=MsoNormal>You may start here but it is slightly better to start with
1807the 1<sup>st</sup> data set; select <b style='mso-bidi-font-weight:normal'><span
1808style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1809mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PWDR 435.gda
1810BANK 1</span></b> from the tree (press the ‘<b style='mso-bidi-font-weight:
1811normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1812minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>+</span></b>’
1813to expand it) and select <b style='mso-bidi-font-weight:normal'><span
1814style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1815mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Limits</span></b></p>
1816
1817<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1818 id="Picture_x0020_17" o:spid="_x0000_i1056" type="#_x0000_t75" style='width:467.25pt;
1819 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1820 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image009.png"
1821  o:title=""/>
1822</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
1823src="TOF%20Sequential%20Single%20Peak%20Fit_files/image032.gif" v:shapes="Picture_x0020_17"><![endif]></span></p>
1824
1825<p class=MsoNormal>The plot shows the current limits as vertical green &amp;
1826red dashed lines.</p>
1827
1828<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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1832  o:title=""/>
1833</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=444
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1835
1836<p class=MsoNormal>Set the <span class=SpellE><b style='mso-bidi-font-weight:
1837normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1838minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmax</span></b></span>
1839value to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1840mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1841minor-latin'>37000</span></b> and the <span class=SpellE><b style='mso-bidi-font-weight:
1842normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1843minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Tmin</span></b></span>
1844to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1845mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1846minor-latin'>11000</span></b>; this will encompass the 1<sup>st</sup> 10 peaks
1847of the powder pattern.</p>
1848
1849<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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1851 height:254.25pt;visibility:visible;mso-wrap-style:square'>
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1853  o:title=""/>
1854</v:shape><![endif]--><![if !vml]><img border=0 width=623 height=339
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1856
1857<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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1859 height:331.5pt;visibility:visible;mso-wrap-style:square'>
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1861  o:title=""/>
1862</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1863src="TOF%20Sequential%20Single%20Peak%20Fit_files/image035.gif" v:shapes="Picture_x0020_20"><![endif]></span></p>
1864
1865<p class=MsoNormal>Next copy these limits to the other PWDR data sets; do <b
1866style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1867mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1868minor-latin'>Edit Limits/Copy</span></b>. A selection dialog box will appear</p>
1869
1870<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1871 id="Picture_x0020_21" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:189.75pt;
1872 height:316.5pt;visibility:visible;mso-wrap-style:square'>
1873 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image017.png"
1874  o:title=""/>
1875</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=422
1876src="TOF%20Sequential%20Single%20Peak%20Fit_files/image036.gif" v:shapes="Picture_x0020_21"><![endif]></span></p>
1877
1878<p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span
1879style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1880mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set All</span></b>
1881and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1882mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1883minor-latin'>OK</span></b>; the limits will be copied to the other histograms.</p>
1884
1885<h2>Step 2. Peak fitting for 1<sup>st</sup> data set.</h2>
1886
1887<p class=MsoNormal>In this step we will select the 10 reflections for single
1888peak fits and fit them. Select <b style='mso-bidi-font-weight:normal'><span
1889style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1890mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak List</span></b>
1891for the 1<sup>st</sup> PWDR data set; it will be empty. To populate it do <b
1892style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1893mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1894minor-latin'>Peak Fitting/Auto Search</span></b>; this will find the 10 peaks
1895and put them in the list and mark them on the plot with vertical blue lines.</p>
1896
1897<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1898 id="Picture_x0020_23" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:466.5pt;
1899 height:254.25pt;visibility:visible;mso-wrap-style:square'>
1900 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image019.png"
1901  o:title=""/>
1902</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=339
1903src="TOF%20Sequential%20Single%20Peak%20Fit_files/image037.gif" v:shapes="Picture_x0020_23"><![endif]></span></p>
1904
1905<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1906 id="Picture_x0020_24" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:466.5pt;
1907 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1908 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image021.png"
1909  o:title=""/>
1910</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1911src="TOF%20Sequential%20Single%20Peak%20Fit_files/image038.gif" v:shapes="Picture_x0020_24"><![endif]></span></p>
1912
1913<p class=MsoNormal>Next do <b style='mso-bidi-font-weight:normal'><span
1914style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1915mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Peak Fitting/<span
1916class=SpellE>Peakfit</span></span></b> from the menu; a file dialog will appear
1917asking for a file name (I used “<b style='mso-bidi-font-weight:normal'><span
1918style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1919mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>steel</span></b>”)
1920to create a new project. The refinement will then do the initial fit to the 10
1921peaks varying only intensity and background (default of 3 term <span
1922class=SpellE>Chebyschev</span> <span class=SpellE>polynominal</span>). The
1923result is </p>
1924
1925<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1926 id="Picture_x0020_25" o:spid="_x0000_i1049" type="#_x0000_t75" style='width:466.5pt;
1927 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1928 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image023.png"
1929  o:title=""/>
1930</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1931src="TOF%20Sequential%20Single%20Peak%20Fit_files/image039.gif" v:shapes="Picture_x0020_25"><![endif]></span></p>
1932
1933<p class=MsoNormal><span class=GramE>and</span> shows the need for further
1934refinement for both position &amp; peak width. To do this double click on the <b
1935style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1936mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1937minor-latin'>refine</span></b> column heading for <b style='mso-bidi-font-weight:
1938normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1939minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>position</span></b>
1940and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1941mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1942minor-latin'>sigma</span></b> selecting ‘<b style='mso-bidi-font-weight:normal'><span
1943style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1944mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Y</span></b>’
1945from the popup in each case. When done the Peak List should look like</p>
1946
1947<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1948 id="Picture_x0020_26" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:466.5pt;
1949 height:168pt;visibility:visible;mso-wrap-style:square'>
1950 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image025.png"
1951  o:title=""/>
1952</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=224
1953src="TOF%20Sequential%20Single%20Peak%20Fit_files/image040.gif" v:shapes="Picture_x0020_26"><![endif]></span></p>
1954
1955<p class=MsoNormal><span class=GramE>with</span> check marks in three columns.
1956Then do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1957mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1958minor-latin'>Peak Fitting/<span class=SpellE>Peakfit</span></span></b>; the fit
1959will be much improved</p>
1960
1961<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1962 id="Picture_x0020_28" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:466.5pt;
1963 height:331.5pt;visibility:visible;mso-wrap-style:square'>
1964 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image027.png"
1965  o:title=""/>
1966</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
1967src="TOF%20Sequential%20Single%20Peak%20Fit_files/image041.gif" v:shapes="Picture_x0020_28"><![endif]></span></p>
1968
1969<p class=MsoNormal>I’ve pressed both ‘<b style='mso-bidi-font-weight:normal'><span
1970style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1971mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>W</span></b>’
1972to get the <span style='font-family:Symbol'>D</span>I/<span style='font-family:
1973Symbol'>s</span>(I) curve and ‘<b style='mso-bidi-font-weight:normal'><span
1974style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1975mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>S</span></b>’
1976to see <span class=SpellE>sqrt</span>(intensity) on the plot. The residual for
1977the fit (see console for this) is ~14%; it perhaps could be improved by more
1978background terms but this will not have much effect on the peak parameters.</p>
1979
1980<h2>Step 3. Sequential peak fit</h2>
1981
1982<p class=MsoNormal>To prepare for the sequential peak fitting we need to copy
1983the results from fitting 10 peaks to the other PWDR histograms. Do <b
1984style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1985mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1986minor-latin'>Peak Fitting/Peak copy</span></b>; a selection dialog will appear.
1987Do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1988mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1989minor-latin'>Set All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
1990style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1991mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
1992the peak fit data will be copied to the other PWDR histograms. Next do <b
1993style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1994mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1995minor-latin'>Peak Fitting/<span class=SpellE>Seq</span> <span class=SpellE>Peakfit</span></span></b>;
1996again a selection dialog will appear</p>
1997
1998<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1999 id="Picture_x0020_29" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:189.75pt;
2000 height:339pt;visibility:visible;mso-wrap-style:square'>
2001 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image042.png"
2002  o:title=""/>
2003</v:shape><![endif]--><![if !vml]><img border=0 width=253 height=452
2004src="TOF%20Sequential%20Single%20Peak%20Fit_files/image043.gif" v:shapes="Picture_x0020_29"><![endif]></span></p>
2005
2006<p class=MsoNormal>Notice this one does offer the possibility of doing the fit
2007in reverse (i.e. start from the last PWDR entry) and also to copy the result
2008from one fit to the next one in sequence as possibly better starting values for
2009its refinement. We’ll not bother with either here. Do <b style='mso-bidi-font-weight:
2010normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2011minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set
2012All</span></b> and press <b style='mso-bidi-font-weight:normal'><span
2013style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2014mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2015GSAS-II will rapidly do the 10 peak fitting on all 61 PWDR histograms. The
2016final sequential result is displayed</p>
2017
2018<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2019 id="Picture_x0020_30" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:472.5pt;
2020 height:166.5pt;visibility:visible;mso-wrap-style:square'>
2021 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image044.png"
2022  o:title=""/>
2023</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=222
2024src="TOF%20Sequential%20Single%20Peak%20Fit_files/image045.gif" v:shapes="Picture_x0020_30"><![endif]></span></p>
2025
2026<p class=MsoNormal>The table is quite large with &gt;30 columns and 61 rows so
2027I’ve shown only a bit of it. If you select a row, the plot will show the corresponding
2028PWDR plot and fit; this is the same as selecting a PWDR entry in the main data
2029tree (this will respond to arrow keys to step from one PWDR entry to the next
2030and show the corresponding plot). For your first view of the sequential result
2031double click on the <b style='mso-bidi-font-weight:normal'><span
2032style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2033mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2034column heading; the variation in this value across the sequence will be
2035plotted; each point has the error bar obtained in the refinement</p>
2036
2037<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2038 id="Picture_x0020_31" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:471.75pt;
2039 height:336pt;visibility:visible;mso-wrap-style:square'>
2040 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image046.png"
2041  o:title=""/>
2042</v:shape><![endif]--><![if !vml]><img border=0 width=629 height=448
2043src="TOF%20Sequential%20Single%20Peak%20Fit_files/image047.gif" v:shapes="Picture_x0020_31"><![endif]></span></p>
2044
2045<p class=MsoNormal>This shows the result of a loading/unloading cycle
2046essentially in time (data collection sequence number). More interesting would
2047be to show the dependence on load; we need to set the applied load used for
2048each data set.</p>
2049
2050<h2>Step 4. Import applied load table</h2>
2051
2052<p class=MsoNormal>A hard way to enter the loads is to do each one by hand;
2053they are entered in the <b style='mso-bidi-font-weight:normal'><span
2054style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2055mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sample
2056Parameters</span></b> tree item for each PWDR entry. Select that now for the 1<sup>st</sup>
2057PWDR entry</p>
2058
2059<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2060 id="Picture_x0020_33" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:445.5pt;
2061 height:395.25pt;visibility:visible;mso-wrap-style:square'>
2062 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image051.png"
2063  o:title=""/>
2064</v:shape><![endif]--><![if !vml]><img border=0 width=594 height=527
2065src="TOF%20Sequential%20Single%20Peak%20Fit_files/image066.gif" v:shapes="Picture_x0020_33"><![endif]></span></p>
2066
2067<p class=MsoNormal>Notice there is an entry at the bottom of the table for <b
2068style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2069mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2070minor-latin'>Applied load (MN)</span></b>; you’d have to fill that in for every
2071PWDR data set. However, there is an easier way since a metadata file with this
2072information was provided by the Vulcan Instrument Scientist. To access it do <b
2073style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2074mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2075minor-latin'>Command/Load all</span></b>; a file selection dialog will appear.
2076Choose <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2077mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2078minor-latin'>28902sampleenv_chopped_mean.txt</span></b> and open it; a Select
2079columns dialog box will appear</p>
2080
2081<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2082 id="Picture_x0020_34" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:469.5pt;
2083 height:321.75pt;visibility:visible;mso-wrap-style:square'>
2084 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image053.png"
2085  o:title=""/>
2086</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=429
2087src="TOF%20Sequential%20Single%20Peak%20Fit_files/image067.gif" v:shapes="Picture_x0020_34"><![endif]></span><o:p></o:p></p>
2088
2089<p class=MsoNormal>Looking over the column headings, one is marked “stress” and
2090another is marked “force”. Their ratio is presumably the cross-section area of
2091the steel rod (in mm<sup>2</sup>). So (counting from zero) the column we want
2092for <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2093mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2094minor-latin'>Applied loa</span></b>d is Column #6 (1<sup>st</sup> value
2095~169.45); select <b style='mso-bidi-font-weight:normal'><span style='font-family:
2096"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2097minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b> from the
2098pulldown under the heading. The table should show</p>
2099
2100<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2101 id="Picture_x0020_35" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:427.5pt;
2102 height:293.25pt;visibility:visible;mso-wrap-style:square'>
2103 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image055.png"
2104  o:title=""/>
2105</v:shape><![endif]--><![if !vml]><img border=0 width=570 height=391
2106src="TOF%20Sequential%20Single%20Peak%20Fit_files/image068.gif" v:shapes="Picture_x0020_35"><![endif]></span></p>
2107
2108<p class=MsoNormal>Notice you can apply conversion factors to the column of
2109values if desired; just enter it in the <b style='mso-bidi-font-weight:normal'><span
2110style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2111mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Modify by</span></b>
2112box.</p>
2113
2114<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
2115style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2116mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2117all the Sample Parameters tables will be updated filling in the appropriate
2118values for <span class=GramE>Applied</span> load.</p>
2119
2120<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2121style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2122mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sequential
2123peak fit results</span></b> from the data tree</p>
2124
2125<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2126 id="Picture_x0020_36" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:426.75pt;
2127 height:198.75pt;visibility:visible;mso-wrap-style:square'>
2128 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image057.png"
2129  o:title=""/>
2130</v:shape><![endif]--><![if !vml]><img border=0 width=569 height=265
2131src="TOF%20Sequential%20Single%20Peak%20Fit_files/image069.gif" v:shapes="Picture_x0020_36"><![endif]></span></p>
2132
2133<p class=MsoNormal>Applied load is a new column entry in the table; double
2134click the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2135mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2136minor-latin'>pos0</span></b> column heading. A new plot will appear</p>
2137
2138<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2139 id="Picture_x0020_37" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:471pt;
2140 height:335.25pt;visibility:visible;mso-wrap-style:square'>
2141 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image046.png"
2142  o:title=""/>
2143</v:shape><![endif]--><![if !vml]><img border=0 width=628 height=447
2144src="TOF%20Sequential%20Single%20Peak%20Fit_files/image070.gif" v:shapes="Picture_x0020_37"><![endif]></span></p>
2145
2146<p class=MsoNormal><span class=GramE>which</span> is unchanged from before.
2147Place the cursor anywhere on the plot (i.e. select it) and press <span
2148class=GramE>the ‘<b style='mso-bidi-font-weight:normal'><span style='font-family:
2149"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2150minor-latin;mso-bidi-theme-font:minor-latin'>s</span></b>’</span> key; a popup
2151dialog will appear.</p>
2152
2153<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2154 id="Picture_x0020_39" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:240pt;
2155 height:232.5pt;visibility:visible;mso-wrap-style:square'>
2156 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image060.png"
2157  o:title=""/>
2158</v:shape><![endif]--><![if !vml]><img border=0 width=320 height=310
2159src="TOF%20Sequential%20Single%20Peak%20Fit_files/image071.gif" v:shapes="Picture_x0020_39"><![endif]></span></p>
2160
2161<p class=MsoNormal>Select <span class=GramE><b style='mso-bidi-font-weight:
2162normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2163minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied</span></b></span><b
2164style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2165mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2166minor-latin'> load</span></b> and press <b style='mso-bidi-font-weight:normal'><span
2167style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2168mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
2169The plot will change (you may have to select ‘<b style='mso-bidi-font-weight:
2170normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2171minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>’
2172again)</p>
2173
2174<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2175 id="Picture_x0020_40" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:466.5pt;
2176 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2177 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image062.png"
2178  o:title=""/>
2179</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2180src="TOF%20Sequential%20Single%20Peak%20Fit_files/image072.gif" v:shapes="Picture_x0020_40"><![endif]></span></p>
2181
2182<p class=MsoNormal>This shows the perfectly linear response of peak position
2183with applied load. Select another <span class=SpellE><b style='mso-bidi-font-weight:
2184normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2185minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos</span></b></span>
2186parameter; the plot will change</p>
2187
2188<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2189 id="Picture_x0020_41" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:464.25pt;
2190 height:330pt;visibility:visible;mso-wrap-style:square'>
2191 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image064.png"
2192  o:title=""/>
2193</v:shape><![endif]--><![if !vml]><img border=0 width=619 height=440
2194src="TOF%20Sequential%20Single%20Peak%20Fit_files/image073.gif" v:shapes="Picture_x0020_41"><![endif]></span></p>
2195
2196<p class=MsoNormal>Pos1 shows hysteresis in a load/unload cycle; some of other
2197peaks will be similar while others will resemble pos0. This would be a good
2198place to do <b style='mso-bidi-font-weight:normal'><span style='font-family:
2199"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2200minor-latin;mso-bidi-theme-font:minor-latin'>File/Save project</span></b>.</p>
2201
2202<h2>Step 5. Sequential data fitting</h2>
2203
2204<p class=MsoNormal>Since pos0 gives a nice straight line response to load, we
2205can try to extract the <span class=SpellE>Hookes</span> Law elastic coefficient
2206for that reflection. To do this we must find the strain from the peak position
2207shift from the zero load value. First select <b style='mso-bidi-font-weight:
2208normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2209minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2210from the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2211mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2212minor-latin'>Sequential results</span></b> table.</p>
2213
2214<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
2215style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_42"
2216 o:spid="_x0000_i1035" type="#_x0000_t75" style='width:466.5pt;height:331.5pt;
2217 visibility:visible;mso-wrap-style:square'>
2218 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image062.png"
2219  o:title=""/>
2220</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2221src="TOF%20Sequential%20Single%20Peak%20Fit_files/image095.gif" v:shapes="Picture_x0020_42"><![endif]></span></p>
2222
2223<p class=MsoNormal>Using the cursor, find the zero load point on the curve and
2224note value for pos0; it will show up in a tool tip displayed as the cursor is
2225positioned. I found pos0=33937 at load=0. We will use this to compute the
2226strain0 = (pos0-33937)/33937; we want this as a new column in the table. To do
2227this do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2228mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2229minor-latin'>Pseudo <span class=SpellE>Vars</span>/Add Formula</span></b>; a
2230new window “Expression Editor” will appear</p>
2231
2232<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2233 id="Picture_x0020_46" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:465pt;
2234 height:255pt;visibility:visible;mso-wrap-style:square'>
2235 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image075.png"
2236  o:title=""/>
2237</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2238src="TOF%20Sequential%20Single%20Peak%20Fit_files/image096.gif" v:shapes="Picture_x0020_46"><![endif]></span></p>
2239
2240<p class=MsoNormal>Enter <b style='mso-bidi-font-weight:normal'><span
2241style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2242mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2243in the box after the + sign; the window will be redrawn</p>
2244
2245<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2246 id="Picture_x0020_47" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:465pt;
2247 height:255pt;visibility:visible;mso-wrap-style:square'>
2248 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image077.png"
2249  o:title=""/>
2250</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2251src="TOF%20Sequential%20Single%20Peak%20Fit_files/image097.gif" v:shapes="Picture_x0020_47"><![endif]></span></p>
2252
2253<p class=MsoNormal>Select ‘<b style='mso-bidi-font-weight:normal'><span
2254style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2255mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>’
2256from the pulldown next to the ‘x’ (your variable name in the equation); a new
2257selection box will appear. Choose <b style='mso-bidi-font-weight:normal'><span
2258style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2259mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>pos0</span></b>
2260(<span class=SpellE>pos</span> for the filter can help reduce the choices) from
2261the list and press <b style='mso-bidi-font-weight:normal'><span
2262style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2263mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>.
2264The window is again redrawn</p>
2265
2266<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2267 id="Picture_x0020_48" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:465pt;
2268 height:255pt;visibility:visible;mso-wrap-style:square'>
2269 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image079.png"
2270  o:title=""/>
2271</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2272src="TOF%20Sequential%20Single%20Peak%20Fit_files/image098.gif" v:shapes="Picture_x0020_48"><![endif]></span></p>
2273
2274<p class=MsoNormal>All looks properly filled in so press <b style='mso-bidi-font-weight:
2275normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2276minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>;
2277the sequential table will now have a new column at the end with the entered
2278equation as its name</p>
2279
2280<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2281 id="Picture_x0020_49" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:466.5pt;
2282 height:192.75pt;visibility:visible;mso-wrap-style:square'>
2283 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image081.png"
2284  o:title=""/>
2285</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=257
2286src="TOF%20Sequential%20Single%20Peak%20Fit_files/image099.gif" v:shapes="Picture_x0020_49"><![endif]></span></p>
2287
2288<p class=MsoNormal>Click on that column heading to see its plot vs load</p>
2289
2290<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2291 id="Picture_x0020_50" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:466.5pt;
2292 height:331.5pt;visibility:visible;mso-wrap-style:square'>
2293 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image083.png"
2294  o:title=""/>
2295</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=442
2296src="TOF%20Sequential%20Single%20Peak%20Fit_files/image100.gif" v:shapes="Picture_x0020_50"><![endif]></span></p>
2297
2298<p class=MsoNormal>This is what we want to fit to get the <span class=SpellE>Hookes</span>
2299Law coefficient. Do <b style='mso-bidi-font-weight:normal'><span
2300style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2301mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Parametric
2302Fit/Add equation</span></b>; the Expression Editor window will appear</p>
2303
2304<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2305 id="Picture_x0020_51" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;
2306 height:255pt;visibility:visible;mso-wrap-style:square'>
2307 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image085.png"
2308  o:title=""/>
2309</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2310src="TOF%20Sequential%20Single%20Peak%20Fit_files/image101.gif" v:shapes="Picture_x0020_51"><![endif]></span></p>
2311
2312<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
2313style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2314mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Global</span></b>
2315from the pull down on the left of the = sign and pick <b style='mso-bidi-font-weight:
2316normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2317minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>(x-33937)/33937</span></b>
2318from the list. Then enter <b style='mso-bidi-font-weight:normal'><span
2319style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2320mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m*<span
2321class=SpellE>y+b</span></span></b> in the box to the right of the = sign. NB: x
2322was used earlier so we can’t use it here. That establishes the equation you are
2323trying to fit to the data. The window will change to give</p>
2324
2325<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2326 id="Picture_x0020_52" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:465pt;
2327 height:255pt;visibility:visible;mso-wrap-style:square'>
2328 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image087.png"
2329  o:title=""/>
2330</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2331src="TOF%20Sequential%20Single%20Peak%20Fit_files/image102.gif" v:shapes="Picture_x0020_52"><![endif]></span></p>
2332
2333<p class=MsoNormal>For the three pull downs, <b style='mso-bidi-font-weight:
2334normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2335minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>b</span></b>
2336is <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2337mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2338minor-latin'>Free</span></b>, <b style='mso-bidi-font-weight:normal'><span
2339style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2340mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>m</span></b>
2341is also <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2342mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2343minor-latin'>Free</span></b> (the fitting variables) and <b style='mso-bidi-font-weight:
2344normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
2345minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>y</span></b>
2346is a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2347mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
2348minor-latin'>Global</span></b>; select <b style='mso-bidi-font-weight:normal'><span
2349style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2350mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Applied load</span></b>
2351for it. The Editor will change again</p>
2352
2353<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2354 id="Picture_x0020_53" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt;
2355 height:255pt;visibility:visible;mso-wrap-style:square'>
2356 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image089.png"
2357  o:title=""/>
2358</v:shape><![endif]--><![if !vml]><img border=0 width=620 height=340
2359src="TOF%20Sequential%20Single%20Peak%20Fit_files/image103.gif" v:shapes="Picture_x0020_53"><![endif]></span></p>
2360
2361<p class=MsoNormal>Press <span class=GramE><b style='mso-bidi-font-weight:normal'><span
2362style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2363mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Fit</span></b></span>
2364or even just <b style='mso-bidi-font-weight:normal'><span style='font-family:
2365"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
2366minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>. The console will
2367show the fitting result</p>
2368
2369<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2370 id="Picture_x0020_54" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:243.75pt;
2371 height:120.75pt;visibility:visible;mso-wrap-style:square'>
2372 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image091.png"
2373  o:title=""/>
2374</v:shape><![endif]--><![if !vml]><img border=0 width=325 height=161
2375src="TOF%20Sequential%20Single%20Peak%20Fit_files/image104.gif" v:shapes="Picture_x0020_54"><![endif]></span></p>
2376
2377<p class=MsoNormal>And the plot will show the best fit line in red; it nicely
2378matches the data.</p>
2379
2380<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2381 id="Picture_x0020_55" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:469.5pt;
2382 height:334.5pt;visibility:visible;mso-wrap-style:square'>
2383 <v:imagedata src="TOF%20Sequential%20Single%20Peak%20Fit_files/image093.png"
2384  o:title=""/>
2385</v:shape><![endif]--><![if !vml]><img border=0 width=626 height=446
2386src="TOF%20Sequential%20Single%20Peak%20Fit_files/image105.gif" v:shapes="Picture_x0020_55"><![endif]></span></p>
2387
2388<p class=MsoNormal>The resulting <span class=SpellE>Hookes</span> Law
2389coefficient is 40.38(13<span class=GramE>)x10</span><sup>-6 </sup>MN for this
2390reflection (austenite 111).<span style='mso-spacerun:yes'>  </span>This end the
2391tutorial; save the project if desired. You can further explore the sequential
2392results and perhaps extract <span class=SpellE>Hookes</span> Law coefficients
2393for the other reflections that show no hysteresis. If you want the look at Bank
23942 data (the opposite detector) you should start with a fresh GSAS-II project file
2395and follow this tutorial for it. The ratio of the corresponding slope for the
2396austenite 111 reflection with what we found here should be the Poisson ratio.</p>
2397
2398</div>
2399
2400</body>
2401
2402</html>
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