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| 5 | xmlns="http://www.w3.org/TR/REC-html40"> |
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| 6 | |
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| 7 | <head> |
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| 8 | <meta http-equiv=Content-Type content="text/html; charset=windows-1252"> |
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| 11 | <meta name=Originator content="Microsoft Word 15"> |
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| 12 | <link rel=File-List |
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| 13 | href="Small%20Angle%20Size%20Distribution_files/filelist.xml"> |
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| 14 | <link rel=Edit-Time-Data |
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| 15 | href="Small%20Angle%20Size%20Distribution_files/editdata.mso"> |
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| 16 | <!--[if !mso]> |
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| 17 | <style> |
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| 18 | v\:* {behavior:url(#default#VML);} |
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| 19 | o\:* {behavior:url(#default#VML);} |
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| 20 | w\:* {behavior:url(#default#VML);} |
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| 21 | .shape {behavior:url(#default#VML);} |
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| 22 | </style> |
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| 23 | <![endif]--><!--[if gte mso 9]><xml> |
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| 24 | <o:DocumentProperties> |
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| 25 | <o:Author>Von Dreele</o:Author> |
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| 26 | <o:LastAuthor>vondreele</o:LastAuthor> |
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| 27 | <o:Revision>17</o:Revision> |
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| 28 | <o:TotalTime>1975</o:TotalTime> |
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| 29 | <o:Created>2014-03-20T16:54:00Z</o:Created> |
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| 30 | <o:LastSaved>2017-08-30T19:25:00Z</o:LastSaved> |
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| 31 | <o:Pages>14</o:Pages> |
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| 32 | <o:Words>1274</o:Words> |
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| 33 | <o:Characters>7265</o:Characters> |
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| 34 | <o:Company>Argonne National Laboratory</o:Company> |
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| 35 | <o:Lines>60</o:Lines> |
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| 36 | <o:Paragraphs>17</o:Paragraphs> |
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| 37 | <o:CharactersWithSpaces>8522</o:CharactersWithSpaces> |
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| 38 | <o:Version>16.00</o:Version> |
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| 39 | </o:DocumentProperties> |
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| 40 | <o:OfficeDocumentSettings> |
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| 41 | <o:AllowPNG/> |
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| 42 | </o:OfficeDocumentSettings> |
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| 43 | </xml><![endif]--> |
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| 45 | href="Small%20Angle%20Size%20Distribution_files/themedata.thmx"> |
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| 46 | <link rel=colorSchemeMapping |
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| 47 | href="Small%20Angle%20Size%20Distribution_files/colorschememapping.xml"> |
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| 48 | <!--[if gte mso 9]><xml> |
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| 64 | <w:Compatibility> |
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| 66 | <w:SnapToGridInCell/> |
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| 67 | <w:WrapTextWithPunct/> |
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| 68 | <w:UseAsianBreakRules/> |
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| 69 | <w:DontGrowAutofit/> |
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| 70 | <w:SplitPgBreakAndParaMark/> |
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| 71 | <w:EnableOpenTypeKerning/> |
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| 72 | <w:DontFlipMirrorIndents/> |
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| 73 | <w:OverrideTableStyleHps/> |
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| 74 | </w:Compatibility> |
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| 79 | <m:brkBinSub m:val="--"/> |
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| 88 | </m:mathPr></w:WordDocument> |
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| 89 | </xml><![endif]--><!--[if gte mso 9]><xml> |
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| 90 | <w:LatentStyles DefLockedState="false" DefUnhideWhenUsed="false" |
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| 111 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 113 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 115 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 117 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 118 | Name="index 4"/> |
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| 119 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 120 | Name="index 5"/> |
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| 121 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 122 | Name="index 6"/> |
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| 145 | <w:LsdException Locked="false" Priority="39" SemiHidden="true" |
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| 146 | UnhideWhenUsed="true" Name="toc 9"/> |
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| 147 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 148 | Name="Normal Indent"/> |
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| 149 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 150 | Name="footnote text"/> |
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| 151 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 152 | Name="annotation text"/> |
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| 153 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 154 | Name="header"/> |
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| 155 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 156 | Name="footer"/> |
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| 157 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 158 | Name="index heading"/> |
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| 159 | <w:LsdException Locked="false" Priority="35" SemiHidden="true" |
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| 160 | UnhideWhenUsed="true" QFormat="true" Name="caption"/> |
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| 161 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 162 | Name="table of figures"/> |
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| 163 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 164 | Name="envelope address"/> |
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| 165 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 166 | Name="envelope return"/> |
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| 167 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 168 | Name="footnote reference"/> |
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| 169 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 170 | Name="annotation reference"/> |
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| 171 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 172 | Name="line number"/> |
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| 173 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 174 | Name="page number"/> |
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| 175 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 176 | Name="endnote reference"/> |
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| 177 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 178 | Name="endnote text"/> |
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| 179 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 180 | Name="table of authorities"/> |
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| 181 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 182 | Name="macro"/> |
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| 183 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 184 | Name="toa heading"/> |
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| 185 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 186 | Name="List"/> |
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| 187 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 188 | Name="List Bullet"/> |
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| 189 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 190 | Name="List Number"/> |
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| 191 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 192 | Name="List 2"/> |
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| 193 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 194 | Name="List 3"/> |
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| 195 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 196 | Name="List 4"/> |
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| 197 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 198 | Name="List 5"/> |
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| 199 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 200 | Name="List Bullet 2"/> |
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| 201 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 202 | Name="List Bullet 3"/> |
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| 203 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 204 | Name="List Bullet 4"/> |
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| 205 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 206 | Name="List Bullet 5"/> |
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| 207 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 208 | Name="List Number 2"/> |
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| 209 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 210 | Name="List Number 3"/> |
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| 211 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 212 | Name="List Number 4"/> |
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| 213 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 214 | Name="List Number 5"/> |
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| 215 | <w:LsdException Locked="false" Priority="10" QFormat="true" Name="Title"/> |
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| 216 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 217 | Name="Closing"/> |
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| 218 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 219 | Name="Signature"/> |
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| 220 | <w:LsdException Locked="false" Priority="1" SemiHidden="true" |
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| 221 | UnhideWhenUsed="true" Name="Default Paragraph Font"/> |
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| 222 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 223 | Name="Body Text"/> |
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| 224 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 225 | Name="Body Text Indent"/> |
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| 226 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 227 | Name="List Continue"/> |
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| 228 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 229 | Name="List Continue 2"/> |
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| 230 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 231 | Name="List Continue 3"/> |
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| 232 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 233 | Name="List Continue 4"/> |
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| 234 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 235 | Name="List Continue 5"/> |
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| 236 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 237 | Name="Message Header"/> |
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| 238 | <w:LsdException Locked="false" Priority="11" QFormat="true" Name="Subtitle"/> |
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| 239 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 240 | Name="Salutation"/> |
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| 241 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 242 | Name="Date"/> |
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| 243 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 244 | Name="Body Text First Indent"/> |
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| 245 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 246 | Name="Body Text First Indent 2"/> |
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| 247 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 248 | Name="Note Heading"/> |
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| 249 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 250 | Name="Body Text 2"/> |
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| 251 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 252 | Name="Body Text 3"/> |
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| 253 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 254 | Name="Body Text Indent 2"/> |
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| 255 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 256 | Name="Body Text Indent 3"/> |
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| 257 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 258 | Name="Block Text"/> |
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| 259 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 260 | Name="Hyperlink"/> |
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| 261 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 262 | Name="FollowedHyperlink"/> |
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| 263 | <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/> |
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| 264 | <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/> |
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| 265 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 266 | Name="Document Map"/> |
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| 267 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 268 | Name="Plain Text"/> |
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| 269 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 270 | Name="E-mail Signature"/> |
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| 271 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 272 | Name="HTML Top of Form"/> |
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| 273 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 274 | Name="HTML Bottom of Form"/> |
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| 275 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 276 | Name="Normal (Web)"/> |
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| 277 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 278 | Name="HTML Acronym"/> |
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| 279 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 280 | Name="HTML Address"/> |
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| 281 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 282 | Name="HTML Cite"/> |
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| 283 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 284 | Name="HTML Code"/> |
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| 285 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 286 | Name="HTML Definition"/> |
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| 287 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 288 | Name="HTML Keyboard"/> |
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| 289 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 290 | Name="HTML Preformatted"/> |
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| 291 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 292 | Name="HTML Sample"/> |
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| 293 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 294 | Name="HTML Typewriter"/> |
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| 295 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 296 | Name="HTML Variable"/> |
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| 297 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 298 | Name="Normal Table"/> |
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| 299 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 300 | Name="annotation subject"/> |
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| 301 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 302 | Name="No List"/> |
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| 303 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 304 | Name="Outline List 1"/> |
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| 305 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 306 | Name="Outline List 2"/> |
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| 307 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 308 | Name="Outline List 3"/> |
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| 309 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 310 | Name="Table Simple 1"/> |
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| 311 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 312 | Name="Table Simple 2"/> |
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| 313 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 314 | Name="Table Simple 3"/> |
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| 315 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 316 | Name="Table Classic 1"/> |
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| 317 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 318 | Name="Table Classic 2"/> |
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| 319 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 320 | Name="Table Classic 3"/> |
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| 321 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 322 | Name="Table Classic 4"/> |
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| 323 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 324 | Name="Table Colorful 1"/> |
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| 325 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 326 | Name="Table Colorful 2"/> |
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| 327 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 328 | Name="Table Colorful 3"/> |
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| 329 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 330 | Name="Table Columns 1"/> |
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| 331 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 332 | Name="Table Columns 2"/> |
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| 333 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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| 334 | Name="Table Columns 3"/> |
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| 335 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 336 | Name="Table Columns 4"/> |
|---|
| 337 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 338 | Name="Table Columns 5"/> |
|---|
| 339 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 340 | Name="Table Grid 1"/> |
|---|
| 341 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 342 | Name="Table Grid 2"/> |
|---|
| 343 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 344 | Name="Table Grid 3"/> |
|---|
| 345 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 346 | Name="Table Grid 4"/> |
|---|
| 347 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 348 | Name="Table Grid 5"/> |
|---|
| 349 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 350 | Name="Table Grid 6"/> |
|---|
| 351 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 352 | Name="Table Grid 7"/> |
|---|
| 353 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 354 | Name="Table Grid 8"/> |
|---|
| 355 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 356 | Name="Table List 1"/> |
|---|
| 357 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 358 | Name="Table List 2"/> |
|---|
| 359 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 360 | Name="Table List 3"/> |
|---|
| 361 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 362 | Name="Table List 4"/> |
|---|
| 363 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 364 | Name="Table List 5"/> |
|---|
| 365 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 366 | Name="Table List 6"/> |
|---|
| 367 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 368 | Name="Table List 7"/> |
|---|
| 369 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 370 | Name="Table List 8"/> |
|---|
| 371 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 372 | Name="Table 3D effects 1"/> |
|---|
| 373 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 374 | Name="Table 3D effects 2"/> |
|---|
| 375 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 376 | Name="Table 3D effects 3"/> |
|---|
| 377 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 378 | Name="Table Contemporary"/> |
|---|
| 379 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 380 | Name="Table Elegant"/> |
|---|
| 381 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 382 | Name="Table Professional"/> |
|---|
| 383 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 384 | Name="Table Subtle 1"/> |
|---|
| 385 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 386 | Name="Table Subtle 2"/> |
|---|
| 387 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 388 | Name="Table Web 1"/> |
|---|
| 389 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 390 | Name="Table Web 2"/> |
|---|
| 391 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 392 | Name="Table Web 3"/> |
|---|
| 393 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 394 | Name="Balloon Text"/> |
|---|
| 395 | <w:LsdException Locked="false" Priority="59" Name="Table Grid"/> |
|---|
| 396 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
|---|
| 397 | Name="Table Theme"/> |
|---|
| 398 | <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/> |
|---|
| 399 | <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/> |
|---|
| 400 | <w:LsdException Locked="false" Priority="60" Name="Light Shading"/> |
|---|
| 401 | <w:LsdException Locked="false" Priority="61" Name="Light List"/> |
|---|
| 402 | <w:LsdException Locked="false" Priority="62" Name="Light Grid"/> |
|---|
| 403 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/> |
|---|
| 404 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/> |
|---|
| 405 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/> |
|---|
| 406 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/> |
|---|
| 407 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/> |
|---|
| 408 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/> |
|---|
| 409 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/> |
|---|
| 410 | <w:LsdException Locked="false" Priority="70" Name="Dark List"/> |
|---|
| 411 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/> |
|---|
| 412 | <w:LsdException Locked="false" Priority="72" Name="Colorful List"/> |
|---|
| 413 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/> |
|---|
| 414 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/> |
|---|
| 415 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/> |
|---|
| 416 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/> |
|---|
| 417 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/> |
|---|
| 418 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/> |
|---|
| 419 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/> |
|---|
| 420 | <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/> |
|---|
| 421 | <w:LsdException Locked="false" Priority="34" QFormat="true" |
|---|
| 422 | Name="List Paragraph"/> |
|---|
| 423 | <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/> |
|---|
| 424 | <w:LsdException Locked="false" Priority="30" QFormat="true" |
|---|
| 425 | Name="Intense Quote"/> |
|---|
| 426 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/> |
|---|
| 427 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/> |
|---|
| 428 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/> |
|---|
| 429 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/> |
|---|
| 430 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/> |
|---|
| 431 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/> |
|---|
| 432 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/> |
|---|
| 433 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/> |
|---|
| 434 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/> |
|---|
| 435 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/> |
|---|
| 436 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/> |
|---|
| 437 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/> |
|---|
| 438 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/> |
|---|
| 439 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/> |
|---|
| 440 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/> |
|---|
| 441 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/> |
|---|
| 442 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/> |
|---|
| 443 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/> |
|---|
| 444 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/> |
|---|
| 445 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/> |
|---|
| 446 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/> |
|---|
| 447 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/> |
|---|
| 448 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/> |
|---|
| 449 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/> |
|---|
| 450 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/> |
|---|
| 451 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/> |
|---|
| 452 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/> |
|---|
| 453 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/> |
|---|
| 454 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/> |
|---|
| 455 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/> |
|---|
| 456 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/> |
|---|
| 457 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/> |
|---|
| 458 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/> |
|---|
| 459 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/> |
|---|
| 460 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/> |
|---|
| 461 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/> |
|---|
| 462 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/> |
|---|
| 463 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/> |
|---|
| 464 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/> |
|---|
| 465 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/> |
|---|
| 466 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/> |
|---|
| 467 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/> |
|---|
| 468 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/> |
|---|
| 469 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/> |
|---|
| 470 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/> |
|---|
| 471 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/> |
|---|
| 472 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/> |
|---|
| 473 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/> |
|---|
| 474 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/> |
|---|
| 475 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/> |
|---|
| 476 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/> |
|---|
| 477 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/> |
|---|
| 478 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/> |
|---|
| 479 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/> |
|---|
| 480 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/> |
|---|
| 481 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/> |
|---|
| 482 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/> |
|---|
| 483 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/> |
|---|
| 484 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/> |
|---|
| 485 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/> |
|---|
| 486 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/> |
|---|
| 487 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/> |
|---|
| 488 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/> |
|---|
| 489 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/> |
|---|
| 490 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/> |
|---|
| 491 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/> |
|---|
| 492 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/> |
|---|
| 493 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/> |
|---|
| 494 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/> |
|---|
| 495 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/> |
|---|
| 496 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/> |
|---|
| 497 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/> |
|---|
| 498 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/> |
|---|
| 499 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/> |
|---|
| 500 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/> |
|---|
| 501 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/> |
|---|
| 502 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/> |
|---|
| 503 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/> |
|---|
| 504 | <w:LsdException Locked="false" Priority="19" QFormat="true" |
|---|
| 505 | Name="Subtle Emphasis"/> |
|---|
| 506 | <w:LsdException Locked="false" Priority="21" QFormat="true" |
|---|
| 507 | Name="Intense Emphasis"/> |
|---|
| 508 | <w:LsdException Locked="false" Priority="31" QFormat="true" |
|---|
| 509 | Name="Subtle Reference"/> |
|---|
| 510 | <w:LsdException Locked="false" Priority="32" QFormat="true" |
|---|
| 511 | Name="Intense Reference"/> |
|---|
| 512 | <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/> |
|---|
| 513 | <w:LsdException Locked="false" Priority="37" SemiHidden="true" |
|---|
| 514 | UnhideWhenUsed="true" Name="Bibliography"/> |
|---|
| 515 | <w:LsdException Locked="false" Priority="39" SemiHidden="true" |
|---|
| 516 | UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/> |
|---|
| 517 | <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/> |
|---|
| 518 | <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/> |
|---|
| 519 | <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/> |
|---|
| 520 | <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/> |
|---|
| 521 | <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/> |
|---|
| 522 | <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/> |
|---|
| 523 | <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/> |
|---|
| 524 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/> |
|---|
| 525 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/> |
|---|
| 526 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/> |
|---|
| 527 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/> |
|---|
| 528 | <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/> |
|---|
| 529 | <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/> |
|---|
| 530 | <w:LsdException Locked="false" Priority="46" |
|---|
| 531 | Name="Grid Table 1 Light Accent 1"/> |
|---|
| 532 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/> |
|---|
| 533 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/> |
|---|
| 534 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/> |
|---|
| 535 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/> |
|---|
| 536 | <w:LsdException Locked="false" Priority="51" |
|---|
| 537 | Name="Grid Table 6 Colorful Accent 1"/> |
|---|
| 538 | <w:LsdException Locked="false" Priority="52" |
|---|
| 539 | Name="Grid Table 7 Colorful Accent 1"/> |
|---|
| 540 | <w:LsdException Locked="false" Priority="46" |
|---|
| 541 | Name="Grid Table 1 Light Accent 2"/> |
|---|
| 542 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/> |
|---|
| 543 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/> |
|---|
| 544 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/> |
|---|
| 545 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/> |
|---|
| 546 | <w:LsdException Locked="false" Priority="51" |
|---|
| 547 | Name="Grid Table 6 Colorful Accent 2"/> |
|---|
| 548 | <w:LsdException Locked="false" Priority="52" |
|---|
| 549 | Name="Grid Table 7 Colorful Accent 2"/> |
|---|
| 550 | <w:LsdException Locked="false" Priority="46" |
|---|
| 551 | Name="Grid Table 1 Light Accent 3"/> |
|---|
| 552 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/> |
|---|
| 553 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/> |
|---|
| 554 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/> |
|---|
| 555 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/> |
|---|
| 556 | <w:LsdException Locked="false" Priority="51" |
|---|
| 557 | Name="Grid Table 6 Colorful Accent 3"/> |
|---|
| 558 | <w:LsdException Locked="false" Priority="52" |
|---|
| 559 | Name="Grid Table 7 Colorful Accent 3"/> |
|---|
| 560 | <w:LsdException Locked="false" Priority="46" |
|---|
| 561 | Name="Grid Table 1 Light Accent 4"/> |
|---|
| 562 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/> |
|---|
| 563 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/> |
|---|
| 564 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/> |
|---|
| 565 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/> |
|---|
| 566 | <w:LsdException Locked="false" Priority="51" |
|---|
| 567 | Name="Grid Table 6 Colorful Accent 4"/> |
|---|
| 568 | <w:LsdException Locked="false" Priority="52" |
|---|
| 569 | Name="Grid Table 7 Colorful Accent 4"/> |
|---|
| 570 | <w:LsdException Locked="false" Priority="46" |
|---|
| 571 | Name="Grid Table 1 Light Accent 5"/> |
|---|
| 572 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/> |
|---|
| 573 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/> |
|---|
| 574 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/> |
|---|
| 575 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/> |
|---|
| 576 | <w:LsdException Locked="false" Priority="51" |
|---|
| 577 | Name="Grid Table 6 Colorful Accent 5"/> |
|---|
| 578 | <w:LsdException Locked="false" Priority="52" |
|---|
| 579 | Name="Grid Table 7 Colorful Accent 5"/> |
|---|
| 580 | <w:LsdException Locked="false" Priority="46" |
|---|
| 581 | Name="Grid Table 1 Light Accent 6"/> |
|---|
| 582 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/> |
|---|
| 583 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/> |
|---|
| 584 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/> |
|---|
| 585 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/> |
|---|
| 586 | <w:LsdException Locked="false" Priority="51" |
|---|
| 587 | Name="Grid Table 6 Colorful Accent 6"/> |
|---|
| 588 | <w:LsdException Locked="false" Priority="52" |
|---|
| 589 | Name="Grid Table 7 Colorful Accent 6"/> |
|---|
| 590 | <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/> |
|---|
| 591 | <w:LsdException Locked="false" Priority="47" Name="List Table 2"/> |
|---|
| 592 | <w:LsdException Locked="false" Priority="48" Name="List Table 3"/> |
|---|
| 593 | <w:LsdException Locked="false" Priority="49" Name="List Table 4"/> |
|---|
| 594 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/> |
|---|
| 595 | <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/> |
|---|
| 596 | <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/> |
|---|
| 597 | <w:LsdException Locked="false" Priority="46" |
|---|
| 598 | Name="List Table 1 Light Accent 1"/> |
|---|
| 599 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/> |
|---|
| 600 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/> |
|---|
| 601 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/> |
|---|
| 602 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/> |
|---|
| 603 | <w:LsdException Locked="false" Priority="51" |
|---|
| 604 | Name="List Table 6 Colorful Accent 1"/> |
|---|
| 605 | <w:LsdException Locked="false" Priority="52" |
|---|
| 606 | Name="List Table 7 Colorful Accent 1"/> |
|---|
| 607 | <w:LsdException Locked="false" Priority="46" |
|---|
| 608 | Name="List Table 1 Light Accent 2"/> |
|---|
| 609 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/> |
|---|
| 610 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/> |
|---|
| 611 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/> |
|---|
| 612 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/> |
|---|
| 613 | <w:LsdException Locked="false" Priority="51" |
|---|
| 614 | Name="List Table 6 Colorful Accent 2"/> |
|---|
| 615 | <w:LsdException Locked="false" Priority="52" |
|---|
| 616 | Name="List Table 7 Colorful Accent 2"/> |
|---|
| 617 | <w:LsdException Locked="false" Priority="46" |
|---|
| 618 | Name="List Table 1 Light Accent 3"/> |
|---|
| 619 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/> |
|---|
| 620 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/> |
|---|
| 621 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/> |
|---|
| 622 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/> |
|---|
| 623 | <w:LsdException Locked="false" Priority="51" |
|---|
| 624 | Name="List Table 6 Colorful Accent 3"/> |
|---|
| 625 | <w:LsdException Locked="false" Priority="52" |
|---|
| 626 | Name="List Table 7 Colorful Accent 3"/> |
|---|
| 627 | <w:LsdException Locked="false" Priority="46" |
|---|
| 628 | Name="List Table 1 Light Accent 4"/> |
|---|
| 629 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/> |
|---|
| 630 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/> |
|---|
| 631 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/> |
|---|
| 632 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/> |
|---|
| 633 | <w:LsdException Locked="false" Priority="51" |
|---|
| 634 | Name="List Table 6 Colorful Accent 4"/> |
|---|
| 635 | <w:LsdException Locked="false" Priority="52" |
|---|
| 636 | Name="List Table 7 Colorful Accent 4"/> |
|---|
| 637 | <w:LsdException Locked="false" Priority="46" |
|---|
| 638 | Name="List Table 1 Light Accent 5"/> |
|---|
| 639 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/> |
|---|
| 640 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/> |
|---|
| 641 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/> |
|---|
| 642 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/> |
|---|
| 643 | <w:LsdException Locked="false" Priority="51" |
|---|
| 644 | Name="List Table 6 Colorful Accent 5"/> |
|---|
| 645 | <w:LsdException Locked="false" Priority="52" |
|---|
| 646 | Name="List Table 7 Colorful Accent 5"/> |
|---|
| 647 | <w:LsdException Locked="false" Priority="46" |
|---|
| 648 | Name="List Table 1 Light Accent 6"/> |
|---|
| 649 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/> |
|---|
| 650 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/> |
|---|
| 651 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/> |
|---|
| 652 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/> |
|---|
| 653 | <w:LsdException Locked="false" Priority="51" |
|---|
| 654 | Name="List Table 6 Colorful Accent 6"/> |
|---|
| 655 | <w:LsdException Locked="false" Priority="52" |
|---|
| 656 | Name="List Table 7 Colorful Accent 6"/> |
|---|
| 657 | </w:LatentStyles> |
|---|
| 658 | </xml><![endif]--> |
|---|
| 659 | <style> |
|---|
| 660 | <!-- |
|---|
| 661 | /* Font Definitions */ |
|---|
| 662 | @font-face |
|---|
| 663 | {font-family:"Cambria Math"; |
|---|
| 664 | panose-1:2 4 5 3 5 4 6 3 2 4; |
|---|
| 665 | mso-font-charset:1; |
|---|
| 666 | mso-generic-font-family:roman; |
|---|
| 667 | mso-font-pitch:variable; |
|---|
| 668 | mso-font-signature:0 0 0 0 0 0;} |
|---|
| 669 | @font-face |
|---|
| 670 | {font-family:Calibri; |
|---|
| 671 | panose-1:2 15 5 2 2 2 4 3 2 4; |
|---|
| 672 | mso-font-charset:0; |
|---|
| 673 | mso-generic-font-family:swiss; |
|---|
| 674 | mso-font-pitch:variable; |
|---|
| 675 | mso-font-signature:-536859905 -1073732485 9 0 511 0;} |
|---|
| 676 | @font-face |
|---|
| 677 | {font-family:Tahoma; |
|---|
| 678 | panose-1:2 11 6 4 3 5 4 4 2 4; |
|---|
| 679 | mso-font-charset:0; |
|---|
| 680 | mso-generic-font-family:swiss; |
|---|
| 681 | mso-font-pitch:variable; |
|---|
| 682 | mso-font-signature:-520081665 -1073717157 41 0 66047 0;} |
|---|
| 683 | /* Style Definitions */ |
|---|
| 684 | p.MsoNormal, li.MsoNormal, div.MsoNormal |
|---|
| 685 | {mso-style-unhide:no; |
|---|
| 686 | mso-style-qformat:yes; |
|---|
| 687 | mso-style-parent:""; |
|---|
| 688 | margin:0in; |
|---|
| 689 | margin-bottom:.0001pt; |
|---|
| 690 | mso-pagination:widow-orphan; |
|---|
| 691 | font-size:12.0pt; |
|---|
| 692 | font-family:"Times New Roman",serif; |
|---|
| 693 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 694 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 695 | h1 |
|---|
| 696 | {mso-style-priority:9; |
|---|
| 697 | mso-style-unhide:no; |
|---|
| 698 | mso-style-qformat:yes; |
|---|
| 699 | mso-style-link:"Heading 1 Char"; |
|---|
| 700 | mso-margin-top-alt:auto; |
|---|
| 701 | margin-right:0in; |
|---|
| 702 | mso-margin-bottom-alt:auto; |
|---|
| 703 | margin-left:0in; |
|---|
| 704 | mso-pagination:widow-orphan; |
|---|
| 705 | mso-outline-level:1; |
|---|
| 706 | font-size:24.0pt; |
|---|
| 707 | font-family:"Times New Roman",serif; |
|---|
| 708 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 709 | mso-fareast-theme-font:minor-fareast; |
|---|
| 710 | font-weight:bold;} |
|---|
| 711 | h2 |
|---|
| 712 | {mso-style-noshow:yes; |
|---|
| 713 | mso-style-priority:9; |
|---|
| 714 | mso-style-qformat:yes; |
|---|
| 715 | mso-style-link:"Heading 2 Char"; |
|---|
| 716 | mso-margin-top-alt:auto; |
|---|
| 717 | margin-right:0in; |
|---|
| 718 | mso-margin-bottom-alt:auto; |
|---|
| 719 | margin-left:0in; |
|---|
| 720 | mso-pagination:widow-orphan; |
|---|
| 721 | mso-outline-level:2; |
|---|
| 722 | font-size:18.0pt; |
|---|
| 723 | font-family:"Times New Roman",serif; |
|---|
| 724 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 725 | mso-fareast-theme-font:minor-fareast; |
|---|
| 726 | font-weight:bold;} |
|---|
| 727 | h3 |
|---|
| 728 | {mso-style-noshow:yes; |
|---|
| 729 | mso-style-priority:9; |
|---|
| 730 | mso-style-qformat:yes; |
|---|
| 731 | mso-style-link:"Heading 3 Char"; |
|---|
| 732 | mso-margin-top-alt:auto; |
|---|
| 733 | margin-right:0in; |
|---|
| 734 | mso-margin-bottom-alt:auto; |
|---|
| 735 | margin-left:0in; |
|---|
| 736 | mso-pagination:widow-orphan; |
|---|
| 737 | mso-outline-level:3; |
|---|
| 738 | font-size:13.5pt; |
|---|
| 739 | font-family:"Times New Roman",serif; |
|---|
| 740 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 741 | mso-fareast-theme-font:minor-fareast; |
|---|
| 742 | font-weight:bold;} |
|---|
| 743 | h4 |
|---|
| 744 | {mso-style-noshow:yes; |
|---|
| 745 | mso-style-priority:9; |
|---|
| 746 | mso-style-qformat:yes; |
|---|
| 747 | mso-style-link:"Heading 4 Char"; |
|---|
| 748 | mso-style-next:Normal; |
|---|
| 749 | margin-top:10.0pt; |
|---|
| 750 | margin-right:0in; |
|---|
| 751 | margin-bottom:0in; |
|---|
| 752 | margin-left:0in; |
|---|
| 753 | margin-bottom:.0001pt; |
|---|
| 754 | mso-pagination:widow-orphan lines-together; |
|---|
| 755 | page-break-after:avoid; |
|---|
| 756 | mso-outline-level:4; |
|---|
| 757 | font-size:13.0pt; |
|---|
| 758 | font-family:"Cambria",serif; |
|---|
| 759 | mso-ascii-font-family:Cambria; |
|---|
| 760 | mso-ascii-theme-font:major-latin; |
|---|
| 761 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 762 | mso-fareast-theme-font:major-fareast; |
|---|
| 763 | mso-hansi-font-family:Cambria; |
|---|
| 764 | mso-hansi-theme-font:major-latin; |
|---|
| 765 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 766 | mso-bidi-theme-font:major-bidi; |
|---|
| 767 | color:#4F81BD; |
|---|
| 768 | mso-themecolor:accent1; |
|---|
| 769 | font-weight:bold; |
|---|
| 770 | font-style:italic;} |
|---|
| 771 | h5 |
|---|
| 772 | {mso-style-noshow:yes; |
|---|
| 773 | mso-style-priority:9; |
|---|
| 774 | mso-style-qformat:yes; |
|---|
| 775 | mso-style-link:"Heading 5 Char"; |
|---|
| 776 | mso-margin-top-alt:auto; |
|---|
| 777 | margin-right:0in; |
|---|
| 778 | mso-margin-bottom-alt:auto; |
|---|
| 779 | margin-left:0in; |
|---|
| 780 | mso-pagination:widow-orphan; |
|---|
| 781 | mso-outline-level:5; |
|---|
| 782 | font-size:12.0pt; |
|---|
| 783 | font-family:"Times New Roman",serif; |
|---|
| 784 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 785 | mso-fareast-theme-font:minor-fareast; |
|---|
| 786 | color:#4F4FFF; |
|---|
| 787 | font-weight:bold;} |
|---|
| 788 | a:link, span.MsoHyperlink |
|---|
| 789 | {mso-style-noshow:yes; |
|---|
| 790 | mso-style-priority:99; |
|---|
| 791 | color:blue; |
|---|
| 792 | text-decoration:underline; |
|---|
| 793 | text-underline:single;} |
|---|
| 794 | a:visited, span.MsoHyperlinkFollowed |
|---|
| 795 | {mso-style-noshow:yes; |
|---|
| 796 | mso-style-priority:99; |
|---|
| 797 | color:purple; |
|---|
| 798 | text-decoration:underline; |
|---|
| 799 | text-underline:single;} |
|---|
| 800 | p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap |
|---|
| 801 | {mso-style-noshow:yes; |
|---|
| 802 | mso-style-priority:99; |
|---|
| 803 | mso-style-link:"Document Map Char"; |
|---|
| 804 | margin:0in; |
|---|
| 805 | margin-bottom:.0001pt; |
|---|
| 806 | mso-pagination:widow-orphan; |
|---|
| 807 | font-size:8.0pt; |
|---|
| 808 | font-family:"Tahoma",sans-serif; |
|---|
| 809 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 810 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 811 | p |
|---|
| 812 | {mso-style-noshow:yes; |
|---|
| 813 | mso-style-priority:99; |
|---|
| 814 | mso-margin-top-alt:auto; |
|---|
| 815 | margin-right:0in; |
|---|
| 816 | mso-margin-bottom-alt:auto; |
|---|
| 817 | margin-left:0in; |
|---|
| 818 | mso-pagination:widow-orphan; |
|---|
| 819 | font-size:12.0pt; |
|---|
| 820 | font-family:"Times New Roman",serif; |
|---|
| 821 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 822 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 823 | pre |
|---|
| 824 | {mso-style-noshow:yes; |
|---|
| 825 | mso-style-priority:99; |
|---|
| 826 | mso-style-link:"HTML Preformatted Char"; |
|---|
| 827 | margin:0in; |
|---|
| 828 | margin-bottom:.0001pt; |
|---|
| 829 | mso-pagination:widow-orphan; |
|---|
| 830 | tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt; |
|---|
| 831 | font-size:10.0pt; |
|---|
| 832 | font-family:"Courier New"; |
|---|
| 833 | mso-fareast-font-family:"Times New Roman";} |
|---|
| 834 | p.MsoAcetate, li.MsoAcetate, div.MsoAcetate |
|---|
| 835 | {mso-style-noshow:yes; |
|---|
| 836 | mso-style-priority:99; |
|---|
| 837 | mso-style-link:"Balloon Text Char"; |
|---|
| 838 | margin:0in; |
|---|
| 839 | margin-bottom:.0001pt; |
|---|
| 840 | mso-pagination:widow-orphan; |
|---|
| 841 | font-size:8.0pt; |
|---|
| 842 | font-family:"Tahoma",sans-serif; |
|---|
| 843 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 844 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 845 | span.MsoPlaceholderText |
|---|
| 846 | {mso-style-noshow:yes; |
|---|
| 847 | mso-style-priority:99; |
|---|
| 848 | mso-style-unhide:no; |
|---|
| 849 | color:gray;} |
|---|
| 850 | p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing |
|---|
| 851 | {mso-style-noshow:yes; |
|---|
| 852 | mso-style-priority:1; |
|---|
| 853 | mso-style-unhide:no; |
|---|
| 854 | mso-style-qformat:yes; |
|---|
| 855 | mso-style-parent:""; |
|---|
| 856 | margin:0in; |
|---|
| 857 | margin-bottom:.0001pt; |
|---|
| 858 | mso-pagination:widow-orphan; |
|---|
| 859 | font-size:12.0pt; |
|---|
| 860 | font-family:"Times New Roman",serif; |
|---|
| 861 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 862 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 863 | p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph |
|---|
| 864 | {mso-style-noshow:yes; |
|---|
| 865 | mso-style-priority:34; |
|---|
| 866 | mso-style-unhide:no; |
|---|
| 867 | mso-style-qformat:yes; |
|---|
| 868 | margin-top:0in; |
|---|
| 869 | margin-right:0in; |
|---|
| 870 | margin-bottom:0in; |
|---|
| 871 | margin-left:.5in; |
|---|
| 872 | margin-bottom:.0001pt; |
|---|
| 873 | mso-add-space:auto; |
|---|
| 874 | mso-pagination:widow-orphan; |
|---|
| 875 | font-size:12.0pt; |
|---|
| 876 | font-family:"Times New Roman",serif; |
|---|
| 877 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 878 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 879 | p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst |
|---|
| 880 | {mso-style-noshow:yes; |
|---|
| 881 | mso-style-priority:34; |
|---|
| 882 | mso-style-unhide:no; |
|---|
| 883 | mso-style-qformat:yes; |
|---|
| 884 | mso-style-type:export-only; |
|---|
| 885 | margin-top:0in; |
|---|
| 886 | margin-right:0in; |
|---|
| 887 | margin-bottom:0in; |
|---|
| 888 | margin-left:.5in; |
|---|
| 889 | margin-bottom:.0001pt; |
|---|
| 890 | mso-add-space:auto; |
|---|
| 891 | mso-pagination:widow-orphan; |
|---|
| 892 | font-size:12.0pt; |
|---|
| 893 | font-family:"Times New Roman",serif; |
|---|
| 894 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 895 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 896 | p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle |
|---|
| 897 | {mso-style-noshow:yes; |
|---|
| 898 | mso-style-priority:34; |
|---|
| 899 | mso-style-unhide:no; |
|---|
| 900 | mso-style-qformat:yes; |
|---|
| 901 | mso-style-type:export-only; |
|---|
| 902 | margin-top:0in; |
|---|
| 903 | margin-right:0in; |
|---|
| 904 | margin-bottom:0in; |
|---|
| 905 | margin-left:.5in; |
|---|
| 906 | margin-bottom:.0001pt; |
|---|
| 907 | mso-add-space:auto; |
|---|
| 908 | mso-pagination:widow-orphan; |
|---|
| 909 | font-size:12.0pt; |
|---|
| 910 | font-family:"Times New Roman",serif; |
|---|
| 911 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 912 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 913 | p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast |
|---|
| 914 | {mso-style-noshow:yes; |
|---|
| 915 | mso-style-priority:34; |
|---|
| 916 | mso-style-unhide:no; |
|---|
| 917 | mso-style-qformat:yes; |
|---|
| 918 | mso-style-type:export-only; |
|---|
| 919 | margin-top:0in; |
|---|
| 920 | margin-right:0in; |
|---|
| 921 | margin-bottom:0in; |
|---|
| 922 | margin-left:.5in; |
|---|
| 923 | margin-bottom:.0001pt; |
|---|
| 924 | mso-add-space:auto; |
|---|
| 925 | mso-pagination:widow-orphan; |
|---|
| 926 | font-size:12.0pt; |
|---|
| 927 | font-family:"Times New Roman",serif; |
|---|
| 928 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 929 | mso-fareast-theme-font:minor-fareast;} |
|---|
| 930 | span.MsoIntenseReference |
|---|
| 931 | {mso-style-priority:32; |
|---|
| 932 | mso-style-unhide:no; |
|---|
| 933 | mso-style-qformat:yes; |
|---|
| 934 | font-variant:small-caps; |
|---|
| 935 | color:#C0504D; |
|---|
| 936 | mso-themecolor:accent2; |
|---|
| 937 | letter-spacing:.25pt; |
|---|
| 938 | font-weight:bold; |
|---|
| 939 | text-decoration:underline; |
|---|
| 940 | text-underline:single;} |
|---|
| 941 | span.Heading1Char |
|---|
| 942 | {mso-style-name:"Heading 1 Char"; |
|---|
| 943 | mso-style-priority:9; |
|---|
| 944 | mso-style-unhide:no; |
|---|
| 945 | mso-style-locked:yes; |
|---|
| 946 | mso-style-link:"Heading 1"; |
|---|
| 947 | mso-ansi-font-size:24.0pt; |
|---|
| 948 | mso-bidi-font-size:24.0pt; |
|---|
| 949 | font-family:"Times New Roman",serif; |
|---|
| 950 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 951 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 952 | mso-fareast-theme-font:minor-fareast; |
|---|
| 953 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 954 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 955 | mso-font-kerning:18.0pt; |
|---|
| 956 | font-weight:bold;} |
|---|
| 957 | span.Heading2Char |
|---|
| 958 | {mso-style-name:"Heading 2 Char"; |
|---|
| 959 | mso-style-noshow:yes; |
|---|
| 960 | mso-style-priority:9; |
|---|
| 961 | mso-style-unhide:no; |
|---|
| 962 | mso-style-locked:yes; |
|---|
| 963 | mso-style-link:"Heading 2"; |
|---|
| 964 | mso-ansi-font-size:18.0pt; |
|---|
| 965 | mso-bidi-font-size:18.0pt; |
|---|
| 966 | font-family:"Times New Roman",serif; |
|---|
| 967 | mso-ascii-font-family:"Times New Roman"; |
|---|
| 968 | mso-fareast-font-family:"Times New Roman"; |
|---|
| 969 | mso-fareast-theme-font:minor-fareast; |
|---|
| 970 | mso-hansi-font-family:"Times New Roman"; |
|---|
| 971 | mso-bidi-font-family:"Times New Roman"; |
|---|
| 972 | font-weight:bold;} |
|---|
| 973 | span.Heading3Char |
|---|
| 974 | {mso-style-name:"Heading 3 Char"; |
|---|
| 975 | mso-style-noshow:yes; |
|---|
| 976 | mso-style-priority:9; |
|---|
| 977 | mso-style-unhide:no; |
|---|
| 978 | mso-style-locked:yes; |
|---|
| 979 | mso-style-link:"Heading 3"; |
|---|
| 980 | mso-ansi-font-size:13.5pt; |
|---|
| 981 | mso-bidi-font-size:13.5pt; |
|---|
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|---|
| 1221 | <h1><strong><span style='mso-bidi-font-weight:normal'>Small Angle X-Ray Data |
|---|
| 1222 | Size Distribution in Alumina Powder</span><o:p></o:p></strong></h1> |
|---|
| 1223 | |
|---|
| 1224 | <P><BL> |
|---|
| 1225 | <LI><B>A video version of this tutorial is available at |
|---|
| 1226 | <A href="https://anl.box.com/v/SmallAngleSizeDistribution" target="_blank"> |
|---|
| 1227 | https://anl.box.com/v/SmallAngleSizeDistribution</A></B> |
|---|
| 1228 | <LI>Exercise files are found <A href="./data/" target="_blank">here</a> |
|---|
| 1229 | </BL></P><P></P> |
|---|
| 1230 | |
|---|
| 1231 | |
|---|
| 1232 | <p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In |
|---|
| 1233 | this tutorial you will determine the size distribution of particles in an |
|---|
| 1234 | alumina polishing powder using data from a constant wavelength synchrotron X-ray |
|---|
| 1235 | USAXS instrument. You will use both Maximum Entropy (<span class=SpellE>MaxEnt</span>) |
|---|
| 1236 | and Total Non-Negative Least Squares (TNNLS) methods assuming spherical |
|---|
| 1237 | particles. The data were collected from <span style='mso-fareast-font-family: |
|---|
| 1238 | Calibri;mso-fareast-theme-font:minor-latin;mso-bidi-font-weight:bold; |
|---|
| 1239 | mso-bidi-font-style:italic'>powders spread onto sticky tape and covered with |
|---|
| 1240 | another layer of the same tape. The data were corrected for background from |
|---|
| 1241 | data collected from two layers of sticky tape. However, the sample thickness is |
|---|
| 1242 | not</span> accurately known <span style='mso-fareast-font-family:Calibri; |
|---|
| 1243 | mso-fareast-theme-font:minor-latin;mso-bidi-font-weight:bold;mso-bidi-font-style: |
|---|
| 1244 | italic'>so the data are not calibrated on an absolute scale.<o:p></o:p></span></p> |
|---|
| 1245 | |
|---|
| 1246 | <p class=MsoNormal>If you have not done so already, start GSAS-II.</p> |
|---|
| 1247 | |
|---|
| 1248 | <h2>Step 1: read in the data file</h2> |
|---|
| 1249 | |
|---|
| 1250 | <p class=MsoListParagraphCxSpFirst style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span |
|---|
| 1251 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span |
|---|
| 1252 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Use |
|---|
| 1253 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1254 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1255 | minor-latin'>Import/Small Angle Data/from q (A-1) step X-ray QIE data file</span></b> |
|---|
| 1256 | menu item to read the data file into GSAS-II. This read option is set to read |
|---|
| 1257 | three column small angle scattering data (SASD) as Q in Å<sup>-1</sup>, |
|---|
| 1258 | intensity and estimated standard deviation in intensity; there may be a header |
|---|
| 1259 | with metadata information in the front of this file.<span |
|---|
| 1260 | style='mso-spacerun:yes'> </span>Change the file directory to <span |
|---|
| 1261 | class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1262 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1263 | minor-latin;mso-bidi-theme-font:minor-latin'>SAsize</span></b></span><b |
|---|
| 1264 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1265 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1266 | minor-latin'>/data</span></b><span style='font-family:"Calibri",sans-serif; |
|---|
| 1267 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1268 | minor-latin'> to find the file</span>; you will have to select the <b |
|---|
| 1269 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1270 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>any file |
|---|
| 1271 | (*.*)</span></b> filter to see it.</p> |
|---|
| 1272 | |
|---|
| 1273 | <p class=MsoListParagraphCxSpLast style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span |
|---|
| 1274 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span |
|---|
| 1275 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Select |
|---|
| 1276 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1277 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1278 | minor-latin'>alumina data.dat</span></b><span style='font-family:"Calibri",sans-serif; |
|---|
| 1279 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1280 | minor-latin'> data</span> file in the first dialog and press <b |
|---|
| 1281 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1282 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1283 | minor-latin'>Open</span></b>. There will be a Dialog box asking <b |
|---|
| 1284 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1285 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
|---|
| 1286 | minor-latin'>Is this the file you want?</span></b> Press <b style='mso-bidi-font-weight: |
|---|
| 1287 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1288 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Yes</span></b> |
|---|
| 1289 | button to proceed.</p> |
|---|
| 1290 | |
|---|
| 1291 | <p class=MsoNormal>At this point the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1292 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1293 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data |
|---|
| 1294 | tree</span></b> window will have several entries and the plot window will show |
|---|
| 1295 | the SASD pattern as a log-log plot of intensity vs. Q</p> |
|---|
| 1296 | |
|---|
| 1297 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype |
|---|
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|---|
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|---|
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| 1306 | <v:f eqn="prod @3 21600 pixelWidth"/> |
|---|
| 1307 | <v:f eqn="prod @3 21600 pixelHeight"/> |
|---|
| 1308 | <v:f eqn="sum @0 0 1"/> |
|---|
| 1309 | <v:f eqn="prod @6 1 2"/> |
|---|
| 1310 | <v:f eqn="prod @7 21600 pixelWidth"/> |
|---|
| 1311 | <v:f eqn="sum @8 21600 0"/> |
|---|
| 1312 | <v:f eqn="prod @7 21600 pixelHeight"/> |
|---|
| 1313 | <v:f eqn="sum @10 21600 0"/> |
|---|
| 1314 | </v:formulas> |
|---|
| 1315 | <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> |
|---|
| 1316 | <o:lock v:ext="edit" aspectratio="t"/> |
|---|
| 1317 | </v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1038" type="#_x0000_t75" |
|---|
| 1318 | style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1319 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image001.png" |
|---|
| 1320 | o:title=""/> |
|---|
| 1321 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
|---|
| 1322 | src="Small%20Angle%20Size%20Distribution_files/image001.png" v:shapes="Picture_x0020_1"><![endif]></span></p> |
|---|
| 1323 | |
|---|
| 1324 | <h2>Step 2: Set Limits</h2> |
|---|
| 1325 | |
|---|
| 1326 | <p class=MsoNormal>For this step we will reposition the limits to enclose only |
|---|
| 1327 | that part of the SASD pattern suitable for size distribution analysis. |
|---|
| 1328 | Typically this covers 10<sup>-3</sup> < Q < 10<sup>-1</sup>; below this |
|---|
| 1329 | range scattering is from very large objects not readily described by the size |
|---|
| 1330 | distribution analysis and above the scattering is mostly background. Select <b |
|---|
| 1331 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1332 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Limits</span></b> |
|---|
| 1333 | under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1334 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina |
|---|
| 1335 | data.dat</span></b> from the GSAS-II tree. Then set <b style='mso-bidi-font-weight: |
|---|
| 1336 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1337 | minor-latin;mso-hansi-theme-font:minor-latin'>changed</span></b> to <b |
|---|
| 1338 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1339 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.001</span></b> |
|---|
| 1340 | for <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
|---|
| 1341 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1342 | mso-hansi-theme-font:minor-latin'>Tmin</span></b></span> and <b |
|---|
| 1343 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1344 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.1</span></b> |
|---|
| 1345 | for <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
|---|
| 1346 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1347 | mso-hansi-theme-font:minor-latin'>Tmax</span></b></span>. You can also set the |
|---|
| 1348 | limits using the cursor on the plot by either picking a point on the curve with |
|---|
| 1349 | the left or right mouse button or by dragging the green and red vertical lines |
|---|
| 1350 | to the desired positions. The limits window should look like</p> |
|---|
| 1351 | |
|---|
| 1352 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1353 | id="Picture_x0020_15" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:415.5pt; |
|---|
| 1354 | height:267pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1355 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image015.png" |
|---|
| 1356 | o:title=""/> |
|---|
| 1357 | </v:shape><![endif]--><![if !vml]><img width=554 height=356 |
|---|
| 1358 | src="Small%20Angle%20Size%20Distribution_files/image016.png" v:shapes="Picture_x0020_15"><![endif]></span><span |
|---|
| 1359 | style='mso-spacerun:yes'> </span></p> |
|---|
| 1360 | |
|---|
| 1361 | <h2>Step 3 Select the scattering substances for your sample</h2> |
|---|
| 1362 | |
|---|
| 1363 | <p class=MsoNormal><span style='mso-no-proof:yes'>Two scattering substances |
|---|
| 1364 | need to be defined for your sample to give the anticipated scattering contrast; |
|---|
| 1365 | in this case one is alumina and the other is vacuum (really air). Parameters |
|---|
| 1366 | for a number of substances are defined in the file </span><b style='mso-bidi-font-weight: |
|---|
| 1367 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1368 | minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span |
|---|
| 1369 | style='mso-no-proof:yes'>. You can add your own substances to this or better |
|---|
| 1370 | put them in </span><b style='mso-bidi-font-weight:normal'><span |
|---|
| 1371 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1372 | mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span |
|---|
| 1373 | style='mso-no-proof:yes'>; this is read after </span><b style='mso-bidi-font-weight: |
|---|
| 1374 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1375 | minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span |
|---|
| 1376 | style='mso-no-proof:yes'> when you load substances for your selection. </span>Select |
|---|
| 1377 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1378 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Substances</span></b> |
|---|
| 1379 | under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1380 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina |
|---|
| 1381 | data.dat</span></b> from the GSAS-II tree. Then do <span class=GramE><b |
|---|
| 1382 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1383 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit</span></b></span><b |
|---|
| 1384 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1385 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> |
|---|
| 1386 | substance/Load</span></b> <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1387 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1388 | mso-hansi-theme-font:minor-latin'>substance</span></b> from the menu; a popup |
|---|
| 1389 | window will appear with possible selections</p> |
|---|
| 1390 | |
|---|
| 1391 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1392 | id="_x0000_i1036" type="#_x0000_t75" style='width:259.5pt;height:252pt; |
|---|
| 1393 | visibility:visible;mso-wrap-style:square'> |
|---|
| 1394 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image003.png" |
|---|
| 1395 | o:title=""/> |
|---|
| 1396 | </v:shape><![endif]--><![if !vml]><img width=346 height=336 |
|---|
| 1397 | src="Small%20Angle%20Size%20Distribution_files/image003.png" v:shapes="_x0000_i1036"><![endif]><o:p></o:p></span></p> |
|---|
| 1398 | |
|---|
| 1399 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1400 | |
|---|
| 1401 | <p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1402 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1403 | mso-hansi-theme-font:minor-latin'>Alumina</span></b> and press <b |
|---|
| 1404 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1405 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>; |
|---|
| 1406 | the relevant data for alumina (and vacuum) are displayed next</p> |
|---|
| 1407 | |
|---|
| 1408 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1409 | id="Picture_x0020_17" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:431.25pt; |
|---|
| 1410 | height:275.25pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1411 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image017.png" |
|---|
| 1412 | o:title=""/> |
|---|
| 1413 | </v:shape><![endif]--><![if !vml]><img width=575 height=367 |
|---|
| 1414 | src="Small%20Angle%20Size%20Distribution_files/image017.png" v:shapes="Picture_x0020_17"><![endif]></span><span |
|---|
| 1415 | style='mso-spacerun:yes'> </span></p> |
|---|
| 1416 | |
|---|
| 1417 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1418 | |
|---|
| 1419 | <p class=MsoNormal>If desired you can load/add as many substances as you want |
|---|
| 1420 | into this list; you can also delete any of them (except vacuum & unit |
|---|
| 1421 | scatter). The composition, volume occupied by the atoms in the composition and |
|---|
| 1422 | the density are given for each substance. These can each be edited; the other |
|---|
| 1423 | values will change accordingly. If your substance isnt in the list, you can <b |
|---|
| 1424 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1425 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit |
|---|
| 1426 | Substance/Add |
|---|
| 1427 | substance</span></b> to create a new one (you will be asked for a name and the |
|---|
| 1428 | set of elements in two successive popup windows). From this information the |
|---|
| 1429 | scattering density and that as affected by resonant scattering for the listed |
|---|
| 1430 | wavelength is displayed (the wavelength can be changed in the <b |
|---|
| 1431 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1432 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Instrument |
|---|
| 1433 | Parameters</span></b> GSAS-II tree item if needed). The real density value is |
|---|
| 1434 | used for contrast calculations.</p> |
|---|
| 1435 | |
|---|
| 1436 | <h2>Step 4: Set Sample parameters </h2> |
|---|
| 1437 | |
|---|
| 1438 | <p class=MsoNormal>Two of the substances you have loaded into GSAS-II next need |
|---|
| 1439 | to be selected for this size distribution analysis; Select <b style='mso-bidi-font-weight: |
|---|
| 1440 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1441 | minor-latin;mso-hansi-theme-font:minor-latin'>Sample Parameters</span></b> |
|---|
| 1442 | under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1443 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina |
|---|
| 1444 | data.dat</span></b> from the GSAS-II tree. Near the bottom of the window will |
|---|
| 1445 | be two rows marked <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1446 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1447 | mso-hansi-theme-font:minor-latin'>Material</span></b>; select <b |
|---|
| 1448 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1449 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Alumina</span></b> |
|---|
| 1450 | from one of the pull downs (leave the other as <b style='mso-bidi-font-weight: |
|---|
| 1451 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1452 | minor-latin;mso-hansi-theme-font:minor-latin'>vacuum</span></b>). The window |
|---|
| 1453 | will show at the bottom the computed contrast between alumina and vacuum |
|---|
| 1454 | without and with consideration of resonant scattering effects; the latter is |
|---|
| 1455 | used in subsequent calculations.</p> |
|---|
| 1456 | |
|---|
| 1457 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1458 | id="Picture_x0020_18" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:459pt; |
|---|
| 1459 | height:447pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1460 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image018.png" |
|---|
| 1461 | o:title=""/> |
|---|
| 1462 | </v:shape><![endif]--><![if !vml]><img width=612 height=596 |
|---|
| 1463 | src="Small%20Angle%20Size%20Distribution_files/image018.png" v:shapes="Picture_x0020_18"><![endif]></span></p> |
|---|
| 1464 | |
|---|
| 1465 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1466 | |
|---|
| 1467 | <p class=MsoNormal>For experiments for which you know the transmission and the |
|---|
| 1468 | sample thickness, you can manipulate the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1469 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1470 | mso-hansi-theme-font:minor-latin'>volume fractions</span></b> to make the |
|---|
| 1471 | calculated transmission match the observed one. Additionally, if you have |
|---|
| 1472 | absolute scaling information, you can rescale the data by adjusting the <b |
|---|
| 1473 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1474 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>histogram |
|---|
| 1475 | scale factor</span></b>; multiple data sets can be scaled together via the <b |
|---|
| 1476 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1477 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Command/Set |
|---|
| 1478 | scale</span></b> menu item.</p> |
|---|
| 1479 | |
|---|
| 1480 | <h2>Step 5 Size distribution via Maximum Entropy</h2> |
|---|
| 1481 | |
|---|
| 1482 | <p class=MsoNormal>You are now ready to attempt a size distribution analysis |
|---|
| 1483 | using the maximum entropy method. Select <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1484 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1485 | mso-hansi-theme-font:minor-latin'>Models</span></b> under <b style='mso-bidi-font-weight: |
|---|
| 1486 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1487 | minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina data.dat</span></b> |
|---|
| 1488 | from the GSAS-II tree; the window will display</p> |
|---|
| 1489 | |
|---|
| 1490 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1491 | id="_x0000_i1033" type="#_x0000_t75" style='width:468pt;height:238.5pt; |
|---|
| 1492 | visibility:visible;mso-wrap-style:square'> |
|---|
| 1493 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image019.png" |
|---|
| 1494 | o:title=""/> |
|---|
| 1495 | </v:shape><![endif]--><![if !vml]><img width=624 height=318 |
|---|
| 1496 | src="Small%20Angle%20Size%20Distribution_files/image020.png" v:shapes="_x0000_i1033"><![endif]></span></p> |
|---|
| 1497 | |
|---|
| 1498 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1499 | |
|---|
| 1500 | <p class=MsoNormal>Many selections are made by default for this analysis; however |
|---|
| 1501 | it is important that an appropriate value is selected for the background. From |
|---|
| 1502 | the high Q end of the data plot</p> |
|---|
| 1503 | |
|---|
| 1504 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1505 | id="Picture_x0020_19" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt; |
|---|
| 1506 | height:450pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1507 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image007.png" |
|---|
| 1508 | o:title=""/> |
|---|
| 1509 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
|---|
| 1510 | src="Small%20Angle%20Size%20Distribution_files/image007.png" v:shapes="Picture_x0020_19"><![endif]></span><span |
|---|
| 1511 | style='mso-spacerun:yes'> </span></p> |
|---|
| 1512 | |
|---|
| 1513 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1514 | |
|---|
| 1515 | <p class=MsoNormal>It is clear that the intensity levels off at an apparent |
|---|
| 1516 | background level of ~<b style='mso-bidi-font-weight:normal'><span |
|---|
| 1517 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1518 | mso-hansi-theme-font:minor-latin'>0.12</span></b>; enter that into the |
|---|
| 1519 | appropriate place in the data window next to <B>Background</B>. The plot will be redrawn showing a |
|---|
| 1520 | horizontal red line for the background. All the other parameters seem |
|---|
| 1521 | reasonable for a 1<sup>st</sup> attempt at a <span class=SpellE>MaxEnt</span> |
|---|
| 1522 | solution. Do <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1523 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1524 | minor-latin'>Models/Fit</span></b>; the console window will show that the |
|---|
| 1525 | calculation did not converge and the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1526 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1527 | mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> plot has a |
|---|
| 1528 | choppy appearance.</p> |
|---|
| 1529 | |
|---|
| 1530 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1531 | id="Picture_x0020_20" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:468pt; |
|---|
| 1532 | height:401.25pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1533 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image021.png" |
|---|
| 1534 | o:title=""/> |
|---|
| 1535 | </v:shape><![endif]--><![if !vml]><img width=624 height=535 |
|---|
| 1536 | src="Small%20Angle%20Size%20Distribution_files/image022.png" v:shapes="Picture_x0020_20"><![endif]></span></p> |
|---|
| 1537 | |
|---|
| 1538 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1539 | |
|---|
| 1540 | <p class=MsoNormal>This is not a satisfactory result, but the suggestion given |
|---|
| 1541 | in the console window is worth trying. Change the <b style='mso-bidi-font-weight: |
|---|
| 1542 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1543 | minor-latin;mso-hansi-theme-font:minor-latin'>Error multiplier</span></b> to <b |
|---|
| 1544 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1545 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>5</span></b> |
|---|
| 1546 | (notice the increased error bars on the data plot) and repeat <b |
|---|
| 1547 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1548 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Model/Fit</span></b>. |
|---|
| 1549 | Convergence is now achieved in <10 cycles (see console window for details) |
|---|
| 1550 | and a much smoother size distribution results</p> |
|---|
| 1551 | |
|---|
| 1552 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1553 | id="Picture_x0020_21" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:468pt; |
|---|
| 1554 | height:401.25pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1555 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image023.png" |
|---|
| 1556 | o:title=""/> |
|---|
| 1557 | </v:shape><![endif]--><![if !vml]><img width=624 height=535 |
|---|
| 1558 | src="Small%20Angle%20Size%20Distribution_files/image024.png" v:shapes="Picture_x0020_21"><![endif]></span></p> |
|---|
| 1559 | |
|---|
| 1560 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1561 | |
|---|
| 1562 | <p class=MsoNormal>This is a good result: clearly the alumina polishing powder |
|---|
| 1563 | has a bimodal distribution with diameters centered about ~1600Å and ~160Å (not |
|---|
| 1564 | 500Å and 1µm as advertised by the manufacturer!).</p> |
|---|
| 1565 | |
|---|
| 1566 | <p class=MsoNormal>You may wish to explore the effect of some of the other |
|---|
| 1567 | parameters in the data window. Most are obvious but <b style='mso-bidi-font-weight: |
|---|
| 1568 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1569 | minor-latin;mso-hansi-theme-font:minor-latin'>Log floor factor</span></b> needs |
|---|
| 1570 | a bit of explanation. This is the log of the minimum size distribution (scaled |
|---|
| 1571 | by the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1572 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>histogram |
|---|
| 1573 | scale factor</span></b> and the <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1574 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1575 | mso-hansi-theme-font:minor-latin'>contrast</span></b>). This size distribution |
|---|
| 1576 | minimum needs to be set within 1-2 orders of magnitude of the optimal value and |
|---|
| 1577 | can differ from the default of 10<sup>-3; </sup>it is worth changing if |
|---|
| 1578 | convergence is poor despite trying different error multipliers. Try changing it |
|---|
| 1579 | to see what effect it has on the result. With the original settings the data |
|---|
| 1580 | fit looks like</p> |
|---|
| 1581 | |
|---|
| 1582 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1583 | id="Picture_x0020_22" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:426.75pt; |
|---|
| 1584 | height:366pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1585 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image025.png" |
|---|
| 1586 | o:title=""/> |
|---|
| 1587 | </v:shape><![endif]--><![if !vml]><img width=569 height=488 |
|---|
| 1588 | src="Small%20Angle%20Size%20Distribution_files/image026.png" v:shapes="Picture_x0020_22"><![endif]></span></p> |
|---|
| 1589 | |
|---|
| 1590 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1591 | |
|---|
| 1592 | <p class=MsoNormal>The green curve is the result calculated from the size |
|---|
| 1593 | distribution. Notice that it is not perfect, there is appreciable misfit around |
|---|
| 1594 | Q=0.003Å<sup>-1</sup>. This may be due to the assumption that the particles are |
|---|
| 1595 | spheres; they could be some other shape (I could get a better fit by setting |
|---|
| 1596 | the Spheroid aspect ratio to 2.0), however this tool is not really the |
|---|
| 1597 | appropriate one to make this determination.</p> |
|---|
| 1598 | |
|---|
| 1599 | <h2>Step 6 Size Distribution <i style='mso-bidi-font-style:normal'>via</i> |
|---|
| 1600 | Total Non-Negative Least Squares (TNNLS)</h2> |
|---|
| 1601 | |
|---|
| 1602 | <p class=MsoNormal>An alternative method for determining size distributions is |
|---|
| 1603 | the TNNLS or Interior-Point Gradient (IPG) method. As the name implies this is |
|---|
| 1604 | a gradient refinement method for the special case of all positive data and |
|---|
| 1605 | parameter values. To try it on this alumina data, select <b style='mso-bidi-font-weight: |
|---|
| 1606 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1607 | minor-latin;mso-hansi-theme-font:minor-latin'>IPG</span></b> from the <b |
|---|
| 1608 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1609 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Fitting |
|---|
| 1610 | method</span></b> pull down. The data window will change to give</p> |
|---|
| 1611 | |
|---|
| 1612 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1613 | id="Picture_x0020_23" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:468pt; |
|---|
| 1614 | height:238.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1615 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image027.png" |
|---|
| 1616 | o:title=""/> |
|---|
| 1617 | </v:shape><![endif]--><![if !vml]><img width=624 height=318 |
|---|
| 1618 | src="Small%20Angle%20Size%20Distribution_files/image028.png" v:shapes="Picture_x0020_23"><![endif]></span></p> |
|---|
| 1619 | |
|---|
| 1620 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1621 | |
|---|
| 1622 | <p class=MsoNormal>Reset the Error multiplier back to <b style='mso-bidi-font-weight: |
|---|
| 1623 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1624 | minor-latin;mso-hansi-theme-font:minor-latin'>1.0</span></b> and then do <b |
|---|
| 1625 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1626 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Fit</span></b> |
|---|
| 1627 | to run the IPG fitting. The IPG algorithm did not converge in 100 cycles and |
|---|
| 1628 | resulting size distribution is a little choppy but has roughly the same bimodal |
|---|
| 1629 | distribution found by <span class=SpellE>MaxEnt</span>.</p> |
|---|
| 1630 | |
|---|
| 1631 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1632 | id="Picture_x0020_24" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:468pt; |
|---|
| 1633 | height:401.25pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1634 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image029.png" |
|---|
| 1635 | o:title=""/> |
|---|
| 1636 | </v:shape><![endif]--><![if !vml]><img width=624 height=535 |
|---|
| 1637 | src="Small%20Angle%20Size%20Distribution_files/image030.png" v:shapes="Picture_x0020_24"><![endif]></span></p> |
|---|
| 1638 | |
|---|
| 1639 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1640 | |
|---|
| 1641 | <p class=MsoNormal>This can be considerably improved by setting the <b |
|---|
| 1642 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1643 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Error |
|---|
| 1644 | multiplier</span></b> to <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1645 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1646 | mso-hansi-theme-font:minor-latin'>2.0</span></b>; the IPG fit con<span |
|---|
| 1647 | style='mso-no-proof:yes'>verges in <20 cycles and gives a smoother size |
|---|
| 1648 | distribution.<o:p></o:p></span></p> |
|---|
| 1649 | |
|---|
| 1650 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1651 | id="Picture_x0020_25" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:468pt; |
|---|
| 1652 | height:401.25pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1653 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image031.png" |
|---|
| 1654 | o:title=""/> |
|---|
| 1655 | </v:shape><![endif]--><![if !vml]><img width=624 height=535 |
|---|
| 1656 | src="Small%20Angle%20Size%20Distribution_files/image032.png" v:shapes="Picture_x0020_25"><![endif]></span></p> |
|---|
| 1657 | |
|---|
| 1658 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1659 | |
|---|
| 1660 | <p class=MsoNormal>The bimodal distribution is again quite clear with ~1400Å |
|---|
| 1661 | and ~150Å diameter particles. This method appears to give a better fit to the |
|---|
| 1662 | data than the <span class=SpellE>MaxEnt</span> method particularly in the |
|---|
| 1663 | Q~0.003Å<sup>-1</sup> region</p> |
|---|
| 1664 | |
|---|
| 1665 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
|---|
| 1666 | id="Picture_x0020_26" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:450pt; |
|---|
| 1667 | height:385.5pt;visibility:visible;mso-wrap-style:square'> |
|---|
| 1668 | <v:imagedata src="Small%20Angle%20Size%20Distribution_files/image033.png" |
|---|
| 1669 | o:title=""/> |
|---|
| 1670 | </v:shape><![endif]--><![if !vml]><img width=600 height=514 |
|---|
| 1671 | src="Small%20Angle%20Size%20Distribution_files/image034.png" v:shapes="Picture_x0020_26"><![endif]></span></p> |
|---|
| 1672 | |
|---|
| 1673 | <p class=MsoNormal><o:p> </o:p></p> |
|---|
| 1674 | |
|---|
| 1675 | <p class=MsoNormal>You may wish to explore the other parameters for the IPG |
|---|
| 1676 | fitting. If <b style='mso-bidi-font-weight:normal'><span style='font-family: |
|---|
| 1677 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
|---|
| 1678 | minor-latin'>Q power weight</span></b> is set to <b style='mso-bidi-font-weight: |
|---|
| 1679 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
|---|
| 1680 | minor-latin;mso-hansi-theme-font:minor-latin'>0-4</span></b>, that changes the |
|---|
| 1681 | data weighting to <span class=SpellE>Q<sup>p</sup></span>. This can change the convergence |
|---|
| 1682 | of the IPG method and yield improved results if one is unsuccessful with the |
|---|
| 1683 | default settings. I got a nice fit with a <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1684 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1685 | mso-hansi-theme-font:minor-latin'>Q power weight</span></b> of <b |
|---|
| 1686 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1687 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>3</span></b> |
|---|
| 1688 | and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1689 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Error |
|---|
| 1690 | multiplier</span></b> of <b style='mso-bidi-font-weight:normal'><span |
|---|
| 1691 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
|---|
| 1692 | mso-hansi-theme-font:minor-latin'>2.0</span></b>.</p> |
|---|
| 1693 | |
|---|
| 1694 | <p class=MsoNormal>You should save this GSAS-II project as it will be used in the |
|---|
| 1695 | tutorial for fitting small angle scattering data; I used <span class=SpellE><b |
|---|
| 1696 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
|---|
| 1697 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>alumina.gpx</span></b></span>.</p> |
|---|
| 1698 | |
|---|
| 1699 | </div> |
|---|
| 1700 | |
|---|
| 1701 | </body> |
|---|
| 1702 | |
|---|
| 1703 | </html> |
|---|
