source: Tutorials/TOF Calibration/Calibration of a TOF powder diffractometer.htm @ 1651

Last change on this file since 1651 was 1651, checked in by vondreele, 8 years ago
File size: 78.1 KB
Line 
1<html xmlns:v="urn:schemas-microsoft-com:vml"
2xmlns:o="urn:schemas-microsoft-com:office:office"
3xmlns:w="urn:schemas-microsoft-com:office:word"
4xmlns:m="http://schemas.microsoft.com/office/2004/12/omml"
5xmlns="http://www.w3.org/TR/REC-html40">
6
7<head>
8<meta http-equiv=Content-Type content="text/html; charset=windows-1252">
9<meta name=ProgId content=Word.Document>
10<meta name=Generator content="Microsoft Word 15">
11<meta name=Originator content="Microsoft Word 15">
12<link rel=File-List
13href="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/filelist.xml">
14<link rel=Edit-Time-Data
15href="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/editdata.mso">
16<!--[if !mso]>
17<style>
18v\:* {behavior:url(#default#VML);}
19o\:* {behavior:url(#default#VML);}
20w\:* {behavior:url(#default#VML);}
21.shape {behavior:url(#default#VML);}
22</style>
23<![endif]--><!--[if gte mso 9]><xml>
24 <o:DocumentProperties>
25  <o:Author>Von Dreele</o:Author>
26  <o:LastAuthor>Von Dreele</o:LastAuthor>
27  <o:Revision>2</o:Revision>
28  <o:TotalTime>409</o:TotalTime>
29  <o:Created>2015-02-12T20:52:00Z</o:Created>
30  <o:LastSaved>2015-02-12T20:52:00Z</o:LastSaved>
31  <o:Pages>1</o:Pages>
32  <o:Words>1108</o:Words>
33  <o:Characters>6322</o:Characters>
34  <o:Company>Argonne National Laboratory</o:Company>
35  <o:Lines>52</o:Lines>
36  <o:Paragraphs>14</o:Paragraphs>
37  <o:CharactersWithSpaces>7416</o:CharactersWithSpaces>
38  <o:Version>15.00</o:Version>
39 </o:DocumentProperties>
40 <o:OfficeDocumentSettings>
41  <o:AllowPNG/>
42 </o:OfficeDocumentSettings>
43</xml><![endif]-->
44<link rel=themeData
45href="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/themedata.thmx">
46<link rel=colorSchemeMapping
47href="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/colorschememapping.xml">
48<!--[if gte mso 9]><xml>
49 <w:WordDocument>
50  <w:TrackMoves>false</w:TrackMoves>
51  <w:TrackFormatting/>
52  <w:PunctuationKerning/>
53  <w:ValidateAgainstSchemas/>
54  <w:SaveIfXMLInvalid>false</w:SaveIfXMLInvalid>
55  <w:IgnoreMixedContent>false</w:IgnoreMixedContent>
56  <w:AlwaysShowPlaceholderText>false</w:AlwaysShowPlaceholderText>
57  <w:DoNotPromoteQF/>
58  <w:LidThemeOther>EN-US</w:LidThemeOther>
59  <w:LidThemeAsian>X-NONE</w:LidThemeAsian>
60  <w:LidThemeComplexScript>X-NONE</w:LidThemeComplexScript>
61  <w:Compatibility>
62   <w:BreakWrappedTables/>
63   <w:SnapToGridInCell/>
64   <w:WrapTextWithPunct/>
65   <w:UseAsianBreakRules/>
66   <w:DontGrowAutofit/>
67   <w:SplitPgBreakAndParaMark/>
68   <w:EnableOpenTypeKerning/>
69   <w:DontFlipMirrorIndents/>
70   <w:OverrideTableStyleHps/>
71  </w:Compatibility>
72  <w:BrowserLevel>MicrosoftInternetExplorer4</w:BrowserLevel>
73  <m:mathPr>
74   <m:mathFont m:val="Cambria Math"/>
75   <m:brkBin m:val="before"/>
76   <m:brkBinSub m:val="&#45;-"/>
77   <m:smallFrac m:val="off"/>
78   <m:dispDef/>
79   <m:lMargin m:val="0"/>
80   <m:rMargin m:val="0"/>
81   <m:defJc m:val="centerGroup"/>
82   <m:wrapIndent m:val="1440"/>
83   <m:intLim m:val="subSup"/>
84   <m:naryLim m:val="undOvr"/>
85  </m:mathPr></w:WordDocument>
86</xml><![endif]--><!--[if gte mso 9]><xml>
87 <w:LatentStyles DefLockedState="false" DefUnhideWhenUsed="false"
88  DefSemiHidden="false" DefQFormat="false" DefPriority="99"
89  LatentStyleCount="371">
90  <w:LsdException Locked="false" Priority="0" QFormat="true" Name="Normal"/>
91  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 1"/>
92  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
93   UnhideWhenUsed="true" QFormat="true" Name="heading 2"/>
94  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
95   UnhideWhenUsed="true" QFormat="true" Name="heading 3"/>
96  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
97   UnhideWhenUsed="true" QFormat="true" Name="heading 4"/>
98  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
99   UnhideWhenUsed="true" QFormat="true" Name="heading 5"/>
100  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
101   UnhideWhenUsed="true" QFormat="true" Name="heading 6"/>
102  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
103   UnhideWhenUsed="true" QFormat="true" Name="heading 7"/>
104  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
105   UnhideWhenUsed="true" QFormat="true" Name="heading 8"/>
106  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
107   UnhideWhenUsed="true" QFormat="true" Name="heading 9"/>
108  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
109   Name="index 1"/>
110  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
111   Name="index 2"/>
112  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
113   Name="index 3"/>
114  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
115   Name="index 4"/>
116  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
117   Name="index 5"/>
118  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
119   Name="index 6"/>
120  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
121   Name="index 7"/>
122  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
123   Name="index 8"/>
124  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
125   Name="index 9"/>
126  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
127   UnhideWhenUsed="true" Name="toc 1"/>
128  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
129   UnhideWhenUsed="true" Name="toc 2"/>
130  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
131   UnhideWhenUsed="true" Name="toc 3"/>
132  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
133   UnhideWhenUsed="true" Name="toc 4"/>
134  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
135   UnhideWhenUsed="true" Name="toc 5"/>
136  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
137   UnhideWhenUsed="true" Name="toc 6"/>
138  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
139   UnhideWhenUsed="true" Name="toc 7"/>
140  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
141   UnhideWhenUsed="true" Name="toc 8"/>
142  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
143   UnhideWhenUsed="true" Name="toc 9"/>
144  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
145   Name="Normal Indent"/>
146  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
147   Name="footnote text"/>
148  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
149   Name="annotation text"/>
150  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
151   Name="header"/>
152  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
153   Name="footer"/>
154  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
155   Name="index heading"/>
156  <w:LsdException Locked="false" Priority="35" SemiHidden="true"
157   UnhideWhenUsed="true" QFormat="true" Name="caption"/>
158  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
159   Name="table of figures"/>
160  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
161   Name="envelope address"/>
162  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
163   Name="envelope return"/>
164  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
165   Name="footnote reference"/>
166  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
167   Name="annotation reference"/>
168  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
169   Name="line number"/>
170  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
171   Name="page number"/>
172  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
173   Name="endnote reference"/>
174  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
175   Name="endnote text"/>
176  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
177   Name="table of authorities"/>
178  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
179   Name="macro"/>
180  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
181   Name="toa heading"/>
182  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
183   Name="List"/>
184  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
185   Name="List Bullet"/>
186  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
187   Name="List Number"/>
188  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
189   Name="List 2"/>
190  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
191   Name="List 3"/>
192  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
193   Name="List 4"/>
194  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
195   Name="List 5"/>
196  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
197   Name="List Bullet 2"/>
198  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
199   Name="List Bullet 3"/>
200  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
201   Name="List Bullet 4"/>
202  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
203   Name="List Bullet 5"/>
204  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
205   Name="List Number 2"/>
206  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
207   Name="List Number 3"/>
208  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
209   Name="List Number 4"/>
210  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
211   Name="List Number 5"/>
212  <w:LsdException Locked="false" Priority="10" QFormat="true" Name="Title"/>
213  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
214   Name="Closing"/>
215  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
216   Name="Signature"/>
217  <w:LsdException Locked="false" Priority="1" SemiHidden="true"
218   UnhideWhenUsed="true" Name="Default Paragraph Font"/>
219  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
220   Name="Body Text"/>
221  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
222   Name="Body Text Indent"/>
223  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
224   Name="List Continue"/>
225  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
226   Name="List Continue 2"/>
227  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
228   Name="List Continue 3"/>
229  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
230   Name="List Continue 4"/>
231  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
232   Name="List Continue 5"/>
233  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
234   Name="Message Header"/>
235  <w:LsdException Locked="false" Priority="11" QFormat="true" Name="Subtitle"/>
236  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
237   Name="Salutation"/>
238  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
239   Name="Date"/>
240  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
241   Name="Body Text First Indent"/>
242  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
243   Name="Body Text First Indent 2"/>
244  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
245   Name="Note Heading"/>
246  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
247   Name="Body Text 2"/>
248  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
249   Name="Body Text 3"/>
250  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
251   Name="Body Text Indent 2"/>
252  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
253   Name="Body Text Indent 3"/>
254  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
255   Name="Block Text"/>
256  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
257   Name="Hyperlink"/>
258  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
259   Name="FollowedHyperlink"/>
260  <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/>
261  <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/>
262  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
263   Name="Document Map"/>
264  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
265   Name="Plain Text"/>
266  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
267   Name="E-mail Signature"/>
268  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
269   Name="HTML Top of Form"/>
270  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
271   Name="HTML Bottom of Form"/>
272  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
273   Name="Normal (Web)"/>
274  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
275   Name="HTML Acronym"/>
276  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
277   Name="HTML Address"/>
278  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
279   Name="HTML Cite"/>
280  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
281   Name="HTML Code"/>
282  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
283   Name="HTML Definition"/>
284  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
285   Name="HTML Keyboard"/>
286  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
287   Name="HTML Preformatted"/>
288  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
289   Name="HTML Sample"/>
290  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
291   Name="HTML Typewriter"/>
292  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
293   Name="HTML Variable"/>
294  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
295   Name="Normal Table"/>
296  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
297   Name="annotation subject"/>
298  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
299   Name="No List"/>
300  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
301   Name="Outline List 1"/>
302  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
303   Name="Outline List 2"/>
304  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
305   Name="Outline List 3"/>
306  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
307   Name="Table Simple 1"/>
308  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
309   Name="Table Simple 2"/>
310  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
311   Name="Table Simple 3"/>
312  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
313   Name="Table Classic 1"/>
314  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
315   Name="Table Classic 2"/>
316  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
317   Name="Table Classic 3"/>
318  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
319   Name="Table Classic 4"/>
320  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
321   Name="Table Colorful 1"/>
322  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
323   Name="Table Colorful 2"/>
324  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
325   Name="Table Colorful 3"/>
326  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
327   Name="Table Columns 1"/>
328  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
329   Name="Table Columns 2"/>
330  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
331   Name="Table Columns 3"/>
332  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
333   Name="Table Columns 4"/>
334  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
335   Name="Table Columns 5"/>
336  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
337   Name="Table Grid 1"/>
338  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
339   Name="Table Grid 2"/>
340  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
341   Name="Table Grid 3"/>
342  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
343   Name="Table Grid 4"/>
344  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
345   Name="Table Grid 5"/>
346  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
347   Name="Table Grid 6"/>
348  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
349   Name="Table Grid 7"/>
350  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
351   Name="Table Grid 8"/>
352  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
353   Name="Table List 1"/>
354  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
355   Name="Table List 2"/>
356  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
357   Name="Table List 3"/>
358  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
359   Name="Table List 4"/>
360  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
361   Name="Table List 5"/>
362  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
363   Name="Table List 6"/>
364  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
365   Name="Table List 7"/>
366  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
367   Name="Table List 8"/>
368  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
369   Name="Table 3D effects 1"/>
370  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
371   Name="Table 3D effects 2"/>
372  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
373   Name="Table 3D effects 3"/>
374  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
375   Name="Table Contemporary"/>
376  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
377   Name="Table Elegant"/>
378  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
379   Name="Table Professional"/>
380  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
381   Name="Table Subtle 1"/>
382  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
383   Name="Table Subtle 2"/>
384  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
385   Name="Table Web 1"/>
386  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
387   Name="Table Web 2"/>
388  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
389   Name="Table Web 3"/>
390  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
391   Name="Balloon Text"/>
392  <w:LsdException Locked="false" Priority="59" Name="Table Grid"/>
393  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
394   Name="Table Theme"/>
395  <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/>
396  <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/>
397  <w:LsdException Locked="false" Priority="60" Name="Light Shading"/>
398  <w:LsdException Locked="false" Priority="61" Name="Light List"/>
399  <w:LsdException Locked="false" Priority="62" Name="Light Grid"/>
400  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/>
401  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/>
402  <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/>
403  <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/>
404  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/>
405  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/>
406  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/>
407  <w:LsdException Locked="false" Priority="70" Name="Dark List"/>
408  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/>
409  <w:LsdException Locked="false" Priority="72" Name="Colorful List"/>
410  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
411  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
412  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
413  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
414  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
415  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
416  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
417  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
418  <w:LsdException Locked="false" Priority="34" QFormat="true"
419   Name="List Paragraph"/>
420  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
421  <w:LsdException Locked="false" Priority="30" QFormat="true"
422   Name="Intense Quote"/>
423  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
424  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
425  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
426  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
427  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
428  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
429  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
430  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
431  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
432  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
433  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
434  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
435  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
436  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
437  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
438  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
439  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
440  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
441  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
442  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
443  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
444  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
445  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
446  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
447  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
448  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
449  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
450  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
451  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
452  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
453  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
454  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
455  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
456  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
457  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
458  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
459  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
460  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
461  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
462  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
463  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
464  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
465  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
466  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
467  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
468  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
469  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
470  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
471  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
472  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
473  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
474  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
475  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
476  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
477  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
478  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
479  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
480  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
481  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
482  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
483  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
484  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
485  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
486  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
487  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
488  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
489  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
490  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
491  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
492  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
493  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
494  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
495  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
496  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
497  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
498  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
499  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
500  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
501  <w:LsdException Locked="false" Priority="19" QFormat="true"
502   Name="Subtle Emphasis"/>
503  <w:LsdException Locked="false" Priority="21" QFormat="true"
504   Name="Intense Emphasis"/>
505  <w:LsdException Locked="false" Priority="31" QFormat="true"
506   Name="Subtle Reference"/>
507  <w:LsdException Locked="false" Priority="32" QFormat="true"
508   Name="Intense Reference"/>
509  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
510  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
511   UnhideWhenUsed="true" Name="Bibliography"/>
512  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
513   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
514  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
515  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
516  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
517  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
518  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
519  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
520  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
521  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
522  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
523  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
524  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
525  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
526  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
527  <w:LsdException Locked="false" Priority="46"
528   Name="Grid Table 1 Light Accent 1"/>
529  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
530  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
531  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
532  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
533  <w:LsdException Locked="false" Priority="51"
534   Name="Grid Table 6 Colorful Accent 1"/>
535  <w:LsdException Locked="false" Priority="52"
536   Name="Grid Table 7 Colorful Accent 1"/>
537  <w:LsdException Locked="false" Priority="46"
538   Name="Grid Table 1 Light Accent 2"/>
539  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
540  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
541  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
542  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
543  <w:LsdException Locked="false" Priority="51"
544   Name="Grid Table 6 Colorful Accent 2"/>
545  <w:LsdException Locked="false" Priority="52"
546   Name="Grid Table 7 Colorful Accent 2"/>
547  <w:LsdException Locked="false" Priority="46"
548   Name="Grid Table 1 Light Accent 3"/>
549  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
550  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
551  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
552  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
553  <w:LsdException Locked="false" Priority="51"
554   Name="Grid Table 6 Colorful Accent 3"/>
555  <w:LsdException Locked="false" Priority="52"
556   Name="Grid Table 7 Colorful Accent 3"/>
557  <w:LsdException Locked="false" Priority="46"
558   Name="Grid Table 1 Light Accent 4"/>
559  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
560  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
561  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
562  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
563  <w:LsdException Locked="false" Priority="51"
564   Name="Grid Table 6 Colorful Accent 4"/>
565  <w:LsdException Locked="false" Priority="52"
566   Name="Grid Table 7 Colorful Accent 4"/>
567  <w:LsdException Locked="false" Priority="46"
568   Name="Grid Table 1 Light Accent 5"/>
569  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
570  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
571  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
572  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
573  <w:LsdException Locked="false" Priority="51"
574   Name="Grid Table 6 Colorful Accent 5"/>
575  <w:LsdException Locked="false" Priority="52"
576   Name="Grid Table 7 Colorful Accent 5"/>
577  <w:LsdException Locked="false" Priority="46"
578   Name="Grid Table 1 Light Accent 6"/>
579  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
580  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
581  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
582  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
583  <w:LsdException Locked="false" Priority="51"
584   Name="Grid Table 6 Colorful Accent 6"/>
585  <w:LsdException Locked="false" Priority="52"
586   Name="Grid Table 7 Colorful Accent 6"/>
587  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
588  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
589  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
590  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
591  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
592  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
593  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
594  <w:LsdException Locked="false" Priority="46"
595   Name="List Table 1 Light Accent 1"/>
596  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
597  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
598  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
599  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
600  <w:LsdException Locked="false" Priority="51"
601   Name="List Table 6 Colorful Accent 1"/>
602  <w:LsdException Locked="false" Priority="52"
603   Name="List Table 7 Colorful Accent 1"/>
604  <w:LsdException Locked="false" Priority="46"
605   Name="List Table 1 Light Accent 2"/>
606  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
607  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
608  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
609  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
610  <w:LsdException Locked="false" Priority="51"
611   Name="List Table 6 Colorful Accent 2"/>
612  <w:LsdException Locked="false" Priority="52"
613   Name="List Table 7 Colorful Accent 2"/>
614  <w:LsdException Locked="false" Priority="46"
615   Name="List Table 1 Light Accent 3"/>
616  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
617  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
618  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
619  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
620  <w:LsdException Locked="false" Priority="51"
621   Name="List Table 6 Colorful Accent 3"/>
622  <w:LsdException Locked="false" Priority="52"
623   Name="List Table 7 Colorful Accent 3"/>
624  <w:LsdException Locked="false" Priority="46"
625   Name="List Table 1 Light Accent 4"/>
626  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
627  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
628  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
629  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
630  <w:LsdException Locked="false" Priority="51"
631   Name="List Table 6 Colorful Accent 4"/>
632  <w:LsdException Locked="false" Priority="52"
633   Name="List Table 7 Colorful Accent 4"/>
634  <w:LsdException Locked="false" Priority="46"
635   Name="List Table 1 Light Accent 5"/>
636  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
637  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
638  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
639  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
640  <w:LsdException Locked="false" Priority="51"
641   Name="List Table 6 Colorful Accent 5"/>
642  <w:LsdException Locked="false" Priority="52"
643   Name="List Table 7 Colorful Accent 5"/>
644  <w:LsdException Locked="false" Priority="46"
645   Name="List Table 1 Light Accent 6"/>
646  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
647  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
648  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
649  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
650  <w:LsdException Locked="false" Priority="51"
651   Name="List Table 6 Colorful Accent 6"/>
652  <w:LsdException Locked="false" Priority="52"
653   Name="List Table 7 Colorful Accent 6"/>
654 </w:LatentStyles>
655</xml><![endif]-->
656<style>
657<!--
658 /* Font Definitions */
659 @font-face
660        {font-family:"Cambria Math";
661        panose-1:2 4 5 3 5 4 6 3 2 4;
662        mso-font-charset:0;
663        mso-generic-font-family:roman;
664        mso-font-pitch:variable;
665        mso-font-signature:-536870145 1107305727 0 0 415 0;}
666@font-face
667        {font-family:Calibri;
668        panose-1:2 15 5 2 2 2 4 3 2 4;
669        mso-font-charset:0;
670        mso-generic-font-family:swiss;
671        mso-font-pitch:variable;
672        mso-font-signature:-536870145 1073786111 1 0 415 0;}
673@font-face
674        {font-family:Tahoma;
675        panose-1:2 11 6 4 3 5 4 4 2 4;
676        mso-font-charset:0;
677        mso-generic-font-family:swiss;
678        mso-font-pitch:variable;
679        mso-font-signature:-520081665 -1073717157 41 0 66047 0;}
680 /* Style Definitions */
681 p.MsoNormal, li.MsoNormal, div.MsoNormal
682        {mso-style-unhide:no;
683        mso-style-qformat:yes;
684        mso-style-parent:"";
685        margin:0in;
686        margin-bottom:.0001pt;
687        mso-pagination:widow-orphan;
688        font-size:12.0pt;
689        font-family:"Times New Roman",serif;
690        mso-fareast-font-family:"Times New Roman";
691        mso-fareast-theme-font:minor-fareast;}
692h1
693        {mso-style-priority:9;
694        mso-style-unhide:no;
695        mso-style-qformat:yes;
696        mso-style-link:"Heading 1 Char";
697        mso-margin-top-alt:auto;
698        margin-right:0in;
699        mso-margin-bottom-alt:auto;
700        margin-left:0in;
701        mso-pagination:widow-orphan;
702        mso-outline-level:1;
703        font-size:24.0pt;
704        font-family:"Times New Roman",serif;
705        mso-fareast-font-family:"Times New Roman";
706        mso-fareast-theme-font:minor-fareast;
707        font-weight:bold;}
708h2
709        {mso-style-noshow:yes;
710        mso-style-priority:9;
711        mso-style-qformat:yes;
712        mso-style-link:"Heading 2 Char";
713        mso-margin-top-alt:auto;
714        margin-right:0in;
715        mso-margin-bottom-alt:auto;
716        margin-left:0in;
717        mso-pagination:widow-orphan;
718        mso-outline-level:2;
719        font-size:18.0pt;
720        font-family:"Times New Roman",serif;
721        mso-fareast-font-family:"Times New Roman";
722        mso-fareast-theme-font:minor-fareast;
723        font-weight:bold;}
724h3
725        {mso-style-noshow:yes;
726        mso-style-priority:9;
727        mso-style-qformat:yes;
728        mso-style-link:"Heading 3 Char";
729        mso-margin-top-alt:auto;
730        margin-right:0in;
731        mso-margin-bottom-alt:auto;
732        margin-left:0in;
733        mso-pagination:widow-orphan;
734        mso-outline-level:3;
735        font-size:13.5pt;
736        font-family:"Times New Roman",serif;
737        mso-fareast-font-family:"Times New Roman";
738        mso-fareast-theme-font:minor-fareast;
739        font-weight:bold;}
740h4
741        {mso-style-noshow:yes;
742        mso-style-priority:9;
743        mso-style-qformat:yes;
744        mso-style-link:"Heading 4 Char";
745        mso-style-next:Normal;
746        margin-top:10.0pt;
747        margin-right:0in;
748        margin-bottom:0in;
749        margin-left:0in;
750        margin-bottom:.0001pt;
751        mso-pagination:widow-orphan lines-together;
752        page-break-after:avoid;
753        mso-outline-level:4;
754        font-size:13.0pt;
755        font-family:"Cambria",serif;
756        mso-ascii-font-family:Cambria;
757        mso-ascii-theme-font:major-latin;
758        mso-fareast-font-family:"Times New Roman";
759        mso-fareast-theme-font:major-fareast;
760        mso-hansi-font-family:Cambria;
761        mso-hansi-theme-font:major-latin;
762        mso-bidi-font-family:"Times New Roman";
763        mso-bidi-theme-font:major-bidi;
764        color:#4F81BD;
765        mso-themecolor:accent1;
766        font-weight:bold;
767        font-style:italic;}
768h5
769        {mso-style-noshow:yes;
770        mso-style-priority:9;
771        mso-style-qformat:yes;
772        mso-style-link:"Heading 5 Char";
773        mso-margin-top-alt:auto;
774        margin-right:0in;
775        mso-margin-bottom-alt:auto;
776        margin-left:0in;
777        mso-pagination:widow-orphan;
778        mso-outline-level:5;
779        font-size:12.0pt;
780        font-family:"Times New Roman",serif;
781        mso-fareast-font-family:"Times New Roman";
782        mso-fareast-theme-font:minor-fareast;
783        color:#4F4FFF;
784        font-weight:bold;}
785a:link, span.MsoHyperlink
786        {mso-style-noshow:yes;
787        mso-style-priority:99;
788        color:black;
789        text-decoration:underline;
790        text-underline:single;}
791a:visited, span.MsoHyperlinkFollowed
792        {mso-style-noshow:yes;
793        mso-style-priority:99;
794        color:purple;
795        text-decoration:underline;
796        text-underline:single;}
797p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap
798        {mso-style-noshow:yes;
799        mso-style-priority:99;
800        mso-style-link:"Document Map Char";
801        margin:0in;
802        margin-bottom:.0001pt;
803        mso-pagination:widow-orphan;
804        font-size:8.0pt;
805        font-family:"Tahoma",sans-serif;
806        mso-fareast-font-family:"Times New Roman";
807        mso-fareast-theme-font:minor-fareast;}
808p
809        {mso-style-noshow:yes;
810        mso-style-priority:99;
811        mso-margin-top-alt:auto;
812        margin-right:0in;
813        mso-margin-bottom-alt:auto;
814        margin-left:0in;
815        mso-pagination:widow-orphan;
816        font-size:12.0pt;
817        font-family:"Times New Roman",serif;
818        mso-fareast-font-family:"Times New Roman";
819        mso-fareast-theme-font:minor-fareast;}
820pre
821        {mso-style-noshow:yes;
822        mso-style-priority:99;
823        mso-style-link:"HTML Preformatted Char";
824        margin:0in;
825        margin-bottom:.0001pt;
826        mso-pagination:widow-orphan;
827        tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt;
828        font-size:10.0pt;
829        font-family:"Courier New";
830        mso-fareast-font-family:"Times New Roman";}
831p.MsoAcetate, li.MsoAcetate, div.MsoAcetate
832        {mso-style-noshow:yes;
833        mso-style-priority:99;
834        mso-style-link:"Balloon Text Char";
835        margin:0in;
836        margin-bottom:.0001pt;
837        mso-pagination:widow-orphan;
838        font-size:8.0pt;
839        font-family:"Tahoma",sans-serif;
840        mso-fareast-font-family:"Times New Roman";
841        mso-fareast-theme-font:minor-fareast;}
842span.MsoPlaceholderText
843        {mso-style-noshow:yes;
844        mso-style-priority:99;
845        mso-style-unhide:no;
846        color:gray;}
847p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing
848        {mso-style-noshow:yes;
849        mso-style-priority:1;
850        mso-style-unhide:no;
851        mso-style-qformat:yes;
852        mso-style-parent:"";
853        margin:0in;
854        margin-bottom:.0001pt;
855        mso-pagination:widow-orphan;
856        font-size:12.0pt;
857        font-family:"Times New Roman",serif;
858        mso-fareast-font-family:"Times New Roman";
859        mso-fareast-theme-font:minor-fareast;}
860p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph
861        {mso-style-noshow:yes;
862        mso-style-priority:34;
863        mso-style-unhide:no;
864        mso-style-qformat:yes;
865        margin-top:0in;
866        margin-right:0in;
867        margin-bottom:0in;
868        margin-left:.5in;
869        margin-bottom:.0001pt;
870        mso-add-space:auto;
871        mso-pagination:widow-orphan;
872        font-size:12.0pt;
873        font-family:"Times New Roman",serif;
874        mso-fareast-font-family:"Times New Roman";
875        mso-fareast-theme-font:minor-fareast;}
876p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst
877        {mso-style-noshow:yes;
878        mso-style-priority:34;
879        mso-style-unhide:no;
880        mso-style-qformat:yes;
881        mso-style-type:export-only;
882        margin-top:0in;
883        margin-right:0in;
884        margin-bottom:0in;
885        margin-left:.5in;
886        margin-bottom:.0001pt;
887        mso-add-space:auto;
888        mso-pagination:widow-orphan;
889        font-size:12.0pt;
890        font-family:"Times New Roman",serif;
891        mso-fareast-font-family:"Times New Roman";
892        mso-fareast-theme-font:minor-fareast;}
893p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle
894        {mso-style-noshow:yes;
895        mso-style-priority:34;
896        mso-style-unhide:no;
897        mso-style-qformat:yes;
898        mso-style-type:export-only;
899        margin-top:0in;
900        margin-right:0in;
901        margin-bottom:0in;
902        margin-left:.5in;
903        margin-bottom:.0001pt;
904        mso-add-space:auto;
905        mso-pagination:widow-orphan;
906        font-size:12.0pt;
907        font-family:"Times New Roman",serif;
908        mso-fareast-font-family:"Times New Roman";
909        mso-fareast-theme-font:minor-fareast;}
910p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast
911        {mso-style-noshow:yes;
912        mso-style-priority:34;
913        mso-style-unhide:no;
914        mso-style-qformat:yes;
915        mso-style-type:export-only;
916        margin-top:0in;
917        margin-right:0in;
918        margin-bottom:0in;
919        margin-left:.5in;
920        margin-bottom:.0001pt;
921        mso-add-space:auto;
922        mso-pagination:widow-orphan;
923        font-size:12.0pt;
924        font-family:"Times New Roman",serif;
925        mso-fareast-font-family:"Times New Roman";
926        mso-fareast-theme-font:minor-fareast;}
927span.MsoIntenseReference
928        {mso-style-priority:32;
929        mso-style-unhide:no;
930        mso-style-qformat:yes;
931        font-variant:small-caps;
932        color:#C0504D;
933        mso-themecolor:accent2;
934        letter-spacing:.25pt;
935        font-weight:bold;
936        text-decoration:underline;
937        text-underline:single;}
938span.Heading1Char
939        {mso-style-name:"Heading 1 Char";
940        mso-style-priority:9;
941        mso-style-unhide:no;
942        mso-style-locked:yes;
943        mso-style-link:"Heading 1";
944        mso-ansi-font-size:24.0pt;
945        mso-bidi-font-size:24.0pt;
946        font-family:"Times New Roman",serif;
947        mso-ascii-font-family:"Times New Roman";
948        mso-fareast-font-family:"Times New Roman";
949        mso-fareast-theme-font:minor-fareast;
950        mso-hansi-font-family:"Times New Roman";
951        mso-bidi-font-family:"Times New Roman";
952        mso-font-kerning:18.0pt;
953        font-weight:bold;}
954span.Heading2Char
955        {mso-style-name:"Heading 2 Char";
956        mso-style-noshow:yes;
957        mso-style-priority:9;
958        mso-style-unhide:no;
959        mso-style-locked:yes;
960        mso-style-link:"Heading 2";
961        mso-ansi-font-size:18.0pt;
962        mso-bidi-font-size:18.0pt;
963        font-family:"Times New Roman",serif;
964        mso-ascii-font-family:"Times New Roman";
965        mso-fareast-font-family:"Times New Roman";
966        mso-fareast-theme-font:minor-fareast;
967        mso-hansi-font-family:"Times New Roman";
968        mso-bidi-font-family:"Times New Roman";
969        font-weight:bold;}
970span.Heading3Char
971        {mso-style-name:"Heading 3 Char";
972        mso-style-noshow:yes;
973        mso-style-priority:9;
974        mso-style-unhide:no;
975        mso-style-locked:yes;
976        mso-style-link:"Heading 3";
977        mso-ansi-font-size:13.5pt;
978        mso-bidi-font-size:13.5pt;
979        font-family:"Times New Roman",serif;
980        mso-ascii-font-family:"Times New Roman";
981        mso-fareast-font-family:"Times New Roman";
982        mso-fareast-theme-font:minor-fareast;
983        mso-hansi-font-family:"Times New Roman";
984        mso-bidi-font-family:"Times New Roman";
985        font-weight:bold;}
986span.Heading4Char
987        {mso-style-name:"Heading 4 Char";
988        mso-style-noshow:yes;
989        mso-style-priority:9;
990        mso-style-unhide:no;
991        mso-style-locked:yes;
992        mso-style-link:"Heading 4";
993        mso-ansi-font-size:13.0pt;
994        mso-bidi-font-size:13.0pt;
995        font-family:"Cambria",serif;
996        mso-ascii-font-family:Cambria;
997        mso-ascii-theme-font:major-latin;
998        mso-fareast-font-family:"Times New Roman";
999        mso-fareast-theme-font:major-fareast;
1000        mso-hansi-font-family:Cambria;
1001        mso-hansi-theme-font:major-latin;
1002        mso-bidi-font-family:"Times New Roman";
1003        mso-bidi-theme-font:major-bidi;
1004        color:#4F81BD;
1005        mso-themecolor:accent1;
1006        font-weight:bold;
1007        font-style:italic;}
1008span.Heading5Char
1009        {mso-style-name:"Heading 5 Char";
1010        mso-style-noshow:yes;
1011        mso-style-priority:9;
1012        mso-style-unhide:no;
1013        mso-style-locked:yes;
1014        mso-style-link:"Heading 5";
1015        mso-ansi-font-size:12.0pt;
1016        mso-bidi-font-size:12.0pt;
1017        font-family:"Times New Roman",serif;
1018        mso-ascii-font-family:"Times New Roman";
1019        mso-fareast-font-family:"Times New Roman";
1020        mso-fareast-theme-font:minor-fareast;
1021        mso-hansi-font-family:"Times New Roman";
1022        mso-bidi-font-family:"Times New Roman";
1023        color:#4F4FFF;
1024        font-weight:bold;}
1025span.HTMLPreformattedChar
1026        {mso-style-name:"HTML Preformatted Char";
1027        mso-style-noshow:yes;
1028        mso-style-priority:99;
1029        mso-style-unhide:no;
1030        mso-style-locked:yes;
1031        mso-style-link:"HTML Preformatted";
1032        font-family:"Courier New";
1033        mso-ascii-font-family:"Courier New";
1034        mso-fareast-font-family:"Times New Roman";
1035        mso-hansi-font-family:"Courier New";
1036        mso-bidi-font-family:"Courier New";}
1037span.DocumentMapChar
1038        {mso-style-name:"Document Map Char";
1039        mso-style-noshow:yes;
1040        mso-style-priority:99;
1041        mso-style-unhide:no;
1042        mso-style-locked:yes;
1043        mso-style-link:"Document Map";
1044        mso-ansi-font-size:8.0pt;
1045        mso-bidi-font-size:8.0pt;
1046        font-family:"Tahoma",sans-serif;
1047        mso-ascii-font-family:Tahoma;
1048        mso-fareast-font-family:"Times New Roman";
1049        mso-fareast-theme-font:minor-fareast;
1050        mso-hansi-font-family:Tahoma;
1051        mso-bidi-font-family:Tahoma;}
1052span.BalloonTextChar
1053        {mso-style-name:"Balloon Text Char";
1054        mso-style-noshow:yes;
1055        mso-style-priority:99;
1056        mso-style-unhide:no;
1057        mso-style-locked:yes;
1058        mso-style-link:"Balloon Text";
1059        mso-ansi-font-size:8.0pt;
1060        mso-bidi-font-size:8.0pt;
1061        font-family:"Tahoma",sans-serif;
1062        mso-ascii-font-family:Tahoma;
1063        mso-fareast-font-family:"Times New Roman";
1064        mso-fareast-theme-font:minor-fareast;
1065        mso-hansi-font-family:Tahoma;
1066        mso-bidi-font-family:Tahoma;}
1067.MsoChpDefault
1068        {mso-style-type:export-only;
1069        mso-default-props:yes;
1070        font-size:10.0pt;
1071        mso-ansi-font-size:10.0pt;
1072        mso-bidi-font-size:10.0pt;
1073        font-family:"Calibri",sans-serif;
1074        mso-ascii-font-family:Calibri;
1075        mso-ascii-theme-font:minor-latin;
1076        mso-fareast-font-family:Calibri;
1077        mso-fareast-theme-font:minor-latin;
1078        mso-hansi-font-family:Calibri;
1079        mso-hansi-theme-font:minor-latin;
1080        mso-bidi-font-family:"Times New Roman";
1081        mso-bidi-theme-font:minor-bidi;}
1082@page WordSection1
1083        {size:8.5in 11.0in;
1084        margin:1.0in 1.0in 1.0in 1.0in;
1085        mso-header-margin:.5in;
1086        mso-footer-margin:.5in;
1087        mso-paper-source:0;}
1088div.WordSection1
1089        {page:WordSection1;}
1090-->
1091</style>
1092<!--[if gte mso 10]>
1093<style>
1094 /* Style Definitions */
1095 table.MsoNormalTable
1096        {mso-style-name:"Table Normal";
1097        mso-tstyle-rowband-size:0;
1098        mso-tstyle-colband-size:0;
1099        mso-style-noshow:yes;
1100        mso-style-priority:99;
1101        mso-style-parent:"";
1102        mso-padding-alt:0in 5.4pt 0in 5.4pt;
1103        mso-para-margin:0in;
1104        mso-para-margin-bottom:.0001pt;
1105        mso-pagination:widow-orphan;
1106        font-size:10.0pt;
1107        font-family:"Calibri",sans-serif;
1108        mso-ascii-font-family:Calibri;
1109        mso-ascii-theme-font:minor-latin;
1110        mso-hansi-font-family:Calibri;
1111        mso-hansi-theme-font:minor-latin;}
1112</style>
1113<![endif]--><!--[if gte mso 9]><xml>
1114 <o:shapedefaults v:ext="edit" spidmax="1026"/>
1115</xml><![endif]--><!--[if gte mso 9]><xml>
1116 <o:shapelayout v:ext="edit">
1117  <o:idmap v:ext="edit" data="1"/>
1118 </o:shapelayout></xml><![endif]-->
1119</head>
1120
1121<body lang=EN-US link=black vlink=purple style='tab-interval:.5in'>
1122
1123<div class=WordSection1>
1124
1125<p class=MsoNormal><span class=Heading1Char><span style='font-size:24.0pt'>Calibration
1126of a TOF powder diffractometer</span></span><b><span style='font-size:14.0pt;
1127color:#365F91;mso-themecolor:accent1;mso-themeshade:191'><o:p></o:p></span></b></p>
1128
1129<p class=MsoNormal>In this tutorial, data collected on the SNS instrument
1130POWGEN, are used. The calibration process will use the fitted positions of all
1131visible peaks in a pattern of NIST SRM 660b La<sup>10</sup>B<sub>6</sub>
1132(a=4.15689Å) obtained in a multiple single peak fit. The positions will be
1133compared to those expected from the known lattice parameters to establish the
1134diffractometer constants (difC, difA, difB and Zero) used for calculating TOF
1135peak positions from d-spacings. Note that menu entries are listed in bold face
1136below as <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1137mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1138Calibri;mso-bidi-theme-font:minor-latin'>Help/About GSAS-II</span></b>, which
1139lists first the name of the menu (here <b style='mso-bidi-font-weight:normal'><span
1140style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1141mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1142minor-latin'>Help</span></b>) and second the name of the entry in the menu
1143(here <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1144mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1145Calibri;mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).</p>
1146
1147<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
1148href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
1149text-underline:none'>start GSAS-II</span></a></span></u>.</p>
1150
1151<h2>Step 1: Read in the data file</h2>
1152
1153<p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the <b
1154style='mso-bidi-font-weight:normal'>Import/Powder data/from GSAS powder data
1155file</b> menu item to read the data file into the current GSAS-II project. </p>
1156
1157<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
1158
1159<p class=MsoNormal>A file selection dialog will be shown; its appearance will
1160depend on your OS. Change the search directory to <b style='mso-bidi-font-weight:
1161normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1162minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1163mso-bidi-theme-font:minor-latin'>/Exercises/TOF Powder Calibration</span></b>
1164and then select the file </p>
1165
1166<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
1167style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1168mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1169minor-latin'>PG3_17541.gsa</span></b> and press <b style='mso-bidi-font-weight:
1170normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1171minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1172mso-bidi-theme-font:minor-latin'>Open</span></b>.<span style='mso-no-proof:
1173yes'> A window will appear “</span><b style='mso-bidi-font-weight:normal'><span
1174style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1175mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Is this the file you want?</span></b><span
1176style='mso-no-proof:yes'>”. Press Yes.<o:p></o:p></span></p>
1177
1178<p class=MsoNormal><span style='mso-no-proof:yes'>The file selection dialog
1179will reappear; select the </span><b style='mso-bidi-font-weight:normal'><span
1180style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1181mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>PGHR_60-2015A.prm</span></b><span
1182style='mso-no-proof:yes'> file. It contains the POWGEN instrument parameters
1183provided along with the data. <o:p></o:p></span></p>
1184
1185<p class=MsoNormal><span style='mso-no-proof:yes'><o:p>&nbsp;</o:p></span></p>
1186
1187<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype
1188 id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t"
1189 path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f">
1190 <v:stroke joinstyle="miter"/>
1191 <v:formulas>
1192  <v:f eqn="if lineDrawn pixelLineWidth 0"/>
1193  <v:f eqn="sum @0 1 0"/>
1194  <v:f eqn="sum 0 0 @1"/>
1195  <v:f eqn="prod @2 1 2"/>
1196  <v:f eqn="prod @3 21600 pixelWidth"/>
1197  <v:f eqn="prod @3 21600 pixelHeight"/>
1198  <v:f eqn="sum @0 0 1"/>
1199  <v:f eqn="prod @6 1 2"/>
1200  <v:f eqn="prod @7 21600 pixelWidth"/>
1201  <v:f eqn="sum @8 21600 0"/>
1202  <v:f eqn="prod @7 21600 pixelHeight"/>
1203  <v:f eqn="sum @10 21600 0"/>
1204 </v:formulas>
1205 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
1206 <o:lock v:ext="edit" aspectratio="t"/>
1207</v:shapetype><v:shape id="Picture_x0020_15" o:spid="_x0000_i1041" type="#_x0000_t75"
1208 style='width:300pt;height:187.5pt;visibility:visible;mso-wrap-style:square'>
1209 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image001.png"
1210  o:title=""/>
1211</v:shape><![endif]--><![if !vml]><img border=0 width=400 height=250
1212src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image001.png"
1213v:shapes="Picture_x0020_15"><![endif]></span></p>
1214
1215<p class=MsoNormal>At this point the data tree window will have several entries
1216and the powder pattern will appear. Although it is not necessary in this case,
1217you may wish to change the limits (green &amp; red vertical dashed lines). If
1218so select the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1219"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1220minor-latin'>Limits</span></b> item in the GSASII Data tree under <b
1221style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1222mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>PWDR
1223PG3_17541.gsa Bank 1</span></b> and set them as appropriate (usually due to
1224unusable data at the ends of the pattern).</p>
1225
1226<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
1227style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_16"
1228 o:spid="_x0000_i1040" type="#_x0000_t75" style='width:468.75pt;height:402pt;
1229 visibility:visible;mso-wrap-style:square'>
1230 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image002.png"
1231  o:title=""/>
1232</v:shape><![endif]--><![if !vml]><img border=0 width=625 height=536
1233src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image003.png"
1234v:shapes="Picture_x0020_16"><![endif]></span></b><span
1235style='mso-spacerun:yes'> </span><b style='mso-bidi-font-weight:normal'><o:p></o:p></b></p>
1236
1237<h2><span style='mso-spacerun:yes'> </span>Step 2: Select peaks</h2>
1238
1239<p class=MsoNormal>Under the <b style='mso-bidi-font-weight:normal'><span
1240style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1241mso-hansi-theme-font:minor-latin'>PWDR PG3_17541.gsa Bank 1 </span></b>GSASII
1242Data tree item find the <b style='mso-bidi-font-weight:normal'><span
1243style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1244mso-hansi-theme-font:minor-latin'>Peak List</span></b> entry; it will be empty.
1245Select the menu item <b style='mso-bidi-font-weight:normal'><span
1246style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1247mso-hansi-theme-font:minor-latin'>Peak Fitting/Auto search</span></b> to populate
1248the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1249mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Peak List</span></b>.
1250This will select almost every peak in the pattern.</p>
1251
1252<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1253 id="Picture_x0020_17" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:466.5pt;
1254 height:399.75pt;visibility:visible;mso-wrap-style:square'>
1255 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image004.png"
1256  o:title=""/>
1257</v:shape><![endif]--><![if !vml]><img border=0 width=622 height=533
1258src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image005.png"
1259v:shapes="Picture_x0020_17"><![endif]></span></p>
1260
1261<p class=MsoNormal>However, it can fail by selecting a peak multiple times if
1262the data is sufficiently noisy. You should check through the list and eliminate
1263any close duplicates (in this instance there didn’t appear to be any). A peak
1264can be eliminated by placing the cursor on the vertical blue line and pressing
1265the right mouse button; the line should vanish and the entry in the table
1266deleted. Notice that the position for the highest TOF peak is misplaced. You
1267can shift it by placing the cursor on the blue line and with the left mouse
1268button down, drag the line to match the peak top (zooming in before can help).
1269If you want you can add more of the unpicked lines to the list (I didn’t). To
1270do this (zooming in helps) place the cursor on a data point at the top of a
1271peak and press the left mouse button. It is easiest to proceed from right to
1272left so the tool tip stays out of the way as you work. For any of these
1273operations the zoom buttons at the bottom left of the plot window must be
1274turned off (NB: one is turned on in the above plot).</p>
1275
1276<h2>Step 3: Fit peaks</h2>
1277
1278<p class=MsoNormal>To do the initial fit to the peaks, select the <b
1279style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1280mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Peak
1281Fitting/Peakfit</span></b> menu item in the <b style='mso-bidi-font-weight:
1282normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1283minor-latin;mso-hansi-theme-font:minor-latin'>Peak List</span></b> data window.
1284GSAS-II will ask for a project name before continuing, enter a name (I chose <b
1285style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1286mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>calibrate</span></b>).
1287The project file (<b style='mso-bidi-font-weight:normal'><span
1288style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1289mso-hansi-theme-font:minor-latin'>calibrate.gpx</span></b>) will be written
1290into your local directory selected in the File Dialog; then the refinement will
1291proceed. The resulting plot will look like (I keyed ‘<b style='mso-bidi-font-weight:
1292normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1293minor-latin;mso-hansi-theme-font:minor-latin'>s</span></b>’ and ‘<b
1294style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1295mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>q</span></b>’
1296on the plot to get a sqrt(I) vs q plot which spread out the peaks a bit better
1297than a I vs TOF plot).</p>
1298
1299<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1300 id="Picture_x0020_18" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:525pt;
1301 height:450pt;visibility:visible;mso-wrap-style:square'>
1302 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image006.png"
1303  o:title=""/>
1304</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1305src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image006.png"
1306v:shapes="Picture_x0020_18"><![endif]></span></p>
1307
1308<p class=MsoNormal>The fit to the background can be improved by adding more
1309terms; I set the number of chebyschev terms to <b style='mso-bidi-font-weight:
1310normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1311minor-latin;mso-hansi-theme-font:minor-latin'>6</span></b>. The peak positions
1312should also be refined; to set them go back to the <b style='mso-bidi-font-weight:
1313normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1314minor-latin;mso-hansi-theme-font:minor-latin'>Peak List</span></b> data window,
1315select one of the items under the 1<sup>st</sup> <b style='mso-bidi-font-weight:
1316normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1317minor-latin;mso-hansi-theme-font:minor-latin'>refine</span></b> column, select
1318the “<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1319mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>refine</span></b>”
1320box (the column will turn blue), then press ‘y. All the position refine boxes
1321will be checked. Then repeat the <b style='mso-bidi-font-weight:normal'><span
1322style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1323mso-hansi-theme-font:minor-latin'>Peak Fitting/Peakfit</span></b> menu item; a
1324new plot will appear with a better fit.</p>
1325
1326<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1327 id="Picture_x0020_19" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:525pt;
1328 height:450pt;visibility:visible;mso-wrap-style:square'>
1329 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image007.png"
1330  o:title=""/>
1331</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1332src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image007.png"
1333v:shapes="Picture_x0020_19"><![endif]></span></p>
1334
1335<h2>Step 4: Setup for calibration</h2>
1336
1337<p class=MsoNormal>Now that we have a reasonably well fit set of peak
1338positions, we next need to index them with respect to the lattice parameters of
1339the standard. Select the <b style='mso-bidi-font-weight:normal'><span
1340style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1341mso-hansi-theme-font:minor-latin'>Index Peak List</span></b> entry in the
1342GSAS-II Data tree, an empty data window will appear. Populate it by selecting <b
1343style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1344mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Load/Reload</span></b>
1345menu item. The data table will show the positions &amp; intensities along with
13460,0,0 for h,k,l for each one.</p>
1347
1348<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1349 id="Picture_x0020_20" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:367.5pt;
1350 height:225pt;visibility:visible;mso-wrap-style:square'>
1351 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image008.png"
1352  o:title=""/>
1353</v:shape><![endif]--><![if !vml]><img border=0 width=490 height=300
1354src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image008.png"
1355v:shapes="Picture_x0020_20"><![endif]></span></p>
1356
1357<p class=MsoNormal>Next, select the <b style='mso-bidi-font-weight:normal'><span
1358style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1359mso-hansi-theme-font:minor-latin'>Unit Cells List</span></b> from the GSAS-II
1360Data tree. A new window will appear. Change Bravais lattice to <b
1361style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1362mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Pm3m</span></b>,
1363select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1364mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>P m 3 m</span></b>
1365for the Space group and enter the lattice parameter (<b style='mso-bidi-font-weight:
1366normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1367minor-latin;mso-hansi-theme-font:minor-latin'>4.15689</span></b>) in the <b
1368style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1369mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Unit cell: a
1370=</span></b> box. The window should look like</p>
1371
1372<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1373 id="Picture_x0020_21" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:546pt;
1374 height:184.5pt;visibility:visible;mso-wrap-style:square'>
1375 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image009.png"
1376  o:title=""/>
1377</v:shape><![endif]--><![if !vml]><img border=0 width=728 height=246
1378src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image009.png"
1379v:shapes="Picture_x0020_21"><![endif]></span></p>
1380
1381<p class=MsoNormal>Press the <b style='mso-bidi-font-weight:normal'><span
1382style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1383mso-hansi-theme-font:minor-latin'>Show hkl positions</span></b> button, the
1384plot should show a suite of red dashed vertical lines giving all the allowed
1385reflection positions which should closely match the blue peak position lines.</p>
1386
1387<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1388 id="Picture_x0020_23" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:560.25pt;
1389 height:450pt;visibility:visible;mso-wrap-style:square'>
1390 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image010.png"
1391  o:title=""/>
1392</v:shape><![endif]--><![if !vml]><img border=0 width=747 height=600
1393src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image010.png"
1394v:shapes="Picture_x0020_23"><![endif]></span></p>
1395
1396<p class=MsoNormal>The Index Peak List window now shows hkl values for each
1397entry</p>
1398
1399<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1400 id="Picture_x0020_24" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:367.5pt;
1401 height:225pt;visibility:visible;mso-wrap-style:square'>
1402 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image011.png"
1403  o:title=""/>
1404</v:shape><![endif]--><![if !vml]><img border=0 width=490 height=300
1405src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image011.png"
1406v:shapes="Picture_x0020_24"><![endif]></span></p>
1407
1408<p class=MsoNormal>The calibration set up is now complete.</p>
1409
1410<h2>Step 5: Calibration of diffractometer constants</h2>
1411
1412<p class=MsoNormal>As we now have a set of reflection positions each properly
1413indexed so that the d-spacings are known, we can now determine the
1414diffractometer coefficients (C, A, B and Z) that give TOF from d-spacing
1415according to</p>
1416
1417<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1418
1419<p class=MsoNormal><!--[if gte msEquation 12]><m:oMathPara><m:oMathParaPr><m:jc
1420   m:val="left"/></m:oMathParaPr><m:oMath><i style='mso-bidi-font-style:normal'><span
1421  style='font-family:"Cambria Math",serif'><m:r>TOF</m:r><m:r>=</m:r><m:r>Cd</m:r><m:r>+</m:r><m:r>A</m:r></span></i><m:sSup><m:sSupPr><span
1422    style='font-family:"Cambria Math",serif;mso-ascii-font-family:"Cambria Math";
1423    mso-hansi-font-family:"Cambria Math";font-style:italic;mso-bidi-font-style:
1424    normal'><m:ctrlPr></m:ctrlPr></span></m:sSupPr><m:e><i style='mso-bidi-font-style:
1425    normal'><span style='font-family:"Cambria Math",serif'><m:r>d</m:r></span></i></m:e><m:sup><i
1426    style='mso-bidi-font-style:normal'><span style='font-family:"Cambria Math",serif'><m:r>2</m:r></span></i></m:sup></m:sSup><i
1427  style='mso-bidi-font-style:normal'><span style='font-family:"Cambria Math",serif'><m:r>+</m:r></span></i><m:f><m:fPr><m:type
1428     m:val="skw"/><span style='font-family:"Cambria Math",serif;mso-ascii-font-family:
1429    "Cambria Math";mso-hansi-font-family:"Cambria Math";font-style:italic;
1430    mso-bidi-font-style:normal'><m:ctrlPr></m:ctrlPr></span></m:fPr><m:num><i
1431    style='mso-bidi-font-style:normal'><span style='font-family:"Cambria Math",serif'><m:r>B</m:r></span></i></m:num><m:den><i
1432    style='mso-bidi-font-style:normal'><span style='font-family:"Cambria Math",serif'><m:r>d</m:r></span></i></m:den></m:f><i
1433  style='mso-bidi-font-style:normal'><span style='font-family:"Cambria Math",serif'><m:r>+</m:r><m:r>Z</m:r></span></i></m:oMath></m:oMathPara><![endif]--><![if !msEquation]><span
1434style='font-size:12.0pt;font-family:"Times New Roman",serif;mso-fareast-font-family:
1435"Times New Roman";mso-fareast-theme-font:minor-fareast;mso-ansi-language:EN-US;
1436mso-fareast-language:EN-US;mso-bidi-language:AR-SA'><!--[if gte vml 1]><v:shape
1437 id="_x0000_i1025" type="#_x0000_t75" style='width:2in;height:18.75pt'>
1438 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image012.png"
1439  o:title="" chromakey="white"/>
1440</v:shape><![endif]--><![if !vml]><img width=192 height=25
1441src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image013.png"
1442v:shapes="_x0000_i1025"><![endif]></span><![endif]></p>
1443
1444<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1445
1446<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
1447style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1448mso-hansi-theme-font:minor-latin'>Instrument Parameters</span></b> from the
1449GSAS-II Data tree. The data window will show</p>
1450
1451<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1452 id="Picture_x0020_25" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:411pt;
1453 height:220.5pt;visibility:visible;mso-wrap-style:square'>
1454 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image014.png"
1455  o:title=""/>
1456</v:shape><![endif]--><![if !vml]><img border=0 width=548 height=294
1457src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image014.png"
1458v:shapes="Picture_x0020_25"><![endif]></span></p>
1459
1460<p class=MsoNormal>And the plot will show the corresponding function curves </p>
1461
1462<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1463 id="Picture_x0020_26" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:560.25pt;
1464 height:450pt;visibility:visible;mso-wrap-style:square'>
1465 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image015.png"
1466  o:title=""/>
1467</v:shape><![endif]--><![if !vml]><img border=0 width=747 height=600
1468src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image015.png"
1469v:shapes="Picture_x0020_26"><![endif]></span></p>
1470
1471<p class=MsoNormal>Although a previous calibration gave values for difA and
1472Zero, we will start fresh; set them both to zero. Select the <b
1473style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1474mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>difC Refine</span></b>?
1475box and do <b style='mso-bidi-font-weight:normal'><span style='font-family:
1476"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1477minor-latin'>Operations/Calibrate</span></b>; the plot will show the result of
1478the calibration</p>
1479
1480<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1481 id="Picture_x0020_27" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:560.25pt;
1482 height:450pt;visibility:visible;mso-wrap-style:square'>
1483 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image016.png"
1484  o:title=""/>
1485</v:shape><![endif]--><![if !vml]><img border=0 width=747 height=600
1486src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image016.png"
1487v:shapes="Picture_x0020_27"><![endif]></span></p>
1488
1489<p class=MsoNormal>It is obvious we have one very bad data point at a short
1490d-spacing. Use the mouse cursor to determine its position (<b style='mso-bidi-font-weight:
1491normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1492minor-latin;mso-hansi-theme-font:minor-latin'>7205.47</span></b>) so we can
1493find it in the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1494"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1495minor-latin'>Index Peak List</span></b>. Select that data item from the tree.
1496The bad point is at the bottom of the table; uncheck the <b style='mso-bidi-font-weight:
1497normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1498minor-latin;mso-hansi-theme-font:minor-latin'>use</span></b> box for it. Go
1499back to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1500mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Instrument
1501Parameters</span></b> and repeat <b style='mso-bidi-font-weight:normal'><span
1502style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1503mso-hansi-theme-font:minor-latin'>Operations/Calibrate</span></b>; the plot
1504will look a lot better.</p>
1505
1506<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1507 id="Picture_x0020_28" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:560.25pt;
1508 height:450pt;visibility:visible;mso-wrap-style:square'>
1509 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image017.png"
1510  o:title=""/>
1511</v:shape><![endif]--><![if !vml]><img border=0 width=747 height=600
1512src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image017.png"
1513v:shapes="Picture_x0020_28"><![endif]></span></p>
1514
1515<p class=MsoNormal>What is shown is the discrepancy between observed and
1516calculated position divided by the position vs d-spacing. The error bars
1517reflect the uncertainty in the fitted peak positions. The red dashed line is
1518obviously zero discrepancy and the blue dashed lines represent the width of a
1519data bin above and below zero (e.g. 2 bins from one blue line to the other) to
1520give you a sense of how significant the discrepancies are. One can improve the
1521fit by including the <b style='mso-bidi-font-weight:normal'><span
1522style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1523mso-hansi-theme-font:minor-latin'>difB</span></b> parameter; select it and
1524repeat <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1525mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Calibrate</span></b>.
1526The fit is much improved.</p>
1527
1528<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1529 id="Picture_x0020_29" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:560.25pt;
1530 height:450pt;visibility:visible;mso-wrap-style:square'>
1531 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image018.png"
1532  o:title=""/>
1533</v:shape><![endif]--><![if !vml]><img border=0 width=747 height=600
1534src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image018.png"
1535v:shapes="Picture_x0020_29"><![endif]></span></p>
1536
1537<p class=MsoNormal>Notice that the deviation is largest at the larger
1538d-spacings; select <b style='mso-bidi-font-weight:normal'><span
1539style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1540mso-hansi-theme-font:minor-latin'>difA</span></b> next and calibrate again. The
1541fit is better especially at the large d-spacings.</p>
1542
1543<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1544 id="Picture_x0020_30" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:560.25pt;
1545 height:450pt;visibility:visible;mso-wrap-style:square'>
1546 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image019.png"
1547  o:title=""/>
1548</v:shape><![endif]--><![if !vml]><img border=0 width=747 height=600
1549src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image019.png"
1550v:shapes="Picture_x0020_30"><![endif]></span></p>
1551
1552<p class=MsoNormal>Further improvement can be gained by including <b
1553style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1554mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Zero</span></b>.
1555The result is</p>
1556
1557<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1558 id="Picture_x0020_31" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:560.25pt;
1559 height:450pt;visibility:visible;mso-wrap-style:square'>
1560 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image020.png"
1561  o:title=""/>
1562</v:shape><![endif]--><![if !vml]><img border=0 width=747 height=600
1563src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image020.png"
1564v:shapes="Picture_x0020_31"><![endif]></span></p>
1565
1566<p class=MsoNormal>with the new parameters</p>
1567
1568<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1569 id="Picture_x0020_32" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:411pt;
1570 height:203.25pt;visibility:visible;mso-wrap-style:square'>
1571 <v:imagedata src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image021.png"
1572  o:title=""/>
1573</v:shape><![endif]--><![if !vml]><img border=0 width=548 height=271
1574src="Calibration%20of%20a%20TOF%20powder%20diffractometer_files/image021.png"
1575v:shapes="Picture_x0020_32"><![endif]></span></p>
1576
1577<p class=MsoNormal>These new instrument parameters can be saved for later use;
1578select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1579mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Save
1580profile…</span></b> from the menu. A file name is requested (no extension);
1581this file can be used in place of the old GSAS instrument parameter file when
1582reading new data for this instrument. Notice that we did not establish values
1583for the instrument profile coefficients (alpha, beta &amp; sig terms). These
1584are best set <i style='mso-bidi-font-style:normal'>via</i> Rietveld refinement
1585of a suitable standard (SRM 660b La<sup>10</sup>B<sub>6</sub> is good for
1586this). This ends this tutorial exercise; you may save the project if you wish,
1587select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1588mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/Save
1589project</span></b> from the GSAS-II data tree window.</p>
1590
1591</div>
1592
1593</body>
1594
1595</html>
Note: See TracBrowser for help on using the repository browser.