source: Tutorials/SAseqref/Sequential Refinement of Small Angle Scattering Data.htm @ 2794

Last change on this file since 2794 was 2794, checked in by vondreele, 6 years ago

update the SAseqref tutorial

  • Property svn:mime-type set to text/html
File size: 102.7 KB
Line 
1<html xmlns:v="urn:schemas-microsoft-com:vml"
2xmlns:o="urn:schemas-microsoft-com:office:office"
3xmlns:w="urn:schemas-microsoft-com:office:word"
4xmlns:m="http://schemas.microsoft.com/office/2004/12/omml"
5xmlns="http://www.w3.org/TR/REC-html40">
6
7<head>
8<meta http-equiv=Content-Type content="text/html; charset=windows-1252">
9<meta name=ProgId content=Word.Document>
10<meta name=Generator content="Microsoft Word 15">
11<meta name=Originator content="Microsoft Word 15">
12<link rel=File-List
13href="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/filelist.xml">
14<link rel=Edit-Time-Data
15href="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/editdata.mso">
16<!--[if !mso]>
17<style>
18v\:* {behavior:url(#default#VML);}
19o\:* {behavior:url(#default#VML);}
20w\:* {behavior:url(#default#VML);}
21.shape {behavior:url(#default#VML);}
22</style>
23<![endif]--><!--[if gte mso 9]><xml>
24 <o:DocumentProperties>
25  <o:Author>Von Dreele</o:Author>
26  <o:LastAuthor>vondreele</o:LastAuthor>
27  <o:Revision>20</o:Revision>
28  <o:TotalTime>2626</o:TotalTime>
29  <o:Created>2014-05-03T14:24:00Z</o:Created>
30  <o:LastSaved>2017-04-19T17:19:00Z</o:LastSaved>
31  <o:Pages>26</o:Pages>
32  <o:Words>1538</o:Words>
33  <o:Characters>8773</o:Characters>
34  <o:Company>Argonne National Laboratory</o:Company>
35  <o:Lines>73</o:Lines>
36  <o:Paragraphs>20</o:Paragraphs>
37  <o:CharactersWithSpaces>10291</o:CharactersWithSpaces>
38  <o:Version>16.00</o:Version>
39 </o:DocumentProperties>
40 <o:OfficeDocumentSettings>
41  <o:AllowPNG/>
42 </o:OfficeDocumentSettings>
43</xml><![endif]-->
44<link rel=themeData
45href="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/themedata.thmx">
46<link rel=colorSchemeMapping
47href="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/colorschememapping.xml">
48<!--[if gte mso 9]><xml>
49 <w:WordDocument>
50  <w:View>Print</w:View>
51  <w:SpellingState>Clean</w:SpellingState>
52  <w:GrammarState>Clean</w:GrammarState>
53  <w:TrackMoves>false</w:TrackMoves>
54  <w:TrackFormatting/>
55  <w:PunctuationKerning/>
56  <w:ValidateAgainstSchemas/>
57  <w:SaveIfXMLInvalid>false</w:SaveIfXMLInvalid>
58  <w:IgnoreMixedContent>false</w:IgnoreMixedContent>
59  <w:AlwaysShowPlaceholderText>false</w:AlwaysShowPlaceholderText>
60  <w:DoNotPromoteQF/>
61  <w:LidThemeOther>EN-US</w:LidThemeOther>
62  <w:LidThemeAsian>X-NONE</w:LidThemeAsian>
63  <w:LidThemeComplexScript>X-NONE</w:LidThemeComplexScript>
64  <w:Compatibility>
65   <w:BreakWrappedTables/>
66   <w:SnapToGridInCell/>
67   <w:WrapTextWithPunct/>
68   <w:UseAsianBreakRules/>
69   <w:DontGrowAutofit/>
70   <w:SplitPgBreakAndParaMark/>
71   <w:EnableOpenTypeKerning/>
72   <w:DontFlipMirrorIndents/>
73   <w:OverrideTableStyleHps/>
74  </w:Compatibility>
75  <w:BrowserLevel>MicrosoftInternetExplorer4</w:BrowserLevel>
76  <m:mathPr>
77   <m:mathFont m:val="Cambria Math"/>
78   <m:brkBin m:val="before"/>
79   <m:brkBinSub m:val="&#45;-"/>
80   <m:smallFrac m:val="off"/>
81   <m:dispDef/>
82   <m:lMargin m:val="0"/>
83   <m:rMargin m:val="0"/>
84   <m:defJc m:val="centerGroup"/>
85   <m:wrapIndent m:val="1440"/>
86   <m:intLim m:val="subSup"/>
87   <m:naryLim m:val="undOvr"/>
88  </m:mathPr></w:WordDocument>
89</xml><![endif]--><!--[if gte mso 9]><xml>
90 <w:LatentStyles DefLockedState="false" DefUnhideWhenUsed="false"
91  DefSemiHidden="false" DefQFormat="false" DefPriority="99"
92  LatentStyleCount="371">
93  <w:LsdException Locked="false" Priority="0" QFormat="true" Name="Normal"/>
94  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 1"/>
95  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
96   UnhideWhenUsed="true" QFormat="true" Name="heading 2"/>
97  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
98   UnhideWhenUsed="true" QFormat="true" Name="heading 3"/>
99  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
100   UnhideWhenUsed="true" QFormat="true" Name="heading 4"/>
101  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
102   UnhideWhenUsed="true" QFormat="true" Name="heading 5"/>
103  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
104   UnhideWhenUsed="true" QFormat="true" Name="heading 6"/>
105  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
106   UnhideWhenUsed="true" QFormat="true" Name="heading 7"/>
107  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
108   UnhideWhenUsed="true" QFormat="true" Name="heading 8"/>
109  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
110   UnhideWhenUsed="true" QFormat="true" Name="heading 9"/>
111  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
112   Name="index 1"/>
113  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
114   Name="index 2"/>
115  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
116   Name="index 3"/>
117  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
118   Name="index 4"/>
119  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
120   Name="index 5"/>
121  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
122   Name="index 6"/>
123  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
124   Name="index 7"/>
125  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
126   Name="index 8"/>
127  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
128   Name="index 9"/>
129  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
130   UnhideWhenUsed="true" Name="toc 1"/>
131  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
132   UnhideWhenUsed="true" Name="toc 2"/>
133  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
134   UnhideWhenUsed="true" Name="toc 3"/>
135  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
136   UnhideWhenUsed="true" Name="toc 4"/>
137  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
138   UnhideWhenUsed="true" Name="toc 5"/>
139  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
140   UnhideWhenUsed="true" Name="toc 6"/>
141  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
142   UnhideWhenUsed="true" Name="toc 7"/>
143  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
144   UnhideWhenUsed="true" Name="toc 8"/>
145  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
146   UnhideWhenUsed="true" Name="toc 9"/>
147  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
148   Name="Normal Indent"/>
149  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
150   Name="footnote text"/>
151  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
152   Name="annotation text"/>
153  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
154   Name="header"/>
155  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
156   Name="footer"/>
157  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
158   Name="index heading"/>
159  <w:LsdException Locked="false" Priority="35" SemiHidden="true"
160   UnhideWhenUsed="true" QFormat="true" Name="caption"/>
161  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
162   Name="table of figures"/>
163  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
164   Name="envelope address"/>
165  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
166   Name="envelope return"/>
167  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
168   Name="footnote reference"/>
169  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
170   Name="annotation reference"/>
171  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
172   Name="line number"/>
173  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
174   Name="page number"/>
175  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
176   Name="endnote reference"/>
177  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
178   Name="endnote text"/>
179  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
180   Name="table of authorities"/>
181  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
182   Name="macro"/>
183  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
184   Name="toa heading"/>
185  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
186   Name="List"/>
187  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
188   Name="List Bullet"/>
189  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
190   Name="List Number"/>
191  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
192   Name="List 2"/>
193  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
194   Name="List 3"/>
195  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
196   Name="List 4"/>
197  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
198   Name="List 5"/>
199  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
200   Name="List Bullet 2"/>
201  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
202   Name="List Bullet 3"/>
203  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
204   Name="List Bullet 4"/>
205  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
206   Name="List Bullet 5"/>
207  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
208   Name="List Number 2"/>
209  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
210   Name="List Number 3"/>
211  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
212   Name="List Number 4"/>
213  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
214   Name="List Number 5"/>
215  <w:LsdException Locked="false" Priority="10" QFormat="true" Name="Title"/>
216  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
217   Name="Closing"/>
218  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
219   Name="Signature"/>
220  <w:LsdException Locked="false" Priority="1" SemiHidden="true"
221   UnhideWhenUsed="true" Name="Default Paragraph Font"/>
222  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
223   Name="Body Text"/>
224  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
225   Name="Body Text Indent"/>
226  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
227   Name="List Continue"/>
228  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
229   Name="List Continue 2"/>
230  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
231   Name="List Continue 3"/>
232  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
233   Name="List Continue 4"/>
234  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
235   Name="List Continue 5"/>
236  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
237   Name="Message Header"/>
238  <w:LsdException Locked="false" Priority="11" QFormat="true" Name="Subtitle"/>
239  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
240   Name="Salutation"/>
241  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
242   Name="Date"/>
243  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
244   Name="Body Text First Indent"/>
245  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
246   Name="Body Text First Indent 2"/>
247  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
248   Name="Note Heading"/>
249  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
250   Name="Body Text 2"/>
251  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
252   Name="Body Text 3"/>
253  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
254   Name="Body Text Indent 2"/>
255  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
256   Name="Body Text Indent 3"/>
257  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
258   Name="Block Text"/>
259  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
260   Name="Hyperlink"/>
261  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
262   Name="FollowedHyperlink"/>
263  <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/>
264  <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/>
265  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
266   Name="Document Map"/>
267  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
268   Name="Plain Text"/>
269  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
270   Name="E-mail Signature"/>
271  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
272   Name="HTML Top of Form"/>
273  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
274   Name="HTML Bottom of Form"/>
275  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
276   Name="Normal (Web)"/>
277  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
278   Name="HTML Acronym"/>
279  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
280   Name="HTML Address"/>
281  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
282   Name="HTML Cite"/>
283  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
284   Name="HTML Code"/>
285  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
286   Name="HTML Definition"/>
287  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
288   Name="HTML Keyboard"/>
289  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
290   Name="HTML Preformatted"/>
291  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
292   Name="HTML Sample"/>
293  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
294   Name="HTML Typewriter"/>
295  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
296   Name="HTML Variable"/>
297  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
298   Name="Normal Table"/>
299  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
300   Name="annotation subject"/>
301  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
302   Name="No List"/>
303  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
304   Name="Outline List 1"/>
305  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
306   Name="Outline List 2"/>
307  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
308   Name="Outline List 3"/>
309  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
310   Name="Table Simple 1"/>
311  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
312   Name="Table Simple 2"/>
313  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
314   Name="Table Simple 3"/>
315  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
316   Name="Table Classic 1"/>
317  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
318   Name="Table Classic 2"/>
319  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
320   Name="Table Classic 3"/>
321  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
322   Name="Table Classic 4"/>
323  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
324   Name="Table Colorful 1"/>
325  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
326   Name="Table Colorful 2"/>
327  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
328   Name="Table Colorful 3"/>
329  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
330   Name="Table Columns 1"/>
331  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
332   Name="Table Columns 2"/>
333  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
334   Name="Table Columns 3"/>
335  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
336   Name="Table Columns 4"/>
337  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
338   Name="Table Columns 5"/>
339  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
340   Name="Table Grid 1"/>
341  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
342   Name="Table Grid 2"/>
343  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
344   Name="Table Grid 3"/>
345  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
346   Name="Table Grid 4"/>
347  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
348   Name="Table Grid 5"/>
349  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
350   Name="Table Grid 6"/>
351  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
352   Name="Table Grid 7"/>
353  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
354   Name="Table Grid 8"/>
355  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
356   Name="Table List 1"/>
357  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
358   Name="Table List 2"/>
359  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
360   Name="Table List 3"/>
361  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
362   Name="Table List 4"/>
363  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
364   Name="Table List 5"/>
365  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
366   Name="Table List 6"/>
367  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
368   Name="Table List 7"/>
369  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
370   Name="Table List 8"/>
371  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
372   Name="Table 3D effects 1"/>
373  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
374   Name="Table 3D effects 2"/>
375  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
376   Name="Table 3D effects 3"/>
377  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
378   Name="Table Contemporary"/>
379  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
380   Name="Table Elegant"/>
381  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
382   Name="Table Professional"/>
383  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
384   Name="Table Subtle 1"/>
385  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
386   Name="Table Subtle 2"/>
387  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
388   Name="Table Web 1"/>
389  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
390   Name="Table Web 2"/>
391  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
392   Name="Table Web 3"/>
393  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
394   Name="Balloon Text"/>
395  <w:LsdException Locked="false" Priority="59" Name="Table Grid"/>
396  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
397   Name="Table Theme"/>
398  <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/>
399  <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/>
400  <w:LsdException Locked="false" Priority="60" Name="Light Shading"/>
401  <w:LsdException Locked="false" Priority="61" Name="Light List"/>
402  <w:LsdException Locked="false" Priority="62" Name="Light Grid"/>
403  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/>
404  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/>
405  <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/>
406  <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/>
407  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/>
408  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/>
409  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/>
410  <w:LsdException Locked="false" Priority="70" Name="Dark List"/>
411  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/>
412  <w:LsdException Locked="false" Priority="72" Name="Colorful List"/>
413  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
414  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
415  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
416  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
417  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
418  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
419  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
420  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
421  <w:LsdException Locked="false" Priority="34" QFormat="true"
422   Name="List Paragraph"/>
423  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
424  <w:LsdException Locked="false" Priority="30" QFormat="true"
425   Name="Intense Quote"/>
426  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
427  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
428  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
429  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
430  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
431  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
432  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
433  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
434  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
435  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
436  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
437  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
438  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
439  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
440  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
441  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
442  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
443  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
444  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
445  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
446  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
447  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
448  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
449  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
450  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
451  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
452  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
453  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
454  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
455  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
456  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
457  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
458  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
459  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
460  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
461  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
462  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
463  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
464  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
465  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
466  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
467  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
468  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
469  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
470  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
471  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
472  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
473  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
474  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
475  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
476  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
477  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
478  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
479  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
480  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
481  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
482  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
483  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
484  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
485  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
486  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
487  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
488  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
489  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
490  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
491  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
492  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
493  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
494  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
495  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
496  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
497  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
498  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
499  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
500  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
501  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
502  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
503  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
504  <w:LsdException Locked="false" Priority="19" QFormat="true"
505   Name="Subtle Emphasis"/>
506  <w:LsdException Locked="false" Priority="21" QFormat="true"
507   Name="Intense Emphasis"/>
508  <w:LsdException Locked="false" Priority="31" QFormat="true"
509   Name="Subtle Reference"/>
510  <w:LsdException Locked="false" Priority="32" QFormat="true"
511   Name="Intense Reference"/>
512  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
513  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
514   UnhideWhenUsed="true" Name="Bibliography"/>
515  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
516   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
517  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
518  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
519  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
520  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
521  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
522  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
523  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
524  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
525  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
526  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
527  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
528  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
529  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
530  <w:LsdException Locked="false" Priority="46"
531   Name="Grid Table 1 Light Accent 1"/>
532  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
533  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
534  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
535  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
536  <w:LsdException Locked="false" Priority="51"
537   Name="Grid Table 6 Colorful Accent 1"/>
538  <w:LsdException Locked="false" Priority="52"
539   Name="Grid Table 7 Colorful Accent 1"/>
540  <w:LsdException Locked="false" Priority="46"
541   Name="Grid Table 1 Light Accent 2"/>
542  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
543  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
544  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
545  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
546  <w:LsdException Locked="false" Priority="51"
547   Name="Grid Table 6 Colorful Accent 2"/>
548  <w:LsdException Locked="false" Priority="52"
549   Name="Grid Table 7 Colorful Accent 2"/>
550  <w:LsdException Locked="false" Priority="46"
551   Name="Grid Table 1 Light Accent 3"/>
552  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
553  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
554  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
555  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
556  <w:LsdException Locked="false" Priority="51"
557   Name="Grid Table 6 Colorful Accent 3"/>
558  <w:LsdException Locked="false" Priority="52"
559   Name="Grid Table 7 Colorful Accent 3"/>
560  <w:LsdException Locked="false" Priority="46"
561   Name="Grid Table 1 Light Accent 4"/>
562  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
563  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
564  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
565  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
566  <w:LsdException Locked="false" Priority="51"
567   Name="Grid Table 6 Colorful Accent 4"/>
568  <w:LsdException Locked="false" Priority="52"
569   Name="Grid Table 7 Colorful Accent 4"/>
570  <w:LsdException Locked="false" Priority="46"
571   Name="Grid Table 1 Light Accent 5"/>
572  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
573  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
574  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
575  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
576  <w:LsdException Locked="false" Priority="51"
577   Name="Grid Table 6 Colorful Accent 5"/>
578  <w:LsdException Locked="false" Priority="52"
579   Name="Grid Table 7 Colorful Accent 5"/>
580  <w:LsdException Locked="false" Priority="46"
581   Name="Grid Table 1 Light Accent 6"/>
582  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
583  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
584  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
585  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
586  <w:LsdException Locked="false" Priority="51"
587   Name="Grid Table 6 Colorful Accent 6"/>
588  <w:LsdException Locked="false" Priority="52"
589   Name="Grid Table 7 Colorful Accent 6"/>
590  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
591  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
592  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
593  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
594  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
595  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
596  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
597  <w:LsdException Locked="false" Priority="46"
598   Name="List Table 1 Light Accent 1"/>
599  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
600  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
601  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
602  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
603  <w:LsdException Locked="false" Priority="51"
604   Name="List Table 6 Colorful Accent 1"/>
605  <w:LsdException Locked="false" Priority="52"
606   Name="List Table 7 Colorful Accent 1"/>
607  <w:LsdException Locked="false" Priority="46"
608   Name="List Table 1 Light Accent 2"/>
609  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
610  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
611  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
612  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
613  <w:LsdException Locked="false" Priority="51"
614   Name="List Table 6 Colorful Accent 2"/>
615  <w:LsdException Locked="false" Priority="52"
616   Name="List Table 7 Colorful Accent 2"/>
617  <w:LsdException Locked="false" Priority="46"
618   Name="List Table 1 Light Accent 3"/>
619  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
620  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
621  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
622  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
623  <w:LsdException Locked="false" Priority="51"
624   Name="List Table 6 Colorful Accent 3"/>
625  <w:LsdException Locked="false" Priority="52"
626   Name="List Table 7 Colorful Accent 3"/>
627  <w:LsdException Locked="false" Priority="46"
628   Name="List Table 1 Light Accent 4"/>
629  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
630  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
631  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
632  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
633  <w:LsdException Locked="false" Priority="51"
634   Name="List Table 6 Colorful Accent 4"/>
635  <w:LsdException Locked="false" Priority="52"
636   Name="List Table 7 Colorful Accent 4"/>
637  <w:LsdException Locked="false" Priority="46"
638   Name="List Table 1 Light Accent 5"/>
639  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
640  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
641  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
642  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
643  <w:LsdException Locked="false" Priority="51"
644   Name="List Table 6 Colorful Accent 5"/>
645  <w:LsdException Locked="false" Priority="52"
646   Name="List Table 7 Colorful Accent 5"/>
647  <w:LsdException Locked="false" Priority="46"
648   Name="List Table 1 Light Accent 6"/>
649  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
650  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
651  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
652  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
653  <w:LsdException Locked="false" Priority="51"
654   Name="List Table 6 Colorful Accent 6"/>
655  <w:LsdException Locked="false" Priority="52"
656   Name="List Table 7 Colorful Accent 6"/>
657 </w:LatentStyles>
658</xml><![endif]-->
659<style>
660<!--
661 /* Font Definitions */
662 @font-face
663        {font-family:"Cambria Math";
664        panose-1:2 4 5 3 5 4 6 3 2 4;
665        mso-font-charset:1;
666        mso-generic-font-family:roman;
667        mso-font-pitch:variable;
668        mso-font-signature:0 0 0 0 0 0;}
669@font-face
670        {font-family:Calibri;
671        panose-1:2 15 5 2 2 2 4 3 2 4;
672        mso-font-charset:0;
673        mso-generic-font-family:swiss;
674        mso-font-pitch:variable;
675        mso-font-signature:-536859905 -1073732485 9 0 511 0;}
676@font-face
677        {font-family:Tahoma;
678        panose-1:2 11 6 4 3 5 4 4 2 4;
679        mso-font-charset:0;
680        mso-generic-font-family:swiss;
681        mso-font-pitch:variable;
682        mso-font-signature:-520081665 -1073717157 41 0 66047 0;}
683 /* Style Definitions */
684 p.MsoNormal, li.MsoNormal, div.MsoNormal
685        {mso-style-unhide:no;
686        mso-style-qformat:yes;
687        mso-style-parent:"";
688        margin:0in;
689        margin-bottom:.0001pt;
690        mso-pagination:widow-orphan;
691        font-size:12.0pt;
692        font-family:"Times New Roman",serif;
693        mso-fareast-font-family:"Times New Roman";
694        mso-fareast-theme-font:minor-fareast;}
695h1
696        {mso-style-priority:9;
697        mso-style-unhide:no;
698        mso-style-qformat:yes;
699        mso-style-link:"Heading 1 Char";
700        mso-margin-top-alt:auto;
701        margin-right:0in;
702        mso-margin-bottom-alt:auto;
703        margin-left:0in;
704        mso-pagination:widow-orphan;
705        mso-outline-level:1;
706        font-size:24.0pt;
707        font-family:"Times New Roman",serif;
708        mso-fareast-font-family:"Times New Roman";
709        mso-fareast-theme-font:minor-fareast;
710        font-weight:bold;}
711h2
712        {mso-style-noshow:yes;
713        mso-style-priority:9;
714        mso-style-qformat:yes;
715        mso-style-link:"Heading 2 Char";
716        mso-margin-top-alt:auto;
717        margin-right:0in;
718        mso-margin-bottom-alt:auto;
719        margin-left:0in;
720        mso-pagination:widow-orphan;
721        mso-outline-level:2;
722        font-size:18.0pt;
723        font-family:"Times New Roman",serif;
724        mso-fareast-font-family:"Times New Roman";
725        mso-fareast-theme-font:minor-fareast;
726        font-weight:bold;}
727h3
728        {mso-style-noshow:yes;
729        mso-style-priority:9;
730        mso-style-qformat:yes;
731        mso-style-link:"Heading 3 Char";
732        mso-margin-top-alt:auto;
733        margin-right:0in;
734        mso-margin-bottom-alt:auto;
735        margin-left:0in;
736        mso-pagination:widow-orphan;
737        mso-outline-level:3;
738        font-size:13.5pt;
739        font-family:"Times New Roman",serif;
740        mso-fareast-font-family:"Times New Roman";
741        mso-fareast-theme-font:minor-fareast;
742        font-weight:bold;}
743h4
744        {mso-style-noshow:yes;
745        mso-style-priority:9;
746        mso-style-qformat:yes;
747        mso-style-link:"Heading 4 Char";
748        mso-style-next:Normal;
749        margin-top:10.0pt;
750        margin-right:0in;
751        margin-bottom:0in;
752        margin-left:0in;
753        margin-bottom:.0001pt;
754        mso-pagination:widow-orphan lines-together;
755        page-break-after:avoid;
756        mso-outline-level:4;
757        font-size:13.0pt;
758        font-family:"Cambria",serif;
759        mso-ascii-font-family:Cambria;
760        mso-ascii-theme-font:major-latin;
761        mso-fareast-font-family:"Times New Roman";
762        mso-fareast-theme-font:major-fareast;
763        mso-hansi-font-family:Cambria;
764        mso-hansi-theme-font:major-latin;
765        mso-bidi-font-family:"Times New Roman";
766        mso-bidi-theme-font:major-bidi;
767        color:#4F81BD;
768        mso-themecolor:accent1;
769        font-weight:bold;
770        font-style:italic;}
771h5
772        {mso-style-noshow:yes;
773        mso-style-priority:9;
774        mso-style-qformat:yes;
775        mso-style-link:"Heading 5 Char";
776        mso-margin-top-alt:auto;
777        margin-right:0in;
778        mso-margin-bottom-alt:auto;
779        margin-left:0in;
780        mso-pagination:widow-orphan;
781        mso-outline-level:5;
782        font-size:12.0pt;
783        font-family:"Times New Roman",serif;
784        mso-fareast-font-family:"Times New Roman";
785        mso-fareast-theme-font:minor-fareast;
786        color:#4F4FFF;
787        font-weight:bold;}
788a:link, span.MsoHyperlink
789        {mso-style-noshow:yes;
790        mso-style-priority:99;
791        color:blue;
792        text-decoration:underline;
793        text-underline:single;}
794a:visited, span.MsoHyperlinkFollowed
795        {mso-style-noshow:yes;
796        mso-style-priority:99;
797        color:purple;
798        text-decoration:underline;
799        text-underline:single;}
800p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap
801        {mso-style-noshow:yes;
802        mso-style-priority:99;
803        mso-style-link:"Document Map Char";
804        margin:0in;
805        margin-bottom:.0001pt;
806        mso-pagination:widow-orphan;
807        font-size:8.0pt;
808        font-family:"Tahoma",sans-serif;
809        mso-fareast-font-family:"Times New Roman";
810        mso-fareast-theme-font:minor-fareast;}
811p
812        {mso-style-noshow:yes;
813        mso-style-priority:99;
814        mso-margin-top-alt:auto;
815        margin-right:0in;
816        mso-margin-bottom-alt:auto;
817        margin-left:0in;
818        mso-pagination:widow-orphan;
819        font-size:12.0pt;
820        font-family:"Times New Roman",serif;
821        mso-fareast-font-family:"Times New Roman";
822        mso-fareast-theme-font:minor-fareast;}
823pre
824        {mso-style-noshow:yes;
825        mso-style-priority:99;
826        mso-style-link:"HTML Preformatted Char";
827        margin:0in;
828        margin-bottom:.0001pt;
829        mso-pagination:widow-orphan;
830        tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt;
831        font-size:10.0pt;
832        font-family:"Courier New";
833        mso-fareast-font-family:"Times New Roman";}
834p.MsoAcetate, li.MsoAcetate, div.MsoAcetate
835        {mso-style-noshow:yes;
836        mso-style-priority:99;
837        mso-style-link:"Balloon Text Char";
838        margin:0in;
839        margin-bottom:.0001pt;
840        mso-pagination:widow-orphan;
841        font-size:8.0pt;
842        font-family:"Tahoma",sans-serif;
843        mso-fareast-font-family:"Times New Roman";
844        mso-fareast-theme-font:minor-fareast;}
845span.MsoPlaceholderText
846        {mso-style-noshow:yes;
847        mso-style-priority:99;
848        mso-style-unhide:no;
849        color:gray;}
850p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing
851        {mso-style-noshow:yes;
852        mso-style-priority:1;
853        mso-style-unhide:no;
854        mso-style-qformat:yes;
855        mso-style-parent:"";
856        margin:0in;
857        margin-bottom:.0001pt;
858        mso-pagination:widow-orphan;
859        font-size:12.0pt;
860        font-family:"Times New Roman",serif;
861        mso-fareast-font-family:"Times New Roman";
862        mso-fareast-theme-font:minor-fareast;}
863p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph
864        {mso-style-noshow:yes;
865        mso-style-priority:34;
866        mso-style-unhide:no;
867        mso-style-qformat:yes;
868        margin-top:0in;
869        margin-right:0in;
870        margin-bottom:0in;
871        margin-left:.5in;
872        margin-bottom:.0001pt;
873        mso-add-space:auto;
874        mso-pagination:widow-orphan;
875        font-size:12.0pt;
876        font-family:"Times New Roman",serif;
877        mso-fareast-font-family:"Times New Roman";
878        mso-fareast-theme-font:minor-fareast;}
879p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst
880        {mso-style-noshow:yes;
881        mso-style-priority:34;
882        mso-style-unhide:no;
883        mso-style-qformat:yes;
884        mso-style-type:export-only;
885        margin-top:0in;
886        margin-right:0in;
887        margin-bottom:0in;
888        margin-left:.5in;
889        margin-bottom:.0001pt;
890        mso-add-space:auto;
891        mso-pagination:widow-orphan;
892        font-size:12.0pt;
893        font-family:"Times New Roman",serif;
894        mso-fareast-font-family:"Times New Roman";
895        mso-fareast-theme-font:minor-fareast;}
896p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle
897        {mso-style-noshow:yes;
898        mso-style-priority:34;
899        mso-style-unhide:no;
900        mso-style-qformat:yes;
901        mso-style-type:export-only;
902        margin-top:0in;
903        margin-right:0in;
904        margin-bottom:0in;
905        margin-left:.5in;
906        margin-bottom:.0001pt;
907        mso-add-space:auto;
908        mso-pagination:widow-orphan;
909        font-size:12.0pt;
910        font-family:"Times New Roman",serif;
911        mso-fareast-font-family:"Times New Roman";
912        mso-fareast-theme-font:minor-fareast;}
913p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast
914        {mso-style-noshow:yes;
915        mso-style-priority:34;
916        mso-style-unhide:no;
917        mso-style-qformat:yes;
918        mso-style-type:export-only;
919        margin-top:0in;
920        margin-right:0in;
921        margin-bottom:0in;
922        margin-left:.5in;
923        margin-bottom:.0001pt;
924        mso-add-space:auto;
925        mso-pagination:widow-orphan;
926        font-size:12.0pt;
927        font-family:"Times New Roman",serif;
928        mso-fareast-font-family:"Times New Roman";
929        mso-fareast-theme-font:minor-fareast;}
930span.MsoIntenseReference
931        {mso-style-priority:32;
932        mso-style-unhide:no;
933        mso-style-qformat:yes;
934        font-variant:small-caps;
935        color:#C0504D;
936        mso-themecolor:accent2;
937        letter-spacing:.25pt;
938        font-weight:bold;
939        text-decoration:underline;
940        text-underline:single;}
941span.Heading1Char
942        {mso-style-name:"Heading 1 Char";
943        mso-style-priority:9;
944        mso-style-unhide:no;
945        mso-style-locked:yes;
946        mso-style-link:"Heading 1";
947        mso-ansi-font-size:24.0pt;
948        mso-bidi-font-size:24.0pt;
949        font-family:"Times New Roman",serif;
950        mso-ascii-font-family:"Times New Roman";
951        mso-fareast-font-family:"Times New Roman";
952        mso-fareast-theme-font:minor-fareast;
953        mso-hansi-font-family:"Times New Roman";
954        mso-bidi-font-family:"Times New Roman";
955        mso-font-kerning:18.0pt;
956        font-weight:bold;}
957span.Heading2Char
958        {mso-style-name:"Heading 2 Char";
959        mso-style-noshow:yes;
960        mso-style-priority:9;
961        mso-style-unhide:no;
962        mso-style-locked:yes;
963        mso-style-link:"Heading 2";
964        mso-ansi-font-size:18.0pt;
965        mso-bidi-font-size:18.0pt;
966        font-family:"Times New Roman",serif;
967        mso-ascii-font-family:"Times New Roman";
968        mso-fareast-font-family:"Times New Roman";
969        mso-fareast-theme-font:minor-fareast;
970        mso-hansi-font-family:"Times New Roman";
971        mso-bidi-font-family:"Times New Roman";
972        font-weight:bold;}
973span.Heading3Char
974        {mso-style-name:"Heading 3 Char";
975        mso-style-noshow:yes;
976        mso-style-priority:9;
977        mso-style-unhide:no;
978        mso-style-locked:yes;
979        mso-style-link:"Heading 3";
980        mso-ansi-font-size:13.5pt;
981        mso-bidi-font-size:13.5pt;
982        font-family:"Times New Roman",serif;
983        mso-ascii-font-family:"Times New Roman";
984        mso-fareast-font-family:"Times New Roman";
985        mso-fareast-theme-font:minor-fareast;
986        mso-hansi-font-family:"Times New Roman";
987        mso-bidi-font-family:"Times New Roman";
988        font-weight:bold;}
989span.Heading4Char
990        {mso-style-name:"Heading 4 Char";
991        mso-style-noshow:yes;
992        mso-style-priority:9;
993        mso-style-unhide:no;
994        mso-style-locked:yes;
995        mso-style-link:"Heading 4";
996        mso-ansi-font-size:13.0pt;
997        mso-bidi-font-size:13.0pt;
998        font-family:"Cambria",serif;
999        mso-ascii-font-family:Cambria;
1000        mso-ascii-theme-font:major-latin;
1001        mso-fareast-font-family:"Times New Roman";
1002        mso-fareast-theme-font:major-fareast;
1003        mso-hansi-font-family:Cambria;
1004        mso-hansi-theme-font:major-latin;
1005        mso-bidi-font-family:"Times New Roman";
1006        mso-bidi-theme-font:major-bidi;
1007        color:#4F81BD;
1008        mso-themecolor:accent1;
1009        font-weight:bold;
1010        font-style:italic;}
1011span.Heading5Char
1012        {mso-style-name:"Heading 5 Char";
1013        mso-style-noshow:yes;
1014        mso-style-priority:9;
1015        mso-style-unhide:no;
1016        mso-style-locked:yes;
1017        mso-style-link:"Heading 5";
1018        mso-ansi-font-size:12.0pt;
1019        mso-bidi-font-size:12.0pt;
1020        font-family:"Times New Roman",serif;
1021        mso-ascii-font-family:"Times New Roman";
1022        mso-fareast-font-family:"Times New Roman";
1023        mso-fareast-theme-font:minor-fareast;
1024        mso-hansi-font-family:"Times New Roman";
1025        mso-bidi-font-family:"Times New Roman";
1026        color:#4F4FFF;
1027        font-weight:bold;}
1028span.HTMLPreformattedChar
1029        {mso-style-name:"HTML Preformatted Char";
1030        mso-style-noshow:yes;
1031        mso-style-priority:99;
1032        mso-style-unhide:no;
1033        mso-style-locked:yes;
1034        mso-style-link:"HTML Preformatted";
1035        font-family:"Courier New";
1036        mso-ascii-font-family:"Courier New";
1037        mso-fareast-font-family:"Times New Roman";
1038        mso-hansi-font-family:"Courier New";
1039        mso-bidi-font-family:"Courier New";}
1040p.msonormal0, li.msonormal0, div.msonormal0
1041        {mso-style-name:msonormal;
1042        mso-style-noshow:yes;
1043        mso-style-priority:99;
1044        mso-style-unhide:no;
1045        mso-margin-top-alt:auto;
1046        margin-right:0in;
1047        mso-margin-bottom-alt:auto;
1048        margin-left:0in;
1049        mso-pagination:widow-orphan;
1050        font-size:12.0pt;
1051        font-family:"Times New Roman",serif;
1052        mso-fareast-font-family:"Times New Roman";
1053        mso-fareast-theme-font:minor-fareast;}
1054span.DocumentMapChar
1055        {mso-style-name:"Document Map Char";
1056        mso-style-noshow:yes;
1057        mso-style-priority:99;
1058        mso-style-unhide:no;
1059        mso-style-locked:yes;
1060        mso-style-link:"Document Map";
1061        mso-ansi-font-size:8.0pt;
1062        mso-bidi-font-size:8.0pt;
1063        font-family:"Tahoma",sans-serif;
1064        mso-ascii-font-family:Tahoma;
1065        mso-fareast-font-family:"Times New Roman";
1066        mso-fareast-theme-font:minor-fareast;
1067        mso-hansi-font-family:Tahoma;
1068        mso-bidi-font-family:Tahoma;}
1069span.BalloonTextChar
1070        {mso-style-name:"Balloon Text Char";
1071        mso-style-noshow:yes;
1072        mso-style-priority:99;
1073        mso-style-unhide:no;
1074        mso-style-locked:yes;
1075        mso-style-link:"Balloon Text";
1076        mso-ansi-font-size:8.0pt;
1077        mso-bidi-font-size:8.0pt;
1078        font-family:"Tahoma",sans-serif;
1079        mso-ascii-font-family:Tahoma;
1080        mso-fareast-font-family:"Times New Roman";
1081        mso-fareast-theme-font:minor-fareast;
1082        mso-hansi-font-family:Tahoma;
1083        mso-bidi-font-family:Tahoma;}
1084span.SpellE
1085        {mso-style-name:"";
1086        mso-spl-e:yes;}
1087span.GramE
1088        {mso-style-name:"";
1089        mso-gram-e:yes;}
1090.MsoChpDefault
1091        {mso-style-type:export-only;
1092        mso-default-props:yes;
1093        font-size:10.0pt;
1094        mso-ansi-font-size:10.0pt;
1095        mso-bidi-font-size:10.0pt;
1096        font-family:"Calibri",sans-serif;
1097        mso-ascii-font-family:Calibri;
1098        mso-ascii-theme-font:minor-latin;
1099        mso-fareast-font-family:Calibri;
1100        mso-fareast-theme-font:minor-latin;
1101        mso-hansi-font-family:Calibri;
1102        mso-hansi-theme-font:minor-latin;
1103        mso-bidi-font-family:"Times New Roman";
1104        mso-bidi-theme-font:minor-bidi;}
1105@page WordSection1
1106        {size:8.5in 11.0in;
1107        margin:1.0in 1.0in 1.0in 1.0in;
1108        mso-header-margin:.5in;
1109        mso-footer-margin:.5in;
1110        mso-paper-source:0;}
1111div.WordSection1
1112        {page:WordSection1;}
1113 /* List Definitions */
1114 @list l0
1115        {mso-list-id:608973138;
1116        mso-list-type:hybrid;
1117        mso-list-template-ids:-1449999034 67698703 67698713 67698715 67698703 67698713 67698715 67698703 67698713 67698715;}
1118@list l0:level1
1119        {mso-level-tab-stop:none;
1120        mso-level-number-position:left;
1121        text-indent:-.25in;}
1122@list l0:level2
1123        {mso-level-number-format:alpha-lower;
1124        mso-level-tab-stop:none;
1125        mso-level-number-position:left;
1126        text-indent:-.25in;}
1127@list l0:level3
1128        {mso-level-number-format:roman-lower;
1129        mso-level-tab-stop:none;
1130        mso-level-number-position:right;
1131        text-indent:-9.0pt;}
1132@list l0:level4
1133        {mso-level-tab-stop:none;
1134        mso-level-number-position:left;
1135        text-indent:-.25in;}
1136@list l0:level5
1137        {mso-level-number-format:alpha-lower;
1138        mso-level-tab-stop:none;
1139        mso-level-number-position:left;
1140        text-indent:-.25in;}
1141@list l0:level6
1142        {mso-level-number-format:roman-lower;
1143        mso-level-tab-stop:none;
1144        mso-level-number-position:right;
1145        text-indent:-9.0pt;}
1146@list l0:level7
1147        {mso-level-tab-stop:none;
1148        mso-level-number-position:left;
1149        text-indent:-.25in;}
1150@list l0:level8
1151        {mso-level-number-format:alpha-lower;
1152        mso-level-tab-stop:none;
1153        mso-level-number-position:left;
1154        text-indent:-.25in;}
1155@list l0:level9
1156        {mso-level-number-format:roman-lower;
1157        mso-level-tab-stop:none;
1158        mso-level-number-position:right;
1159        text-indent:-9.0pt;}
1160ol
1161        {margin-bottom:0in;}
1162ul
1163        {margin-bottom:0in;}
1164-->
1165</style>
1166<!--[if gte mso 10]>
1167<style>
1168 /* Style Definitions */
1169 table.MsoNormalTable
1170        {mso-style-name:"Table Normal";
1171        mso-tstyle-rowband-size:0;
1172        mso-tstyle-colband-size:0;
1173        mso-style-noshow:yes;
1174        mso-style-priority:99;
1175        mso-style-parent:"";
1176        mso-padding-alt:0in 5.4pt 0in 5.4pt;
1177        mso-para-margin:0in;
1178        mso-para-margin-bottom:.0001pt;
1179        mso-pagination:widow-orphan;
1180        font-size:10.0pt;
1181        font-family:"Calibri",sans-serif;
1182        mso-ascii-font-family:Calibri;
1183        mso-ascii-theme-font:minor-latin;
1184        mso-hansi-font-family:Calibri;
1185        mso-hansi-theme-font:minor-latin;
1186        mso-bidi-font-family:"Times New Roman";
1187        mso-bidi-theme-font:minor-bidi;}
1188table.MsoTableGrid
1189        {mso-style-name:"Table Grid";
1190        mso-tstyle-rowband-size:0;
1191        mso-tstyle-colband-size:0;
1192        mso-style-priority:59;
1193        mso-style-unhide:no;
1194        border:solid windowtext 1.0pt;
1195        mso-border-alt:solid windowtext .5pt;
1196        mso-padding-alt:0in 5.4pt 0in 5.4pt;
1197        mso-border-insideh:.5pt solid windowtext;
1198        mso-border-insidev:.5pt solid windowtext;
1199        mso-para-margin:0in;
1200        mso-para-margin-bottom:.0001pt;
1201        mso-pagination:widow-orphan;
1202        font-size:10.0pt;
1203        font-family:"Calibri",sans-serif;
1204        mso-ascii-font-family:Calibri;
1205        mso-ascii-theme-font:minor-latin;
1206        mso-hansi-font-family:Calibri;
1207        mso-hansi-theme-font:minor-latin;}
1208</style>
1209<![endif]--><!--[if gte mso 9]><xml>
1210 <o:shapedefaults v:ext="edit" spidmax="1026"/>
1211</xml><![endif]--><!--[if gte mso 9]><xml>
1212 <o:shapelayout v:ext="edit">
1213  <o:idmap v:ext="edit" data="1"/>
1214 </o:shapelayout></xml><![endif]-->
1215</head>
1216
1217<body lang=EN-US link=blue vlink=purple style='tab-interval:.5in'>
1218
1219<div class=WordSection1>
1220
1221<h1><strong><span style='mso-bidi-font-weight:normal'>Sequential Refinement of
1222Small Angle Scattering Data</span><o:p></o:p></strong></h1>
1223
1224<p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In
1225this tutorial you will fit USAXS small angle scattering data for “<span
1226class=SpellE>Ludox</span>” colloidal silica (Aldrich, LUDOX TM-50?) prepared in
1227a range of dilutions to demonstrate the sequential refinement technique in
1228GSAS-II for SASD and demonstrate fitting with a hard sphere structure factor
1229for non-dilute systems.<span style='mso-fareast-font-family:Calibri;mso-fareast-theme-font:
1230minor-latin;mso-bidi-font-weight:bold;mso-bidi-font-style:italic'><o:p></o:p></span></p>
1231
1232<p class=MsoNormal>If you have not done so already, start GSAS-II.</p>
1233
1234<h2>Step 1: read in the data files</h2>
1235
1236<p class=MsoListParagraphCxSpFirst style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span
1237style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span
1238style='font:7.0pt "Times New Roman"'>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp; </span></span></span><![endif]>Use
1239the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1240mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1241minor-latin'>Import/Small Angle Data/from q (A-1) step X-ray QIE data file</span></b>
1242menu item to read the data files into GSAS-II. This read option is set to read
1243three column small angle scattering data (SASD) as Q in Å<sup>-1</sup>,
1244intensity and estimated standard deviation in intensity; there may be a header
1245with metadata information in the front of this file.<span
1246style='mso-spacerun:yes'>  </span>It will read multiple files from a single
1247directory. Change the file directory to <span class=SpellE><b style='mso-bidi-font-weight:
1248normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1249minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>SAseqref</span></b></span><b
1250style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1251mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1252minor-latin'>/data</span></b><span style='font-family:"Calibri",sans-serif;
1253mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1254minor-latin'> to find the files.</span></p>
1255
1256<p class=MsoListParagraphCxSpMiddle style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span
1257style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span
1258style='font:7.0pt "Times New Roman"'>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp; </span></span></span><![endif]>Select
1259the six<span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1260mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'> data</span>
1261files with ‘<span class=SpellE><b style='mso-bidi-font-weight:normal'><span
1262style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1263mso-hansi-theme-font:minor-latin'>Ludox</span></b></span>’ in their name in the
1264first dialog and press <b style='mso-bidi-font-weight:normal'><span
1265style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1266mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Open</span></b>.
1267All six will immediately be read into GSAS-II; you will have to select the <b
1268style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1269mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>any file
1270(*.*)</span></b> filter to see them.</p>
1271
1272<p class=MsoListParagraphCxSpLast><o:p>&nbsp;</o:p></p>
1273
1274<p class=MsoNormal>At this point the <b style='mso-bidi-font-weight:normal'><span
1275style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1276mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data
1277tree</span></b> window will have several entries and the plot window will show
1278the SASD pattern for one as a log-log plot of intensity vs. Q; enter ‘<b
1279style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1280mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>m</span></b>’
1281on the plot. Now all are shown; one shows error bars (<b style='mso-bidi-font-weight:
1282normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1283minor-latin;mso-hansi-theme-font:minor-latin'>SASD S49_Ludox6_1pct.dat</span></b>)
1284as it is the selected tree entry and the others as lines.</p>
1285
1286<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype
1287 id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t"
1288 path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f">
1289 <v:stroke joinstyle="miter"/>
1290 <v:formulas>
1291  <v:f eqn="if lineDrawn pixelLineWidth 0"/>
1292  <v:f eqn="sum @0 1 0"/>
1293  <v:f eqn="sum 0 0 @1"/>
1294  <v:f eqn="prod @2 1 2"/>
1295  <v:f eqn="prod @3 21600 pixelWidth"/>
1296  <v:f eqn="prod @3 21600 pixelHeight"/>
1297  <v:f eqn="sum @0 0 1"/>
1298  <v:f eqn="prod @6 1 2"/>
1299  <v:f eqn="prod @7 21600 pixelWidth"/>
1300  <v:f eqn="sum @8 21600 0"/>
1301  <v:f eqn="prod @7 21600 pixelHeight"/>
1302  <v:f eqn="sum @10 21600 0"/>
1303 </v:formulas>
1304 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
1305 <o:lock v:ext="edit" aspectratio="t"/>
1306</v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1056" type="#_x0000_t75"
1307 style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'>
1308 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image001.png"
1309  o:title=""/>
1310</v:shape><![endif]--><![if !vml]><img width=700 height=600
1311src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image001.png"
1312v:shapes="Picture_x0020_1"><![endif]></span></p>
1313
1314<h2><a name="_Ref386704789">Step 2: Set Limits</a></h2>
1315
1316<p class=MsoNormal>For this step we will reposition the limits to exclude the
1317low-Q (&lt;10<sup>-3</sup>) part of the patterns which do not seem to follow
1318the sequence evident in the 10<sup>-2</sup> – 10<sup>-1</sup> part. Select <b
1319style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1320mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Limits</span></b>
1321under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1322mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD
1323S35_Ludox_40pct.dat</span></b> from the GSAS-II tree. Set the lower limit using
1324the cursor on the plot by picking a point somewhere in the flat region at
1325Q~3x10<sup>-3</sup> with the left mouse button. The limits window should look
1326something like</p>
1327
1328<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1329 id="_x0000_i1055" type="#_x0000_t75" style='width:225pt;height:96.75pt;
1330 visibility:visible;mso-wrap-style:square'>
1331 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image033.png"
1332  o:title=""/>
1333</v:shape><![endif]--><![if !vml]><img width=300 height=129
1334src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image033.png"
1335v:shapes="_x0000_i1055"><![endif]></span><span
1336style='mso-spacerun:yes'> </span></p>
1337
1338<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1339
1340<p class=MsoNormal>To copy these limits to the other data sets use the <b
1341style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1342mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit Limits/Copy</span></b>
1343command from the data window menu; a popup window will give the selection of
1344targets.<br>
1345<span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_27"
1346 o:spid="_x0000_i1054" type="#_x0000_t75" style='width:240pt;height:232.5pt;
1347 visibility:visible;mso-wrap-style:square'>
1348 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image003.png"
1349  o:title=""/>
1350</v:shape><![endif]--><![if !vml]><img width=320 height=310
1351src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image003.png"
1352v:shapes="Picture_x0020_27"><![endif]></span></p>
1353
1354<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1355
1356<p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span
1357style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1358mso-hansi-theme-font:minor-latin'>Set All</span></b> (all boxes will be
1359checked) and then press <b style='mso-bidi-font-weight:normal'><span
1360style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1361mso-hansi-theme-font:minor-latin'>Enter</span></b> to do the copy.</p>
1362
1363<h2>Step 3 Select the scattering substances for your sample</h2>
1364
1365<p class=MsoNormal><span style='mso-no-proof:yes'>Two substances need to be
1366defined for your sample to give the anticipated scattering contrast; in this
1367case one is silica and the other is water. Parameters for a number of
1368substances are defined in the file </span><b style='mso-bidi-font-weight:normal'><span
1369style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1370mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span
1371style='mso-no-proof:yes'>. You can add your own substances to this or better
1372put them in </span><b style='mso-bidi-font-weight:normal'><span
1373style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1374mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span
1375style='mso-no-proof:yes'>; this is read after Substances.py when you load substances
1376for your selection. </span>Select <b style='mso-bidi-font-weight:normal'><span
1377style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1378mso-hansi-theme-font:minor-latin'>Substances</span></b> from the GSAS-II tree.
1379Then do <span class=GramE><b style='mso-bidi-font-weight:normal'><span
1380style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1381mso-hansi-theme-font:minor-latin'>Edit</span></b></span><b style='mso-bidi-font-weight:
1382normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1383minor-latin;mso-hansi-theme-font:minor-latin'> substance/Load substance</span></b>
1384from the menu; a popup window will appear with possible selections</p>
1385
1386<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1387 id="Picture_x0020_3" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:259.5pt;
1388 height:252pt;visibility:visible;mso-wrap-style:square'>
1389 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image004.png"
1390  o:title=""/>
1391</v:shape><![endif]--><![if !vml]><img width=346 height=336
1392src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image004.png"
1393v:shapes="Picture_x0020_3"><![endif]><o:p></o:p></span></p>
1394
1395<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1396
1397<p class=MsoNormal>Notice that silica is not one of the choices; we will add it
1398in a moment. Select <b style='mso-bidi-font-weight:normal'><span
1399style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1400mso-hansi-theme-font:minor-latin'>Water</span></b> and press <b
1401style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1402mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>;
1403the relevant data for water (and vacuum) are displayed next</p>
1404
1405<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1406 id="_x0000_i1052" type="#_x0000_t75" style='width:280.5pt;height:246pt;
1407 visibility:visible;mso-wrap-style:square'>
1408 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image034.png"
1409  o:title=""/>
1410</v:shape><![endif]--><![if !vml]><img width=374 height=328
1411src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image034.png"
1412v:shapes="_x0000_i1052"><![endif]></span><span
1413style='mso-spacerun:yes'> </span></p>
1414
1415<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1416
1417<p class=MsoNormal>If desired, you can load/add as many substances as you want
1418to this list; you can also delete any of them (except vacuum or unit scatter).
1419The composition, volume occupied by the atoms in the composition and the
1420density are given for each substance. These can each be edited; the other
1421values will change accordingly. Since silica wasn’t in the list of known
1422substances, do <b style='mso-bidi-font-weight:normal'><span style='font-family:
1423"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1424minor-latin'>Edit substance/Add substance</span></b> to create it; you will be
1425asked for a name – enter <b style='mso-bidi-font-weight:normal'><span
1426style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1427mso-hansi-theme-font:minor-latin'>silica</span></b> and then a periodic table
1428of the elements will be shown. Select <b style='mso-bidi-font-weight:normal'><span
1429style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1430mso-hansi-theme-font:minor-latin'>Si</span></b> and <b style='mso-bidi-font-weight:
1431normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1432minor-latin;mso-hansi-theme-font:minor-latin'>O</span></b></p>
1433
1434<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1435 id="Picture_x0020_6" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:435pt;
1436 height:270pt;visibility:visible;mso-wrap-style:square'>
1437 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image006.png"
1438  o:title=""/>
1439</v:shape><![endif]--><![if !vml]><img width=580 height=360
1440src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image006.png"
1441v:shapes="Picture_x0020_6"><![endif]></span><span
1442style='mso-spacerun:yes'> </span></p>
1443
1444<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1445
1446<p class=MsoNormal>They appear in red. Press <b style='mso-bidi-font-weight:
1447normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1448minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b> and silica will be
1449added to your substance list</p>
1450
1451<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1452 id="Picture_x0020_35" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:280.5pt;
1453 height:350.25pt;visibility:visible;mso-wrap-style:square'>
1454 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image035.png"
1455  o:title=""/>
1456</v:shape><![endif]--><![if !vml]><img width=374 height=467
1457src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image035.png"
1458v:shapes="Picture_x0020_35"><![endif]></span></p>
1459
1460<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1461
1462<p class=MsoNormal>Change the O-atom entry to <b style='mso-bidi-font-weight:
1463normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1464minor-latin;mso-hansi-theme-font:minor-latin'>2.0</span></b> and the density to
1465<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1466mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>2.65</span></b>;
1467the window will change each time giving new values and should finally show</p>
1468
1469<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1470 id="_x0000_i1049" type="#_x0000_t75" style='width:280.5pt;height:350.25pt;
1471 visibility:visible;mso-wrap-style:square'>
1472 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image036.png"
1473  o:title=""/>
1474</v:shape><![endif]--><![if !vml]><img width=374 height=467
1475src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image036.png"
1476v:shapes="_x0000_i1049"><![endif]></span><span
1477style='mso-spacerun:yes'> </span></p>
1478
1479<p class=MsoNormal>From this information the scattering density and that as
1480affected by resonant scattering for the listed wavelength is displayed (the
1481wavelength can be changed in the <b style='mso-bidi-font-weight:normal'><span
1482style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1483mso-hansi-theme-font:minor-latin'>Instrument Parameters</span></b> GSAS-II tree
1484item if needed). The real density value is used for contrast calculations.</p>
1485
1486<p class=MsoNormal>Just as for Limits, this information needs to be copied to
1487the other SASD entries in the GSAS-II tree. Do <b style='mso-bidi-font-weight:
1488normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1489minor-latin;mso-hansi-theme-font:minor-latin'>Edit substance/Copy substances</span></b>
1490from the data window menu and follow the same selection procedure as you used
1491for limits above.</p>
1492
1493<h2><a name="_Ref386699210">Step 4: Set Sample parameters</a> </h2>
1494
1495<p class=MsoNormal><span style='mso-no-proof:yes'>As these data sets were
1496collected from a sequence of samples where there was some variable changed in
1497their preparation, it would be useful to have this information available to
1498GSAS-II for subsequent analysis. Select Sample parameters from the data tree.
1499It shows (for </span><b style='mso-bidi-font-weight:normal'><span
1500style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1501mso-hansi-theme-font:minor-latin'>SASD S49_Ludox6_1pct.dat)<o:p></o:p></span></b></p>
1502
1503<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1504 id="Picture_x0020_9" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:291.75pt;
1505 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1506 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image009.png"
1507  o:title=""/>
1508</v:shape><![endif]--><![if !vml]><img width=389 height=518
1509src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image009.png"
1510v:shapes="Picture_x0020_9"><![endif]><o:p></o:p></span></p>
1511
1512<p class=MsoNormal><span style='mso-no-proof:yes'><o:p>&nbsp;</o:p></span></p>
1513
1514<p class=MsoNormal><span style='mso-no-proof:yes'>NB: we will not be needing to
1515select the </span><b style='mso-bidi-font-weight:normal'><span
1516style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1517mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Material</span></b><span
1518style='mso-no-proof:yes'> for this analysis; material selection is only
1519required for </span><b style='mso-bidi-font-weight:normal'><span
1520style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1521mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Size distribution</span></b><span
1522style='mso-no-proof:yes'> analysis. Notice that the last three column names can
1523be changed; pick the first one and change it to </span><b style='mso-bidi-font-weight:
1524normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1525minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>fraction</span></b><span
1526style='mso-no-proof:yes'>. Then enter </span><b style='mso-bidi-font-weight:
1527normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1528minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>0.01</span></b><span
1529style='mso-no-proof:yes'> which corresponds to the ‘</span><b style='mso-bidi-font-weight:
1530normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1531minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>1pct</span></b><span
1532style='mso-no-proof:yes'>’ in the file name. The data window should look like<o:p></o:p></span></p>
1533
1534<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1535 id="Picture_x0020_10" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:291.75pt;
1536 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1537 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image010.png"
1538  o:title=""/>
1539</v:shape><![endif]--><![if !vml]><img width=389 height=518
1540src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image010.png"
1541v:shapes="Picture_x0020_10"><![endif]><o:p></o:p></span></p>
1542
1543<p class=MsoNormal><span style='mso-no-proof:yes'><o:p>&nbsp;</o:p></span></p>
1544
1545<p class=MsoNormal><span style='mso-no-proof:yes'>Now do the same for the </span><b
1546style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1547mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:
1548yes'>Sample Parameters</span></b><span style='mso-no-proof:yes'> for the other
1549data sets putting in the correct fraction from the respective file names. If
1550you first </span><b style='mso-bidi-font-weight:normal'><span style='font-family:
1551"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1552minor-latin;mso-no-proof:yes'>Copy</span></b><span style='mso-no-proof:yes'>
1553this one to the others, that will save you the step of changing the names. You
1554will end up on the </span><b style='mso-bidi-font-weight:normal'><span
1555style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1556mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Sample parameters</span></b><span
1557style='mso-no-proof:yes'> page for </span><b style='mso-bidi-font-weight:normal'><span
1558style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1559mso-hansi-theme-font:minor-latin'>SASD S53_Ludox6_40pct.dat </span></b>GSAS-II
1560data tree.</p>
1561
1562<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1563 id="Picture_x0020_11" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:291.75pt;
1564 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1565 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image011.png"
1566  o:title=""/>
1567</v:shape><![endif]--><![if !vml]><img width=389 height=518
1568src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image011.png"
1569v:shapes="Picture_x0020_11"><![endif]></span><span
1570style='mso-spacerun:yes'> </span><span style='mso-no-proof:yes'><o:p></o:p></span></p>
1571
1572<h2>Step 5: Set Model parameters </h2>
1573
1574<p class=MsoNormal>Looking at the data plot (key ‘<b style='mso-bidi-font-weight:
1575normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1576minor-latin;mso-hansi-theme-font:minor-latin'>m</span></b>’ to select a single
1577data set) for <b style='mso-bidi-font-weight:normal'><span style='font-family:
1578"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1579minor-latin'>SASD S53_Ludox6_40pct.dat</span></b>, one sees just one feature
1580with oscillations at higher Q. This is the signal for a non-dilute <span
1581class=SpellE>scatterer</span>. </p>
1582
1583<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1584 id="Picture_x0020_12" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:525pt;
1585 height:450pt;visibility:visible;mso-wrap-style:square'>
1586 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image012.png"
1587  o:title=""/>
1588</v:shape><![endif]--><![if !vml]><img width=700 height=600
1589src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image012.png"
1590v:shapes="Picture_x0020_12"><![endif]></span></p>
1591
1592<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1593
1594<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
1595style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1596mso-hansi-theme-font:minor-latin'>Models</span></b> from the GSASII data tree
1597under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1598mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD
1599S35_Ludox1_40pct.dat</span></b>, switch <b style='mso-bidi-font-weight:normal'><span
1600style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1601mso-hansi-theme-font:minor-latin'>Size dist.</span></b> to <b style='mso-bidi-font-weight:
1602normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1603minor-latin;mso-hansi-theme-font:minor-latin'>Particle fit</span></b>, and add
1604a reasonable value (<b style='mso-bidi-font-weight:normal'><span
1605style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1606mso-hansi-theme-font:minor-latin'>0.25</span></b>) for the <b style='mso-bidi-font-weight:
1607normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1608minor-latin;mso-hansi-theme-font:minor-latin'>Background</span></b>; a
1609horizontal red line will appear. Next do <b style='mso-bidi-font-weight:normal'><span
1610style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1611mso-hansi-theme-font:minor-latin'>Models/Add</span></b>; the window will
1612display a default component; change the <b style='mso-bidi-font-weight:normal'><span
1613style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1614mso-hansi-theme-font:minor-latin'>Material</span></b> to <b style='mso-bidi-font-weight:
1615normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1616minor-latin;mso-hansi-theme-font:minor-latin'>silica</span></b>. Also change
1617the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1618mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Matrix</span></b>
1619to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1620mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Water</span></b>;
1621the calculated contrast should be 175.60 10<sup>20</sup>cm<sup>-4</sup>. The
1622plot will show a green curve corresponding to the default values.</p>
1623
1624<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1625 id="Picture_x0020_13" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:525pt;
1626 height:450pt;visibility:visible;mso-wrap-style:square'>
1627 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image013.png"
1628  o:title=""/>
1629</v:shape><![endif]--><![if !vml]><img width=700 height=600
1630src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image013.png"
1631v:shapes="Picture_x0020_13"><![endif]></span></p>
1632
1633<p class=MsoNormal><span style='mso-no-proof:yes'><o:p>&nbsp;</o:p></span></p>
1634
1635<p class=MsoNormal>The default <span class=SpellE><b style='mso-bidi-font-weight:
1636normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1637minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
1638style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1639mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b>
1640of <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1641mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1e+03</span></b>
1642is too large, try something smaller and increase the <span class=SpellE><b
1643style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1644mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
1645style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1646mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b>
1647(the sliders work well for this). Since this is a non-dilute system, change the
1648<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1649mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Structure
1650factor</span></b> to <b style='mso-bidi-font-weight:normal'><span
1651style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1652mso-hansi-theme-font:minor-latin'>Hard sphere</span></b> and set the <b
1653style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1654mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SF <span
1655class=SpellE>VolFr</span></span></b> to <b style='mso-bidi-font-weight:normal'><span
1656style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1657mso-hansi-theme-font:minor-latin'>0.4</span></b>. Your data window should look
1658something like</p>
1659
1660<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1661 id="Picture_x0020_14" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:384.75pt;
1662 height:358.5pt;visibility:visible;mso-wrap-style:square'>
1663 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image014.png"
1664  o:title=""/>
1665</v:shape><![endif]--><![if !vml]><img width=513 height=478
1666src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image014.png"
1667v:shapes="Picture_x0020_14"><![endif]></span></p>
1668
1669<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1670
1671<p class=MsoNormal>And the plot will be</p>
1672
1673<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1674 id="Picture_x0020_34" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:525pt;
1675 height:450pt;visibility:visible;mso-wrap-style:square'>
1676 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image015.png"
1677  o:title=""/>
1678</v:shape><![endif]--><![if !vml]><img width=700 height=600
1679src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image015.png"
1680v:shapes="Picture_x0020_34"><![endif]></span><br clear=all style='mso-special-character:
1681line-break'>
1682</p>
1683
1684<p class=MsoNormal>The calculated curve shows oscillations but they are not in
1685the right place and are too broad. Try the <span class=SpellE><b
1686style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1687mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
1688style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1689mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> <span
1690class=SpellE>StdDev</span></span></b> slider and make it smaller; somewhere
1691about <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1692mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.132</span></b>
1693gives a curve with the right shape but too high. Reduce the <span class=SpellE><b
1694style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1695mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
1696style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1697mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b>
1698to improve the match. Shift the <b style='mso-bidi-font-weight:normal'><span
1699style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1700mso-hansi-theme-font:minor-latin'>SF <span class=SpellE>Dist</span></span></b>
1701and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1702mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SF <span
1703class=SpellE>VolFr</span></span></b> as well to get the curves to match.
1704Carefully manipulate each of the sliders to see what effect they have on the
1705calculated curve. With some adjustments I got</p>
1706
1707<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1708 id="Picture_x0020_36" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:384.75pt;
1709 height:358.5pt;visibility:visible;mso-wrap-style:square'>
1710 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image016.png"
1711  o:title=""/>
1712</v:shape><![endif]--><![if !vml]><img width=513 height=478
1713src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image016.png"
1714v:shapes="Picture_x0020_36"><![endif]></span></p>
1715
1716<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1717
1718<p class=MsoNormal>to give a pretty nice initial fit.</p>
1719
1720<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1721 id="_x0000_i1040" type="#_x0000_t75" style='width:525pt;height:450pt;
1722 visibility:visible;mso-wrap-style:square'>
1723 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image017.png"
1724  o:title=""/>
1725</v:shape><![endif]--><![if !vml]><img width=700 height=600
1726src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image017.png"
1727v:shapes="_x0000_i1040"><![endif]></span></p>
1728
1729<h2>Step 6: Initial refinement</h2>
1730
1731<p class=MsoNormal>We can be brave and set all six <b style='mso-bidi-font-weight:
1732normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1733minor-latin;mso-hansi-theme-font:minor-latin'>Refine?</span></b> boxes (NB: the
1734one for <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1735mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Matrix
1736Volume fraction</span></b> currently does not operate – ignore it). Then do <b
1737style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1738mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Fit</span></b>;
1739the least squares very quickly minimizes to give</p>
1740
1741<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1742 id="_x0000_i1039" type="#_x0000_t75" style='width:384.75pt;height:358.5pt;
1743 visibility:visible;mso-wrap-style:square'>
1744 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image018.png"
1745  o:title=""/>
1746</v:shape><![endif]--><![if !vml]><img width=513 height=478
1747src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image018.png"
1748v:shapes="_x0000_i1039"><![endif]></span></p>
1749
1750<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1751
1752<p class=MsoNormal>The console window lists the results</p>
1753
1754<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1755 id="Picture_x0020_39" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:609.75pt;
1756 height:152.25pt;visibility:visible;mso-wrap-style:square'>
1757 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image019.png"
1758  o:title=""/>
1759</v:shape><![endif]--><![if !vml]><img width=813 height=203
1760src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image019.png"
1761v:shapes="Picture_x0020_39"><![endif]></span></p>
1762
1763<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1764
1765<p class=MsoNormal>And the plot shows the fit graphically</p>
1766
1767<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1768 id="Picture_x0020_40" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:525pt;
1769 height:450pt;visibility:visible;mso-wrap-style:square'>
1770 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image020.png"
1771  o:title=""/>
1772</v:shape><![endif]--><![if !vml]><img width=700 height=600
1773src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image020.png"
1774v:shapes="Picture_x0020_40"><![endif]></span></p>
1775
1776<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1777
1778<p class=MsoNormal>The fit is OK except for a region Q~0.03Å<sup>-1</sup>; this
1779is probably due to a failure of the simple hard sphere model in this
1780concentrated system.</p>
1781
1782<h2>Step 7: Sequential refinement</h2>
1783
1784<p class=MsoNormal>We are now ready to try a sequential refinement starting
1785with this fit for the 1<sup>st</sup> data set. Do <b style='mso-bidi-font-weight:
1786normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1787minor-latin;mso-hansi-theme-font:minor-latin'>Models/Sequential fit</span></b>;
1788a dialog box will appear for selection of the data sets.</p>
1789
1790<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1791 id="Picture_x0020_21" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:240pt;
1792 height:232.5pt;visibility:visible;mso-wrap-style:square'>
1793 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image021.png"
1794  o:title=""/>
1795</v:shape><![endif]--><![if !vml]><img width=320 height=310
1796src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image021.png"
1797v:shapes="Picture_x0020_21"><![endif]></span></p>
1798
1799<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1800
1801<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
1802style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1803mso-hansi-theme-font:minor-latin'>Set All</span></b>, all boxes will be checked
1804showing selection of the data sets. Then press <b style='mso-bidi-font-weight:
1805normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1806minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>; a new dialog box
1807will appear</p>
1808
1809<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1810 id="Picture_x0020_33" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:259.5pt;
1811 height:252pt;visibility:visible;mso-wrap-style:square'>
1812 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image022.png"
1813  o:title=""/>
1814</v:shape><![endif]--><![if !vml]><img width=346 height=336
1815src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image022.png"
1816v:shapes="Picture_x0020_33"><![endif]></span></p>
1817
1818<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1819
1820<p class=MsoNormal>This allows you to instruct the sequential refinement to
1821start at the last data set and proceed backwards through them (<b
1822style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1823mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Reverse
1824sequence</span></b>). It also allows you to instruct the sequential refinement
1825to use the current parameters as starting values for the next data set. This
1826works in either direction and facilitates the initial sequential refinements.
1827NB: some sequential refinements do not work well in both directions; in this
1828particular case starting with a fitted 1% pattern and going in reverse through
1829the data fails on the 5% data set. Apparently the change in parameters is too
1830great for the least squares to handle; going in the forward direction works
1831just fine (as you will see next). Select <b style='mso-bidi-font-weight:normal'><span
1832style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1833mso-hansi-theme-font:minor-latin'>Copy from prev.</span></b> and press <b
1834style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1835mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>;
1836the sequential refinement will proceed very rapidly displaying results for each
1837data set on the console and finally ending by displaying the <b
1838style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1839mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sequential
1840results.<o:p></o:p></span></b></p>
1841
1842<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1843 id="Picture_x0020_42" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:564pt;
1844 height:262.5pt;visibility:visible;mso-wrap-style:square'>
1845 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image023.png"
1846  o:title=""/>
1847</v:shape><![endif]--><![if !vml]><img width=752 height=350
1848src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image023.png"
1849v:shapes="Picture_x0020_42"><![endif]></span></p>
1850
1851<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1852
1853<p class=MsoNormal>Note the comment in the plot status bar: double click on the
1854<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1855mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0<span
1856class=GramE>;Volume</span></span></b> and a new plot will appear.</p>
1857
1858<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1859 id="Picture_x0020_43" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:525pt;
1860 height:450pt;visibility:visible;mso-wrap-style:square'>
1861 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image024.png"
1862  o:title=""/>
1863</v:shape><![endif]--><![if !vml]><img width=700 height=600
1864src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image024.png"
1865v:shapes="Picture_x0020_43"><![endif]></span></p>
1866
1867<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1868
1869<p class=MsoNormal>Each point has an error bar extracted from the least squares
1870– it represents a 1 &#963; variation in the value. Now press the <b
1871style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1872mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>s</span></b>
1873key (or select <b style='mso-bidi-font-weight:normal'><span style='font-family:
1874"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1875minor-latin'>s</span></b> from the <b style='mso-bidi-font-weight:normal'><span
1876style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1877mso-hansi-theme-font:minor-latin'>K</span></b> box); a dialog box will appear
1878with a selection of parameters to plot along the x-axis. Select <b
1879style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1880mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>fraction</span></b>
1881and the plot will be redrawn (it may require selection of another column &amp;
1882then <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1883mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0<span
1884class=GramE>;Volume</span></span></b> to make it appear).</p>
1885
1886<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1887 id="Picture_x0020_44" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:525pt;
1888 height:450pt;visibility:visible;mso-wrap-style:square'>
1889 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image025.png"
1890  o:title=""/>
1891</v:shape><![endif]--><![if !vml]><img width=700 height=600
1892src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image025.png"
1893v:shapes="Picture_x0020_44"><![endif]></span></p>
1894
1895<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1896
1897<p class=MsoNormal>It is gratifying how this relation between Volume and the
1898composition is linear. You can now determine the slope &amp; intercept (or fit
1899to some other function!) directly with GSAS-II; do <b style='mso-bidi-font-weight:
1900normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1901minor-latin;mso-hansi-theme-font:minor-latin'>Parametric Fit/Add equation</span></b>
1902and the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1903mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Expression
1904Editor</span></b> dialog box will appear.</p>
1905
1906<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1907 id="Picture_x0020_26" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:465pt;
1908 height:225pt;visibility:visible;mso-wrap-style:square'>
1909 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image026.png"
1910  o:title=""/>
1911</v:shape><![endif]--><![if !vml]><img width=620 height=300
1912src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image026.png"
1913v:shapes="Picture_x0020_26"><![endif]></span></p>
1914
1915<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1916
1917<p class=MsoNormal>The pull down in the upper left corner has two choices;
1918select <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1919mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Global</span></b>
1920and a new dialog box will appear giving you choices from the <b
1921style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1922mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sequential
1923results</span></b> table. Select <b style='mso-bidi-font-weight:normal'><span
1924style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1925mso-hansi-theme-font:minor-latin'>0<span class=GramE>;Volume</span></span></b>
1926and the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1927mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Expression
1928Editor</span></b> will reappear.</p>
1929
1930<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1931 id="Picture_x0020_45" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:465pt;
1932 height:255pt;visibility:visible;mso-wrap-style:square'>
1933 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image027.png"
1934  o:title=""/>
1935</v:shape><![endif]--><![if !vml]><img width=620 height=340
1936src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image027.png"
1937v:shapes="Picture_x0020_45"><![endif]></span></p>
1938
1939<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1940
1941<p class=MsoNormal>Next enter the function you wish to use in fitting <b
1942style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1943mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0<span
1944class=GramE>:Volume</span></span></b>; enter <b style='mso-bidi-font-weight:
1945normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1946minor-latin;mso-hansi-theme-font:minor-latin'>m*<span class=SpellE>x+b</span></span></b>
1947(equation for a straight line). After a pause, the <b style='mso-bidi-font-weight:
1948normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1949minor-latin;mso-hansi-theme-font:minor-latin'>Expression Editor</span></b> will
1950be redrawn allowing you to assign <b style='mso-bidi-font-weight:normal'><span
1951style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1952mso-hansi-theme-font:minor-latin'>b</span></b>, <b style='mso-bidi-font-weight:
1953normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1954minor-latin;mso-hansi-theme-font:minor-latin'>m</span></b> &amp; <b
1955style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1956mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>x</span></b>.</p>
1957
1958<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1959 id="Picture_x0020_46" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;
1960 height:255pt;visibility:visible;mso-wrap-style:square'>
1961 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image028.png"
1962  o:title=""/>
1963</v:shape><![endif]--><![if !vml]><img width=620 height=340
1964src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image028.png"
1965v:shapes="Picture_x0020_46"><![endif]></span></p>
1966
1967<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1968
1969<p class=MsoNormal>For <b style='mso-bidi-font-weight:normal'><span
1970style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1971mso-hansi-theme-font:minor-latin'>b</span></b> &amp; <b style='mso-bidi-font-weight:
1972normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1973minor-latin;mso-hansi-theme-font:minor-latin'>m</span></b> select <b
1974style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1975mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Free</span></b>;
1976these will be the parameters for your fit. For <b style='mso-bidi-font-weight:
1977normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1978minor-latin;mso-hansi-theme-font:minor-latin'>x</span></b> select <b
1979style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1980mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Global</span></b>;
1981a new dialog box will appear giving you several choices.</p>
1982
1983<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1984 id="Picture_x0020_37" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:468pt;
1985 height:187.5pt;visibility:visible;mso-wrap-style:square'>
1986 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image037.png"
1987  o:title=""/>
1988</v:shape><![endif]--><![if !vml]><img width=624 height=250
1989src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image037.png"
1990v:shapes="Picture_x0020_37"><![endif]></span></p>
1991
1992<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1993
1994<p class=MsoNormal>Select the last line (<b style='mso-bidi-font-weight:normal'><span
1995style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1996mso-hansi-theme-font:minor-latin'>fraction…</span></b>); it will appear in
1997blue. Then press <b style='mso-bidi-font-weight:normal'><span style='font-family:
1998"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1999minor-latin'>OK</span></b>; the <b style='mso-bidi-font-weight:normal'><span
2000style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2001mso-hansi-theme-font:minor-latin'>Expression Editor</span></b> will reappear
2002with more information.</p>
2003
2004<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2005 id="Picture_x0020_47" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:465pt;
2006 height:255pt;visibility:visible;mso-wrap-style:square'>
2007 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image030.png"
2008  o:title=""/>
2009</v:shape><![endif]--><![if !vml]><img width=620 height=340
2010src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image030.png"
2011v:shapes="Picture_x0020_47"><![endif]></span></p>
2012
2013<p class=MsoNormal><o:p>&nbsp;</o:p></p>
2014
2015<p class=MsoNormal>Next press <b style='mso-bidi-font-weight:normal'><span
2016style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
2017mso-hansi-theme-font:minor-latin'>OK</span></b>; the equation will be fitted to
2018the data and the results displayed on the console</p>
2019
2020<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2021 id="Picture_x0020_49" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:303.75pt;
2022 height:98.25pt;visibility:visible;mso-wrap-style:square'>
2023 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image031.png"
2024  o:title=""/>
2025</v:shape><![endif]--><![if !vml]><img width=405 height=131
2026src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image031.png"
2027v:shapes="Picture_x0020_49"><![endif]></span></p>
2028
2029<p class=MsoNormal><o:p>&nbsp;</o:p></p>
2030
2031<p class=MsoNormal>And the plot shows the curve (in blue) calculated from the
2032best fit, weighted by the <span class=SpellE>esds</span> on the data points, to
2033the model equation for a straight line.</p>
2034
2035<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
2036 id="Picture_x0020_38" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:468pt;
2037 height:401.25pt;visibility:visible;mso-wrap-style:square'>
2038 <v:imagedata src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image038.png"
2039  o:title=""/>
2040</v:shape><![endif]--><![if !vml]><img width=624 height=535
2041src="Sequential%20Refinement%20of%20Small%20Angle%20Scattering%20Data_files/image039.png"
2042v:shapes="Picture_x0020_38"><![endif]></span></p>
2043
2044<p class=MsoNormal><o:p>&nbsp;</o:p></p>
2045
2046<p class=MsoNormal>For this particular experiment there was an expectation that
2047the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
2048mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Volume</span></b>s
2049obtained from the SASD model fits would match the makeup concentrations for
2050these samples so that the slope for this plot would be unity. One possible
2051explanation for the discrepancy is that the silica particles are partially
2052hydrated thus reducing the contrast from 175.6x10<sup>20</sup> cm<sup>-4</sup>
2053to something like 98x10<sup>20</sup>cm<sup>-4</sup>.</p>
2054
2055</div>
2056
2057</body>
2058
2059</html>
Note: See TracBrowser for help on using the repository browser.