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23 | <o:DocumentProperties> |
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24 | <o:Author>Von Dreele</o:Author> |
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25 | <o:LastAuthor>Von Dreele</o:LastAuthor> |
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26 | <o:Revision>14</o:Revision> |
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27 | <o:TotalTime>2504</o:TotalTime> |
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28 | <o:Created>2014-05-13T20:30:00Z</o:Created> |
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29 | <o:LastSaved>2016-07-28T18:47:00Z</o:LastSaved> |
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30 | <o:Pages>1</o:Pages> |
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31 | <o:Words>1981</o:Words> |
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32 | <o:Characters>11295</o:Characters> |
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33 | <o:Company>Argonne National Laboratory</o:Company> |
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336 | Name="Table Columns 5"/> |
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352 | Name="Table Grid 8"/> |
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355 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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356 | Name="Table List 2"/> |
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357 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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358 | Name="Table List 3"/> |
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359 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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361 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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364 | Name="Table List 6"/> |
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365 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
366 | Name="Table List 7"/> |
---|
367 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
368 | Name="Table List 8"/> |
---|
369 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
370 | Name="Table 3D effects 1"/> |
---|
371 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
372 | Name="Table 3D effects 2"/> |
---|
373 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
374 | Name="Table 3D effects 3"/> |
---|
375 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
376 | Name="Table Contemporary"/> |
---|
377 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
378 | Name="Table Elegant"/> |
---|
379 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
380 | Name="Table Professional"/> |
---|
381 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
382 | Name="Table Subtle 1"/> |
---|
383 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
384 | Name="Table Subtle 2"/> |
---|
385 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
386 | Name="Table Web 1"/> |
---|
387 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
388 | Name="Table Web 2"/> |
---|
389 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
390 | Name="Table Web 3"/> |
---|
391 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
392 | Name="Balloon Text"/> |
---|
393 | <w:LsdException Locked="false" Priority="59" Name="Table Grid"/> |
---|
394 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
395 | Name="Table Theme"/> |
---|
396 | <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/> |
---|
397 | <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/> |
---|
398 | <w:LsdException Locked="false" Priority="60" Name="Light Shading"/> |
---|
399 | <w:LsdException Locked="false" Priority="61" Name="Light List"/> |
---|
400 | <w:LsdException Locked="false" Priority="62" Name="Light Grid"/> |
---|
401 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/> |
---|
402 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/> |
---|
403 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/> |
---|
404 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/> |
---|
405 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/> |
---|
406 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/> |
---|
407 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/> |
---|
408 | <w:LsdException Locked="false" Priority="70" Name="Dark List"/> |
---|
409 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/> |
---|
410 | <w:LsdException Locked="false" Priority="72" Name="Colorful List"/> |
---|
411 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/> |
---|
412 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/> |
---|
413 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/> |
---|
414 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/> |
---|
415 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/> |
---|
416 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/> |
---|
417 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/> |
---|
418 | <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/> |
---|
419 | <w:LsdException Locked="false" Priority="34" QFormat="true" |
---|
420 | Name="List Paragraph"/> |
---|
421 | <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/> |
---|
422 | <w:LsdException Locked="false" Priority="30" QFormat="true" |
---|
423 | Name="Intense Quote"/> |
---|
424 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/> |
---|
425 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/> |
---|
426 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/> |
---|
427 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/> |
---|
428 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/> |
---|
429 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/> |
---|
430 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/> |
---|
431 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/> |
---|
432 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/> |
---|
433 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/> |
---|
434 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/> |
---|
435 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/> |
---|
436 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/> |
---|
437 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/> |
---|
438 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/> |
---|
439 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/> |
---|
440 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/> |
---|
441 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/> |
---|
442 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/> |
---|
443 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/> |
---|
444 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/> |
---|
445 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/> |
---|
446 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/> |
---|
447 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/> |
---|
448 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/> |
---|
449 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/> |
---|
450 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/> |
---|
451 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/> |
---|
452 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/> |
---|
453 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/> |
---|
454 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/> |
---|
455 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/> |
---|
456 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/> |
---|
457 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/> |
---|
458 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/> |
---|
459 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/> |
---|
460 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/> |
---|
461 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/> |
---|
462 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/> |
---|
463 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/> |
---|
464 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/> |
---|
465 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/> |
---|
466 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/> |
---|
467 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/> |
---|
468 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/> |
---|
469 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/> |
---|
470 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/> |
---|
471 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/> |
---|
472 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/> |
---|
473 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/> |
---|
474 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/> |
---|
475 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/> |
---|
476 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/> |
---|
477 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/> |
---|
478 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/> |
---|
479 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/> |
---|
480 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/> |
---|
481 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/> |
---|
482 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/> |
---|
483 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/> |
---|
484 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/> |
---|
485 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/> |
---|
486 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/> |
---|
487 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/> |
---|
488 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/> |
---|
489 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/> |
---|
490 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/> |
---|
491 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/> |
---|
492 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/> |
---|
493 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/> |
---|
494 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/> |
---|
495 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/> |
---|
496 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/> |
---|
497 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/> |
---|
498 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/> |
---|
499 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/> |
---|
500 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/> |
---|
501 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/> |
---|
502 | <w:LsdException Locked="false" Priority="19" QFormat="true" |
---|
503 | Name="Subtle Emphasis"/> |
---|
504 | <w:LsdException Locked="false" Priority="21" QFormat="true" |
---|
505 | Name="Intense Emphasis"/> |
---|
506 | <w:LsdException Locked="false" Priority="31" QFormat="true" |
---|
507 | Name="Subtle Reference"/> |
---|
508 | <w:LsdException Locked="false" Priority="32" QFormat="true" |
---|
509 | Name="Intense Reference"/> |
---|
510 | <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/> |
---|
511 | <w:LsdException Locked="false" Priority="37" SemiHidden="true" |
---|
512 | UnhideWhenUsed="true" Name="Bibliography"/> |
---|
513 | <w:LsdException Locked="false" Priority="39" SemiHidden="true" |
---|
514 | UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/> |
---|
515 | <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/> |
---|
516 | <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/> |
---|
517 | <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/> |
---|
518 | <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/> |
---|
519 | <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/> |
---|
520 | <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/> |
---|
521 | <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/> |
---|
522 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/> |
---|
523 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/> |
---|
524 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/> |
---|
525 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/> |
---|
526 | <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/> |
---|
527 | <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/> |
---|
528 | <w:LsdException Locked="false" Priority="46" |
---|
529 | Name="Grid Table 1 Light Accent 1"/> |
---|
530 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/> |
---|
531 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/> |
---|
532 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/> |
---|
533 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/> |
---|
534 | <w:LsdException Locked="false" Priority="51" |
---|
535 | Name="Grid Table 6 Colorful Accent 1"/> |
---|
536 | <w:LsdException Locked="false" Priority="52" |
---|
537 | Name="Grid Table 7 Colorful Accent 1"/> |
---|
538 | <w:LsdException Locked="false" Priority="46" |
---|
539 | Name="Grid Table 1 Light Accent 2"/> |
---|
540 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/> |
---|
541 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/> |
---|
542 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/> |
---|
543 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/> |
---|
544 | <w:LsdException Locked="false" Priority="51" |
---|
545 | Name="Grid Table 6 Colorful Accent 2"/> |
---|
546 | <w:LsdException Locked="false" Priority="52" |
---|
547 | Name="Grid Table 7 Colorful Accent 2"/> |
---|
548 | <w:LsdException Locked="false" Priority="46" |
---|
549 | Name="Grid Table 1 Light Accent 3"/> |
---|
550 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/> |
---|
551 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/> |
---|
552 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/> |
---|
553 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/> |
---|
554 | <w:LsdException Locked="false" Priority="51" |
---|
555 | Name="Grid Table 6 Colorful Accent 3"/> |
---|
556 | <w:LsdException Locked="false" Priority="52" |
---|
557 | Name="Grid Table 7 Colorful Accent 3"/> |
---|
558 | <w:LsdException Locked="false" Priority="46" |
---|
559 | Name="Grid Table 1 Light Accent 4"/> |
---|
560 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/> |
---|
561 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/> |
---|
562 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/> |
---|
563 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/> |
---|
564 | <w:LsdException Locked="false" Priority="51" |
---|
565 | Name="Grid Table 6 Colorful Accent 4"/> |
---|
566 | <w:LsdException Locked="false" Priority="52" |
---|
567 | Name="Grid Table 7 Colorful Accent 4"/> |
---|
568 | <w:LsdException Locked="false" Priority="46" |
---|
569 | Name="Grid Table 1 Light Accent 5"/> |
---|
570 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/> |
---|
571 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/> |
---|
572 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/> |
---|
573 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/> |
---|
574 | <w:LsdException Locked="false" Priority="51" |
---|
575 | Name="Grid Table 6 Colorful Accent 5"/> |
---|
576 | <w:LsdException Locked="false" Priority="52" |
---|
577 | Name="Grid Table 7 Colorful Accent 5"/> |
---|
578 | <w:LsdException Locked="false" Priority="46" |
---|
579 | Name="Grid Table 1 Light Accent 6"/> |
---|
580 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/> |
---|
581 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/> |
---|
582 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/> |
---|
583 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/> |
---|
584 | <w:LsdException Locked="false" Priority="51" |
---|
585 | Name="Grid Table 6 Colorful Accent 6"/> |
---|
586 | <w:LsdException Locked="false" Priority="52" |
---|
587 | Name="Grid Table 7 Colorful Accent 6"/> |
---|
588 | <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/> |
---|
589 | <w:LsdException Locked="false" Priority="47" Name="List Table 2"/> |
---|
590 | <w:LsdException Locked="false" Priority="48" Name="List Table 3"/> |
---|
591 | <w:LsdException Locked="false" Priority="49" Name="List Table 4"/> |
---|
592 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/> |
---|
593 | <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/> |
---|
594 | <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/> |
---|
595 | <w:LsdException Locked="false" Priority="46" |
---|
596 | Name="List Table 1 Light Accent 1"/> |
---|
597 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/> |
---|
598 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/> |
---|
599 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/> |
---|
600 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/> |
---|
601 | <w:LsdException Locked="false" Priority="51" |
---|
602 | Name="List Table 6 Colorful Accent 1"/> |
---|
603 | <w:LsdException Locked="false" Priority="52" |
---|
604 | Name="List Table 7 Colorful Accent 1"/> |
---|
605 | <w:LsdException Locked="false" Priority="46" |
---|
606 | Name="List Table 1 Light Accent 2"/> |
---|
607 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/> |
---|
608 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/> |
---|
609 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/> |
---|
610 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/> |
---|
611 | <w:LsdException Locked="false" Priority="51" |
---|
612 | Name="List Table 6 Colorful Accent 2"/> |
---|
613 | <w:LsdException Locked="false" Priority="52" |
---|
614 | Name="List Table 7 Colorful Accent 2"/> |
---|
615 | <w:LsdException Locked="false" Priority="46" |
---|
616 | Name="List Table 1 Light Accent 3"/> |
---|
617 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/> |
---|
618 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/> |
---|
619 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/> |
---|
620 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/> |
---|
621 | <w:LsdException Locked="false" Priority="51" |
---|
622 | Name="List Table 6 Colorful Accent 3"/> |
---|
623 | <w:LsdException Locked="false" Priority="52" |
---|
624 | Name="List Table 7 Colorful Accent 3"/> |
---|
625 | <w:LsdException Locked="false" Priority="46" |
---|
626 | Name="List Table 1 Light Accent 4"/> |
---|
627 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/> |
---|
628 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/> |
---|
629 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/> |
---|
630 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/> |
---|
631 | <w:LsdException Locked="false" Priority="51" |
---|
632 | Name="List Table 6 Colorful Accent 4"/> |
---|
633 | <w:LsdException Locked="false" Priority="52" |
---|
634 | Name="List Table 7 Colorful Accent 4"/> |
---|
635 | <w:LsdException Locked="false" Priority="46" |
---|
636 | Name="List Table 1 Light Accent 5"/> |
---|
637 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/> |
---|
638 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/> |
---|
639 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/> |
---|
640 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/> |
---|
641 | <w:LsdException Locked="false" Priority="51" |
---|
642 | Name="List Table 6 Colorful Accent 5"/> |
---|
643 | <w:LsdException Locked="false" Priority="52" |
---|
644 | Name="List Table 7 Colorful Accent 5"/> |
---|
645 | <w:LsdException Locked="false" Priority="46" |
---|
646 | Name="List Table 1 Light Accent 6"/> |
---|
647 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/> |
---|
648 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/> |
---|
649 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/> |
---|
650 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/> |
---|
651 | <w:LsdException Locked="false" Priority="51" |
---|
652 | Name="List Table 6 Colorful Accent 6"/> |
---|
653 | <w:LsdException Locked="false" Priority="52" |
---|
654 | Name="List Table 7 Colorful Accent 6"/> |
---|
655 | </w:LatentStyles> |
---|
656 | </xml><![endif]--> |
---|
657 | <style> |
---|
658 | <!-- |
---|
659 | /* Font Definitions */ |
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660 | @font-face |
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661 | {font-family:"Cambria Math"; |
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662 | panose-1:2 4 5 3 5 4 6 3 2 4; |
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663 | mso-font-charset:1; |
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664 | mso-generic-font-family:roman; |
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665 | mso-font-pitch:variable; |
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666 | mso-font-signature:0 0 0 0 0 0;} |
---|
667 | @font-face |
---|
668 | {font-family:Calibri; |
---|
669 | panose-1:2 15 5 2 2 2 4 3 2 4; |
---|
670 | mso-font-charset:0; |
---|
671 | mso-generic-font-family:swiss; |
---|
672 | mso-font-pitch:variable; |
---|
673 | mso-font-signature:-536870145 1073786111 1 0 415 0;} |
---|
674 | @font-face |
---|
675 | {font-family:Tahoma; |
---|
676 | panose-1:2 11 6 4 3 5 4 4 2 4; |
---|
677 | mso-font-charset:0; |
---|
678 | mso-generic-font-family:swiss; |
---|
679 | mso-font-pitch:variable; |
---|
680 | mso-font-signature:-520081665 -1073717157 41 0 66047 0;} |
---|
681 | /* Style Definitions */ |
---|
682 | p.MsoNormal, li.MsoNormal, div.MsoNormal |
---|
683 | {mso-style-unhide:no; |
---|
684 | mso-style-qformat:yes; |
---|
685 | mso-style-parent:""; |
---|
686 | margin:0in; |
---|
687 | margin-bottom:.0001pt; |
---|
688 | mso-pagination:widow-orphan; |
---|
689 | font-size:12.0pt; |
---|
690 | font-family:"Times New Roman",serif; |
---|
691 | mso-fareast-font-family:"Times New Roman"; |
---|
692 | mso-fareast-theme-font:minor-fareast;} |
---|
693 | h1 |
---|
694 | {mso-style-priority:9; |
---|
695 | mso-style-unhide:no; |
---|
696 | mso-style-qformat:yes; |
---|
697 | mso-style-link:"Heading 1 Char"; |
---|
698 | mso-margin-top-alt:auto; |
---|
699 | margin-right:0in; |
---|
700 | mso-margin-bottom-alt:auto; |
---|
701 | margin-left:0in; |
---|
702 | mso-pagination:widow-orphan; |
---|
703 | mso-outline-level:1; |
---|
704 | font-size:24.0pt; |
---|
705 | font-family:"Times New Roman",serif; |
---|
706 | mso-fareast-font-family:"Times New Roman"; |
---|
707 | mso-fareast-theme-font:minor-fareast; |
---|
708 | font-weight:bold;} |
---|
709 | h2 |
---|
710 | {mso-style-noshow:yes; |
---|
711 | mso-style-priority:9; |
---|
712 | mso-style-qformat:yes; |
---|
713 | mso-style-link:"Heading 2 Char"; |
---|
714 | mso-margin-top-alt:auto; |
---|
715 | margin-right:0in; |
---|
716 | mso-margin-bottom-alt:auto; |
---|
717 | margin-left:0in; |
---|
718 | mso-pagination:widow-orphan; |
---|
719 | mso-outline-level:2; |
---|
720 | font-size:18.0pt; |
---|
721 | font-family:"Times New Roman",serif; |
---|
722 | mso-fareast-font-family:"Times New Roman"; |
---|
723 | mso-fareast-theme-font:minor-fareast; |
---|
724 | font-weight:bold;} |
---|
725 | h3 |
---|
726 | {mso-style-noshow:yes; |
---|
727 | mso-style-priority:9; |
---|
728 | mso-style-qformat:yes; |
---|
729 | mso-style-link:"Heading 3 Char"; |
---|
730 | mso-margin-top-alt:auto; |
---|
731 | margin-right:0in; |
---|
732 | mso-margin-bottom-alt:auto; |
---|
733 | margin-left:0in; |
---|
734 | mso-pagination:widow-orphan; |
---|
735 | mso-outline-level:3; |
---|
736 | font-size:13.5pt; |
---|
737 | font-family:"Times New Roman",serif; |
---|
738 | mso-fareast-font-family:"Times New Roman"; |
---|
739 | mso-fareast-theme-font:minor-fareast; |
---|
740 | font-weight:bold;} |
---|
741 | h4 |
---|
742 | {mso-style-noshow:yes; |
---|
743 | mso-style-priority:9; |
---|
744 | mso-style-qformat:yes; |
---|
745 | mso-style-link:"Heading 4 Char"; |
---|
746 | mso-style-next:Normal; |
---|
747 | margin-top:10.0pt; |
---|
748 | margin-right:0in; |
---|
749 | margin-bottom:0in; |
---|
750 | margin-left:0in; |
---|
751 | margin-bottom:.0001pt; |
---|
752 | mso-pagination:widow-orphan lines-together; |
---|
753 | page-break-after:avoid; |
---|
754 | mso-outline-level:4; |
---|
755 | font-size:13.0pt; |
---|
756 | font-family:"Cambria",serif; |
---|
757 | mso-ascii-font-family:Cambria; |
---|
758 | mso-ascii-theme-font:major-latin; |
---|
759 | mso-fareast-font-family:"Times New Roman"; |
---|
760 | mso-fareast-theme-font:major-fareast; |
---|
761 | mso-hansi-font-family:Cambria; |
---|
762 | mso-hansi-theme-font:major-latin; |
---|
763 | mso-bidi-font-family:"Times New Roman"; |
---|
764 | mso-bidi-theme-font:major-bidi; |
---|
765 | color:#4F81BD; |
---|
766 | mso-themecolor:accent1; |
---|
767 | font-weight:bold; |
---|
768 | font-style:italic;} |
---|
769 | h5 |
---|
770 | {mso-style-noshow:yes; |
---|
771 | mso-style-priority:9; |
---|
772 | mso-style-qformat:yes; |
---|
773 | mso-style-link:"Heading 5 Char"; |
---|
774 | mso-margin-top-alt:auto; |
---|
775 | margin-right:0in; |
---|
776 | mso-margin-bottom-alt:auto; |
---|
777 | margin-left:0in; |
---|
778 | mso-pagination:widow-orphan; |
---|
779 | mso-outline-level:5; |
---|
780 | font-size:12.0pt; |
---|
781 | font-family:"Times New Roman",serif; |
---|
782 | mso-fareast-font-family:"Times New Roman"; |
---|
783 | mso-fareast-theme-font:minor-fareast; |
---|
784 | color:#4F4FFF; |
---|
785 | font-weight:bold;} |
---|
786 | a:link, span.MsoHyperlink |
---|
787 | {mso-style-noshow:yes; |
---|
788 | mso-style-priority:99; |
---|
789 | color:blue; |
---|
790 | text-decoration:underline; |
---|
791 | text-underline:single;} |
---|
792 | a:visited, span.MsoHyperlinkFollowed |
---|
793 | {mso-style-noshow:yes; |
---|
794 | mso-style-priority:99; |
---|
795 | color:purple; |
---|
796 | text-decoration:underline; |
---|
797 | text-underline:single;} |
---|
798 | p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap |
---|
799 | {mso-style-noshow:yes; |
---|
800 | mso-style-priority:99; |
---|
801 | mso-style-link:"Document Map Char"; |
---|
802 | margin:0in; |
---|
803 | margin-bottom:.0001pt; |
---|
804 | mso-pagination:widow-orphan; |
---|
805 | font-size:8.0pt; |
---|
806 | font-family:"Tahoma",sans-serif; |
---|
807 | mso-fareast-font-family:"Times New Roman"; |
---|
808 | mso-fareast-theme-font:minor-fareast;} |
---|
809 | p |
---|
810 | {mso-style-noshow:yes; |
---|
811 | mso-style-priority:99; |
---|
812 | mso-margin-top-alt:auto; |
---|
813 | margin-right:0in; |
---|
814 | mso-margin-bottom-alt:auto; |
---|
815 | margin-left:0in; |
---|
816 | mso-pagination:widow-orphan; |
---|
817 | font-size:12.0pt; |
---|
818 | font-family:"Times New Roman",serif; |
---|
819 | mso-fareast-font-family:"Times New Roman"; |
---|
820 | mso-fareast-theme-font:minor-fareast;} |
---|
821 | pre |
---|
822 | {mso-style-noshow:yes; |
---|
823 | mso-style-priority:99; |
---|
824 | mso-style-link:"HTML Preformatted Char"; |
---|
825 | margin:0in; |
---|
826 | margin-bottom:.0001pt; |
---|
827 | mso-pagination:widow-orphan; |
---|
828 | tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt; |
---|
829 | font-size:10.0pt; |
---|
830 | font-family:"Courier New"; |
---|
831 | mso-fareast-font-family:"Times New Roman";} |
---|
832 | p.MsoAcetate, li.MsoAcetate, div.MsoAcetate |
---|
833 | {mso-style-noshow:yes; |
---|
834 | mso-style-priority:99; |
---|
835 | mso-style-link:"Balloon Text Char"; |
---|
836 | margin:0in; |
---|
837 | margin-bottom:.0001pt; |
---|
838 | mso-pagination:widow-orphan; |
---|
839 | font-size:8.0pt; |
---|
840 | font-family:"Tahoma",sans-serif; |
---|
841 | mso-fareast-font-family:"Times New Roman"; |
---|
842 | mso-fareast-theme-font:minor-fareast;} |
---|
843 | span.MsoPlaceholderText |
---|
844 | {mso-style-noshow:yes; |
---|
845 | mso-style-priority:99; |
---|
846 | mso-style-unhide:no; |
---|
847 | color:gray;} |
---|
848 | p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing |
---|
849 | {mso-style-noshow:yes; |
---|
850 | mso-style-priority:1; |
---|
851 | mso-style-unhide:no; |
---|
852 | mso-style-qformat:yes; |
---|
853 | mso-style-parent:""; |
---|
854 | margin:0in; |
---|
855 | margin-bottom:.0001pt; |
---|
856 | mso-pagination:widow-orphan; |
---|
857 | font-size:12.0pt; |
---|
858 | font-family:"Times New Roman",serif; |
---|
859 | mso-fareast-font-family:"Times New Roman"; |
---|
860 | mso-fareast-theme-font:minor-fareast;} |
---|
861 | p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph |
---|
862 | {mso-style-noshow:yes; |
---|
863 | mso-style-priority:34; |
---|
864 | mso-style-unhide:no; |
---|
865 | mso-style-qformat:yes; |
---|
866 | margin-top:0in; |
---|
867 | margin-right:0in; |
---|
868 | margin-bottom:0in; |
---|
869 | margin-left:.5in; |
---|
870 | margin-bottom:.0001pt; |
---|
871 | mso-add-space:auto; |
---|
872 | mso-pagination:widow-orphan; |
---|
873 | font-size:12.0pt; |
---|
874 | font-family:"Times New Roman",serif; |
---|
875 | mso-fareast-font-family:"Times New Roman"; |
---|
876 | mso-fareast-theme-font:minor-fareast;} |
---|
877 | p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst |
---|
878 | {mso-style-noshow:yes; |
---|
879 | mso-style-priority:34; |
---|
880 | mso-style-unhide:no; |
---|
881 | mso-style-qformat:yes; |
---|
882 | mso-style-type:export-only; |
---|
883 | margin-top:0in; |
---|
884 | margin-right:0in; |
---|
885 | margin-bottom:0in; |
---|
886 | margin-left:.5in; |
---|
887 | margin-bottom:.0001pt; |
---|
888 | mso-add-space:auto; |
---|
889 | mso-pagination:widow-orphan; |
---|
890 | font-size:12.0pt; |
---|
891 | font-family:"Times New Roman",serif; |
---|
892 | mso-fareast-font-family:"Times New Roman"; |
---|
893 | mso-fareast-theme-font:minor-fareast;} |
---|
894 | p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle |
---|
895 | {mso-style-noshow:yes; |
---|
896 | mso-style-priority:34; |
---|
897 | mso-style-unhide:no; |
---|
898 | mso-style-qformat:yes; |
---|
899 | mso-style-type:export-only; |
---|
900 | margin-top:0in; |
---|
901 | margin-right:0in; |
---|
902 | margin-bottom:0in; |
---|
903 | margin-left:.5in; |
---|
904 | margin-bottom:.0001pt; |
---|
905 | mso-add-space:auto; |
---|
906 | mso-pagination:widow-orphan; |
---|
907 | font-size:12.0pt; |
---|
908 | font-family:"Times New Roman",serif; |
---|
909 | mso-fareast-font-family:"Times New Roman"; |
---|
910 | mso-fareast-theme-font:minor-fareast;} |
---|
911 | p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast |
---|
912 | {mso-style-noshow:yes; |
---|
913 | mso-style-priority:34; |
---|
914 | mso-style-unhide:no; |
---|
915 | mso-style-qformat:yes; |
---|
916 | mso-style-type:export-only; |
---|
917 | margin-top:0in; |
---|
918 | margin-right:0in; |
---|
919 | margin-bottom:0in; |
---|
920 | margin-left:.5in; |
---|
921 | margin-bottom:.0001pt; |
---|
922 | mso-add-space:auto; |
---|
923 | mso-pagination:widow-orphan; |
---|
924 | font-size:12.0pt; |
---|
925 | font-family:"Times New Roman",serif; |
---|
926 | mso-fareast-font-family:"Times New Roman"; |
---|
927 | mso-fareast-theme-font:minor-fareast;} |
---|
928 | span.MsoIntenseReference |
---|
929 | {mso-style-priority:32; |
---|
930 | mso-style-unhide:no; |
---|
931 | mso-style-qformat:yes; |
---|
932 | font-variant:small-caps; |
---|
933 | color:#C0504D; |
---|
934 | mso-themecolor:accent2; |
---|
935 | letter-spacing:.25pt; |
---|
936 | font-weight:bold; |
---|
937 | text-decoration:underline; |
---|
938 | text-underline:single;} |
---|
939 | span.Heading1Char |
---|
940 | {mso-style-name:"Heading 1 Char"; |
---|
941 | mso-style-priority:9; |
---|
942 | mso-style-unhide:no; |
---|
943 | mso-style-locked:yes; |
---|
944 | mso-style-link:"Heading 1"; |
---|
945 | mso-ansi-font-size:24.0pt; |
---|
946 | mso-bidi-font-size:24.0pt; |
---|
947 | font-family:"Times New Roman",serif; |
---|
948 | mso-ascii-font-family:"Times New Roman"; |
---|
949 | mso-fareast-font-family:"Times New Roman"; |
---|
950 | mso-fareast-theme-font:minor-fareast; |
---|
951 | mso-hansi-font-family:"Times New Roman"; |
---|
952 | mso-bidi-font-family:"Times New Roman"; |
---|
953 | mso-font-kerning:18.0pt; |
---|
954 | font-weight:bold;} |
---|
955 | span.Heading2Char |
---|
956 | {mso-style-name:"Heading 2 Char"; |
---|
957 | mso-style-noshow:yes; |
---|
958 | mso-style-priority:9; |
---|
959 | mso-style-unhide:no; |
---|
960 | mso-style-locked:yes; |
---|
961 | mso-style-link:"Heading 2"; |
---|
962 | mso-ansi-font-size:18.0pt; |
---|
963 | mso-bidi-font-size:18.0pt; |
---|
964 | font-family:"Times New Roman",serif; |
---|
965 | mso-ascii-font-family:"Times New Roman"; |
---|
966 | mso-fareast-font-family:"Times New Roman"; |
---|
967 | mso-fareast-theme-font:minor-fareast; |
---|
968 | mso-hansi-font-family:"Times New Roman"; |
---|
969 | mso-bidi-font-family:"Times New Roman"; |
---|
970 | font-weight:bold;} |
---|
971 | span.Heading3Char |
---|
972 | {mso-style-name:"Heading 3 Char"; |
---|
973 | mso-style-noshow:yes; |
---|
974 | mso-style-priority:9; |
---|
975 | mso-style-unhide:no; |
---|
976 | mso-style-locked:yes; |
---|
977 | mso-style-link:"Heading 3"; |
---|
978 | mso-ansi-font-size:13.5pt; |
---|
979 | mso-bidi-font-size:13.5pt; |
---|
980 | font-family:"Times New Roman",serif; |
---|
981 | mso-ascii-font-family:"Times New Roman"; |
---|
982 | mso-fareast-font-family:"Times New Roman"; |
---|
983 | mso-fareast-theme-font:minor-fareast; |
---|
984 | mso-hansi-font-family:"Times New Roman"; |
---|
985 | mso-bidi-font-family:"Times New Roman"; |
---|
986 | font-weight:bold;} |
---|
987 | span.Heading4Char |
---|
988 | {mso-style-name:"Heading 4 Char"; |
---|
989 | mso-style-noshow:yes; |
---|
990 | mso-style-priority:9; |
---|
991 | mso-style-unhide:no; |
---|
992 | mso-style-locked:yes; |
---|
993 | mso-style-link:"Heading 4"; |
---|
994 | mso-ansi-font-size:13.0pt; |
---|
995 | mso-bidi-font-size:13.0pt; |
---|
996 | font-family:"Cambria",serif; |
---|
997 | mso-ascii-font-family:Cambria; |
---|
998 | mso-ascii-theme-font:major-latin; |
---|
999 | mso-fareast-font-family:"Times New Roman"; |
---|
1000 | mso-fareast-theme-font:major-fareast; |
---|
1001 | mso-hansi-font-family:Cambria; |
---|
1002 | mso-hansi-theme-font:major-latin; |
---|
1003 | mso-bidi-font-family:"Times New Roman"; |
---|
1004 | mso-bidi-theme-font:major-bidi; |
---|
1005 | color:#4F81BD; |
---|
1006 | mso-themecolor:accent1; |
---|
1007 | font-weight:bold; |
---|
1008 | font-style:italic;} |
---|
1009 | span.Heading5Char |
---|
1010 | {mso-style-name:"Heading 5 Char"; |
---|
1011 | mso-style-noshow:yes; |
---|
1012 | mso-style-priority:9; |
---|
1013 | mso-style-unhide:no; |
---|
1014 | mso-style-locked:yes; |
---|
1015 | mso-style-link:"Heading 5"; |
---|
1016 | mso-ansi-font-size:12.0pt; |
---|
1017 | mso-bidi-font-size:12.0pt; |
---|
1018 | font-family:"Times New Roman",serif; |
---|
1019 | mso-ascii-font-family:"Times New Roman"; |
---|
1020 | mso-fareast-font-family:"Times New Roman"; |
---|
1021 | mso-fareast-theme-font:minor-fareast; |
---|
1022 | mso-hansi-font-family:"Times New Roman"; |
---|
1023 | mso-bidi-font-family:"Times New Roman"; |
---|
1024 | color:#4F4FFF; |
---|
1025 | font-weight:bold;} |
---|
1026 | span.HTMLPreformattedChar |
---|
1027 | {mso-style-name:"HTML Preformatted Char"; |
---|
1028 | mso-style-noshow:yes; |
---|
1029 | mso-style-priority:99; |
---|
1030 | mso-style-unhide:no; |
---|
1031 | mso-style-locked:yes; |
---|
1032 | mso-style-link:"HTML Preformatted"; |
---|
1033 | font-family:"Courier New"; |
---|
1034 | mso-ascii-font-family:"Courier New"; |
---|
1035 | mso-fareast-font-family:"Times New Roman"; |
---|
1036 | mso-hansi-font-family:"Courier New"; |
---|
1037 | mso-bidi-font-family:"Courier New";} |
---|
1038 | p.msonormal0, li.msonormal0, div.msonormal0 |
---|
1039 | {mso-style-name:msonormal; |
---|
1040 | mso-style-noshow:yes; |
---|
1041 | mso-style-priority:99; |
---|
1042 | mso-style-unhide:no; |
---|
1043 | mso-margin-top-alt:auto; |
---|
1044 | margin-right:0in; |
---|
1045 | mso-margin-bottom-alt:auto; |
---|
1046 | margin-left:0in; |
---|
1047 | mso-pagination:widow-orphan; |
---|
1048 | font-size:12.0pt; |
---|
1049 | font-family:"Times New Roman",serif; |
---|
1050 | mso-fareast-font-family:"Times New Roman"; |
---|
1051 | mso-fareast-theme-font:minor-fareast;} |
---|
1052 | span.DocumentMapChar |
---|
1053 | {mso-style-name:"Document Map Char"; |
---|
1054 | mso-style-noshow:yes; |
---|
1055 | mso-style-priority:99; |
---|
1056 | mso-style-unhide:no; |
---|
1057 | mso-style-locked:yes; |
---|
1058 | mso-style-link:"Document Map"; |
---|
1059 | mso-ansi-font-size:8.0pt; |
---|
1060 | mso-bidi-font-size:8.0pt; |
---|
1061 | font-family:"Tahoma",sans-serif; |
---|
1062 | mso-ascii-font-family:Tahoma; |
---|
1063 | mso-fareast-font-family:"Times New Roman"; |
---|
1064 | mso-fareast-theme-font:minor-fareast; |
---|
1065 | mso-hansi-font-family:Tahoma; |
---|
1066 | mso-bidi-font-family:Tahoma;} |
---|
1067 | span.BalloonTextChar |
---|
1068 | {mso-style-name:"Balloon Text Char"; |
---|
1069 | mso-style-noshow:yes; |
---|
1070 | mso-style-priority:99; |
---|
1071 | mso-style-unhide:no; |
---|
1072 | mso-style-locked:yes; |
---|
1073 | mso-style-link:"Balloon Text"; |
---|
1074 | mso-ansi-font-size:8.0pt; |
---|
1075 | mso-bidi-font-size:8.0pt; |
---|
1076 | font-family:"Tahoma",sans-serif; |
---|
1077 | mso-ascii-font-family:Tahoma; |
---|
1078 | mso-fareast-font-family:"Times New Roman"; |
---|
1079 | mso-fareast-theme-font:minor-fareast; |
---|
1080 | mso-hansi-font-family:Tahoma; |
---|
1081 | mso-bidi-font-family:Tahoma;} |
---|
1082 | span.SpellE |
---|
1083 | {mso-style-name:""; |
---|
1084 | mso-spl-e:yes;} |
---|
1085 | span.GramE |
---|
1086 | {mso-style-name:""; |
---|
1087 | mso-gram-e:yes;} |
---|
1088 | .MsoChpDefault |
---|
1089 | {mso-style-type:export-only; |
---|
1090 | mso-default-props:yes; |
---|
1091 | font-size:10.0pt; |
---|
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1097 | mso-fareast-font-family:Calibri; |
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1098 | mso-fareast-theme-font:minor-latin; |
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1099 | mso-hansi-font-family:Calibri; |
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1100 | mso-hansi-theme-font:minor-latin; |
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1109 | div.WordSection1 |
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1110 | {page:WordSection1;} |
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1111 | --> |
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1112 | </style> |
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1113 | <!--[if gte mso 10]> |
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1114 | <style> |
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1115 | /* Style Definitions */ |
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1116 | table.MsoNormalTable |
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1117 | {mso-style-name:"Table Normal"; |
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1118 | mso-tstyle-rowband-size:0; |
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1119 | mso-tstyle-colband-size:0; |
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1120 | mso-style-noshow:yes; |
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1121 | mso-style-priority:99; |
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1122 | mso-style-parent:""; |
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1123 | mso-padding-alt:0in 5.4pt 0in 5.4pt; |
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1124 | mso-para-margin:0in; |
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1125 | mso-para-margin-bottom:.0001pt; |
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1128 | font-family:"Calibri",sans-serif; |
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1129 | mso-ascii-font-family:Calibri; |
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1130 | mso-ascii-theme-font:minor-latin; |
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1131 | mso-hansi-font-family:Calibri; |
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1132 | mso-hansi-theme-font:minor-latin;} |
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1133 | table.MsoTableGrid |
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1134 | {mso-style-name:"Table Grid"; |
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1146 | mso-pagination:widow-orphan; |
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1149 | mso-ascii-font-family:Calibri; |
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1150 | mso-ascii-theme-font:minor-latin; |
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1151 | mso-hansi-font-family:Calibri; |
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1152 | mso-hansi-theme-font:minor-latin;} |
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1153 | </style> |
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1154 | <![endif]--><!--[if gte mso 9]><xml> |
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1155 | <o:shapedefaults v:ext="edit" spidmax="1027"/> |
---|
1156 | </xml><![endif]--><!--[if gte mso 9]><xml> |
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1157 | <o:shapelayout v:ext="edit"> |
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1158 | <o:idmap v:ext="edit" data="1"/> |
---|
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1160 | <o:r id="V:Rule1" type="connector" idref="#Straight_x0020_Arrow_x0020_Connector_x0020_21"/> |
---|
1161 | </o:rules> |
---|
1162 | </o:shapelayout></xml><![endif]--> |
---|
1163 | </head> |
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1164 | |
---|
1165 | <body lang=EN-US link=blue vlink=purple style='tab-interval:.5in'> |
---|
1166 | |
---|
1167 | <div class=WordSection1> |
---|
1168 | |
---|
1169 | <h1><strong>Small Angle X-Ray Data Image Processing<o:p></o:p></strong></h1> |
---|
1170 | |
---|
1171 | <p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In |
---|
1172 | this tutorial you will reduce 2D SAXS data to create 1D absolute scaled data. |
---|
1173 | The data were collected at APS on beam line 15ID on some polymer base materials |
---|
1174 | to be used for liquid crystal displays. The processing has several steps |
---|
1175 | including detector calibration (i.e. determine sample-detector distance & |
---|
1176 | tilt), integration and scaling to an absolute scaled glassy carbon measurement. |
---|
1177 | The data were collected at a wavelength of 1.0332Å with a <span class=SpellE>MarCCD</span> |
---|
1178 | detector placed ~570mm from the sample. Note that menu entries are listed in |
---|
1179 | bold face below as <b style='mso-bidi-font-weight:normal'><span |
---|
1180 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1181 | mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font: |
---|
1182 | minor-latin'>Help/About GSAS-II</span></b>, which lists first the name of the |
---|
1183 | menu (here <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1184 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1185 | minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Help</span></b>) |
---|
1186 | and second the name of the entry in the menu (here <b style='mso-bidi-font-weight: |
---|
1187 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1188 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri; |
---|
1189 | mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).<span |
---|
1190 | style='mso-spacerun:yes'> </span><span style='mso-fareast-font-family:Calibri; |
---|
1191 | mso-fareast-theme-font:minor-latin;mso-bidi-font-weight:bold;mso-bidi-font-style: |
---|
1192 | italic'><o:p></o:p></span></p> |
---|
1193 | |
---|
1194 | <p class=MsoNormal>If you have not done so already, start GSAS-II.</p> |
---|
1195 | |
---|
1196 | <h2>Step 1: Detector calibration</h2> |
---|
1197 | |
---|
1198 | <p class=MsoNormal>The detector position is determined by using an image |
---|
1199 | collected from silver <span class=SpellE>behenate</span>; do <b |
---|
1200 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1201 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Data/Read |
---|
1202 | Image data
</span></b> and a file selection dialog box will appear. Go to <span |
---|
1203 | class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1204 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1205 | minor-latin'>SAimages</span></b></span><b style='mso-bidi-font-weight:normal'><span |
---|
1206 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1207 | mso-hansi-theme-font:minor-latin'>/data</span></b> and select <b |
---|
1208 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1209 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>AgBehenate_003.tif</span></b> |
---|
1210 | with either a mouse button double click or <b style='mso-bidi-font-weight:normal'><span |
---|
1211 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1212 | mso-hansi-theme-font:minor-latin'>Open</span></b>; the image will appear</p> |
---|
1213 | |
---|
1214 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype |
---|
1215 | id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t" |
---|
1216 | path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f"> |
---|
1217 | <v:stroke joinstyle="miter"/> |
---|
1218 | <v:formulas> |
---|
1219 | <v:f eqn="if lineDrawn pixelLineWidth 0"/> |
---|
1220 | <v:f eqn="sum @0 1 0"/> |
---|
1221 | <v:f eqn="sum 0 0 @1"/> |
---|
1222 | <v:f eqn="prod @2 1 2"/> |
---|
1223 | <v:f eqn="prod @3 21600 pixelWidth"/> |
---|
1224 | <v:f eqn="prod @3 21600 pixelHeight"/> |
---|
1225 | <v:f eqn="sum @0 0 1"/> |
---|
1226 | <v:f eqn="prod @6 1 2"/> |
---|
1227 | <v:f eqn="prod @7 21600 pixelWidth"/> |
---|
1228 | <v:f eqn="sum @8 21600 0"/> |
---|
1229 | <v:f eqn="prod @7 21600 pixelHeight"/> |
---|
1230 | <v:f eqn="sum @10 21600 0"/> |
---|
1231 | </v:formulas> |
---|
1232 | <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/> |
---|
1233 | <o:lock v:ext="edit" aspectratio="t"/> |
---|
1234 | </v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1062" type="#_x0000_t75" |
---|
1235 | style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1236 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image001.png" |
---|
1237 | o:title=""/> |
---|
1238 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1239 | src="Small%20Angle%20Image%20Processing_files/image001.png" v:shapes="Picture_x0020_1"><![endif]></span></p> |
---|
1240 | |
---|
1241 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1242 | |
---|
1243 | <p class=MsoNormal>And the <b style='mso-bidi-font-weight:normal'><span |
---|
1244 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1245 | mso-hansi-theme-font:minor-latin'>Image controls</span></b> window will show</p> |
---|
1246 | |
---|
1247 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1248 | id="Picture_x0020_2" o:spid="_x0000_i1061" type="#_x0000_t75" style='width:472.5pt; |
---|
1249 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1250 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image002.png" |
---|
1251 | o:title=""/> |
---|
1252 | </v:shape><![endif]--><![if !vml]><img width=630 height=518 |
---|
1253 | src="Small%20Angle%20Image%20Processing_files/image002.png" v:shapes="Picture_x0020_2"><![endif]></span></p> |
---|
1254 | |
---|
1255 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1256 | |
---|
1257 | <p class=MsoNormal>Note the default <b style='mso-bidi-font-weight:normal'><span |
---|
1258 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1259 | mso-hansi-theme-font:minor-latin'>Type of image data</span></b> is <b |
---|
1260 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1261 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>PWDR - |
---|
1262 | powder diffraction data</span></b>; you will change that <span |
---|
1263 | style='mso-no-proof:yes'>now.</span> Select <b style='mso-bidi-font-weight: |
---|
1264 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1265 | minor-latin;mso-hansi-theme-font:minor-latin'>SASD small angle scattering |
---|
1266 | data</span></b> (the window will change). Enter the <b style='mso-bidi-font-weight: |
---|
1267 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1268 | minor-latin;mso-hansi-theme-font:minor-latin'>wavelength</span></b> (<b |
---|
1269 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1270 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1.0332</span></b>), |
---|
1271 | and select the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
---|
1272 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1273 | mso-hansi-theme-font:minor-latin'>Calibrant</span></b></span> (near bottom of |
---|
1274 | window) as <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1275 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1276 | minor-latin'>Ag <span class=SpellE>behenate</span></span></b>. Note that the |
---|
1277 | calibration info for Ag <span class=SpellE>behenate</span> was read from a |
---|
1278 | python file <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1279 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1280 | minor-latin'>GSASII/ImageCalibrants.py</span></b>. If you have a <span |
---|
1281 | class=SpellE>calibrant</span> that isnt in this file you should enter it in |
---|
1282 | the file <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1283 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>UserCalibrants.py</span></b>; |
---|
1284 | just follow the format of the examples within <b style='mso-bidi-font-weight: |
---|
1285 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1286 | minor-latin;mso-hansi-theme-font:minor-latin'>ImageCalibrants.py</span></b>. |
---|
1287 | You should move the <b style='mso-bidi-font-weight:normal'><span |
---|
1288 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1289 | mso-hansi-theme-font:minor-latin'>Max intensity</span></b> slider to near the |
---|
1290 | middle of the range that will improve the image. When done the <b |
---|
1291 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1292 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
---|
1293 | controls</span></b> window should look like</p> |
---|
1294 | |
---|
1295 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1296 | id="Picture_x0020_3" o:spid="_x0000_i1060" type="#_x0000_t75" style='width:472.5pt; |
---|
1297 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1298 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image003.png" |
---|
1299 | o:title=""/> |
---|
1300 | </v:shape><![endif]--><![if !vml]><img width=630 height=518 |
---|
1301 | src="Small%20Angle%20Image%20Processing_files/image003.png" v:shapes="Picture_x0020_3"><![endif]></span></p> |
---|
1302 | |
---|
1303 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1304 | |
---|
1305 | <p class=MsoNormal>And the image will be</p> |
---|
1306 | |
---|
1307 | <p class=MsoNormal><!--[if gte vml 1]><v:shapetype id="_x0000_t32" coordsize="21600,21600" |
---|
1308 | o:spt="32" o:oned="t" path="m,l21600,21600e" filled="f"> |
---|
1309 | <v:path arrowok="t" fillok="f" o:connecttype="none"/> |
---|
1310 | <o:lock v:ext="edit" shapetype="t"/> |
---|
1311 | </v:shapetype><v:shape id="Straight_x0020_Arrow_x0020_Connector_x0020_21" |
---|
1312 | o:spid="_x0000_s1026" type="#_x0000_t32" style='position:absolute; |
---|
1313 | margin-left:177pt;margin-top:214.5pt;width:48pt;height:15.75pt;flip:y; |
---|
1314 | z-index:251659264;visibility:visible;mso-wrap-style:square; |
---|
1315 | mso-width-percent:0;mso-height-percent:0;mso-wrap-distance-left:9pt; |
---|
1316 | mso-wrap-distance-top:0;mso-wrap-distance-right:9pt; |
---|
1317 | mso-wrap-distance-bottom:0;mso-position-horizontal:absolute; |
---|
1318 | mso-position-horizontal-relative:text;mso-position-vertical:absolute; |
---|
1319 | mso-position-vertical-relative:text;mso-width-percent:0;mso-height-percent:0; |
---|
1320 | mso-width-relative:page;mso-height-relative:page' o:gfxdata="UEsDBBQABgAIAAAAIQC2gziS/gAAAOEBAAATAAAAW0NvbnRlbnRfVHlwZXNdLnhtbJSRQU7DMBBF |
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1346 | c1BLAQItABQABgAIAAAAIQB9d1Df6wEAACkEAAAOAAAAAAAAAAAAAAAAAC4CAABkcnMvZTJvRG9j |
---|
1347 | LnhtbFBLAQItABQABgAIAAAAIQCB0qld3wAAAAsBAAAPAAAAAAAAAAAAAAAAAEUEAABkcnMvZG93 |
---|
1348 | bnJldi54bWxQSwUGAAAAAAQABADzAAAAUQUAAAAA |
---|
1349 | " strokecolor="#c0504d [3205]" strokeweight="3pt"> |
---|
1350 | <v:stroke endarrow="open"/> |
---|
1351 | <v:shadow on="t" color="black" opacity="22937f" origin=",.5" offset="0,.63889mm"/> |
---|
1352 | <o:lock v:ext="edit" shapetype="f"/> |
---|
1353 | </v:shape><![endif]--><![if !vml]><span style='mso-ignore:vglayout;position: |
---|
1354 | absolute;z-index:251659264;margin-left:234px;margin-top:273px;width:73px; |
---|
1355 | height:38px'><img width=73 height=38 |
---|
1356 | src="Small%20Angle%20Image%20Processing_files/image040.png" v:shapes="Straight_x0020_Arrow_x0020_Connector_x0020_21"></span><![endif]><span |
---|
1357 | style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_4" |
---|
1358 | o:spid="_x0000_i1059" type="#_x0000_t75" style='width:525pt;height:450pt; |
---|
1359 | visibility:visible;mso-wrap-style:square'> |
---|
1360 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image005.png" |
---|
1361 | o:title=""/> |
---|
1362 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1363 | src="Small%20Angle%20Image%20Processing_files/image005.png" v:shapes="Picture_x0020_4"><![endif]></span></p> |
---|
1364 | |
---|
1365 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1366 | |
---|
1367 | <p class=MsoNormal>Next select <b style='mso-bidi-font-weight:normal'><span |
---|
1368 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1369 | mso-hansi-theme-font:minor-latin'>Operations/Calibrate</span></b> from the <b |
---|
1370 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1371 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
---|
1372 | Controls</span></b> menu; a bit of instruction will appear on the status line |
---|
1373 | of this window. Select 5 points on the innermost ring (arrowed above); a small |
---|
1374 | red cross will appear at each selection point. Press the right mouse button to |
---|
1375 | finish; calibration will proceed. A sequence of concentric red rings will |
---|
1376 | appear; they will switch to blue when calibration is finished. Select <b |
---|
1377 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1378 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Show ring |
---|
1379 | picks</span></b> (near bottom right of <b style='mso-bidi-font-weight:normal'><span |
---|
1380 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1381 | mso-hansi-theme-font:minor-latin'>Image Controls</span></b> window). The <b |
---|
1382 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1383 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
---|
1384 | Controls</span></b> window will show the results of the calibration</p> |
---|
1385 | |
---|
1386 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1387 | id="Picture_x0020_5" o:spid="_x0000_i1058" type="#_x0000_t75" style='width:472.5pt; |
---|
1388 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1389 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image006.png" |
---|
1390 | o:title=""/> |
---|
1391 | </v:shape><![endif]--><![if !vml]><img width=630 height=518 |
---|
1392 | src="Small%20Angle%20Image%20Processing_files/image006.png" v:shapes="Picture_x0020_5"><![endif]></span></p> |
---|
1393 | |
---|
1394 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1395 | |
---|
1396 | <p class=MsoNormal>And the plot will show the points (very sparse!) used in the |
---|
1397 | calibration calculations.</p> |
---|
1398 | |
---|
1399 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1400 | id="Picture_x0020_6" o:spid="_x0000_i1057" type="#_x0000_t75" style='width:525pt; |
---|
1401 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1402 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image007.png" |
---|
1403 | o:title=""/> |
---|
1404 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1405 | src="Small%20Angle%20Image%20Processing_files/image007.png" v:shapes="Picture_x0020_6"><![endif]></span></p> |
---|
1406 | |
---|
1407 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1408 | |
---|
1409 | <p class=MsoNormal>You would like to use more points from just the visible |
---|
1410 | rings. I suggest you change <b style='mso-bidi-font-weight:normal'><span |
---|
1411 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1412 | mso-hansi-theme-font:minor-latin'>Min ring I/<span class=SpellE>Ib</span></span></b> |
---|
1413 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1414 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.5</span></b> |
---|
1415 | and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1416 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Min <span |
---|
1417 | class=SpellE>calib</span> d-spacing</span></b> to <b style='mso-bidi-font-weight: |
---|
1418 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1419 | minor-latin;mso-hansi-theme-font:minor-latin'>10.0</span></b>. Do <b |
---|
1420 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1421 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Recalibrate</span></b>; |
---|
1422 | more points will be used and they will be limited to the 5 visible rings in the |
---|
1423 | pattern.</p> |
---|
1424 | |
---|
1425 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1426 | id="Picture_x0020_7" o:spid="_x0000_i1056" type="#_x0000_t75" style='width:525pt; |
---|
1427 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1428 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image008.png" |
---|
1429 | o:title=""/> |
---|
1430 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1431 | src="Small%20Angle%20Image%20Processing_files/image008.png" v:shapes="Picture_x0020_7"><![endif]></span></p> |
---|
1432 | |
---|
1433 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1434 | |
---|
1435 | <p class=MsoNormal>And give the calibration result as</p> |
---|
1436 | |
---|
1437 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1438 | id="Picture_x0020_8" o:spid="_x0000_i1055" type="#_x0000_t75" style='width:472.5pt; |
---|
1439 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1440 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image009.png" |
---|
1441 | o:title=""/> |
---|
1442 | </v:shape><![endif]--><![if !vml]><img width=630 height=518 |
---|
1443 | src="Small%20Angle%20Image%20Processing_files/image009.png" v:shapes="Picture_x0020_8"><![endif]></span></p> |
---|
1444 | |
---|
1445 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1446 | |
---|
1447 | <p class=MsoNormal>You will need this calibration information to process the |
---|
1448 | other images in this tutorial. To save it for future use do <b |
---|
1449 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1450 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Save |
---|
1451 | controls</span></b>; a file dialog will appear. Makeup a file name (no |
---|
1452 | extension needed) for this; I chose <b style='mso-bidi-font-weight:normal'><span |
---|
1453 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1454 | mso-hansi-theme-font:minor-latin'>SASD</span></b>. Press <b style='mso-bidi-font-weight: |
---|
1455 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1456 | minor-latin;mso-hansi-theme-font:minor-latin'>Save</span></b> and the file <span |
---|
1457 | class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1458 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1459 | minor-latin'>SASD.imctrl</span></b></span> will be written to the local |
---|
1460 | directory. If you are continuing on to the next step do <b style='mso-bidi-font-weight: |
---|
1461 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1462 | minor-latin;mso-hansi-theme-font:minor-latin'>File/New Project</span></b> |
---|
1463 | (dont bother saving the project file unless you want it; we will not need it |
---|
1464 | here); otherwise you can exit GSAS-II.</p> |
---|
1465 | |
---|
1466 | <h2>Step 2: Data image integration</h2> |
---|
1467 | |
---|
1468 | <p class=MsoNormal>The objective here is to read in the four polymer sample |
---|
1469 | images, a glassy carbon image, an empty container image and a dark image. The |
---|
1470 | images will be integrated after creating masks to remove the beam stop and |
---|
1471 | other objectionable parts of the images. If you have not done so already, start |
---|
1472 | GSAS-II. </p> |
---|
1473 | |
---|
1474 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1475 | |
---|
1476 | <p class=MsoNormal>First do <b style='mso-bidi-font-weight:normal'><span |
---|
1477 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1478 | mso-hansi-theme-font:minor-latin'>Data/Read image data
</span></b>, go to <b |
---|
1479 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1480 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>exercises/<span |
---|
1481 | class=SpellE>SAimages</span></span></b> and select all images except <b |
---|
1482 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1483 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>AgBehenate_003.tif</span></b>; |
---|
1484 | then press <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1485 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1486 | minor-latin'>Open</span></b> to read all of them. The GSAS-II data tree window |
---|
1487 | will show entries for 7 images and will expand the last one</p> |
---|
1488 | |
---|
1489 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1490 | id="Picture_x0020_9" o:spid="_x0000_i1054" type="#_x0000_t75" style='width:300pt; |
---|
1491 | height:310.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1492 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image010.png" |
---|
1493 | o:title=""/> |
---|
1494 | </v:shape><![endif]--><![if !vml]><img width=400 height=414 |
---|
1495 | src="Small%20Angle%20Image%20Processing_files/image010.png" v:shapes="Picture_x0020_9"><![endif]></span></p> |
---|
1496 | |
---|
1497 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1498 | |
---|
1499 | <p class=MsoNormal>Notice that the Dark, Empty and GC (glassy carbon) are all |
---|
1500 | 5s images and the Sa1-4 ones are 40s images; this time information is needed |
---|
1501 | later to obtain correct scaling. First select the <b style='mso-bidi-font-weight: |
---|
1502 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1503 | minor-latin;mso-hansi-theme-font:minor-latin'>IMG GC_5s_200.tif</span></b> |
---|
1504 | entry from the tree and expand it (press the <b style='mso-bidi-font-weight: |
---|
1505 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1506 | minor-latin;mso-hansi-theme-font:minor-latin'>+</span></b> box); then select <b |
---|
1507 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1508 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
---|
1509 | controls</span></b>. The data window (<b style='mso-bidi-font-weight:normal'><span |
---|
1510 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1511 | mso-hansi-theme-font:minor-latin'>Image Controls</span></b>) will show the |
---|
1512 | default settings.</p> |
---|
1513 | |
---|
1514 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1515 | id="Picture_x0020_10" o:spid="_x0000_i1053" type="#_x0000_t75" style='width:472.5pt; |
---|
1516 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1517 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image011.png" |
---|
1518 | o:title=""/> |
---|
1519 | </v:shape><![endif]--><![if !vml]><img width=630 height=518 |
---|
1520 | src="Small%20Angle%20Image%20Processing_files/image011.png" v:shapes="Picture_x0020_10"><![endif]></span></p> |
---|
1521 | |
---|
1522 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1523 | |
---|
1524 | <p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span |
---|
1525 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1526 | mso-hansi-theme-font:minor-latin'>Operations/Load controls</span></b> from the |
---|
1527 | menu; a file selection dialog will appear showing the available *.<span |
---|
1528 | class=SpellE>imctrl</span> files (the one you made in Step 1 should be seen). |
---|
1529 | Select it and press <b style='mso-bidi-font-weight:normal'><span |
---|
1530 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1531 | mso-hansi-theme-font:minor-latin'>Open</span></b>; the <b style='mso-bidi-font-weight: |
---|
1532 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1533 | minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> window |
---|
1534 | will be redrawn with the settings obtained in <b style='mso-bidi-font-weight: |
---|
1535 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1536 | minor-latin;mso-hansi-theme-font:minor-latin'>Step 1: Detector calibration</span></b></p> |
---|
1537 | |
---|
1538 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1539 | id="Picture_x0020_11" o:spid="_x0000_i1052" type="#_x0000_t75" style='width:472.5pt; |
---|
1540 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1541 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image012.png" |
---|
1542 | o:title=""/> |
---|
1543 | </v:shape><![endif]--><![if !vml]><img width=630 height=518 |
---|
1544 | src="Small%20Angle%20Image%20Processing_files/image012.png" v:shapes="Picture_x0020_11"><![endif]></span></p> |
---|
1545 | |
---|
1546 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1547 | |
---|
1548 | <p class=MsoNormal>and the image will be that of glassy carbon. Changing the <b |
---|
1549 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1550 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Max intensity</span></b> |
---|
1551 | slider on the <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1552 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1553 | minor-latin'>Image Controls</span></b> window will show that the image from the |
---|
1554 | <span class=SpellE>MarCCD</span> is circular and slightly offset from the beam |
---|
1555 | center. A beam stop shadow is evident as well as an arc-like fault in the image |
---|
1556 | (toward the upper left corner of the image). We will sort those out later.</p> |
---|
1557 | |
---|
1558 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1559 | id="Picture_x0020_55" o:spid="_x0000_i1051" type="#_x0000_t75" style='width:525pt; |
---|
1560 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1561 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image013.png" |
---|
1562 | o:title=""/> |
---|
1563 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1564 | src="Small%20Angle%20Image%20Processing_files/image013.png" v:shapes="Picture_x0020_55"><![endif]></span></p> |
---|
1565 | |
---|
1566 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1567 | |
---|
1568 | <p class=MsoNormal>The next step we will be doing is to set up the integration |
---|
1569 | controls. The <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1570 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1571 | minor-latin'>Dark image</span></b> is <b style='mso-bidi-font-weight:normal'><span |
---|
1572 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1573 | mso-hansi-theme-font:minor-latin'>IMG Dark_5s_003.tif</span></b>, the <b |
---|
1574 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1575 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background |
---|
1576 | image</span></b> is <b style='mso-bidi-font-weight:normal'><span |
---|
1577 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1578 | mso-hansi-theme-font:minor-latin'>IMG Empty_5s_014.tif</span></b>; select these |
---|
1579 | two. The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1580 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
---|
1581 | for each are <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1582 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1583 | minor-latin'>-1.0</span></b> because their exposures were the same as this |
---|
1584 | glassy carbon image (5s). Next check the boxes for <b style='mso-bidi-font-weight: |
---|
1585 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1586 | minor-latin;mso-hansi-theme-font:minor-latin'>Show integration limits?</span></b> |
---|
1587 | and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1588 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Do full |
---|
1589 | integration?</span></b> A pair of circles with a connecting diagonal line will |
---|
1590 | appear on the plot. Set the <b style='mso-bidi-font-weight:normal'><span |
---|
1591 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1592 | mso-hansi-theme-font:minor-latin'>Inner/Outer q</span></b> values to <b |
---|
1593 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1594 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.05</span></b> |
---|
1595 | and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1596 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.9</span></b>, |
---|
1597 | respectively, and set the <b style='mso-bidi-font-weight:normal'><span |
---|
1598 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1599 | mso-hansi-theme-font:minor-latin'>Start azimuth</span></b> to <b |
---|
1600 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1601 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0</span></b>. |
---|
1602 | Set the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1603 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>No. 2-theta |
---|
1604 | bins</span></b> to <b style='mso-bidi-font-weight:normal'><span |
---|
1605 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1606 | mso-hansi-theme-font:minor-latin'>250</span></b>, which is more appropriate for |
---|
1607 | small angle scattering, and set the <b style='mso-bidi-font-weight:normal'><span |
---|
1608 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1609 | mso-hansi-theme-font:minor-latin'>Bin style: Constant step bins in</span></b> |
---|
1610 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1611 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>log(q)</span></b>. |
---|
1612 | You should also check the <b style='mso-bidi-font-weight:normal'><span |
---|
1613 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1614 | mso-hansi-theme-font:minor-latin'>Apply sample absorption?</span></b> and <b |
---|
1615 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1616 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Apply |
---|
1617 | polarization?</span></b> boxes; enter the measured <b style='mso-bidi-font-weight: |
---|
1618 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1619 | minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> (<b |
---|
1620 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1621 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.818</span></b>) |
---|
1622 | for the glassy carbon sample. When done the <b style='mso-bidi-font-weight: |
---|
1623 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1624 | minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> data |
---|
1625 | window should look like</p> |
---|
1626 | |
---|
1627 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1628 | id="Picture_x0020_40" o:spid="_x0000_i1050" type="#_x0000_t75" style='width:472.5pt; |
---|
1629 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1630 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image014.png" |
---|
1631 | o:title=""/> |
---|
1632 | </v:shape><![endif]--><![if !vml]><img width=630 height=518 |
---|
1633 | src="Small%20Angle%20Image%20Processing_files/image014.png" v:shapes="Picture_x0020_40"><![endif]></span></p> |
---|
1634 | |
---|
1635 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1636 | |
---|
1637 | <p class=MsoNormal>And the plot should look like</p> |
---|
1638 | |
---|
1639 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1640 | id="Picture_x0020_41" o:spid="_x0000_i1049" type="#_x0000_t75" style='width:525pt; |
---|
1641 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1642 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image015.png" |
---|
1643 | o:title=""/> |
---|
1644 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1645 | src="Small%20Angle%20Image%20Processing_files/image015.png" v:shapes="Picture_x0020_41"><![endif]></span></p> |
---|
1646 | |
---|
1647 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1648 | |
---|
1649 | <p class=MsoNormal>Now copy these controls to the other images. Do <b |
---|
1650 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1651 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Copy |
---|
1652 | controls</span></b> and select just the <b style='mso-bidi-font-weight:normal'><span |
---|
1653 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1654 | mso-hansi-theme-font:minor-latin'>Sa1-4</span></b> data names. </p> |
---|
1655 | |
---|
1656 | <p class=MsoNormal>We now need to go to the <b style='mso-bidi-font-weight: |
---|
1657 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1658 | minor-latin;mso-hansi-theme-font:minor-latin'>Image Controls</span></b> for |
---|
1659 | each of <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1660 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sa1-Sa4</span></b> |
---|
1661 | to enter the correct transmission for each and change the Dark & Background |
---|
1662 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1663 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
---|
1664 | to account for the different exposure times. Start with <b style='mso-bidi-font-weight: |
---|
1665 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1666 | minor-latin;mso-hansi-theme-font:minor-latin'>IMG Sa1_40s_067.tif</span></b> |
---|
1667 | and change <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1668 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1669 | minor-latin'>transmission</span></b> to <b style='mso-bidi-font-weight:normal'><span |
---|
1670 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1671 | mso-hansi-theme-font:minor-latin'>0.943</span></b> and the two <b |
---|
1672 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1673 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
---|
1674 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1675 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. |
---|
1676 | Then go to <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1677 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1678 | minor-latin'>IMG Sa2_40s_069.tif</span></b> and change <b style='mso-bidi-font-weight: |
---|
1679 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1680 | minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> to <b |
---|
1681 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1682 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.979</span></b>; |
---|
1683 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1684 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
---|
1685 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1686 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. |
---|
1687 | Next go <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1688 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>to IMG |
---|
1689 | Sa3_40s_059.tif</span></b> and change <b style='mso-bidi-font-weight:normal'><span |
---|
1690 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1691 | mso-hansi-theme-font:minor-latin'>transmission</span></b> to <b |
---|
1692 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1693 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.960</span></b>; |
---|
1694 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1695 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
---|
1696 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1697 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. |
---|
1698 | Finally, go to <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1699 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1700 | minor-latin'>IMG Sa4_40s_061.tif</span></b> and change <b style='mso-bidi-font-weight: |
---|
1701 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1702 | minor-latin;mso-hansi-theme-font:minor-latin'>transmission</span></b> to <b |
---|
1703 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1704 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.968</span></b>; |
---|
1705 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1706 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>multipliers</span></b> |
---|
1707 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1708 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-8.0</span></b>. |
---|
1709 | The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1710 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Image |
---|
1711 | Controls</span></b> data window for this should look like</p> |
---|
1712 | |
---|
1713 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1714 | id="Picture_x0020_43" o:spid="_x0000_i1048" type="#_x0000_t75" style='width:472.5pt; |
---|
1715 | height:388.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1716 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image016.png" |
---|
1717 | o:title=""/> |
---|
1718 | </v:shape><![endif]--><![if !vml]><img width=630 height=518 |
---|
1719 | src="Small%20Angle%20Image%20Processing_files/image016.png" v:shapes="Picture_x0020_43"><![endif]></span></p> |
---|
1720 | |
---|
1721 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1722 | |
---|
1723 | <p class=MsoNormal>This is a reasonable time to save the project; do <b |
---|
1724 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1725 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/Save |
---|
1726 | project as
</span></b> from the main GSAS-II data tree menu. Choose a file name |
---|
1727 | (I assumed <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1728 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1729 | minor-latin'>image</span></b>) and it will be written on the local file |
---|
1730 | directory. </p> |
---|
1731 | |
---|
1732 | <p class=MsoNormal>As noted earlier, the images contain some unwanted features; |
---|
1733 | so lets create masks to remove them. Select <b style='mso-bidi-font-weight: |
---|
1734 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1735 | minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> from the GSAS-II |
---|
1736 | data tree under <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1737 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1738 | minor-latin'>IMG GC_5s_200.tif</span></b>; the data window will show</p> |
---|
1739 | |
---|
1740 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1741 | id="Picture_x0020_17" o:spid="_x0000_i1047" type="#_x0000_t75" style='width:337.5pt; |
---|
1742 | height:99.75pt;visibility:visible;mso-wrap-style:square'> |
---|
1743 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image017.png" |
---|
1744 | o:title=""/> |
---|
1745 | </v:shape><![endif]--><![if !vml]><img width=450 height=133 |
---|
1746 | src="Small%20Angle%20Image%20Processing_files/image017.png" v:shapes="Picture_x0020_17"><![endif]></span></p> |
---|
1747 | |
---|
1748 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1749 | |
---|
1750 | <p class=MsoNormal>To mask out the regions beyond the circular <span |
---|
1751 | class=SpellE>MarCCD</span> image change the <span class=GramE><b |
---|
1752 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1753 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Lower<span |
---|
1754 | style='mso-spacerun:yes'> </span><span class=SpellE>threshhold</span></span></b></span> |
---|
1755 | from <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1756 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0</span></b> |
---|
1757 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1758 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1</span></b>; |
---|
1759 | the image will be redrawn with these regions in red</p> |
---|
1760 | |
---|
1761 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1762 | id="Picture_x0020_45" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:525pt; |
---|
1763 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1764 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image018.png" |
---|
1765 | o:title=""/> |
---|
1766 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1767 | src="Small%20Angle%20Image%20Processing_files/image018.png" v:shapes="Picture_x0020_45"><![endif]></span></p> |
---|
1768 | |
---|
1769 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1770 | |
---|
1771 | <p class=MsoNormal>These are now excluded. The status line for the <b |
---|
1772 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1773 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> |
---|
1774 | data window gives the directions for adding additional masks. You can make arcs |
---|
1775 | (well use that here), rings, spots (this too) and polygons (this as well) as |
---|
1776 | masks. These enclose areas to be excluded. The frame works in the opposite |
---|
1777 | sense in that everything outside the frame is excluded (NB: only one frame is |
---|
1778 | allowed). So lets first mask the bad arc in the upper left zoom in on that |
---|
1779 | part of the image</p> |
---|
1780 | |
---|
1781 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1782 | id="Picture_x0020_62" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:525pt; |
---|
1783 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1784 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image019.png" |
---|
1785 | o:title=""/> |
---|
1786 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1787 | src="Small%20Angle%20Image%20Processing_files/image019.png" v:shapes="Picture_x0020_62"><![endif]></span></p> |
---|
1788 | |
---|
1789 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1790 | |
---|
1791 | <p class=MsoNormal>To add the mask 1: be sure the focus is on the image and the |
---|
1792 | zoom buttons are off, 2: type <b style='mso-bidi-font-weight:normal'><span |
---|
1793 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1794 | mso-hansi-theme-font:minor-latin'>a</span></b> to activate the arc mask entry |
---|
1795 | 3: press the left mouse button (<b style='mso-bidi-font-weight:normal'><span |
---|
1796 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1797 | mso-hansi-theme-font:minor-latin'>LB</span></b>) with the cursor centered on |
---|
1798 | the bad arc. The <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1799 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1800 | minor-latin'>Masks</span></b> window will show a new entry </p> |
---|
1801 | |
---|
1802 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1803 | id="Picture_x0020_63" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:342pt; |
---|
1804 | height:136.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1805 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image020.png" |
---|
1806 | o:title=""/> |
---|
1807 | </v:shape><![endif]--><![if !vml]><img width=456 height=182 |
---|
1808 | src="Small%20Angle%20Image%20Processing_files/image020.png" v:shapes="Picture_x0020_63"><![endif]></span><span |
---|
1809 | style='mso-spacerun:yes'> </span></p> |
---|
1810 | |
---|
1811 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1812 | |
---|
1813 | <p class=MsoNormal>and an arc mask will be drawn on the plot.</p> |
---|
1814 | |
---|
1815 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1816 | id="Picture_x0020_64" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:525pt; |
---|
1817 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1818 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image021.png" |
---|
1819 | o:title=""/> |
---|
1820 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1821 | src="Small%20Angle%20Image%20Processing_files/image021.png" v:shapes="Picture_x0020_64"><![endif]></span></p> |
---|
1822 | |
---|
1823 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1824 | |
---|
1825 | <p class=MsoNormal>You can change the angular width of the arc by changing <b |
---|
1826 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1827 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>thickness</span></b> |
---|
1828 | in the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1829 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> |
---|
1830 | data window, you can change the angular range of the arc by dragging either end |
---|
1831 | of the arc (NB: increments only in whole degrees), and you can move the |
---|
1832 | arc<span style='mso-spacerun:yes'> </span>along a constant 2Θ angle by |
---|
1833 | dragging on any point inside the mask. The curvature is centered on the beam |
---|
1834 | center position and follows a constant 2Θ curve established by the |
---|
1835 | detector calibration.<span style='mso-no-proof:yes'> </span></p> |
---|
1836 | |
---|
1837 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1838 | id="Picture_x0020_65" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:525pt; |
---|
1839 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1840 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image022.png" |
---|
1841 | o:title=""/> |
---|
1842 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1843 | src="Small%20Angle%20Image%20Processing_files/image022.png" v:shapes="Picture_x0020_65"><![endif]></span></p> |
---|
1844 | |
---|
1845 | <p class=MsoNormal>Next lets deal with the beam stop. Im going to use both a |
---|
1846 | polygon and a spot to cover it. Move the zoom area to be around the center, |
---|
1847 | make sure the zoom buttons are off, enter <b style='mso-bidi-font-weight:normal'><span |
---|
1848 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1849 | mso-hansi-theme-font:minor-latin'>s</span></b> on the plot and press mouse <b |
---|
1850 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1851 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>LB</span></b> |
---|
1852 | with the cursor positioned where you want the spot. A 1mm diameter red circle |
---|
1853 | will appear on the plot</p> |
---|
1854 | |
---|
1855 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1856 | id="Picture_x0020_66" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:525pt; |
---|
1857 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1858 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image023.png" |
---|
1859 | o:title=""/> |
---|
1860 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1861 | src="Small%20Angle%20Image%20Processing_files/image023.png" v:shapes="Picture_x0020_66"><![endif]></span></p> |
---|
1862 | |
---|
1863 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1864 | |
---|
1865 | <p class=MsoNormal>And the <b style='mso-bidi-font-weight:normal'><span |
---|
1866 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1867 | mso-hansi-theme-font:minor-latin'>Masks</span></b> window will have new |
---|
1868 | information</p> |
---|
1869 | |
---|
1870 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1871 | id="Picture_x0020_24" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:337.5pt; |
---|
1872 | height:170.25pt;visibility:visible;mso-wrap-style:square'> |
---|
1873 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image024.png" |
---|
1874 | o:title=""/> |
---|
1875 | </v:shape><![endif]--><![if !vml]><img width=450 height=227 |
---|
1876 | src="Small%20Angle%20Image%20Processing_files/image024.png" v:shapes="Picture_x0020_24"><![endif]></span></p> |
---|
1877 | |
---|
1878 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1879 | |
---|
1880 | <p class=MsoNormal>You can change the diameter of the spot, I used <b |
---|
1881 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1882 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>7.0</span></b>; |
---|
1883 | the plot now shows a ring that just covers the beam stop. You may have to drag |
---|
1884 | it a bit (Hint: drag the center of the spot) to get it well centered.</p> |
---|
1885 | |
---|
1886 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1887 | id="Picture_x0020_67" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:525pt; |
---|
1888 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1889 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image025.png" |
---|
1890 | o:title=""/> |
---|
1891 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1892 | src="Small%20Angle%20Image%20Processing_files/image025.png" v:shapes="Picture_x0020_67"><![endif]></span></p> |
---|
1893 | |
---|
1894 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1895 | |
---|
1896 | <p class=MsoNormal>Next we need to mask the stick holding the beam stop; well |
---|
1897 | use a 4 sided polygon for this. Adjust the zoom & position so you can see |
---|
1898 | the entire beam stop stick. Make sure all zoom buttons are off, press <b |
---|
1899 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1900 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>p</span></b> |
---|
1901 | on the plot, then press the mouse <b style='mso-bidi-font-weight:normal'><span |
---|
1902 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1903 | mso-hansi-theme-font:minor-latin'>LB</span></b> at four points in succession |
---|
1904 | around the beam stop stick. A line segment for the polygon will be drawn |
---|
1905 | following your mouse clicks. Finally press the mouse <b style='mso-bidi-font-weight: |
---|
1906 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1907 | minor-latin;mso-hansi-theme-font:minor-latin'>RB</span></b> to close the |
---|
1908 | polygon. You should see something like</p> |
---|
1909 | |
---|
1910 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1911 | id="Picture_x0020_68" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:525pt; |
---|
1912 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1913 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image026.png" |
---|
1914 | o:title=""/> |
---|
1915 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1916 | src="Small%20Angle%20Image%20Processing_files/image026.png" v:shapes="Picture_x0020_68"><![endif]></span></p> |
---|
1917 | |
---|
1918 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1919 | |
---|
1920 | <p class=MsoNormal>You can adjust the position of the polygon vertices by |
---|
1921 | closely dragging it with mouse <b style='mso-bidi-font-weight:normal'><span |
---|
1922 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1923 | mso-hansi-theme-font:minor-latin'>LB</span></b> pressed; a new vertex can be |
---|
1924 | added by dragging an existing vertex with the mouse <b style='mso-bidi-font-weight: |
---|
1925 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1926 | minor-latin;mso-hansi-theme-font:minor-latin'>RB</span></b> pressed. If you |
---|
1927 | drag one vertex onto another, they are merged and cannot be separated.</p> |
---|
1928 | |
---|
1929 | <p class=MsoNormal>We want to use these masks for all the Sa1-4 images. Do <b |
---|
1930 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1931 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Copy |
---|
1932 | mask</span></b>; a <b style='mso-bidi-font-weight:normal'><span |
---|
1933 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1934 | mso-hansi-theme-font:minor-latin'>Copy mask information</span></b> dialog box |
---|
1935 | will appear. Select the <b style='mso-bidi-font-weight:normal'><span |
---|
1936 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1937 | mso-hansi-theme-font:minor-latin'>Sa1-4</span></b> items and press <b |
---|
1938 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1939 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ok</span></b>. |
---|
1940 | Here is a useful place to save your project; do <b style='mso-bidi-font-weight: |
---|
1941 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1942 | minor-latin;mso-hansi-theme-font:minor-latin'>File/Save project</span></b> from |
---|
1943 | the main GSAS-II data tree menu.</p> |
---|
1944 | |
---|
1945 | <h2>Step 3: Integration of images</h2> |
---|
1946 | |
---|
1947 | <p class=MsoNormal>We are now ready to integrate the glassy carbon and the four |
---|
1948 | Sa images. Select any <b style='mso-bidi-font-weight:normal'><span |
---|
1949 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1950 | mso-hansi-theme-font:minor-latin'>Image Controls</span></b> and then do <b |
---|
1951 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1952 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Integrate |
---|
1953 | all</span></b>. A selection dialog will appear; select only the <b |
---|
1954 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1955 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>GC</span></b> |
---|
1956 | and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1957 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sa1-Sa4</span></b> |
---|
1958 | data sets and press <b style='mso-bidi-font-weight:normal'><span |
---|
1959 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1960 | mso-hansi-theme-font:minor-latin'>Ok</span></b>. The image integration will |
---|
1961 | proceed; a progress bar shows as each one is done. Five SASD data items will |
---|
1962 | appear on the GSAS-II data tree; the last one (<b style='mso-bidi-font-weight: |
---|
1963 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1964 | minor-latin;mso-hansi-theme-font:minor-latin'>SASD Sa4_40s_061.tif <span |
---|
1965 | class=SpellE>Azm</span>=45.00</span></b>) will be expanded and plotted (you may |
---|
1966 | have to select the <b style='mso-bidi-font-weight:normal'><span |
---|
1967 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1968 | mso-hansi-theme-font:minor-latin'>Powder Patterns</span></b> tab to see it).</p> |
---|
1969 | |
---|
1970 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1971 | id="Picture_x0020_26" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:525pt; |
---|
1972 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1973 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image027.png" |
---|
1974 | o:title=""/> |
---|
1975 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1976 | src="Small%20Angle%20Image%20Processing_files/image027.png" v:shapes="Picture_x0020_26"><![endif]></span></p> |
---|
1977 | |
---|
1978 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1979 | |
---|
1980 | <p class=MsoNormal>Pretty obviously the SASD pattern is down to background at |
---|
1981 | Q~0.25Å<sup>-1</sup>; the other Sa1-Sa4 patterns are similar. The glassy carbon |
---|
1982 | pattern extends nicely to the highest Q (~1.0Å<sup>-1</sup>) measured.</p> |
---|
1983 | |
---|
1984 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1985 | id="Picture_x0020_48" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt; |
---|
1986 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
1987 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image028.png" |
---|
1988 | o:title=""/> |
---|
1989 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
1990 | src="Small%20Angle%20Image%20Processing_files/image028.png" v:shapes="Picture_x0020_48"><![endif]></span></p> |
---|
1991 | |
---|
1992 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1993 | |
---|
1994 | <h2>Step 4: Scaling of SASD patterns</h2> |
---|
1995 | |
---|
1996 | <p class=MsoNormal>To set this data on an absolute scale, we compare it to an |
---|
1997 | absolute scaled glassy carbon scan. One of these is in the same directory as |
---|
1998 | the image data; do <b style='mso-bidi-font-weight:normal'><span |
---|
1999 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2000 | mso-hansi-theme-font:minor-latin'>Import/Small Angle Data/ from q(A-1) step |
---|
2001 | X-ray QIE data file</span></b> and select <b style='mso-bidi-font-weight:normal'><span |
---|
2002 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2003 | mso-hansi-theme-font:minor-latin'>GC calibrated data.txt</span></b> from the |
---|
2004 | file selection dialog. You will need to select <b style='mso-bidi-font-weight: |
---|
2005 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
2006 | minor-latin;mso-hansi-theme-font:minor-latin'>any <span class=GramE>file(</span>*.*)</span></b> |
---|
2007 | to see it. A <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
2008 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
2009 | minor-latin'>Is this the file you want</span></b> dialog will appear respond <b |
---|
2010 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2011 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Yes</span></b> |
---|
2012 | to read the file; it will be plotted.</p> |
---|
2013 | |
---|
2014 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2015 | id="Picture_x0020_49" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:525pt; |
---|
2016 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
2017 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image029.png" |
---|
2018 | o:title=""/> |
---|
2019 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
2020 | src="Small%20Angle%20Image%20Processing_files/image029.png" v:shapes="Picture_x0020_49"><![endif]></span></p> |
---|
2021 | |
---|
2022 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2023 | |
---|
2024 | <p class=MsoNormal>If you enter <b style='mso-bidi-font-weight:normal'><span |
---|
2025 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2026 | mso-hansi-theme-font:minor-latin'>m</span></b> on the plot window, all of the |
---|
2027 | SASD patterns will be plotted together (Ive adjusted the zoom to see them |
---|
2028 | all).</p> |
---|
2029 | |
---|
2030 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2031 | id="Picture_x0020_50" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt; |
---|
2032 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
2033 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image030.png" |
---|
2034 | o:title=""/> |
---|
2035 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
2036 | src="Small%20Angle%20Image%20Processing_files/image030.png" v:shapes="Picture_x0020_50"><![endif]></span></p> |
---|
2037 | |
---|
2038 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2039 | |
---|
2040 | <p class=MsoNormal>Clearly the measured image data need to be scaled down to |
---|
2041 | have them on absolute scale. First is to discover the scaling between the two |
---|
2042 | glassy carbon patterns. Go to the measured one (<b style='mso-bidi-font-weight: |
---|
2043 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
2044 | minor-latin;mso-hansi-theme-font:minor-latin'>SASD GC_5s_200.tif</span></b>) |
---|
2045 | and select <b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
2046 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
2047 | minor-latin'>Sample Parameters</span></b>.</p> |
---|
2048 | |
---|
2049 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2050 | id="Picture_x0020_51" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:291.75pt; |
---|
2051 | height:408pt;visibility:visible;mso-wrap-style:square'> |
---|
2052 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image031.png" |
---|
2053 | o:title=""/> |
---|
2054 | </v:shape><![endif]--><![if !vml]><img width=389 height=544 |
---|
2055 | src="Small%20Angle%20Image%20Processing_files/image031.png" v:shapes="Picture_x0020_51"><![endif]></span></p> |
---|
2056 | |
---|
2057 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2058 | |
---|
2059 | <p class=MsoNormal>We will change <b style='mso-bidi-font-weight:normal'><span |
---|
2060 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2061 | mso-hansi-theme-font:minor-latin'>Histogram scale factor</span></b> by |
---|
2062 | comparison with the absolute glassy carbon scan. Do <b style='mso-bidi-font-weight: |
---|
2063 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
2064 | minor-latin;mso-hansi-theme-font:minor-latin'>Command/Set scale</span></b> from |
---|
2065 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2066 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sample |
---|
2067 | Parameters</span></b> menu; a <b style='mso-bidi-font-weight:normal'><span |
---|
2068 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2069 | mso-hansi-theme-font:minor-latin'>Reference histogram</span></b> dialog will |
---|
2070 | appear.</p> |
---|
2071 | |
---|
2072 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2073 | id="Picture_x0020_44" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:259.5pt; |
---|
2074 | height:252pt;visibility:visible;mso-wrap-style:square'> |
---|
2075 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image032.png" |
---|
2076 | o:title=""/> |
---|
2077 | </v:shape><![endif]--><![if !vml]><img width=346 height=336 |
---|
2078 | src="Small%20Angle%20Image%20Processing_files/image032.png" v:shapes="Picture_x0020_44"><![endif]></span></p> |
---|
2079 | |
---|
2080 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2081 | |
---|
2082 | <p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span |
---|
2083 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2084 | mso-hansi-theme-font:minor-latin'>SASD GC calibrated data.txt</span></b> (shown |
---|
2085 | in blue above) and press <b style='mso-bidi-font-weight:normal'><span |
---|
2086 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2087 | mso-hansi-theme-font:minor-latin'>Ok</span></b>; the <b style='mso-bidi-font-weight: |
---|
2088 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
2089 | minor-latin;mso-hansi-theme-font:minor-latin'>GC_5s_200.tif</span></b> data |
---|
2090 | will be rescaled to the <b style='mso-bidi-font-weight:normal'><span |
---|
2091 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2092 | mso-hansi-theme-font:minor-latin'>GC calibrated data</span></b> and the <b |
---|
2093 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2094 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Histogram scale |
---|
2095 | factor</span></b> will be changed to the new scaling factor (<b |
---|
2096 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2097 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.0008536</span></b>). |
---|
2098 | The plot will be redrawn with the scaled data.</p> |
---|
2099 | |
---|
2100 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2101 | id="Picture_x0020_52" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt; |
---|
2102 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
2103 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image033.png" |
---|
2104 | o:title=""/> |
---|
2105 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
2106 | src="Small%20Angle%20Image%20Processing_files/image033.png" v:shapes="Picture_x0020_52"><![endif]></span></p> |
---|
2107 | |
---|
2108 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2109 | |
---|
2110 | <p class=MsoNormal>The divergence at high Q is probably from a background |
---|
2111 | contribution to the standard that is not present in our measured one. Next we |
---|
2112 | have to apply this scale factor to the Sa1-Sa4 data sets. Do <b |
---|
2113 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2114 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Command/Copy |
---|
2115 | selected
</span></b> from the <b style='mso-bidi-font-weight:normal'><span |
---|
2116 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2117 | mso-hansi-theme-font:minor-latin'>Sample Parameters</span></b> menu; a <b |
---|
2118 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2119 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Select |
---|
2120 | sample parameters</span></b> dialog will appear</p> |
---|
2121 | |
---|
2122 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2123 | id="Picture_x0020_46" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:240pt; |
---|
2124 | height:232.5pt;visibility:visible;mso-wrap-style:square'> |
---|
2125 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image034.png" |
---|
2126 | o:title=""/> |
---|
2127 | </v:shape><![endif]--><![if !vml]><img width=320 height=310 |
---|
2128 | src="Small%20Angle%20Image%20Processing_files/image034.png" v:shapes="Picture_x0020_46"><![endif]></span></p> |
---|
2129 | |
---|
2130 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2131 | |
---|
2132 | <p class=MsoNormal>Select only <b style='mso-bidi-font-weight:normal'><span |
---|
2133 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2134 | mso-hansi-theme-font:minor-latin'>Histogram scale factor</span></b> and press <b |
---|
2135 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2136 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ok</span></b>; |
---|
2137 | a <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2138 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Copy sample |
---|
2139 | parameters</span></b> dialog will appear</p> |
---|
2140 | |
---|
2141 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2142 | id="Picture_x0020_47" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:240pt; |
---|
2143 | height:232.5pt;visibility:visible;mso-wrap-style:square'> |
---|
2144 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image035.png" |
---|
2145 | o:title=""/> |
---|
2146 | </v:shape><![endif]--><![if !vml]><img width=320 height=310 |
---|
2147 | src="Small%20Angle%20Image%20Processing_files/image035.png" v:shapes="Picture_x0020_47"><![endif]></span></p> |
---|
2148 | |
---|
2149 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2150 | |
---|
2151 | <p class=MsoNormal>Select only the <b style='mso-bidi-font-weight:normal'><span |
---|
2152 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2153 | mso-hansi-theme-font:minor-latin'>Sa1-Sa4</span></b> data sets and press <b |
---|
2154 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2155 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Ok</span></b>. |
---|
2156 | The copy will occur and the plot redrawn</p> |
---|
2157 | |
---|
2158 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2159 | id="Picture_x0020_53" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:525pt; |
---|
2160 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
2161 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image036.png" |
---|
2162 | o:title=""/> |
---|
2163 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
2164 | src="Small%20Angle%20Image%20Processing_files/image036.png" v:shapes="Picture_x0020_53"><![endif]></span></p> |
---|
2165 | |
---|
2166 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2167 | |
---|
2168 | <p class=MsoNormal>Ive changed the zoom to show all the data. We are not quite |
---|
2169 | done; the scales for the Sa1-Sa4 data sets have to be further reduced by a factor |
---|
2170 | of 8 to account for the longer exposure time. Select <b style='mso-bidi-font-weight: |
---|
2171 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
2172 | minor-latin;mso-hansi-theme-font:minor-latin'>SASD Sa1_40s_067.tif</span></b> |
---|
2173 | from the GSAS-II data tree, expand it and choose <b style='mso-bidi-font-weight: |
---|
2174 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
2175 | minor-latin;mso-hansi-theme-font:minor-latin'>Sample Parameters</span></b></p> |
---|
2176 | |
---|
2177 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2178 | id="Picture_x0020_54" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:291.75pt; |
---|
2179 | height:408pt;visibility:visible;mso-wrap-style:square'> |
---|
2180 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image037.png" |
---|
2181 | o:title=""/> |
---|
2182 | </v:shape><![endif]--><![if !vml]><img width=389 height=544 |
---|
2183 | src="Small%20Angle%20Image%20Processing_files/image037.png" v:shapes="Picture_x0020_54"><![endif]></span></p> |
---|
2184 | |
---|
2185 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2186 | |
---|
2187 | <p class=MsoNormal>The data items here can take simple mathematical expressions |
---|
2188 | so change <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2189 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Histogram |
---|
2190 | scale factor</span></b> to <b style='mso-bidi-font-weight:normal'><span |
---|
2191 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2192 | mso-hansi-theme-font:minor-latin'>0.0008536/8</span></b> and press <b |
---|
2193 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
2194 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Enter</span></b>. |
---|
2195 | The value will change to <b style='mso-bidi-font-weight:normal'><span |
---|
2196 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2197 | mso-hansi-theme-font:minor-latin'>0.0001067</span></b> and the plot redrawn.</p> |
---|
2198 | |
---|
2199 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2200 | id="Picture_x0020_56" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:525pt; |
---|
2201 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
2202 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image038.png" |
---|
2203 | o:title=""/> |
---|
2204 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
2205 | src="Small%20Angle%20Image%20Processing_files/image038.png" v:shapes="Picture_x0020_56"><![endif]></span></p> |
---|
2206 | |
---|
2207 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2208 | |
---|
2209 | <p class=MsoNormal>Next do <b style='mso-bidi-font-weight:normal'><span |
---|
2210 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2211 | mso-hansi-theme-font:minor-latin'>Command/Copy selected</span></b> as before to |
---|
2212 | copy this new scale factor to the other Sa data sets. The plot will again be |
---|
2213 | redrawn</p> |
---|
2214 | |
---|
2215 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
2216 | id="Picture_x0020_57" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:525pt; |
---|
2217 | height:450pt;visibility:visible;mso-wrap-style:square'> |
---|
2218 | <v:imagedata src="Small%20Angle%20Image%20Processing_files/image039.png" |
---|
2219 | o:title=""/> |
---|
2220 | </v:shape><![endif]--><![if !vml]><img width=700 height=600 |
---|
2221 | src="Small%20Angle%20Image%20Processing_files/image039.png" v:shapes="Picture_x0020_57"><![endif]></span></p> |
---|
2222 | |
---|
2223 | <p class=MsoNormal><o:p> </o:p></p> |
---|
2224 | |
---|
2225 | <p class=MsoNormal>Everything is now on absolute scale and these polymer |
---|
2226 | samples are quite weak small angle <span class=SpellE>scatterers</span>. This |
---|
2227 | is a good point to do a <b style='mso-bidi-font-weight:normal'><span |
---|
2228 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
2229 | mso-hansi-theme-font:minor-latin'>File/Save project</span></b> from the main |
---|
2230 | GSAS-II data tree menu. You can try to fit unified & <span class=SpellE>Porod</span> |
---|
2231 | models to them following the procedures demonstrated in the <strong><span |
---|
2232 | style='font-weight:normal'>Fitting Small Angle X-Ray Data</span></strong><strong><span |
---|
2233 | style='font-weight:normal;mso-bidi-font-weight:bold'> tutorial. Id set the |
---|
2234 | high Q limit to about 0.25Å<sup>-1</sup> as above that is only noisy |
---|
2235 | background.</span></strong></p> |
---|
2236 | |
---|
2237 | </div> |
---|
2238 | |
---|
2239 | </body> |
---|
2240 | |
---|
2241 | </html> |
---|