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	408	<w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/>
	409	<w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/>
	410	<w:LsdException Locked="false" Priority="70" Name="Dark List"/>
	411	<w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/>
	412	<w:LsdException Locked="false" Priority="72" Name="Colorful List"/>
	413	<w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
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	415	<w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
	416	<w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
	417	<w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
	418	<w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
	419	<w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
	420	<w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
	421	<w:LsdException Locked="false" Priority="34" QFormat="true"
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	423	<w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
	424	<w:LsdException Locked="false" Priority="30" QFormat="true"
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	426	<w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
	427	<w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
	428	<w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
	429	<w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
	430	<w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
	431	<w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
	432	<w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
	433	<w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
	434	<w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
	435	<w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
	436	<w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
	437	<w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
	438	<w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
	439	<w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
	440	<w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
	441	<w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
	442	<w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
	443	<w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
	444	<w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
	445	<w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
	446	<w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
	447	<w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
	448	<w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
	449	<w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
	450	<w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
	451	<w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
	452	<w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
	453	<w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
	454	<w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
	455	<w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
	456	<w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
	457	<w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
	458	<w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
	459	<w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
	460	<w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
	461	<w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
	462	<w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
	463	<w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
	464	<w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
	465	<w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
	466	<w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
	467	<w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
	468	<w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
	469	<w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
	470	<w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
	471	<w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
	472	<w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
	473	<w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
	474	<w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
	475	<w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
	476	<w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
	477	<w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
	478	<w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
	479	<w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
	480	<w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
	481	<w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
	482	<w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
	483	<w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
	484	<w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
	485	<w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
	486	<w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
	487	<w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
	488	<w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
	489	<w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
	490	<w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
	491	<w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
	492	<w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
	493	<w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
	494	<w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
	495	<w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
	496	<w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
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	498	<w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
	499	<w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
	500	<w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
	501	<w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
	502	<w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
	503	<w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
	504	<w:LsdException Locked="false" Priority="19" QFormat="true"
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	506	<w:LsdException Locked="false" Priority="21" QFormat="true"
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	508	<w:LsdException Locked="false" Priority="31" QFormat="true"
	509	Name="Subtle Reference"/>
	510	<w:LsdException Locked="false" Priority="32" QFormat="true"
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	512	<w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
	513	<w:LsdException Locked="false" Priority="37" SemiHidden="true"
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	515	<w:LsdException Locked="false" Priority="39" SemiHidden="true"
	516	UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
	517	<w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
	518	<w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
	519	<w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
	520	<w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
	521	<w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
	522	<w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
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	524	<w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
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	526	<w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
	527	<w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
	528	<w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
	529	<w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
	530	<w:LsdException Locked="false" Priority="46"
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	532	<w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
	533	<w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
	534	<w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
	535	<w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
	536	<w:LsdException Locked="false" Priority="51"
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	538	<w:LsdException Locked="false" Priority="52"
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	540	<w:LsdException Locked="false" Priority="46"
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	543	<w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
	544	<w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
	545	<w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
	546	<w:LsdException Locked="false" Priority="51"
	547	Name="Grid Table 6 Colorful Accent 2"/>
	548	<w:LsdException Locked="false" Priority="52"
	549	Name="Grid Table 7 Colorful Accent 2"/>
	550	<w:LsdException Locked="false" Priority="46"
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	552	<w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
	553	<w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
	554	<w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
	555	<w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
	556	<w:LsdException Locked="false" Priority="51"
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	558	<w:LsdException Locked="false" Priority="52"
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	560	<w:LsdException Locked="false" Priority="46"
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	564	<w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
	565	<w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
	566	<w:LsdException Locked="false" Priority="51"
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	568	<w:LsdException Locked="false" Priority="52"
	569	Name="Grid Table 7 Colorful Accent 4"/>
	570	<w:LsdException Locked="false" Priority="46"
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	572	<w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
	573	<w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
	574	<w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
	575	<w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
	576	<w:LsdException Locked="false" Priority="51"
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	578	<w:LsdException Locked="false" Priority="52"
	579	Name="Grid Table 7 Colorful Accent 5"/>
	580	<w:LsdException Locked="false" Priority="46"
	581	Name="Grid Table 1 Light Accent 6"/>
	582	<w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
	583	<w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
	584	<w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
	585	<w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
	586	<w:LsdException Locked="false" Priority="51"
	587	Name="Grid Table 6 Colorful Accent 6"/>
	588	<w:LsdException Locked="false" Priority="52"
	589	Name="Grid Table 7 Colorful Accent 6"/>
	590	<w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
	591	<w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
	592	<w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
	593	<w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
	594	<w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
	595	<w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
	596	<w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
	597	<w:LsdException Locked="false" Priority="46"
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	600	<w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
	601	<w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
	602	<w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
	603	<w:LsdException Locked="false" Priority="51"
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	605	<w:LsdException Locked="false" Priority="52"
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	607	<w:LsdException Locked="false" Priority="46"
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	609	<w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
	610	<w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
	611	<w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
	612	<w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
	613	<w:LsdException Locked="false" Priority="51"
	614	Name="List Table 6 Colorful Accent 2"/>
	615	<w:LsdException Locked="false" Priority="52"
	616	Name="List Table 7 Colorful Accent 2"/>
	617	<w:LsdException Locked="false" Priority="46"
	618	Name="List Table 1 Light Accent 3"/>
	619	<w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
	620	<w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
	621	<w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
	622	<w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
	623	<w:LsdException Locked="false" Priority="51"
	624	Name="List Table 6 Colorful Accent 3"/>
	625	<w:LsdException Locked="false" Priority="52"
	626	Name="List Table 7 Colorful Accent 3"/>
	627	<w:LsdException Locked="false" Priority="46"
	628	Name="List Table 1 Light Accent 4"/>
	629	<w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
	630	<w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
	631	<w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
	632	<w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
	633	<w:LsdException Locked="false" Priority="51"
	634	Name="List Table 6 Colorful Accent 4"/>
	635	<w:LsdException Locked="false" Priority="52"
	636	Name="List Table 7 Colorful Accent 4"/>
	637	<w:LsdException Locked="false" Priority="46"
	638	Name="List Table 1 Light Accent 5"/>
	639	<w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
	640	<w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
	641	<w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
	642	<w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
	643	<w:LsdException Locked="false" Priority="51"
	644	Name="List Table 6 Colorful Accent 5"/>
	645	<w:LsdException Locked="false" Priority="52"
	646	Name="List Table 7 Colorful Accent 5"/>
	647	<w:LsdException Locked="false" Priority="46"
	648	Name="List Table 1 Light Accent 6"/>
	649	<w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
	650	<w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
	651	<w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
	652	<w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
	653	<w:LsdException Locked="false" Priority="51"
	654	Name="List Table 6 Colorful Accent 6"/>
	655	<w:LsdException Locked="false" Priority="52"
	656	Name="List Table 7 Colorful Accent 6"/>
[1705]	657	</w:LatentStyles>
	658	</xml><![endif]-->
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[3032]	665	mso-font-charset:1;
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	667	mso-font-pitch:variable;
[3032]	668	mso-font-signature:0 0 0 0 0 0;}
[1740]	669	@font-face
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	674	mso-font-pitch:variable;
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	681	mso-font-pitch:variable;
	682	mso-font-signature:-520081665 -1073717157 41 0 66047 0;}
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[1705]	693	mso-fareast-font-family:"Times New Roman";
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	698	mso-style-qformat:yes;
	699	mso-style-link:"Heading 1 Char";
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[1705]	708	mso-fareast-font-family:"Times New Roman";
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	711	h2
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	713	mso-style-priority:9;
	714	mso-style-qformat:yes;
	715	mso-style-link:"Heading 2 Char";
	716	mso-margin-top-alt:auto;
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	718	mso-margin-bottom-alt:auto;
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[1740]	723	font-family:"Times New Roman",serif;
[1705]	724	mso-fareast-font-family:"Times New Roman";
	725	mso-fareast-theme-font:minor-fareast;
	726	font-weight:bold;}
	727	h3
	728	{mso-style-noshow:yes;
	729	mso-style-priority:9;
	730	mso-style-qformat:yes;
	731	mso-style-link:"Heading 3 Char";
	732	mso-margin-top-alt:auto;
	733	margin-right:0in;
	734	mso-margin-bottom-alt:auto;
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[1740]	739	font-family:"Times New Roman",serif;
[1705]	740	mso-fareast-font-family:"Times New Roman";
	741	mso-fareast-theme-font:minor-fareast;
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	743	h4
	744	{mso-style-noshow:yes;
	745	mso-style-priority:9;
	746	mso-style-qformat:yes;
	747	mso-style-link:"Heading 4 Char";
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	766	mso-bidi-theme-font:major-bidi;
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	768	mso-themecolor:accent1;
	769	font-weight:bold;
	770	font-style:italic;}
	771	h5
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	774	mso-style-qformat:yes;
	775	mso-style-link:"Heading 5 Char";
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	1220
	1221	<h1><strong>Fitting</strong><strong><span style='mso-bidi-font-weight:normal'>
	1222	Small Angle X-Ray Data Alumina Powder</span><o:p></o:p></strong></h1>
	1223
[3553]	1224	<P><B>A video version of this tutorial is available at
	1225	<A href="https://anl.box.com/v/FittingSmallAngleScatteringDat" target="_blank">
	1226	https://anl.box.com/v/FittingSmallAngleScatteringDat</A></B></P>
	1227
[1705]	1228	<p class=MsoNormal style='mso-layout-grid-align:none;text-autospace:none'>In
	1229	this tutorial you will fit small angle scattering data for an alumina polishing
[3032]	1230	powder using data from a constant wavelength synchrotron X-ray USAXS
	1231	instrument. You will use both a lognormal distribution of spherical particles
	1232	model and a unified <span class=SpellE>Guinier-Porod</span> model. The data
	1233	were collected from <span style='mso-fareast-font-family:Calibri;mso-fareast-theme-font:
	1234	minor-latin;mso-bidi-font-weight:bold;mso-bidi-font-style:italic'>powders
	1235	spread onto sticky tape and covered with another layer of the same tape. The
	1236	data were corrected for background using data collected from two layers of
	1237	sticky tape. However, the sample thickness is not</span> accurately known <span
[1705]	1238	style='mso-fareast-font-family:Calibri;mso-fareast-theme-font:minor-latin;
	1239	mso-bidi-font-weight:bold;mso-bidi-font-style:italic'>so the data are not
	1240	calibrated on an absolute scale.<o:p></o:p></span></p>
	1241
[1740]	1242	<p class=MsoNormal>If you have not done so already, start GSAS-II.</p>
[1705]	1243
	1244	<h2>Step 1: read in the data file</h2>
	1245
	1246	<p class=MsoListParagraphCxSpFirst style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span
	1247	style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span
	1248	style='font:7.0pt "Times New Roman"'>      </span></span></span><![endif]>If
	1249	you have saved the GSAS-II project file from the <b style='mso-bidi-font-weight:
[1740]	1250	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1251	minor-latin;mso-hansi-theme-font:minor-latin'>Size Distribution</span></b>
	1252	tutorial, use <b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1253	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1254	minor-latin'>File/Open project</span></b> menu item to retrieve the data;
	1255	plots of the size distribution and the data will appear. Then go to <!--[if supportFields]><b
[1740]	1256	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1257	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'><span
	1258	style='mso-element:field-begin'></span><span
	1259	style='mso-spacerun:yes'> </span>REF _Ref386704789 \h<span
	1260	style='mso-spacerun:yes'> </span>\* MERGEFORMAT <span style='mso-element:field-separator'></span></span></b><![endif]--><b
[1740]	1261	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1262	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Step 2: Set
	1263	Limits<!--[if gte mso 9]><xml>
	1264	<w:data>08D0C9EA79F9BACE118C8200AA004BA90B02000000080000000E0000005F005200650066003300380036003700300034003700380039000000</w:data>
	1265	</xml><![endif]--></span></b><!--[if supportFields]><b style='mso-bidi-font-weight:
[1740]	1266	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1267	minor-latin;mso-hansi-theme-font:minor-latin'><span style='mso-element:field-end'></span></span></b><![endif]-->.
	1268	Otherwise, use the <b style='mso-bidi-font-weight:normal'><span
[1740]	1269	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[2791]	1270	mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Import/Small
	1271	Angle Data/from q (A-1) step X-ray QIE data file</span></b> menu item to read
	1272	the data file into GSAS-II. This read option is set to read three column small
	1273	angle scattering data (SASD) as Q in Å<sup>-1</sup>, intensity and estimated
	1274	standard deviation in intensity; there may be a header with metadata
	1275	information in the front of this file.<span style='mso-spacerun:yes'>
	1276	</span>Change the file directory to <span class=SpellE><b style='mso-bidi-font-weight:
	1277	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
	1278	minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>SAfit</span></b></span><b
[1740]	1279	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[2791]	1280	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
	1281	minor-latin'>/data</span></b><span style='font-family:"Calibri",sans-serif;
	1282	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
[1705]	1283	minor-latin'> to find the file</span>; you will have to select the <b
[1740]	1284	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1285	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>any file
	1286	(.)</span></b> filter to see it.</p>
	1287
	1288	<p class=MsoListParagraphCxSpLast style='text-indent:-.25in;mso-list:l0 level1 lfo2'><![if !supportLists]><span
	1289	style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span
	1290	style='font:7.0pt "Times New Roman"'>      </span></span></span><![endif]>Select
[1740]	1291	the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[2791]	1292	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
	1293	minor-latin'>alumina data.dat</span></b><span style='font-family:"Calibri",sans-serif;
	1294	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
[1705]	1295	minor-latin'> data</span> file in the first dialog and press <b
[1740]	1296	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[2791]	1297	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
	1298	minor-latin'>Open</span></b>. There will be a Dialog box asking <span
	1299	class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family:
	1300	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
	1301	minor-latin;mso-bidi-theme-font:minor-latin'>Is</span></b></span><b
	1302	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
	1303	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
	1304	minor-latin'> this the file you want?</span></b> Press <span class=GramE><b
	1305	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
	1306	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
	1307	minor-latin'>Yes</span></b></span> button to proceed.</p>
[1705]	1308
	1309	<p class=MsoNormal>At this point the <b style='mso-bidi-font-weight:normal'><span
[1740]	1310	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[2791]	1311	mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data
	1312	tree</span></b> window will have several entries and the plot window will show
	1313	the SASD pattern as a log-log plot of intensity vs. Q</p>
[1705]	1314
	1315	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype
	1316	id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t"
	1317	path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f">
	1318	<v:stroke joinstyle="miter"/>
	1319	<v:formulas>
	1320	<v:f eqn="if lineDrawn pixelLineWidth 0"/>
	1321	<v:f eqn="sum @0 1 0"/>
	1322	<v:f eqn="sum 0 0 @1"/>
	1323	<v:f eqn="prod @2 1 2"/>
	1324	<v:f eqn="prod @3 21600 pixelWidth"/>
	1325	<v:f eqn="prod @3 21600 pixelHeight"/>
	1326	<v:f eqn="sum @0 0 1"/>
	1327	<v:f eqn="prod @6 1 2"/>
	1328	<v:f eqn="prod @7 21600 pixelWidth"/>
	1329	<v:f eqn="sum @8 21600 0"/>
	1330	<v:f eqn="prod @7 21600 pixelHeight"/>
	1331	<v:f eqn="sum @10 21600 0"/>
	1332	</v:formulas>
	1333	<v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
	1334	<o:lock v:ext="edit" aspectratio="t"/>
[3032]	1335	</v:shapetype><v:shape id="Picture_x0020_24" o:spid="_x0000_i1047" type="#_x0000_t75"
	1336	style='width:468pt;height:401.25pt;visibility:visible;mso-wrap-style:square'>
	1337	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image002.png"
[1705]	1338	o:title=""/>
[3032]	1339	</v:shape><![endif]--><![if !vml]><img width=624 height=535
	1340	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image001.png" v:shapes="Picture_x0020_24"><![endif]></span></p>
[1705]	1341
	1342	<h2><a name="_Ref386704789">Step 2: Set Limits</a></h2>
	1343
	1344	<p class=MsoNormal>For this step we will reposition the limits to exclude only
	1345	the last point in the pattern as it does appear to be somewhat suspect (see
	1346	plot). Select <b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1347	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1348	minor-latin'>Limits</span></b> under <b style='mso-bidi-font-weight:normal'><span
[1740]	1349	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1350	mso-hansi-theme-font:minor-latin'>SASD alumina data.dat</span></b> from the
	1351	GSAS-II tree. Set the upper limit using the cursor on the plot by picking the
[2791]	1352	next-to-last point on the curve with the left or right mouse button. If needed
[3032]	1353	reposition the lower limit to be the 1<sup>st</sup> data point. The limits window
	1354	should look like</p>
[1705]	1355
	1356	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1357	id="Picture_x0020_25" o:spid="_x0000_i1046" type="#_x0000_t75" style='width:382.5pt;
	1358	height:276pt;visibility:visible;mso-wrap-style:square'>
	1359	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image005.png"
[1705]	1360	o:title=""/>
[3032]	1361	</v:shape><![endif]--><![if !vml]><img width=510 height=368
	1362	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image005.png" v:shapes="Picture_x0020_25"><![endif]></span><span
[1705]	1363	style='mso-spacerun:yes'> </span></p>
	1364
	1365	<h2>Step 3 Select the scattering substances for your sample</h2>
	1366
	1367	<p class=MsoNormal><span style='mso-no-proof:yes'>If you have already done this
	1368	step in the </span><b style='mso-bidi-font-weight:normal'><span
[1740]	1369	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1370	mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Size Distribution</span></b><span
	1371	style='mso-no-proof:yes'> tutorial, skip to </span><!--[if supportFields]><b
[1740]	1372	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1373	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:
	1374	yes'><span style='mso-element:field-begin'></span><span
	1375	style='mso-spacerun:yes'> </span>REF _Ref386699439 \h<span
	1376	style='mso-spacerun:yes'> </span>\* MERGEFORMAT <span style='mso-element:field-separator'></span></span></b><![endif]--><b
[1740]	1377	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[3032]	1378	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Step 4 Creation
	1379	and Refinement of Log Normal Particle Model<span style='mso-no-proof:yes'><!--[if gte mso 9]><xml>
[1705]	1380	<w:data>08D0C9EA79F9BACE118C8200AA004BA90B02000000080000000E0000005F005200650066003300380036003600390039003400330039000000</w:data>
	1381	</xml><![endif]--></span></span></b><!--[if supportFields]><b style='mso-bidi-font-weight:
[1740]	1382	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1383	minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'><span
	1384	style='mso-element:field-end'></span></span></b><![endif]--><span
	1385	style='mso-no-proof:yes'>. Two substances need to be defined for your sample to
	1386	give the anticipated scattering contrast; in this case one is alumina and the
	1387	other is vacuum (really air). Parameters for a number of substances are
	1388	defined in the file </span><b style='mso-bidi-font-weight:normal'><span
[1740]	1389	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1390	mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Substances.py</span></b><span
	1391	style='mso-no-proof:yes'>. You can add your own substances to this or better
	1392	put them in </span><b style='mso-bidi-font-weight:normal'><span
[1740]	1393	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1394	mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>UserSubstances.py</span></b><span
	1395	style='mso-no-proof:yes'>; this is read after Substances.py when you load
	1396	substances for your selection. </span>Select <b style='mso-bidi-font-weight:
[1740]	1397	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1398	minor-latin;mso-hansi-theme-font:minor-latin'>Substances</span></b> under <b
[1740]	1399	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1400	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina
[2791]	1401	data.dat</span></b> from the GSAS-II tree. Then do <span class=GramE><b
	1402	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
	1403	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Edit</span></b></span><b
	1404	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[3032]	1405	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>
	1406	substance/Load</span></b> <b style='mso-bidi-font-weight:normal'><span
	1407	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
	1408	mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>substance</span></b>
	1409	from the menu; a popup window will appear with possible selections</p>
[1705]	1410
	1411	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
	1412	id="Picture_x0020_3" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:259.5pt;
	1413	height:252pt;visibility:visible;mso-wrap-style:square'>
	1414	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image003.png"
	1415	o:title=""/>
[1740]	1416	</v:shape><![endif]--><![if !vml]><img width=346 height=336
[1705]	1417	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image003.png" v:shapes="Picture_x0020_3"><![endif]><o:p></o:p></span></p>
	1418
	1419	<p class=MsoNormal><o:p> </o:p></p>
	1420
	1421	<p class=MsoNormal>Select <b style='mso-bidi-font-weight:normal'><span
[1740]	1422	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1423	mso-hansi-theme-font:minor-latin'>Alumina</span></b> and press <b
[1740]	1424	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1425	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>;
[2791]	1426	the relevant data for alumina (and vacuum& unit scatter) are displayed next</p>
[1705]	1427
	1428	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1429	id="Picture_x0020_26" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:417pt;
	1430	height:269.25pt;visibility:visible;mso-wrap-style:square'>
	1431	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image017.png"
[1705]	1432	o:title=""/>
[3032]	1433	</v:shape><![endif]--><![if !vml]><img width=556 height=359
	1434	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image017.png" v:shapes="Picture_x0020_26"><![endif]></span><span
[1705]	1435	style='mso-spacerun:yes'> </span></p>
	1436
	1437	<p class=MsoNormal><o:p> </o:p></p>
	1438
	1439	<p class=MsoNormal>If desired you can load/add as many substances as you desire
[2791]	1440	into this list; you can also delete any of them (except vacuum & unit
	1441	scatter). The composition, volume occupied by the atoms in the composition and
	1442	the density are given for each substance. These can each be edited; the other
	1443	values will change accordingly. If your substance isnt in the list, you can <span
	1444	class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family:
	1445	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
	1446	minor-latin'>Edit</span></b></span><b style='mso-bidi-font-weight:normal'><span
	1447	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
	1448	mso-hansi-theme-font:minor-latin'> substance/Add substance</span></b> to create
[3032]	1449	a new one (you will be asked for a name and the set of elements in two successive
	1450	popup windows). From this information the scattering density and that as
	1451	affected by resonant scattering for the listed wavelength is displayed (the
	1452	wavelength can be changed in the <b style='mso-bidi-font-weight:normal'><span
[2791]	1453	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
	1454	mso-hansi-theme-font:minor-latin'>Instrument Parameters</span></b> GSAS-II tree
	1455	item if needed). The resonant scattering value is used for contrast
	1456	calculations.</p>
[1705]	1457
	1458	<h2><a name="_Ref386699439"></a><a name="_Ref386699331"><span style='mso-bookmark:
	1459	_Ref386699439'>Step 4 </span></a><span style='mso-bookmark:_Ref386699439'>Creation
	1460	and Refinement of Log Normal Particle Model</span></h2>
	1461
	1462	<p class=MsoNormal>You are now ready to attempt fitting the data with a log
	1463	normal distribution of spherical particles. Thus youll need to select <b
[1740]	1464	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1465	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models</span></b>
[1740]	1466	under <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1467	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>SASD alumina
	1468	data.dat</span></b> from the GSAS-II tree; the data window will display the <b
[1740]	1469	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1470	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Size dist.</span></b>
	1471	display;<span style='mso-no-proof:yes'> </span>change this to <b
[1740]	1472	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1473	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Particle fit</span></b>
[1740]	1474	using the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1475	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Modeling by</span></b>
	1476	pull down. NB: GSAS-II will remember your selection the next time you enter
[1740]	1477	this <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1478	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models</span></b>
	1479	data tree item.</p>
	1480
	1481	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1482	id="Picture_x0020_27" o:spid="_x0000_i1043" type="#_x0000_t75" style='width:468pt;
	1483	height:227.25pt;visibility:visible;mso-wrap-style:square'>
	1484	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image029.png"
[1705]	1485	o:title=""/>
[3032]	1486	</v:shape><![endif]--><![if !vml]><img width=624 height=303
	1487	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image006.png" v:shapes="Picture_x0020_27"><![endif]></span></p>
[1705]	1488
	1489	<p class=MsoNormal><o:p> </o:p></p>
	1490
	1491	<p class=MsoNormal>If you had done the <b style='mso-bidi-font-weight:normal'><span
[1740]	1492	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1493	mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> tutorial, you
	1494	would know that there were two populations of particles in the sample. One had
	1495	a mean diameter of ~1300A and the other had a mean diameter of ~150A. You will
	1496	also need something to describe the very lowest Q portion of the data. Do <b
[1740]	1497	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1498	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Add</span></b>
	1499	from the menu; the data window will change and the plots will be refreshed.
	1500	Your first step is to change the <b style='mso-bidi-font-weight:normal'><span
[1740]	1501	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1502	mso-hansi-theme-font:minor-latin'>Material</span></b> to <b style='mso-bidi-font-weight:
[1740]	1503	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1504	minor-latin;mso-hansi-theme-font:minor-latin'>Alumina</span></b> and make sure
[1740]	1505	the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1506	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background</span></b>
	1507	is something reasonable (<b style='mso-bidi-font-weight:normal'><span
[1740]	1508	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[2791]	1509	mso-hansi-theme-font:minor-latin'>0.12</span></b>) based on the data at highest
[1740]	1510	Q; again the data window and plots will be refreshed. Click on one of the
	1511	slider buttons to force a calculation.</p>
[1705]	1512
	1513	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1514	id="Picture_x0020_28" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:468pt;
	1515	height:258pt;visibility:visible;mso-wrap-style:square'>
	1516	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image031.png"
[1705]	1517	o:title=""/>
[3032]	1518	</v:shape><![endif]--><![if !vml]><img width=624 height=344
	1519	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image007.png" v:shapes="Picture_x0020_28"><![endif]></span></p>
[1705]	1520
	1521	<p class=MsoNormal><o:p> </o:p></p>
	1522
	1523	<p class=MsoNormal>The data plot shows a horizontal red line for the background
	1524	and a green one calculated from your selected model. </p>
	1525
	1526	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1527	id="Picture_x0020_29" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:412.5pt;
	1528	height:354pt;visibility:visible;mso-wrap-style:square'>
	1529	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image033.png"
[1705]	1530	o:title=""/>
[3032]	1531	</v:shape><![endif]--><![if !vml]><img width=550 height=472
	1532	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image008.png" v:shapes="Picture_x0020_29"><![endif]></span></p>
[1705]	1533
	1534	<p class=MsoNormal><o:p> </o:p></p>
	1535
	1536	<p class=MsoNormal>You can manually adjust the calculated curve by using the
	1537	sliders: increase <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[1740]	1538	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1539	mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:
[1740]	1540	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1541	minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b> and decrease <span
	1542	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1543	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1544	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1545	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1546	mso-hansi-theme-font:minor-latin'> Mean</span></b> to improve the fit. NB: The <span
	1547	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1548	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1549	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1550	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1551	mso-hansi-theme-font:minor-latin'> Mean</span></b> is a radius so its value is
	1552	roughly œ the <b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1553	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1554	minor-latin'>Size Distribution</span></b> result. The sliders cover 2 orders of
	1555	magnitude; their range is reset if a value is entered in the value field. After
	1556	changing <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[1740]	1557	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1558	mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:
[1740]	1559	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1560	minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b> to <b
[1740]	1561	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1562	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>700</span></b>
	1563	and <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[1740]	1564	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1565	mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:
[1740]	1566	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1567	minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b> to <b
[1740]	1568	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1569	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0.0953</span></b>
	1570	my plot is</p>
	1571
	1572	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1573	id="Picture_x0020_30" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:441.75pt;
	1574	height:378.75pt;visibility:visible;mso-wrap-style:square'>
	1575	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image035.png"
[1705]	1576	o:title=""/>
[3032]	1577	</v:shape><![endif]--><![if !vml]><img width=589 height=505
	1578	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image009.png" v:shapes="Picture_x0020_30"><![endif]></span></p>
[1705]	1579
	1580	<p class=MsoNormal><o:p> </o:p></p>
	1581
	1582	<p class=MsoNormal>There is an obvious discrepancy at low Q and a much less
	1583	obvious one at Q~0.03-4Å<sup>-1</sup>; the latter is responsible for the ~150Å
	1584	peak in the <b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1585	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1586	minor-latin'>Size Distribution</span></b> result. Do another <b
[1740]	1587	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1588	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Models/Add</span></b>
	1589	to include it. The data window now shows two components</p>
	1590
	1591	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1592	id="Picture_x0020_31" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:468pt;
	1593	height:398.25pt;visibility:visible;mso-wrap-style:square'>
	1594	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image037.png"
[1705]	1595	o:title=""/>
[3032]	1596	</v:shape><![endif]--><![if !vml]><img width=624 height=531
	1597	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image010.png" v:shapes="Picture_x0020_31"><![endif]></span></p>
[1705]	1598
	1599	<p class=MsoNormal><o:p> </o:p></p>
	1600
	1601	<p class=MsoNormal>Note the <b style='mso-bidi-font-weight:normal'><span
[1740]	1602	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1603	mso-hansi-theme-font:minor-latin'>Material</span></b> for the new one is preset
[1740]	1604	to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1605	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Alumina</span></b>
	1606	to save you the easily forgotten step of setting it. Change <span class=SpellE><b
[1740]	1607	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1608	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
[1740]	1609	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1610	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b>
[1740]	1611	to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1612	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>75</span></b>
	1613	(i.e. œ of 150) and reduce <span class=SpellE><b style='mso-bidi-font-weight:
[1740]	1614	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1615	minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
[1740]	1616	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1617	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Volume</span></b>
	1618	to make the green curve better match the data (you can inset <b
[1740]	1619	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1620	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>0</span></b>s
	1621	in the value & play with the slider something like <b style='mso-bidi-font-weight:
[1740]	1622	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1623	minor-latin;mso-hansi-theme-font:minor-latin'>0.0003</span></b> looks good). My
	1624	fit looked like</p>
	1625
	1626	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1627	id="Picture_x0020_32" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:435pt;
	1628	height:372.75pt;visibility:visible;mso-wrap-style:square'>
	1629	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image039.png"
[1705]	1630	o:title=""/>
[3032]	1631	</v:shape><![endif]--><![if !vml]><img width=580 height=497
	1632	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image011.png" v:shapes="Picture_x0020_32"><![endif]></span></p>
[1705]	1633
	1634	<p class=MsoNormal><o:p> </o:p></p>
	1635
	1636	<p class=MsoNormal>Finally we need to deal with the low Q region this is
	1637	probably due to some agglomeration of the 1300Å articles which is best
	1638	described by a pure <span class=SpellE>Porod</span> power law scattering model.
	1639	Do another <b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1640	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1641	minor-latin'>Models/Add</span></b> and change the <b style='mso-bidi-font-weight:
[1740]	1642	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1643	minor-latin;mso-hansi-theme-font:minor-latin'>Distribution </span></b>selection
	1644	to <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[1740]	1645	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1646	mso-hansi-theme-font:minor-latin'>Porod</span></b></span>. The third component
	1647	is then (Ive shrunk the window & moved the scroll bar).</p>
	1648
	1649	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1650	id="Picture_x0020_33" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:468pt;
	1651	height:313.5pt;visibility:visible;mso-wrap-style:square'>
	1652	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image041.png"
[1705]	1653	o:title=""/>
[3032]	1654	</v:shape><![endif]--><![if !vml]><img width=624 height=418
	1655	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image012.png" v:shapes="Picture_x0020_33"><![endif]></span></p>
[1705]	1656
	1657	<p class=MsoNormal><o:p> </o:p></p>
	1658
	1659	<p class=MsoNormal>The green curve on the plot looks very poor</p>
	1660
	1661	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1662	id="Picture_x0020_34" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:444pt;
	1663	height:380.25pt;visibility:visible;mso-wrap-style:square'>
	1664	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image043.png"
[1705]	1665	o:title=""/>
[3032]	1666	</v:shape><![endif]--><![if !vml]><img width=592 height=507
	1667	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image013.png" v:shapes="Picture_x0020_34"><![endif]></span></p>
[1705]	1668
	1669	<p class=MsoNormal><o:p> </o:p></p>
	1670
	1671	<p class=MsoNormal>Not to worry, all the problem is in the <span class=SpellE>Porod</span>
	1672	component variables. Remembering that this is likely to be an agglomeration of
	1673	1300Å particles; set the <span class=SpellE><b style='mso-bidi-font-weight:
[1740]	1674	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1675	minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
[1740]	1676	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1677	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Cutoff</span></b>
	1678	to that value. That immediately restores the higher Q portion of the fit.</p>
	1679
	1680	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1681	id="Picture_x0020_35" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:468pt;
	1682	height:401.25pt;visibility:visible;mso-wrap-style:square'>
	1683	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image045.png"
[1705]	1684	o:title=""/>
[3032]	1685	</v:shape><![endif]--><![if !vml]><img width=624 height=535
	1686	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image014.png" v:shapes="Picture_x0020_35"><![endif]></span></p>
[1705]	1687
	1688	<p class=MsoNormal><o:p> </o:p></p>
	1689
	1690	<p class=MsoNormal>Next use the <span class=SpellE><b style='mso-bidi-font-weight:
[1740]	1691	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1692	minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
[1740]	1693	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1694	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> P</span></b>
	1695	(power law exponent) slider to adjust the fit. In this case setting <span
	1696	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1697	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1698	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1699	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1700	mso-hansi-theme-font:minor-latin'> P</span></b> to ~<b style='mso-bidi-font-weight:
[1740]	1701	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1702	minor-latin;mso-hansi-theme-font:minor-latin'>3.25</span></b> gives a pretty
	1703	good fit without needing to adjust the <span class=SpellE><b style='mso-bidi-font-weight:
[1740]	1704	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1705	minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
[1740]	1706	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1707	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> B</span></b>
	1708	<span class=SpellE>prefactor</span>.</p>
	1709
	1710	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1711	id="Picture_x0020_36" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:468pt;
	1712	height:401.25pt;visibility:visible;mso-wrap-style:square'>
	1713	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image047.png"
[1705]	1714	o:title=""/>
[3032]	1715	</v:shape><![endif]--><![if !vml]><img width=624 height=535
	1716	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image015.png" v:shapes="Picture_x0020_36"><![endif]></span></p>
[1705]	1717
	1718	<p class=MsoNormal><o:p> </o:p></p>
	1719
[1740]	1720	<p class=MsoNormal>Finally, you can refine these coefficients to find the best
	1721	fit to the data. As a beginner, Id start by refining just the two <span
[1705]	1722	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1723	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1724	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1725	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1726	mso-hansi-theme-font:minor-latin'> Volume</span></b> and the <span
	1727	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1728	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1729	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1730	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1731	mso-hansi-theme-font:minor-latin'> B</span></b> along with the <b
[1740]	1732	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1733	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background</span></b>
[3032]	1734	parameter (one might be able to refine everything at once, but then again it
[1705]	1735	might not work). Check the <b style='mso-bidi-font-weight:normal'><span
[1740]	1736	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[2791]	1737	mso-hansi-theme-font:minor-latin'>Refine?</span></b> <span class=GramE>boxes</span>
	1738	for these parameters. Do <b style='mso-bidi-font-weight:normal'><span
[1740]	1739	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[2791]	1740	mso-hansi-theme-font:minor-latin'>Models/Fit </span></b>to do the least squares
	1741	refinement; convergence will occur very quickly. NB: if the refinement messes
	1742	up, you can recover the previous result; do <b style='mso-bidi-font-weight:
	1743	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
	1744	minor-latin;mso-hansi-theme-font:minor-latin'>Models/Undo</span></b> to
	1745	recover. Then add the two <span class=SpellE><b style='mso-bidi-font-weight:
	1746	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
	1747	minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
	1748	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
	1749	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b>
	1750	and <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[1740]	1751	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1752	mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:
[1740]	1753	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[2791]	1754	minor-latin;mso-hansi-theme-font:minor-latin'> P</span></b> parameters to the
	1755	refinement, again convergence is easily obtained. Finally, add the two <span
[1705]	1756	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1757	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1758	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1759	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[3032]	1760	mso-hansi-theme-font:minor-latin'> <span class=SpellE>StdDev</span></span></b>
	1761	and <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[2791]	1762	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
	1763	mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:
	1764	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
	1765	minor-latin;mso-hansi-theme-font:minor-latin'> Cutoff</span></b> parameters (a
	1766	total of ten) to the list. The result is a really nice fit to the data with
	1767	reasonable values; the console window shows the full results of the refinement</p>
[1705]	1768
	1769	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1770	id="Picture_x0020_37" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:468pt;
	1771	height:196.5pt;visibility:visible;mso-wrap-style:square'>
	1772	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image049.png"
[1705]	1773	o:title=""/>
[3032]	1774	</v:shape><![endif]--><![if !vml]><img width=624 height=262
	1775	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image016.png" v:shapes="Picture_x0020_37"><![endif]></span></p>
[1705]	1776
	1777	<p class=MsoNormal><o:p> </o:p></p>
	1778
	1779	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1780	id="Picture_x0020_38" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:429pt;
	1781	height:367.5pt;visibility:visible;mso-wrap-style:square'>
	1782	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image051.png"
[1705]	1783	o:title=""/>
[3032]	1784	</v:shape><![endif]--><![if !vml]><img width=572 height=490
	1785	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image024.png" v:shapes="Picture_x0020_38"><![endif]></span></p>
[1705]	1786
	1787	<p class=MsoNormal><o:p> </o:p></p>
	1788
	1789	<p class=MsoNormal>If you had done a <b style='mso-bidi-font-weight:normal'><span
[1740]	1790	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1791	mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> analysis, these
	1792	results are plotted as component curves on that plot as well</p>
	1793
	1794	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1795	id="Picture_x0020_39" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:468pt;
[2791]	1796	height:401.25pt;visibility:visible;mso-wrap-style:square'>
[3032]	1797	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image053.png"
[1705]	1798	o:title=""/>
[2791]	1799	</v:shape><![endif]--><![if !vml]><img width=624 height=535
[3032]	1800	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image025.png" v:shapes="Picture_x0020_39"><![endif]></span></p>
[1705]	1801
	1802	<p class=MsoNormal><o:p> </o:p></p>
	1803
[3032]	1804	<p class=MsoNormal>This is the sort of agreement one should expect between the best
	1805	log normal fit and the size distribution. To save these results you must do <b
	1806	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1807	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/Save
	1808	project </span></b>in the main <b style='mso-bidi-font-weight:normal'><span
[1740]	1809	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[3032]	1810	mso-hansi-theme-font:minor-latin'>GSAS-II data tree</span></b> menu.</p>
[1705]	1811
	1812	<h2>Step 6 Creation of a Unified <span class=SpellE>Guinier-Porod</span> Model</h2>
	1813
[3032]	1814	<p class=MsoNormal>For the Unified model there is assumed to be particles with some
	1815	radius of gyration (<span class=SpellE>Guinier</span> model) with a power law
	1816	distribution tail (<span class=SpellE>Porod</span> model). This can be set for
	1817	your model by changing the <b style='mso-bidi-font-weight:normal'><span
[1740]	1818	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1819	mso-hansi-theme-font:minor-latin'>Distribution</span></b> for the first two
	1820	components to <b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1821	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1822	minor-latin'>Unified</span></b>. NB: the log normal coefficients are not lost
	1823	by this step; they can be recovered by simply changing the <b style='mso-bidi-font-weight:
[1740]	1824	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1825	minor-latin;mso-hansi-theme-font:minor-latin'>Distribution</span></b> back to <span
	1826	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1827	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1828	minor-latin'>LogNormal</span></b></span>. The data window values give the
	1829	defaults for these components</p>
	1830
	1831	<p class=MsoNormal><span style='mso-no-proof:yes'><span
[3032]	1832	style='mso-spacerun:yes'> </span><!--[if gte vml 1]><v:shape id="Picture_x0020_40"
	1833	o:spid="_x0000_i1030" type="#_x0000_t75" style='width:468pt;height:459.75pt;
[1705]	1834	visibility:visible;mso-wrap-style:square'>
[3032]	1835	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image026.png"
[1705]	1836	o:title=""/>
[3032]	1837	</v:shape><![endif]--><![if !vml]><img width=624 height=613
	1838	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image027.png" v:shapes="Picture_x0020_40"><![endif]></span></p>
[1705]	1839
	1840	<p class=MsoNormal><o:p> </o:p></p>
	1841
	1842	<p class=MsoNormal>And the plot shows a poor fit</p>
	1843
	1844	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1845	id="Picture_x0020_41" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:468pt;
	1846	height:401.25pt;visibility:visible;mso-wrap-style:square'>
	1847	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image028.png"
[1705]	1848	o:title=""/>
[3032]	1849	</v:shape><![endif]--><![if !vml]><img width=624 height=535
	1850	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image055.png" v:shapes="Picture_x0020_41"><![endif]></span></p>
[1705]	1851
	1852	<p class=MsoNormal><o:p> </o:p></p>
	1853
	1854	<p class=MsoNormal>First, change the <span class=SpellE><b style='mso-bidi-font-weight:
[1740]	1855	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1856	minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
[1740]	1857	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1858	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> <span
	1859	class=SpellE>Rg</span></span></b> values to be about œ the <b style='mso-bidi-font-weight:
[1740]	1860	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1861	minor-latin;mso-hansi-theme-font:minor-latin'>Size Distribution</span></b>
	1862	results (e.g. <b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1863	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1864	minor-latin'>700</span></b> & <b style='mso-bidi-font-weight:normal'><span
[1740]	1865	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1866	mso-hansi-theme-font:minor-latin'>75</span></b>), then set the <span
	1867	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1868	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1869	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1870	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1871	mso-hansi-theme-font:minor-latin'> Cutoff</span></b> value for the <span
	1872	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1873	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1874	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1875	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1876	mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span></span></b>=700
[1740]	1877	one to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1878	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>100</span></b>.
	1879	Next, change the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[1740]	1880	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1881	mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:
[1740]	1882	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1883	minor-latin;mso-hansi-theme-font:minor-latin'> G</span></b> for the <span
	1884	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1885	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1886	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1887	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1888	mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span>=700</span></b>
	1889	one to be about the Intensity value for the lower Q bump in the data (~<b
[1740]	1890	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1891	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1.0e6</span></b>).
	1892	Finally, reduce the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[1740]	1893	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1894	mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:
[1740]	1895	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1896	minor-latin;mso-hansi-theme-font:minor-latin'> G</span></b> value for the <span
	1897	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1898	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1899	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1900	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1901	mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span>=75</span></b>
	1902	component to get the best fit to the data (~<b style='mso-bidi-font-weight:
[1740]	1903	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1904	minor-latin;mso-hansi-theme-font:minor-latin'>210</span></b>). The data window
	1905	looks like</p>
	1906
	1907	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1908	id="Picture_x0020_42" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:446.25pt;
	1909	height:438.75pt;visibility:visible;mso-wrap-style:square'>
	1910	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image056.png"
[1705]	1911	o:title=""/>
[3032]	1912	</v:shape><![endif]--><![if !vml]><img width=595 height=585
	1913	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image057.png" v:shapes="Picture_x0020_42"><![endif]></span></p>
[1705]	1914
	1915	<p class=MsoNormal><o:p> </o:p></p>
	1916
	1917	<p class=MsoNormal>And the plot looks like</p>
	1918
	1919	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1920	id="Picture_x0020_43" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:468pt;
	1921	height:401.25pt;visibility:visible;mso-wrap-style:square'>
	1922	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image058.png"
[1705]	1923	o:title=""/>
[3032]	1924	</v:shape><![endif]--><![if !vml]><img width=624 height=535
	1925	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image059.png" v:shapes="Picture_x0020_43"><![endif]></span></p>
[1705]	1926
	1927	<p class=MsoNormal><o:p> </o:p></p>
	1928
	1929	<p class=MsoNormal>This is probably close enough to do a refinement. Select <b
[1740]	1930	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1931	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Refine?</span></b>
	1932	For <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[1740]	1933	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1934	mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:
[1740]	1935	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1936	minor-latin;mso-hansi-theme-font:minor-latin'> G</span></b>, <span
	1937	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1938	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1939	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1940	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1941	mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span></span></b> and <span
	1942	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1943	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1944	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1945	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1946	mso-hansi-theme-font:minor-latin'> B</span></b> for both components (the <span
	1947	class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
[1740]	1948	"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
[1705]	1949	minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:normal'><span
[1740]	1950	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1951	mso-hansi-theme-font:minor-latin'> B</span></b>, <span class=SpellE><b
[1740]	1952	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1953	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
[1740]	1954	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1955	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> P</span></b>
[1740]	1956	and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1957	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Background
	1958	Refine?</span></b> boxes should also be checked). Then do <b style='mso-bidi-font-weight:
[1740]	1959	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1960	minor-latin;mso-hansi-theme-font:minor-latin'>Models/Fit</span></b>; it should
	1961	rapidly converge to give in the console window</p>
	1962
	1963	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1964	id="Picture_x0020_44" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:449.25pt;
	1965	height:198pt;visibility:visible;mso-wrap-style:square'>
	1966	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image060.png"
[1705]	1967	o:title=""/>
[3032]	1968	</v:shape><![endif]--><![if !vml]><img width=599 height=264
	1969	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image061.png" v:shapes="Picture_x0020_44"><![endif]></span></p>
[1705]	1970
	1971	<p class=MsoNormal><o:p> </o:p></p>
	1972
	1973	<p class=MsoNormal>And the closeness of the fit to the data in the plot is</p>
	1974
	1975	<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
[3032]	1976	id="Picture_x0020_45" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:439.5pt;
	1977	height:376.5pt;visibility:visible;mso-wrap-style:square'>
	1978	<v:imagedata src="Fitting%20Small%20Angle%20Scattering%20Data_files/image062.png"
[1705]	1979	o:title=""/>
[3032]	1980	</v:shape><![endif]--><![if !vml]><img width=586 height=502
	1981	src="Fitting%20Small%20Angle%20Scattering%20Data_files/image063.png" v:shapes="Picture_x0020_45"><![endif]></span></p>
[1705]	1982
	1983	<p class=MsoNormal><o:p> </o:p></p>
	1984
	1985	<p class=MsoNormal>This fit is almost as close as the log normal one done
	1986	earlier. However, the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
[1740]	1987	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1988	mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b style='mso-bidi-font-weight:
[1740]	1989	normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
[1705]	1990	minor-latin;mso-hansi-theme-font:minor-latin'> <span class=SpellE>Rg</span></span></b>
	1991	values are a bit less than the corresponding <span class=SpellE><b
[1740]	1992	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1993	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Dist</span></b></span><b
[1740]	1994	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	1995	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> Mean</span></b>
[1740]	1996	values obtained earlier. Also note that this model makes no reference to the
	1997	substance contrast used earlier (the <b style='mso-bidi-font-weight:normal'><span
	1998	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	1999	mso-hansi-theme-font:minor-latin'>Size Distribution</span></b> plot will not
	2000	have curves calculated from this model). To save these results you must do <b
[1740]	2001	style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
[1705]	2002	mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>File/Save
	2003	project </span></b>in the main <b style='mso-bidi-font-weight:normal'><span
[1740]	2004	style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
[1705]	2005	mso-hansi-theme-font:minor-latin'>GSAS-II data tree</span></b> window.</p>
	2006
	2007	<p class=MsoNormal>This concludes the SASD modeling tutorial.</p>
	2008
	2009	<p class=MsoNormal><o:p> </o:p></p>
	2010
	2011	<p class=MsoNormal><o:p> </o:p></p>
	2012
	2013	</div>
	2014
	2015	</body>
	2016
	2017	</html>

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