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22 | <o:DocumentProperties> |
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23 | <o:Author>Von Dreele</o:Author> |
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24 | <o:LastAuthor>vondreele</o:LastAuthor> |
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25 | <o:Revision>5</o:Revision> |
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26 | <o:TotalTime>335</o:TotalTime> |
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27 | <o:Created>2018-10-01T13:36:00Z</o:Created> |
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28 | <o:LastSaved>2018-10-01T18:15:00Z</o:LastSaved> |
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29 | <o:Pages>14</o:Pages> |
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35 | <o:Version>16.00</o:Version> |
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152 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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184 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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186 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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187 | Name="List Number"/> |
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188 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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189 | Name="List 2"/> |
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190 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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198 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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200 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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202 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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204 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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205 | Name="List Number 2"/> |
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206 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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207 | Name="List Number 3"/> |
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208 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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210 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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212 | <w:LsdException Locked="false" Priority="10" QFormat="true" Name="Title"/> |
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213 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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214 | Name="Closing"/> |
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215 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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216 | Name="Signature"/> |
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217 | <w:LsdException Locked="false" Priority="1" SemiHidden="true" |
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218 | UnhideWhenUsed="true" Name="Default Paragraph Font"/> |
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219 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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220 | Name="Body Text"/> |
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221 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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222 | Name="Body Text Indent"/> |
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223 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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224 | Name="List Continue"/> |
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225 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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226 | Name="List Continue 2"/> |
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227 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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228 | Name="List Continue 3"/> |
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229 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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230 | Name="List Continue 4"/> |
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231 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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232 | Name="List Continue 5"/> |
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233 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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234 | Name="Message Header"/> |
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235 | <w:LsdException Locked="false" Priority="11" QFormat="true" Name="Subtitle"/> |
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236 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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237 | Name="Salutation"/> |
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238 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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239 | Name="Date"/> |
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240 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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241 | Name="Body Text First Indent"/> |
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242 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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243 | Name="Body Text First Indent 2"/> |
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244 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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245 | Name="Note Heading"/> |
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246 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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247 | Name="Body Text 2"/> |
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248 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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249 | Name="Body Text 3"/> |
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250 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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251 | Name="Body Text Indent 2"/> |
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252 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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253 | Name="Body Text Indent 3"/> |
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254 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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255 | Name="Block Text"/> |
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256 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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257 | Name="Hyperlink"/> |
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258 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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259 | Name="FollowedHyperlink"/> |
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260 | <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/> |
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261 | <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/> |
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262 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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263 | Name="Document Map"/> |
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264 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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265 | Name="Plain Text"/> |
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266 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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267 | Name="E-mail Signature"/> |
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268 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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269 | Name="HTML Top of Form"/> |
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270 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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272 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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273 | Name="Normal (Web)"/> |
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274 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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275 | Name="HTML Acronym"/> |
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276 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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277 | Name="HTML Address"/> |
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278 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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279 | Name="HTML Cite"/> |
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280 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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281 | Name="HTML Code"/> |
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282 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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283 | Name="HTML Definition"/> |
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284 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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285 | Name="HTML Keyboard"/> |
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286 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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287 | Name="HTML Preformatted"/> |
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288 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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289 | Name="HTML Sample"/> |
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290 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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291 | Name="HTML Typewriter"/> |
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292 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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293 | Name="HTML Variable"/> |
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294 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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295 | Name="Normal Table"/> |
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296 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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297 | Name="annotation subject"/> |
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298 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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299 | Name="No List"/> |
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300 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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301 | Name="Outline List 1"/> |
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302 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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303 | Name="Outline List 2"/> |
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304 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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305 | Name="Outline List 3"/> |
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306 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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307 | Name="Table Simple 1"/> |
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308 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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309 | Name="Table Simple 2"/> |
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310 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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311 | Name="Table Simple 3"/> |
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312 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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313 | Name="Table Classic 1"/> |
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314 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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315 | Name="Table Classic 2"/> |
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316 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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317 | Name="Table Classic 3"/> |
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318 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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319 | Name="Table Classic 4"/> |
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320 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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321 | Name="Table Colorful 1"/> |
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322 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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323 | Name="Table Colorful 2"/> |
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324 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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325 | Name="Table Colorful 3"/> |
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326 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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327 | Name="Table Columns 1"/> |
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328 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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329 | Name="Table Columns 2"/> |
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330 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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331 | Name="Table Columns 3"/> |
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332 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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333 | Name="Table Columns 4"/> |
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334 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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335 | Name="Table Columns 5"/> |
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336 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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337 | Name="Table Grid 1"/> |
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338 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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339 | Name="Table Grid 2"/> |
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340 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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341 | Name="Table Grid 3"/> |
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342 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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343 | Name="Table Grid 4"/> |
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344 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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345 | Name="Table Grid 5"/> |
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346 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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347 | Name="Table Grid 6"/> |
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348 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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349 | Name="Table Grid 7"/> |
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350 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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351 | Name="Table Grid 8"/> |
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352 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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353 | Name="Table List 1"/> |
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354 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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355 | Name="Table List 2"/> |
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356 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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357 | Name="Table List 3"/> |
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358 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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359 | Name="Table List 4"/> |
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360 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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361 | Name="Table List 5"/> |
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362 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
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363 | Name="Table List 6"/> |
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364 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
365 | Name="Table List 7"/> |
---|
366 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
367 | Name="Table List 8"/> |
---|
368 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
369 | Name="Table 3D effects 1"/> |
---|
370 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
371 | Name="Table 3D effects 2"/> |
---|
372 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
373 | Name="Table 3D effects 3"/> |
---|
374 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
375 | Name="Table Contemporary"/> |
---|
376 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
377 | Name="Table Elegant"/> |
---|
378 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
379 | Name="Table Professional"/> |
---|
380 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
381 | Name="Table Subtle 1"/> |
---|
382 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
383 | Name="Table Subtle 2"/> |
---|
384 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
385 | Name="Table Web 1"/> |
---|
386 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
387 | Name="Table Web 2"/> |
---|
388 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
389 | Name="Table Web 3"/> |
---|
390 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
391 | Name="Balloon Text"/> |
---|
392 | <w:LsdException Locked="false" Priority="59" Name="Table Grid"/> |
---|
393 | <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true" |
---|
394 | Name="Table Theme"/> |
---|
395 | <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/> |
---|
396 | <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/> |
---|
397 | <w:LsdException Locked="false" Priority="60" Name="Light Shading"/> |
---|
398 | <w:LsdException Locked="false" Priority="61" Name="Light List"/> |
---|
399 | <w:LsdException Locked="false" Priority="62" Name="Light Grid"/> |
---|
400 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/> |
---|
401 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/> |
---|
402 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/> |
---|
403 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/> |
---|
404 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/> |
---|
405 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/> |
---|
406 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/> |
---|
407 | <w:LsdException Locked="false" Priority="70" Name="Dark List"/> |
---|
408 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/> |
---|
409 | <w:LsdException Locked="false" Priority="72" Name="Colorful List"/> |
---|
410 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/> |
---|
411 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/> |
---|
412 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/> |
---|
413 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/> |
---|
414 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/> |
---|
415 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/> |
---|
416 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/> |
---|
417 | <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/> |
---|
418 | <w:LsdException Locked="false" Priority="34" QFormat="true" |
---|
419 | Name="List Paragraph"/> |
---|
420 | <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/> |
---|
421 | <w:LsdException Locked="false" Priority="30" QFormat="true" |
---|
422 | Name="Intense Quote"/> |
---|
423 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/> |
---|
424 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/> |
---|
425 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/> |
---|
426 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/> |
---|
427 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/> |
---|
428 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/> |
---|
429 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/> |
---|
430 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/> |
---|
431 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/> |
---|
432 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/> |
---|
433 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/> |
---|
434 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/> |
---|
435 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/> |
---|
436 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/> |
---|
437 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/> |
---|
438 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/> |
---|
439 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/> |
---|
440 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/> |
---|
441 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/> |
---|
442 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/> |
---|
443 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/> |
---|
444 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/> |
---|
445 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/> |
---|
446 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/> |
---|
447 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/> |
---|
448 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/> |
---|
449 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/> |
---|
450 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/> |
---|
451 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/> |
---|
452 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/> |
---|
453 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/> |
---|
454 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/> |
---|
455 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/> |
---|
456 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/> |
---|
457 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/> |
---|
458 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/> |
---|
459 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/> |
---|
460 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/> |
---|
461 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/> |
---|
462 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/> |
---|
463 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/> |
---|
464 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/> |
---|
465 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/> |
---|
466 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/> |
---|
467 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/> |
---|
468 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/> |
---|
469 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/> |
---|
470 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/> |
---|
471 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/> |
---|
472 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/> |
---|
473 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/> |
---|
474 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/> |
---|
475 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/> |
---|
476 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/> |
---|
477 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/> |
---|
478 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/> |
---|
479 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/> |
---|
480 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/> |
---|
481 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/> |
---|
482 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/> |
---|
483 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/> |
---|
484 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/> |
---|
485 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/> |
---|
486 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/> |
---|
487 | <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/> |
---|
488 | <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/> |
---|
489 | <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/> |
---|
490 | <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/> |
---|
491 | <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/> |
---|
492 | <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/> |
---|
493 | <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/> |
---|
494 | <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/> |
---|
495 | <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/> |
---|
496 | <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/> |
---|
497 | <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/> |
---|
498 | <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/> |
---|
499 | <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/> |
---|
500 | <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/> |
---|
501 | <w:LsdException Locked="false" Priority="19" QFormat="true" |
---|
502 | Name="Subtle Emphasis"/> |
---|
503 | <w:LsdException Locked="false" Priority="21" QFormat="true" |
---|
504 | Name="Intense Emphasis"/> |
---|
505 | <w:LsdException Locked="false" Priority="31" QFormat="true" |
---|
506 | Name="Subtle Reference"/> |
---|
507 | <w:LsdException Locked="false" Priority="32" QFormat="true" |
---|
508 | Name="Intense Reference"/> |
---|
509 | <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/> |
---|
510 | <w:LsdException Locked="false" Priority="37" SemiHidden="true" |
---|
511 | UnhideWhenUsed="true" Name="Bibliography"/> |
---|
512 | <w:LsdException Locked="false" Priority="39" SemiHidden="true" |
---|
513 | UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/> |
---|
514 | <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/> |
---|
515 | <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/> |
---|
516 | <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/> |
---|
517 | <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/> |
---|
518 | <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/> |
---|
519 | <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/> |
---|
520 | <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/> |
---|
521 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/> |
---|
522 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/> |
---|
523 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/> |
---|
524 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/> |
---|
525 | <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/> |
---|
526 | <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/> |
---|
527 | <w:LsdException Locked="false" Priority="46" |
---|
528 | Name="Grid Table 1 Light Accent 1"/> |
---|
529 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/> |
---|
530 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/> |
---|
531 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/> |
---|
532 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/> |
---|
533 | <w:LsdException Locked="false" Priority="51" |
---|
534 | Name="Grid Table 6 Colorful Accent 1"/> |
---|
535 | <w:LsdException Locked="false" Priority="52" |
---|
536 | Name="Grid Table 7 Colorful Accent 1"/> |
---|
537 | <w:LsdException Locked="false" Priority="46" |
---|
538 | Name="Grid Table 1 Light Accent 2"/> |
---|
539 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/> |
---|
540 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/> |
---|
541 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/> |
---|
542 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/> |
---|
543 | <w:LsdException Locked="false" Priority="51" |
---|
544 | Name="Grid Table 6 Colorful Accent 2"/> |
---|
545 | <w:LsdException Locked="false" Priority="52" |
---|
546 | Name="Grid Table 7 Colorful Accent 2"/> |
---|
547 | <w:LsdException Locked="false" Priority="46" |
---|
548 | Name="Grid Table 1 Light Accent 3"/> |
---|
549 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/> |
---|
550 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/> |
---|
551 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/> |
---|
552 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/> |
---|
553 | <w:LsdException Locked="false" Priority="51" |
---|
554 | Name="Grid Table 6 Colorful Accent 3"/> |
---|
555 | <w:LsdException Locked="false" Priority="52" |
---|
556 | Name="Grid Table 7 Colorful Accent 3"/> |
---|
557 | <w:LsdException Locked="false" Priority="46" |
---|
558 | Name="Grid Table 1 Light Accent 4"/> |
---|
559 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/> |
---|
560 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/> |
---|
561 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/> |
---|
562 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/> |
---|
563 | <w:LsdException Locked="false" Priority="51" |
---|
564 | Name="Grid Table 6 Colorful Accent 4"/> |
---|
565 | <w:LsdException Locked="false" Priority="52" |
---|
566 | Name="Grid Table 7 Colorful Accent 4"/> |
---|
567 | <w:LsdException Locked="false" Priority="46" |
---|
568 | Name="Grid Table 1 Light Accent 5"/> |
---|
569 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/> |
---|
570 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/> |
---|
571 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/> |
---|
572 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/> |
---|
573 | <w:LsdException Locked="false" Priority="51" |
---|
574 | Name="Grid Table 6 Colorful Accent 5"/> |
---|
575 | <w:LsdException Locked="false" Priority="52" |
---|
576 | Name="Grid Table 7 Colorful Accent 5"/> |
---|
577 | <w:LsdException Locked="false" Priority="46" |
---|
578 | Name="Grid Table 1 Light Accent 6"/> |
---|
579 | <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/> |
---|
580 | <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/> |
---|
581 | <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/> |
---|
582 | <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/> |
---|
583 | <w:LsdException Locked="false" Priority="51" |
---|
584 | Name="Grid Table 6 Colorful Accent 6"/> |
---|
585 | <w:LsdException Locked="false" Priority="52" |
---|
586 | Name="Grid Table 7 Colorful Accent 6"/> |
---|
587 | <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/> |
---|
588 | <w:LsdException Locked="false" Priority="47" Name="List Table 2"/> |
---|
589 | <w:LsdException Locked="false" Priority="48" Name="List Table 3"/> |
---|
590 | <w:LsdException Locked="false" Priority="49" Name="List Table 4"/> |
---|
591 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/> |
---|
592 | <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/> |
---|
593 | <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/> |
---|
594 | <w:LsdException Locked="false" Priority="46" |
---|
595 | Name="List Table 1 Light Accent 1"/> |
---|
596 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/> |
---|
597 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/> |
---|
598 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/> |
---|
599 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/> |
---|
600 | <w:LsdException Locked="false" Priority="51" |
---|
601 | Name="List Table 6 Colorful Accent 1"/> |
---|
602 | <w:LsdException Locked="false" Priority="52" |
---|
603 | Name="List Table 7 Colorful Accent 1"/> |
---|
604 | <w:LsdException Locked="false" Priority="46" |
---|
605 | Name="List Table 1 Light Accent 2"/> |
---|
606 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/> |
---|
607 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/> |
---|
608 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/> |
---|
609 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/> |
---|
610 | <w:LsdException Locked="false" Priority="51" |
---|
611 | Name="List Table 6 Colorful Accent 2"/> |
---|
612 | <w:LsdException Locked="false" Priority="52" |
---|
613 | Name="List Table 7 Colorful Accent 2"/> |
---|
614 | <w:LsdException Locked="false" Priority="46" |
---|
615 | Name="List Table 1 Light Accent 3"/> |
---|
616 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/> |
---|
617 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/> |
---|
618 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/> |
---|
619 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/> |
---|
620 | <w:LsdException Locked="false" Priority="51" |
---|
621 | Name="List Table 6 Colorful Accent 3"/> |
---|
622 | <w:LsdException Locked="false" Priority="52" |
---|
623 | Name="List Table 7 Colorful Accent 3"/> |
---|
624 | <w:LsdException Locked="false" Priority="46" |
---|
625 | Name="List Table 1 Light Accent 4"/> |
---|
626 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/> |
---|
627 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/> |
---|
628 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/> |
---|
629 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/> |
---|
630 | <w:LsdException Locked="false" Priority="51" |
---|
631 | Name="List Table 6 Colorful Accent 4"/> |
---|
632 | <w:LsdException Locked="false" Priority="52" |
---|
633 | Name="List Table 7 Colorful Accent 4"/> |
---|
634 | <w:LsdException Locked="false" Priority="46" |
---|
635 | Name="List Table 1 Light Accent 5"/> |
---|
636 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/> |
---|
637 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/> |
---|
638 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/> |
---|
639 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/> |
---|
640 | <w:LsdException Locked="false" Priority="51" |
---|
641 | Name="List Table 6 Colorful Accent 5"/> |
---|
642 | <w:LsdException Locked="false" Priority="52" |
---|
643 | Name="List Table 7 Colorful Accent 5"/> |
---|
644 | <w:LsdException Locked="false" Priority="46" |
---|
645 | Name="List Table 1 Light Accent 6"/> |
---|
646 | <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/> |
---|
647 | <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/> |
---|
648 | <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/> |
---|
649 | <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/> |
---|
650 | <w:LsdException Locked="false" Priority="51" |
---|
651 | Name="List Table 6 Colorful Accent 6"/> |
---|
652 | <w:LsdException Locked="false" Priority="52" |
---|
653 | Name="List Table 7 Colorful Accent 6"/> |
---|
654 | </w:LatentStyles> |
---|
655 | </xml><![endif]--> |
---|
656 | <style> |
---|
657 | <!-- |
---|
658 | /* Font Definitions */ |
---|
659 | @font-face |
---|
660 | {font-family:"Cambria Math"; |
---|
661 | panose-1:2 4 5 3 5 4 6 3 2 4; |
---|
662 | mso-font-charset:0; |
---|
663 | mso-generic-font-family:roman; |
---|
664 | mso-font-pitch:variable; |
---|
665 | mso-font-signature:-536869121 1107305727 33554432 0 415 0;} |
---|
666 | @font-face |
---|
667 | {font-family:Calibri; |
---|
668 | panose-1:2 15 5 2 2 2 4 3 2 4; |
---|
669 | mso-font-alt:Calibri; |
---|
670 | mso-font-charset:0; |
---|
671 | mso-generic-font-family:swiss; |
---|
672 | mso-font-pitch:variable; |
---|
673 | mso-font-signature:-536859905 -1073732485 9 0 511 0;} |
---|
674 | @font-face |
---|
675 | {font-family:Tahoma; |
---|
676 | panose-1:2 11 6 4 3 5 4 4 2 4; |
---|
677 | mso-font-charset:0; |
---|
678 | mso-generic-font-family:swiss; |
---|
679 | mso-font-pitch:variable; |
---|
680 | mso-font-signature:-520081665 -1073717157 41 0 66047 0;} |
---|
681 | /* Style Definitions */ |
---|
682 | p.MsoNormal, li.MsoNormal, div.MsoNormal |
---|
683 | {mso-style-unhide:no; |
---|
684 | mso-style-qformat:yes; |
---|
685 | mso-style-parent:""; |
---|
686 | margin:0in; |
---|
687 | margin-bottom:.0001pt; |
---|
688 | mso-pagination:widow-orphan; |
---|
689 | font-size:12.0pt; |
---|
690 | font-family:"Times New Roman",serif; |
---|
691 | mso-fareast-font-family:"Times New Roman"; |
---|
692 | mso-fareast-theme-font:minor-fareast;} |
---|
693 | h1 |
---|
694 | {mso-style-priority:9; |
---|
695 | mso-style-unhide:no; |
---|
696 | mso-style-qformat:yes; |
---|
697 | mso-style-link:"Heading 1 Char"; |
---|
698 | mso-margin-top-alt:auto; |
---|
699 | margin-right:0in; |
---|
700 | mso-margin-bottom-alt:auto; |
---|
701 | margin-left:0in; |
---|
702 | mso-pagination:widow-orphan; |
---|
703 | mso-outline-level:1; |
---|
704 | font-size:24.0pt; |
---|
705 | font-family:"Times New Roman",serif; |
---|
706 | mso-fareast-font-family:"Times New Roman"; |
---|
707 | mso-fareast-theme-font:minor-fareast; |
---|
708 | font-weight:bold;} |
---|
709 | h2 |
---|
710 | {mso-style-noshow:yes; |
---|
711 | mso-style-priority:9; |
---|
712 | mso-style-qformat:yes; |
---|
713 | mso-style-link:"Heading 2 Char"; |
---|
714 | mso-margin-top-alt:auto; |
---|
715 | margin-right:0in; |
---|
716 | mso-margin-bottom-alt:auto; |
---|
717 | margin-left:0in; |
---|
718 | mso-pagination:widow-orphan; |
---|
719 | mso-outline-level:2; |
---|
720 | font-size:18.0pt; |
---|
721 | font-family:"Times New Roman",serif; |
---|
722 | mso-fareast-font-family:"Times New Roman"; |
---|
723 | mso-fareast-theme-font:minor-fareast; |
---|
724 | font-weight:bold;} |
---|
725 | h3 |
---|
726 | {mso-style-noshow:yes; |
---|
727 | mso-style-priority:9; |
---|
728 | mso-style-qformat:yes; |
---|
729 | mso-style-link:"Heading 3 Char"; |
---|
730 | mso-margin-top-alt:auto; |
---|
731 | margin-right:0in; |
---|
732 | mso-margin-bottom-alt:auto; |
---|
733 | margin-left:0in; |
---|
734 | mso-pagination:widow-orphan; |
---|
735 | mso-outline-level:3; |
---|
736 | font-size:13.5pt; |
---|
737 | font-family:"Times New Roman",serif; |
---|
738 | mso-fareast-font-family:"Times New Roman"; |
---|
739 | mso-fareast-theme-font:minor-fareast; |
---|
740 | font-weight:bold;} |
---|
741 | h4 |
---|
742 | {mso-style-noshow:yes; |
---|
743 | mso-style-priority:9; |
---|
744 | mso-style-qformat:yes; |
---|
745 | mso-style-link:"Heading 4 Char"; |
---|
746 | mso-style-next:Normal; |
---|
747 | margin-top:10.0pt; |
---|
748 | margin-right:0in; |
---|
749 | margin-bottom:0in; |
---|
750 | margin-left:0in; |
---|
751 | margin-bottom:.0001pt; |
---|
752 | mso-pagination:widow-orphan lines-together; |
---|
753 | page-break-after:avoid; |
---|
754 | mso-outline-level:4; |
---|
755 | font-size:13.0pt; |
---|
756 | font-family:"Cambria",serif; |
---|
757 | mso-ascii-font-family:Cambria; |
---|
758 | mso-ascii-theme-font:major-latin; |
---|
759 | mso-fareast-font-family:"Times New Roman"; |
---|
760 | mso-fareast-theme-font:major-fareast; |
---|
761 | mso-hansi-font-family:Cambria; |
---|
762 | mso-hansi-theme-font:major-latin; |
---|
763 | mso-bidi-font-family:"Times New Roman"; |
---|
764 | mso-bidi-theme-font:major-bidi; |
---|
765 | color:#4F81BD; |
---|
766 | mso-themecolor:accent1; |
---|
767 | font-weight:bold; |
---|
768 | font-style:italic;} |
---|
769 | h5 |
---|
770 | {mso-style-noshow:yes; |
---|
771 | mso-style-priority:9; |
---|
772 | mso-style-qformat:yes; |
---|
773 | mso-style-link:"Heading 5 Char"; |
---|
774 | mso-margin-top-alt:auto; |
---|
775 | margin-right:0in; |
---|
776 | mso-margin-bottom-alt:auto; |
---|
777 | margin-left:0in; |
---|
778 | mso-pagination:widow-orphan; |
---|
779 | mso-outline-level:5; |
---|
780 | font-size:12.0pt; |
---|
781 | font-family:"Times New Roman",serif; |
---|
782 | mso-fareast-font-family:"Times New Roman"; |
---|
783 | mso-fareast-theme-font:minor-fareast; |
---|
784 | color:#4F4FFF; |
---|
785 | font-weight:bold;} |
---|
786 | a:link, span.MsoHyperlink |
---|
787 | {mso-style-priority:99; |
---|
788 | color:blue; |
---|
789 | text-decoration:underline; |
---|
790 | text-underline:single;} |
---|
791 | a:visited, span.MsoHyperlinkFollowed |
---|
792 | {mso-style-noshow:yes; |
---|
793 | mso-style-priority:99; |
---|
794 | color:purple; |
---|
795 | text-decoration:underline; |
---|
796 | text-underline:single;} |
---|
797 | p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap |
---|
798 | {mso-style-noshow:yes; |
---|
799 | mso-style-priority:99; |
---|
800 | mso-style-link:"Document Map Char"; |
---|
801 | margin:0in; |
---|
802 | margin-bottom:.0001pt; |
---|
803 | mso-pagination:widow-orphan; |
---|
804 | font-size:8.0pt; |
---|
805 | font-family:"Tahoma",sans-serif; |
---|
806 | mso-fareast-font-family:"Times New Roman"; |
---|
807 | mso-fareast-theme-font:minor-fareast;} |
---|
808 | p |
---|
809 | {mso-style-noshow:yes; |
---|
810 | mso-style-priority:99; |
---|
811 | mso-margin-top-alt:auto; |
---|
812 | margin-right:0in; |
---|
813 | mso-margin-bottom-alt:auto; |
---|
814 | margin-left:0in; |
---|
815 | mso-pagination:widow-orphan; |
---|
816 | font-size:12.0pt; |
---|
817 | font-family:"Times New Roman",serif; |
---|
818 | mso-fareast-font-family:"Times New Roman"; |
---|
819 | mso-fareast-theme-font:minor-fareast;} |
---|
820 | pre |
---|
821 | {mso-style-noshow:yes; |
---|
822 | mso-style-priority:99; |
---|
823 | mso-style-link:"HTML Preformatted Char"; |
---|
824 | margin:0in; |
---|
825 | margin-bottom:.0001pt; |
---|
826 | mso-pagination:widow-orphan; |
---|
827 | tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt; |
---|
828 | font-size:10.0pt; |
---|
829 | font-family:"Courier New"; |
---|
830 | mso-fareast-font-family:"Times New Roman";} |
---|
831 | p.MsoAcetate, li.MsoAcetate, div.MsoAcetate |
---|
832 | {mso-style-noshow:yes; |
---|
833 | mso-style-priority:99; |
---|
834 | mso-style-link:"Balloon Text Char"; |
---|
835 | margin:0in; |
---|
836 | margin-bottom:.0001pt; |
---|
837 | mso-pagination:widow-orphan; |
---|
838 | font-size:8.0pt; |
---|
839 | font-family:"Tahoma",sans-serif; |
---|
840 | mso-fareast-font-family:"Times New Roman"; |
---|
841 | mso-fareast-theme-font:minor-fareast;} |
---|
842 | span.MsoPlaceholderText |
---|
843 | {mso-style-noshow:yes; |
---|
844 | mso-style-priority:99; |
---|
845 | mso-style-unhide:no; |
---|
846 | color:gray;} |
---|
847 | p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing |
---|
848 | {mso-style-noshow:yes; |
---|
849 | mso-style-priority:1; |
---|
850 | mso-style-unhide:no; |
---|
851 | mso-style-qformat:yes; |
---|
852 | mso-style-parent:""; |
---|
853 | margin:0in; |
---|
854 | margin-bottom:.0001pt; |
---|
855 | mso-pagination:widow-orphan; |
---|
856 | font-size:12.0pt; |
---|
857 | font-family:"Times New Roman",serif; |
---|
858 | mso-fareast-font-family:"Times New Roman"; |
---|
859 | mso-fareast-theme-font:minor-fareast;} |
---|
860 | p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph |
---|
861 | {mso-style-noshow:yes; |
---|
862 | mso-style-priority:34; |
---|
863 | mso-style-unhide:no; |
---|
864 | mso-style-qformat:yes; |
---|
865 | margin-top:0in; |
---|
866 | margin-right:0in; |
---|
867 | margin-bottom:0in; |
---|
868 | margin-left:.5in; |
---|
869 | margin-bottom:.0001pt; |
---|
870 | mso-add-space:auto; |
---|
871 | mso-pagination:widow-orphan; |
---|
872 | font-size:12.0pt; |
---|
873 | font-family:"Times New Roman",serif; |
---|
874 | mso-fareast-font-family:"Times New Roman"; |
---|
875 | mso-fareast-theme-font:minor-fareast;} |
---|
876 | p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst |
---|
877 | {mso-style-noshow:yes; |
---|
878 | mso-style-priority:34; |
---|
879 | mso-style-unhide:no; |
---|
880 | mso-style-qformat:yes; |
---|
881 | mso-style-type:export-only; |
---|
882 | margin-top:0in; |
---|
883 | margin-right:0in; |
---|
884 | margin-bottom:0in; |
---|
885 | margin-left:.5in; |
---|
886 | margin-bottom:.0001pt; |
---|
887 | mso-add-space:auto; |
---|
888 | mso-pagination:widow-orphan; |
---|
889 | font-size:12.0pt; |
---|
890 | font-family:"Times New Roman",serif; |
---|
891 | mso-fareast-font-family:"Times New Roman"; |
---|
892 | mso-fareast-theme-font:minor-fareast;} |
---|
893 | p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle |
---|
894 | {mso-style-noshow:yes; |
---|
895 | mso-style-priority:34; |
---|
896 | mso-style-unhide:no; |
---|
897 | mso-style-qformat:yes; |
---|
898 | mso-style-type:export-only; |
---|
899 | margin-top:0in; |
---|
900 | margin-right:0in; |
---|
901 | margin-bottom:0in; |
---|
902 | margin-left:.5in; |
---|
903 | margin-bottom:.0001pt; |
---|
904 | mso-add-space:auto; |
---|
905 | mso-pagination:widow-orphan; |
---|
906 | font-size:12.0pt; |
---|
907 | font-family:"Times New Roman",serif; |
---|
908 | mso-fareast-font-family:"Times New Roman"; |
---|
909 | mso-fareast-theme-font:minor-fareast;} |
---|
910 | p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast |
---|
911 | {mso-style-noshow:yes; |
---|
912 | mso-style-priority:34; |
---|
913 | mso-style-unhide:no; |
---|
914 | mso-style-qformat:yes; |
---|
915 | mso-style-type:export-only; |
---|
916 | margin-top:0in; |
---|
917 | margin-right:0in; |
---|
918 | margin-bottom:0in; |
---|
919 | margin-left:.5in; |
---|
920 | margin-bottom:.0001pt; |
---|
921 | mso-add-space:auto; |
---|
922 | mso-pagination:widow-orphan; |
---|
923 | font-size:12.0pt; |
---|
924 | font-family:"Times New Roman",serif; |
---|
925 | mso-fareast-font-family:"Times New Roman"; |
---|
926 | mso-fareast-theme-font:minor-fareast;} |
---|
927 | span.MsoIntenseReference |
---|
928 | {mso-style-priority:32; |
---|
929 | mso-style-unhide:no; |
---|
930 | mso-style-qformat:yes; |
---|
931 | font-variant:small-caps; |
---|
932 | color:#C0504D; |
---|
933 | mso-themecolor:accent2; |
---|
934 | letter-spacing:.25pt; |
---|
935 | font-weight:bold; |
---|
936 | text-decoration:underline; |
---|
937 | text-underline:single;} |
---|
938 | span.Heading1Char |
---|
939 | {mso-style-name:"Heading 1 Char"; |
---|
940 | mso-style-priority:9; |
---|
941 | mso-style-unhide:no; |
---|
942 | mso-style-locked:yes; |
---|
943 | mso-style-link:"Heading 1"; |
---|
944 | mso-ansi-font-size:24.0pt; |
---|
945 | mso-bidi-font-size:24.0pt; |
---|
946 | font-family:"Times New Roman",serif; |
---|
947 | mso-ascii-font-family:"Times New Roman"; |
---|
948 | mso-fareast-font-family:"Times New Roman"; |
---|
949 | mso-fareast-theme-font:minor-fareast; |
---|
950 | mso-hansi-font-family:"Times New Roman"; |
---|
951 | mso-bidi-font-family:"Times New Roman"; |
---|
952 | mso-font-kerning:18.0pt; |
---|
953 | font-weight:bold;} |
---|
954 | span.Heading2Char |
---|
955 | {mso-style-name:"Heading 2 Char"; |
---|
956 | mso-style-noshow:yes; |
---|
957 | mso-style-priority:9; |
---|
958 | mso-style-unhide:no; |
---|
959 | mso-style-locked:yes; |
---|
960 | mso-style-link:"Heading 2"; |
---|
961 | mso-ansi-font-size:18.0pt; |
---|
962 | mso-bidi-font-size:18.0pt; |
---|
963 | font-family:"Times New Roman",serif; |
---|
964 | mso-ascii-font-family:"Times New Roman"; |
---|
965 | mso-fareast-font-family:"Times New Roman"; |
---|
966 | mso-fareast-theme-font:minor-fareast; |
---|
967 | mso-hansi-font-family:"Times New Roman"; |
---|
968 | mso-bidi-font-family:"Times New Roman"; |
---|
969 | font-weight:bold;} |
---|
970 | span.Heading3Char |
---|
971 | {mso-style-name:"Heading 3 Char"; |
---|
972 | mso-style-noshow:yes; |
---|
973 | mso-style-priority:9; |
---|
974 | mso-style-unhide:no; |
---|
975 | mso-style-locked:yes; |
---|
976 | mso-style-link:"Heading 3"; |
---|
977 | mso-ansi-font-size:13.5pt; |
---|
978 | mso-bidi-font-size:13.5pt; |
---|
979 | font-family:"Times New Roman",serif; |
---|
980 | mso-ascii-font-family:"Times New Roman"; |
---|
981 | mso-fareast-font-family:"Times New Roman"; |
---|
982 | mso-fareast-theme-font:minor-fareast; |
---|
983 | mso-hansi-font-family:"Times New Roman"; |
---|
984 | mso-bidi-font-family:"Times New Roman"; |
---|
985 | font-weight:bold;} |
---|
986 | span.Heading4Char |
---|
987 | {mso-style-name:"Heading 4 Char"; |
---|
988 | mso-style-noshow:yes; |
---|
989 | mso-style-priority:9; |
---|
990 | mso-style-unhide:no; |
---|
991 | mso-style-locked:yes; |
---|
992 | mso-style-link:"Heading 4"; |
---|
993 | mso-ansi-font-size:13.0pt; |
---|
994 | mso-bidi-font-size:13.0pt; |
---|
995 | font-family:"Cambria",serif; |
---|
996 | mso-ascii-font-family:Cambria; |
---|
997 | mso-ascii-theme-font:major-latin; |
---|
998 | mso-fareast-font-family:"Times New Roman"; |
---|
999 | mso-fareast-theme-font:major-fareast; |
---|
1000 | mso-hansi-font-family:Cambria; |
---|
1001 | mso-hansi-theme-font:major-latin; |
---|
1002 | mso-bidi-font-family:"Times New Roman"; |
---|
1003 | mso-bidi-theme-font:major-bidi; |
---|
1004 | color:#4F81BD; |
---|
1005 | mso-themecolor:accent1; |
---|
1006 | font-weight:bold; |
---|
1007 | font-style:italic;} |
---|
1008 | span.Heading5Char |
---|
1009 | {mso-style-name:"Heading 5 Char"; |
---|
1010 | mso-style-noshow:yes; |
---|
1011 | mso-style-priority:9; |
---|
1012 | mso-style-unhide:no; |
---|
1013 | mso-style-locked:yes; |
---|
1014 | mso-style-link:"Heading 5"; |
---|
1015 | mso-ansi-font-size:12.0pt; |
---|
1016 | mso-bidi-font-size:12.0pt; |
---|
1017 | font-family:"Times New Roman",serif; |
---|
1018 | mso-ascii-font-family:"Times New Roman"; |
---|
1019 | mso-fareast-font-family:"Times New Roman"; |
---|
1020 | mso-fareast-theme-font:minor-fareast; |
---|
1021 | mso-hansi-font-family:"Times New Roman"; |
---|
1022 | mso-bidi-font-family:"Times New Roman"; |
---|
1023 | color:#4F4FFF; |
---|
1024 | font-weight:bold;} |
---|
1025 | span.HTMLPreformattedChar |
---|
1026 | {mso-style-name:"HTML Preformatted Char"; |
---|
1027 | mso-style-noshow:yes; |
---|
1028 | mso-style-priority:99; |
---|
1029 | mso-style-unhide:no; |
---|
1030 | mso-style-locked:yes; |
---|
1031 | mso-style-link:"HTML Preformatted"; |
---|
1032 | mso-ansi-font-size:10.0pt; |
---|
1033 | mso-bidi-font-size:10.0pt; |
---|
1034 | font-family:"Courier New"; |
---|
1035 | mso-ascii-font-family:"Courier New"; |
---|
1036 | mso-fareast-font-family:"Times New Roman"; |
---|
1037 | mso-hansi-font-family:"Courier New"; |
---|
1038 | mso-bidi-font-family:"Courier New";} |
---|
1039 | p.msonormal0, li.msonormal0, div.msonormal0 |
---|
1040 | {mso-style-name:msonormal; |
---|
1041 | mso-style-noshow:yes; |
---|
1042 | mso-style-priority:99; |
---|
1043 | mso-style-unhide:no; |
---|
1044 | mso-margin-top-alt:auto; |
---|
1045 | margin-right:0in; |
---|
1046 | mso-margin-bottom-alt:auto; |
---|
1047 | margin-left:0in; |
---|
1048 | mso-pagination:widow-orphan; |
---|
1049 | font-size:12.0pt; |
---|
1050 | font-family:"Times New Roman",serif; |
---|
1051 | mso-fareast-font-family:"Times New Roman"; |
---|
1052 | mso-fareast-theme-font:minor-fareast;} |
---|
1053 | span.DocumentMapChar |
---|
1054 | {mso-style-name:"Document Map Char"; |
---|
1055 | mso-style-noshow:yes; |
---|
1056 | mso-style-priority:99; |
---|
1057 | mso-style-unhide:no; |
---|
1058 | mso-style-locked:yes; |
---|
1059 | mso-style-link:"Document Map"; |
---|
1060 | mso-ansi-font-size:8.0pt; |
---|
1061 | mso-bidi-font-size:8.0pt; |
---|
1062 | font-family:"Tahoma",sans-serif; |
---|
1063 | mso-ascii-font-family:Tahoma; |
---|
1064 | mso-fareast-font-family:"Times New Roman"; |
---|
1065 | mso-fareast-theme-font:minor-fareast; |
---|
1066 | mso-hansi-font-family:Tahoma; |
---|
1067 | mso-bidi-font-family:Tahoma;} |
---|
1068 | span.BalloonTextChar |
---|
1069 | {mso-style-name:"Balloon Text Char"; |
---|
1070 | mso-style-noshow:yes; |
---|
1071 | mso-style-priority:99; |
---|
1072 | mso-style-unhide:no; |
---|
1073 | mso-style-locked:yes; |
---|
1074 | mso-style-link:"Balloon Text"; |
---|
1075 | mso-ansi-font-size:8.0pt; |
---|
1076 | mso-bidi-font-size:8.0pt; |
---|
1077 | font-family:"Tahoma",sans-serif; |
---|
1078 | mso-ascii-font-family:Tahoma; |
---|
1079 | mso-fareast-font-family:"Times New Roman"; |
---|
1080 | mso-fareast-theme-font:minor-fareast; |
---|
1081 | mso-hansi-font-family:Tahoma; |
---|
1082 | mso-bidi-font-family:Tahoma;} |
---|
1083 | span.GSAS-IItextChar |
---|
1084 | {mso-style-name:"GSAS-II text Char"; |
---|
1085 | mso-style-unhide:no; |
---|
1086 | mso-style-locked:yes; |
---|
1087 | mso-style-link:"GSAS-II text"; |
---|
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1280 | |
---|
1281 | <div class=WordSection1> |
---|
1282 | |
---|
1283 | <h1>Magnetic Structures in GSAS-II - IV<o:p></o:p></h1> |
---|
1284 | |
---|
1285 | <h2>Introduction<o:p></o:p></h2> |
---|
1286 | |
---|
1287 | <p class=MsoNormal>In this tutorial, we will show how GSAS-II makes use of the |
---|
1288 | Bilbao crystallographic server (<a href="http://www.cryst.ehu.es/">www.cryst.ehu.es/</a>) |
---|
1289 | <i style='mso-bidi-font-style:normal'>Magnetic Symmetry and Applications</i> routine |
---|
1290 | k-SUBGROUPSMAG (<a href="http://iopscience.iop.org/0953-8984/28/28/286001"><span |
---|
1291 | style='font-size:10.0pt;font-family:"Arial",sans-serif'>Perez-Mato, JM; <span |
---|
1292 | class=SpellE>Gallego</span>, SV; <span class=SpellE>Elcoro</span>, L; <span |
---|
1293 | class=SpellE>Tasci</span>, E and <span class=SpellE>Aroyo</span>, MI, <i>J. of |
---|
1294 | Phys.: <span class=SpellE>Condens</span> Matter</i> (2016), <b>28</b>:28601</span></a>) |
---|
1295 | to determine a magnetic crystal structure with a non-zero propagation vector. |
---|
1296 | If you have not done so already, you may wish to do the Simple Magnetic |
---|
1297 | Structures tutorial first as it contains some background information that will |
---|
1298 | not be covered here. It is also helpful to do parts I - III of the series of |
---|
1299 | Magnetic Structures tutorials. To make this work, your computer must have an |
---|
1300 | internet connection for GSAS-II to access this site. (We will supply the |
---|
1301 | project file that results after k-SUBGROUPSMAG is called in case you lack |
---|
1302 | internet access).<o:p></o:p></p> |
---|
1303 | |
---|
1304 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype |
---|
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---|
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---|
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---|
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---|
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---|
1325 | style='width:356.25pt;height:316.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1326 | <v:imagedata src="Magnetic-IV_files/image005.png" o:title=""/> |
---|
1327 | </v:shape><![endif]--><![if !vml]><img border=0 width=475 height=422 |
---|
1328 | src="Magnetic-IV_files/image006.gif" v:shapes="Picture_x0020_3"><![endif]></span></p> |
---|
1329 | |
---|
1330 | <p class=MsoNormal>In this tutorial we will be examining the perovskite (Pr<sub>.5</sub>Sr<sub>.5</sub><span |
---|
1331 | class=GramE>)MnO<sub>3</sub></span>, which at low temperature is a doubled <span |
---|
1332 | class=SpellE>a,b,c</span>-axis variant due to a rotation of the MnO<sub>6</sub> |
---|
1333 | <span class=SpellE>octahedra</span> about the assigned c-axis (drawing above) |
---|
1334 | to give the <span class=SpellE>Fmmm</span>, a=7.508, b=7.812, c=7.684 Å unit |
---|
1335 | cell. The neutron powder diffraction data was collected on the 3T2 |
---|
1336 | diffractometer (LLB, <span class=SpellE>Saclay</span> France) at 10K and |
---|
1337 | λ=1.227 Å and this tutorial is based on Example 12.3 in the Jana2006 |
---|
1338 | Cookbook (<span class=SpellE>Duek</span>, et al., 2017). The antiferromagnetic |
---|
1339 | structure was originally determined by <span class=SpellE><span |
---|
1340 | style='font-size:11.5pt'>Kníek</span></span><span class=GramE><span |
---|
1341 | style='font-size:11.5pt'>, <span style='mso-spacerun:yes'> </span>et</span></span><span |
---|
1342 | style='font-size:11.5pt'> al. (K. <span class=SpellE>Kníek</span>, J. <span |
---|
1343 | class=SpellE>Hejtmánek</span>, and Z. <span class=SpellE>Jirák</span>, C. |
---|
1344 | Martin, M. <span class=SpellE>Hervieu</span>, and B. <span class=SpellE>Raveau</span>, |
---|
1345 | G. André and F. <span class=SpellE>Bourée</span>, <i style='mso-bidi-font-style: |
---|
1346 | normal'>Chemistry of Materials</i>, (2004), <b style='mso-bidi-font-weight: |
---|
1347 | normal'>16</b>, 1104-1110). As we will see the magnetic space group is a |
---|
1348 | subgroup of <span class=SpellE>Fmmm</span> principally by a loss of some of the |
---|
1349 | face centering symmetry. </span>We will use k-SUBGROUPSMAG to help sort this |
---|
1350 | out.<o:p></o:p></p> |
---|
1351 | |
---|
1352 | <p class=MsoNormal><o:p> </o:p></p> |
---|
1353 | |
---|
1354 | <p class=MsoNormal>If you have not done so already, start GSAS-II (make sure |
---|
1355 | about the internet connection!).<o:p></o:p></p> |
---|
1356 | |
---|
1357 | <h3>Step 1. Read in the data file<o:p></o:p></h3> |
---|
1358 | |
---|
1359 | <p class=MsoListParagraphCxSpFirst style='text-indent:-.25in;mso-list:l1 level1 lfo1'><![if !supportLists]><span |
---|
1360 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span |
---|
1361 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Use |
---|
1362 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1363 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1364 | minor-latin'>Import/Powder Data/from <span class=SpellE>gsas</span> powder data |
---|
1365 | file</span></b> menu item to read the data file into the current GSAS-II |
---|
1366 | project. Because you used <span style='mso-fareast-font-family:Calibri; |
---|
1367 | mso-fareast-theme-font:minor-latin'>the </span><b style='mso-bidi-font-weight: |
---|
1368 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1369 | minor-latin;mso-fareast-font-family:Calibri;mso-fareast-theme-font:minor-latin; |
---|
1370 | mso-hansi-theme-font:minor-latin'>Help/Download tutorial</span></b><span |
---|
1371 | style='mso-fareast-font-family:Calibri;mso-fareast-theme-font:minor-latin'> |
---|
1372 | menu entry to open this page and downloaded the exercise files (recommended), |
---|
1373 | then the </span><b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1374 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-fareast-font-family: |
---|
1375 | Calibri;mso-fareast-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Magnetic-IV/data/...</span></b><span |
---|
1376 | style='mso-fareast-font-family:Calibri;mso-fareast-theme-font:minor-latin'> |
---|
1377 | entry will bring you to the location where the files have been downloaded. (It |
---|
1378 | is also possible to download them manually from <a |
---|
1379 | href="https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-IV/data/">https://subversion.xray.aps.anl.gov/pyGSAS/Tutorials/Magnetic-IV/data/</a>. |
---|
1380 | In this case you will need to navigate to the download location manually.)<br> |
---|
1381 | For this tutorial the extension on the data file is the expected one, so it |
---|
1382 | should be immediately visible.</span></p> |
---|
1383 | |
---|
1384 | <p class=MsoListParagraphCxSpMiddle style='text-indent:-.25in;mso-list:l1 level1 lfo1'><![if !supportLists]><span |
---|
1385 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span |
---|
1386 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Select |
---|
1387 | the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
---|
1388 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1389 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PrSrMnO.gda</span></b></span><span |
---|
1390 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1391 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'> data</span> |
---|
1392 | file in the first dialog and press <b style='mso-bidi-font-weight:normal'><span |
---|
1393 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1394 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Open</span></b>. |
---|
1395 | There will be a Dialog box asking <span class=GramE><b style='mso-bidi-font-weight: |
---|
1396 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1397 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Is</span></b></span><b |
---|
1398 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1399 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1400 | minor-latin'> this the file you want?</span></b> Press <span class=GramE><b |
---|
1401 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1402 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1403 | minor-latin'>Yes</span></b></span> button to proceed.<o:p></o:p></p> |
---|
1404 | |
---|
1405 | <p class=MsoListParagraphCxSpMiddle style='text-indent:-.25in;mso-list:l1 level1 lfo1'><![if !supportLists]><span |
---|
1406 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>3.<span |
---|
1407 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Since |
---|
1408 | this data file does not define an instrument parameter file, a file dialog will |
---|
1409 | appear for you to select the correct instrument parameter file. Select <span |
---|
1410 | class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1411 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1412 | minor-latin;mso-bidi-theme-font:minor-latin'>Saclay</span></b></span><b |
---|
1413 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1414 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1415 | minor-latin'> 3T2. <span class=SpellE><span class=GramE>instprm</span></span></span></b>; |
---|
1416 | you may have to change the file type in the file selection Dialog box to <b |
---|
1417 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1418 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1419 | minor-latin'>GSAS-II <span class=SpellE>instparm</span> file</span></b> to see |
---|
1420 | it. At this point the <b style='mso-bidi-font-weight:normal'><span |
---|
1421 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1422 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data |
---|
1423 | tree</span></b> window will have several entries and the plot window will show |
---|
1424 | the powder pattern</p> |
---|
1425 | |
---|
1426 | <p class=MsoListParagraphCxSpMiddle><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1427 | id="Picture_x0020_4" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:323.25pt; |
---|
1428 | height:287.25pt;visibility:visible;mso-wrap-style:square'> |
---|
1429 | <v:imagedata src="Magnetic-IV_files/image007.png" o:title=""/> |
---|
1430 | </v:shape><![endif]--><![if !vml]><img border=0 width=431 height=383 |
---|
1431 | src="Magnetic-IV_files/image008.gif" v:shapes="Picture_x0020_4"><![endif]></span><o:p></o:p></p> |
---|
1432 | |
---|
1433 | <p class=MsoListParagraphCxSpLast style='text-indent:-.25in;mso-list:l1 level1 lfo1'><![if !supportLists]><span |
---|
1434 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>4.<span |
---|
1435 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>The |
---|
1436 | last few points in the profile are problematic; I set the upper Limit to <b |
---|
1437 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1438 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1439 | minor-latin'>123.5</span></b> to avoid them.</p> |
---|
1440 | |
---|
1441 | <h3>Step 2. Read in the chemical structure for (Pr<sub>.5</sub>Sr<sub>.5</sub><span |
---|
1442 | class=GramE>)MnO<sub>3</sub></span><o:p></o:p></h3> |
---|
1443 | |
---|
1444 | <p class=MsoListParagraphCxSpFirst style='text-indent:-.25in;mso-list:l0 level1 lfo3'><![if !supportLists]><span |
---|
1445 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>1.<span |
---|
1446 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Use |
---|
1447 | the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1448 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1449 | minor-latin'>Import/Phase/from CIF file</span></b> menu item to read the phase |
---|
1450 | information for (Pr<sub>.5</sub>Sr<sub>.5</sub><span class=GramE>)MnO<sub>3</sub></span> |
---|
1451 | into the current GSAS-II project. The file you want is <span class=SpellE><b |
---|
1452 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1453 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1454 | minor-latin'>PrSrMnO.cif</span></b></span> and should be in your current |
---|
1455 | directory. Other submenu items can read phase information in other |
---|
1456 | formats.<span style='mso-spacerun:yes'> </span><o:p></o:p></p> |
---|
1457 | |
---|
1458 | <p class=MsoListParagraphCxSpMiddle style='text-indent:-.25in;mso-list:l0 level1 lfo3'><![if !supportLists]><span |
---|
1459 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>2.<span |
---|
1460 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Select |
---|
1461 | the <span class=SpellE><b style='mso-bidi-font-weight:normal'><span |
---|
1462 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1463 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PrSrMnO.cif</span></b></span><b |
---|
1464 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1465 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1466 | minor-latin'> </span></b><span style='font-family:"Calibri",sans-serif; |
---|
1467 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1468 | minor-latin'>data</span> file in the first dialog and press <b |
---|
1469 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1470 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1471 | minor-latin'>Open</span></b>. There will be a Dialog box asking <span |
---|
1472 | class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family: |
---|
1473 | "Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font: |
---|
1474 | minor-latin;mso-bidi-theme-font:minor-latin'>Is</span></b></span><b |
---|
1475 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1476 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1477 | minor-latin'> this the file you want?</span></b> Press <span class=GramE><b |
---|
1478 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1479 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1480 | minor-latin'>Yes</span></b></span> button to proceed. You will get the |
---|
1481 | opportunity to change the phase name next (I changed it to <b style='mso-bidi-font-weight: |
---|
1482 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1483 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PrSrMnO3</span></b>); |
---|
1484 | press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1485 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1486 | minor-latin'>OK</span></b> to continue.<o:p></o:p></p> |
---|
1487 | |
---|
1488 | <p class=MsoListParagraphCxSpMiddle style='text-indent:-.25in;mso-list:l1 level1 lfo1'><![if !supportLists]><span |
---|
1489 | style='mso-fareast-font-family:"Times New Roman"'><span style='mso-list:Ignore'>5.<span |
---|
1490 | style='font:7.0pt "Times New Roman"'> </span></span></span><![endif]>Next |
---|
1491 | is the histogram selection window; this connects the phase to the data so it |
---|
1492 | can be used in subsequent calculations.<span style='mso-no-proof:yes'> </span>Select |
---|
1493 | the histogram (or press <b style='mso-bidi-font-weight:normal'><span |
---|
1494 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1495 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set All</span></b>) |
---|
1496 | and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1497 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1498 | minor-latin'>OK</span></b>. The General tab for the phase is shown next</p> |
---|
1499 | |
---|
1500 | <p class=MsoListParagraphCxSpLast><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1501 | id="Picture_x0020_5" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:324.75pt; |
---|
1502 | height:174pt;visibility:visible;mso-wrap-style:square'> |
---|
1503 | <v:imagedata src="Magnetic-IV_files/image009.png" o:title=""/> |
---|
1504 | </v:shape><![endif]--><![if !vml]><img border=0 width=433 height=232 |
---|
1505 | src="Magnetic-IV_files/image010.gif" v:shapes="Picture_x0020_5"><![endif]></span></p> |
---|
1506 | |
---|
1507 | <h3>Step 3. Check powder pattern indexing<o:p></o:p></h3> |
---|
1508 | |
---|
1509 | <p class=MsoNormal>Here the objective is to determine how the reflection |
---|
1510 | positions generated from the chemical (nuclear) crystal structure lattice |
---|
1511 | match up with the peaks observed for this antiferromagnet. <o:p></o:p></p> |
---|
1512 | |
---|
1513 | <p class=MsoListParagraph style='margin-left:0in;mso-add-space:auto'>Select <b |
---|
1514 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1515 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1516 | minor-latin'>Unit Cells List</span></b> from the tree entries under the |
---|
1517 | histogram (begins with PWDR); the Indexing controls will be shown<br> |
---|
1518 | <span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_6" |
---|
1519 | o:spid="_x0000_i1043" type="#_x0000_t75" style='width:369pt;height:128.25pt; |
---|
1520 | visibility:visible;mso-wrap-style:square'> |
---|
1521 | <v:imagedata src="Magnetic-IV_files/image011.png" o:title=""/> |
---|
1522 | </v:shape><![endif]--><![if !vml]><img border=0 width=492 height=171 |
---|
1523 | src="Magnetic-IV_files/image012.gif" v:shapes="Picture_x0020_6"><![endif]></span><br> |
---|
1524 | <span class=GramE>This</span> can use lattice parameters & space groups to |
---|
1525 | generate expected reflection positions to check against the peaks in the powder |
---|
1526 | pattern. One could then enter this information by hand, but the easy way is to |
---|
1527 | use the chemical lattice directly. Do <b style='mso-bidi-font-weight:normal'><span |
---|
1528 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1529 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Cell |
---|
1530 | Index/Refine/Load Cell</span></b> from the menu; a Phase selection box will |
---|
1531 | appear with only one choice (<b style='mso-bidi-font-weight:normal'><span |
---|
1532 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1533 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PrSrMnO3</span></b>). |
---|
1534 | This was taken from the Phases present in this project; there could be more |
---|
1535 | than one depending on what you loaded/created earlier. The <b style='mso-bidi-font-weight: |
---|
1536 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1537 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Import</span></b> |
---|
1538 | menu item allows you to get lattice information from any one of the other phase |
---|
1539 | containing files known to GSAS-II. Press <b style='mso-bidi-font-weight:normal'><span |
---|
1540 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1541 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b> |
---|
1542 | and the Indexing controls will be change<br> |
---|
1543 | <span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_7" |
---|
1544 | o:spid="_x0000_i1042" type="#_x0000_t75" style='width:362.25pt;height:126pt; |
---|
1545 | visibility:visible;mso-wrap-style:square'> |
---|
1546 | <v:imagedata src="Magnetic-IV_files/image013.png" o:title=""/> |
---|
1547 | </v:shape><![endif]--><![if !vml]><img border=0 width=483 height=168 |
---|
1548 | src="Magnetic-IV_files/image014.gif" v:shapes="Picture_x0020_7"><![endif]></span></p> |
---|
1549 | |
---|
1550 | <p class=MsoNormal><span class=GramE>showing</span> the lattice constants for (Pr<sub>.5</sub>Sr<sub>.5</sub>)MnO<sub>3</sub> |
---|
1551 | you had obtained from the <span class=SpellE>cif</span> file and the powder |
---|
1552 | pattern will change showing the lines for F mmm and those lattice parameters.</p> |
---|
1553 | |
---|
1554 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1555 | id="Picture_x0020_9" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:360.75pt; |
---|
1556 | height:320.25pt;visibility:visible;mso-wrap-style:square'> |
---|
1557 | <v:imagedata src="Magnetic-IV_files/image015.png" o:title=""/> |
---|
1558 | </v:shape><![endif]--><![if !vml]><img border=0 width=481 height=427 |
---|
1559 | src="Magnetic-IV_files/image016.gif" v:shapes="Picture_x0020_9"><![endif]></span><o:p></o:p></p> |
---|
1560 | |
---|
1561 | <p class=MsoNormal>Ive zoomed into the 6-40 <span class=SpellE>deg</span> |
---|
1562 | range to see that a number of peaks are not indexed by this space group (NB: F |
---|
1563 | mmm lacks space group extinctions apart from F-centering so there is no need to |
---|
1564 | change it as in previous tutorials) and lattice. As noted in the previous |
---|
1565 | tutorial, antiferromagnetic ordering may force an increase in the unit cell |
---|
1566 | dimensions (usually a doubling or tripling of one or more cell dimensions) or |
---|
1567 | by removing a space group centering. Here we are starting with an F-centered chemical |
---|
1568 | cell so a loss of centering to get either A-, B- or C- centering is a |
---|
1569 | possibility to consider. To explore this we will try each in turn and see how |
---|
1570 | the generated reflection positions match up with the observed peaks. </p> |
---|
1571 | |
---|
1572 | <p class=MsoNormal>Change the <span class=SpellE>Bravais</span> lattice to <span |
---|
1573 | class=SpellE>Ammm</span> and the Space group to <span class=GramE>A</span> m <span |
---|
1574 | class=SpellE>m</span> <span class=SpellE>m</span>; the plot will change on each |
---|
1575 | choice to give</p> |
---|
1576 | |
---|
1577 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1578 | id="Picture_x0020_10" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:357.75pt; |
---|
1579 | height:317.25pt;visibility:visible;mso-wrap-style:square'> |
---|
1580 | <v:imagedata src="Magnetic-IV_files/image019.png" o:title=""/> |
---|
1581 | </v:shape><![endif]--><![if !vml]><img border=0 width=477 height=423 |
---|
1582 | src="Magnetic-IV_files/image031.gif" v:shapes="Picture_x0020_10"><![endif]></span><o:p></o:p></p> |
---|
1583 | |
---|
1584 | <p class=MsoListParagraph style='margin-left:0in;mso-add-space:auto'>Those line |
---|
1585 | up pretty well; note the lowest angle peak & the one at about 21º2Θ. |
---|
1586 | Now change <span class=SpellE>Bravais</span> lattice and Space group to B mmm; |
---|
1587 | a new plot will appear<o:p></o:p></p> |
---|
1588 | |
---|
1589 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1590 | id="Picture_x0020_11" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:360.75pt; |
---|
1591 | height:320.25pt;visibility:visible;mso-wrap-style:square'> |
---|
1592 | <v:imagedata src="Magnetic-IV_files/image021.png" o:title=""/> |
---|
1593 | </v:shape><![endif]--><![if !vml]><img border=0 width=481 height=427 |
---|
1594 | src="Magnetic-IV_files/image032.gif" v:shapes="Picture_x0020_11"><![endif]></span></p> |
---|
1595 | |
---|
1596 | <p class=MsoNormal>The match is not quite as good; the 1<sup>st</sup> line just |
---|
1597 | misses the 1<sup>st</sup> peak top and the one at 21º2Θ also misses the |
---|
1598 | peak top. Lastly, lets try <span class=SpellE>Cmmm</span>; enter it for <span |
---|
1599 | class=SpellE>Bravais</span> lattice and space group. A new plot appears</p> |
---|
1600 | |
---|
1601 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1602 | id="Picture_x0020_12" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:363pt; |
---|
1603 | height:322.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1604 | <v:imagedata src="Magnetic-IV_files/image023.png" o:title=""/> |
---|
1605 | </v:shape><![endif]--><![if !vml]><img border=0 width=484 height=430 |
---|
1606 | src="Magnetic-IV_files/image033.gif" v:shapes="Picture_x0020_12"><![endif]></span></p> |
---|
1607 | |
---|
1608 | <p class=MsoNormal>This fit seems even worse, so the right description is lose |
---|
1609 | the B- and C-centering leaving just A-centering. However, we want the A-center |
---|
1610 | to be magnetic; the way to do this is to assign the propagation vector <span |
---|
1611 | class=SpellE>k<sub>x</sub><span class=GramE>,k<sub>y</sub>,k<sub>z</sub></span></span> |
---|
1612 | = (1,0,0) when we run k-SUBGROUPSMAG on the parent space group (<span |
---|
1613 | class=SpellE>Fmmm</span>).</p> |
---|
1614 | |
---|
1615 | <h3>Step 4. Run k-SUBGROUPSMAG<o:p></o:p></h3> |
---|
1616 | |
---|
1617 | <p class=MsoNormal>In this next step, you will be accessing the Bilbao |
---|
1618 | crystallographic server so you must be connected to the internet. In the Cell |
---|
1619 | Index/Refine menu select <b style='mso-bidi-font-weight:normal'><span |
---|
1620 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1621 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Run |
---|
1622 | k-SUBGROUPSMAG</span></b>; a small popup dialog will appear<o:p></o:p></p> |
---|
1623 | |
---|
1624 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1625 | id="Picture_x0020_14" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:166.5pt; |
---|
1626 | height:278.25pt;visibility:visible;mso-wrap-style:square'> |
---|
1627 | <v:imagedata src="Magnetic-IV_files/image025.png" o:title=""/> |
---|
1628 | </v:shape><![endif]--><![if !vml]><img border=0 width=222 height=371 |
---|
1629 | src="Magnetic-IV_files/image034.gif" v:shapes="Picture_x0020_14"><![endif]></span><o:p></o:p></p> |
---|
1630 | |
---|
1631 | <p class=MsoNormal>These are the controls for running the Bilbao routine. The |
---|
1632 | space group (F mmm) is taken from the Space Group entry on the Unit Cells |
---|
1633 | window. Since we just discovered the prop<span class=SpellE>agation</span> |
---|
1634 | vector as (1<span class=GramE>,0,0</span>) change <b style='mso-bidi-font-weight: |
---|
1635 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1636 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>kx1</span></b> |
---|
1637 | to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1638 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1639 | minor-latin'>1</span></b>. The available selections were determined by |
---|
1640 | surveying the known magnetic crystal structures given in the Bilbao Magnetic |
---|
1641 | Structures database. Select <span class=SpellE><b style='mso-bidi-font-weight: |
---|
1642 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1643 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Mn</span></b></span> |
---|
1644 | for the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1645 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1646 | minor-latin'>test for mag atoms</span></b> and then press <b style='mso-bidi-font-weight: |
---|
1647 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1648 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>OK</span></b>. |
---|
1649 | A popup dialog will appear reminding you how to cite the Bilbao routine in any |
---|
1650 | paper you write using this facility.<o:p></o:p></p> |
---|
1651 | |
---|
1652 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1653 | id="_x0000_i1036" type="#_x0000_t75" style='width:357.75pt;height:123.75pt; |
---|
1654 | visibility:visible;mso-wrap-style:square'> |
---|
1655 | <v:imagedata src="Magnetic-IV_files/image027.png" o:title=""/> |
---|
1656 | </v:shape><![endif]--><![if !vml]><img border=0 width=477 height=165 |
---|
1657 | src="Magnetic-IV_files/image035.gif" v:shapes="_x0000_i1036"><![endif]></span><o:p></o:p></p> |
---|
1658 | |
---|
1659 | <p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span |
---|
1660 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1661 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Ok</span></b>, |
---|
1662 | the nag note will also appear on the console and after a pause, the console |
---|
1663 | will show request OK indicating that the Bilbao site has responded with some |
---|
1664 | results. GSAS-II will next display a File Dialog asking for a project name to |
---|
1665 | save this project; change the directory to a useful place for your work on this |
---|
1666 | tutorial and give the project a name; I used <b style='mso-bidi-font-weight: |
---|
1667 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1668 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PrSrMnO3.<o:p></o:p></span></b></p> |
---|
1669 | |
---|
1670 | <p class=MsoNormal>The GSAS-II data window will display the results from |
---|
1671 | k-SUBGROUPSMAG. (If k-SUBGROUPSMAG failed because you lack internet access, |
---|
1672 | this file is located in the same location as the powder data and <span |
---|
1673 | class=SpellE>cif</span> files used above were found. Do <b style='mso-bidi-font-weight: |
---|
1674 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1675 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>File/Open |
---|
1676 | Project</span></b> from the main menu to access it as <b style='mso-bidi-font-weight: |
---|
1677 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1678 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PrSrMnO3.gpx</span></b>, |
---|
1679 | then do <span class=GramE><b style='mso-bidi-font-weight:normal'><span |
---|
1680 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1681 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Save</span></b></span><b |
---|
1682 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1683 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1684 | minor-latin'> as</span></b> to save it immediately in your working directory.). |
---|
1685 | The Unit Cells List window will show the results<o:p></o:p></p> |
---|
1686 | |
---|
1687 | <p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span |
---|
1688 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1689 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin;mso-no-proof: |
---|
1690 | yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_15" o:spid="_x0000_i1035" |
---|
1691 | type="#_x0000_t75" style='width:360.75pt;height:323.25pt;visibility:visible; |
---|
1692 | mso-wrap-style:square'> |
---|
1693 | <v:imagedata src="Magnetic-IV_files/image029.png" o:title=""/> |
---|
1694 | </v:shape><![endif]--><![if !vml]><img border=0 width=481 height=431 |
---|
1695 | src="Magnetic-IV_files/image036.gif" v:shapes="Picture_x0020_15"><![endif]></span></b></p> |
---|
1696 | |
---|
1697 | <p class=MsoNormal>The <b style='mso-bidi-font-weight:normal'><span |
---|
1698 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1699 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>preserve axes</span></b> |
---|
1700 | option on the k-SUBGROUPSMAG is set by default to transform the standard |
---|
1701 | setting result from k-SUBGROUPSMAG for orthorhombic to one that closely is |
---|
1702 | aligned, if possible, to the parent cell axes. So this list contains |
---|
1703 | non-standard settings of orthorhombic space groups (e.g. the chemical version |
---|
1704 | of #3 P<sub>C</sub> <span class=SpellE>bmn</span> is a non-standard version of P |
---|
1705 | <span class=SpellE>mna</span>, #53 in International Tables for Crystallography |
---|
1706 | Vol A.). If desired, clearing the flag and rerunning k-SUBGROUPSMAG will produce |
---|
1707 | magnetic space groups in standard settings; we will continue with the above set |
---|
1708 | so the chemical cell and magnetic cell axes line up together.</p> |
---|
1709 | |
---|
1710 | <p class=MsoNormal>Use the <b style='mso-bidi-font-weight:normal'><span |
---|
1711 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1712 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Try</span></b> |
---|
1713 | on the 4 marked Keep out of the 1<sup>st</sup> 8 solutions. Only #7 & #8 |
---|
1714 | will index the low angle peaks correctly. Well go with these. The solutions |
---|
1715 | further down are ones in which more than one symmetry generator was removed; if |
---|
1716 | need be we can go back and look at those. NB: running k-SUBGROUPSMAG with the Landau |
---|
1717 | transition checked will give just these 1<sup>st</sup> 8 solutions. This might |
---|
1718 | be appropriate because the magnetic transition for (Pr<sub>.5</sub>Sr<sub>.5</sub><span |
---|
1719 | class=GramE>)MnO<sub>3</sub></span><sub> </sub>is a continuous 2<sup>nd</sup> |
---|
1720 | order transition. However, by doing this one might not see the correct result!</p> |
---|
1721 | |
---|
1722 | <h3>Step 5. Select 1<sup>st</sup> magnetic structure<o:p></o:p></h3> |
---|
1723 | |
---|
1724 | <p class=MsoNormal>Select the <b style='mso-bidi-font-weight:normal'><span |
---|
1725 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1726 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PrSrMnO3</span></b> |
---|
1727 | phase from the GSAS-II data tree (under Phases). The General tab is shown for |
---|
1728 | this nuclear phase.<o:p></o:p></p> |
---|
1729 | |
---|
1730 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1731 | id="Picture_x0020_16" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:358.5pt; |
---|
1732 | height:200.25pt;visibility:visible;mso-wrap-style:square'> |
---|
1733 | <v:imagedata src="Magnetic-IV_files/image037.png" o:title=""/> |
---|
1734 | </v:shape><![endif]--><![if !vml]><img border=0 width=478 height=267 |
---|
1735 | src="Magnetic-IV_files/image038.gif" v:shapes="Picture_x0020_16"><![endif]></span></p> |
---|
1736 | |
---|
1737 | <p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span |
---|
1738 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1739 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Compute/Select |
---|
1740 | magnetic phase</span></b>; that will make a small popup dialog<o:p></o:p></p> |
---|
1741 | |
---|
1742 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1743 | id="Picture_x0020_17" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:276.75pt; |
---|
1744 | height:222.75pt;visibility:visible;mso-wrap-style:square'> |
---|
1745 | <v:imagedata src="Magnetic-IV_files/image039.png" o:title=""/> |
---|
1746 | </v:shape><![endif]--><![if !vml]><img border=0 width=369 height=297 |
---|
1747 | src="Magnetic-IV_files/image040.gif" v:shapes="Picture_x0020_17"><![endif]></span></p> |
---|
1748 | |
---|
1749 | <p class=MsoNormal>This shows all magnetic phases that were marked <span |
---|
1750 | class=GramE>Keep</span> in the Unit Cells List; for each you see the |
---|
1751 | transformation and vector (the first two results we had checked to see if they |
---|
1752 | indexed the pattern). Select the 1<sup>st</sup> one and press <b |
---|
1753 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1754 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1755 | minor-latin'>OK</span></b>; a new popup dialog will appear.<o:p></o:p></p> |
---|
1756 | |
---|
1757 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1758 | id="Picture_x0020_18" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:276.75pt; |
---|
1759 | height:92.25pt;visibility:visible;mso-wrap-style:square'> |
---|
1760 | <v:imagedata src="Magnetic-IV_files/image041.png" o:title=""/> |
---|
1761 | </v:shape><![endif]--><![if !vml]><img border=0 width=369 height=123 |
---|
1762 | src="Magnetic-IV_files/image042.gif" v:shapes="Picture_x0020_18"><![endif]></span></p> |
---|
1763 | |
---|
1764 | <p class=MsoNormal>This one <span class=SpellE>Mn</span> atom has an allowed |
---|
1765 | moment component (My). Press <span class=GramE>Yes</span> to use it. The |
---|
1766 | project will be saved first, then a file dialog box will appear offering a |
---|
1767 | project name for this magnetic structure. It is named with the number from the |
---|
1768 | space group list (<b style='mso-bidi-font-weight:normal'><span |
---|
1769 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1770 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PrSrMnO3 |
---|
1771 | mag_7.gpx</span></b>); press <b style='mso-bidi-font-weight:normal'><span |
---|
1772 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1773 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Save.</span></b> |
---|
1774 | The new project will be opened to the General tab for the A<sub>B</sub> <span |
---|
1775 | class=SpellE>mma</span> magnetic phase just created.</p> |
---|
1776 | |
---|
1777 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1778 | id="Picture_x0020_19" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:354pt; |
---|
1779 | height:197.25pt;visibility:visible;mso-wrap-style:square'> |
---|
1780 | <v:imagedata src="Magnetic-IV_files/image043.png" o:title=""/> |
---|
1781 | </v:shape><![endif]--><![if !vml]><img border=0 width=472 height=263 |
---|
1782 | src="Magnetic-IV_files/image044.gif" v:shapes="Picture_x0020_19"><![endif]></span><o:p></o:p></p> |
---|
1783 | |
---|
1784 | <p class=MsoNormal>Select Atoms, enter <b style='mso-bidi-font-weight:normal'><span |
---|
1785 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1786 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>1.0</span></b> |
---|
1787 | for the <span class=SpellE>mn</span> atom <span class=GramE>My</span> values. |
---|
1788 | Then go to Draw Atoms, select them all and do <span class=GramE><b |
---|
1789 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1790 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1791 | minor-latin'>Edit</span></b></span><b style='mso-bidi-font-weight:normal'><span |
---|
1792 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1793 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'> Figure/Fill |
---|
1794 | unit cell</span></b>; youll see this antiferromagnetic structure<o:p></o:p></p> |
---|
1795 | |
---|
1796 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1797 | id="Picture_x0020_20" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:5in; |
---|
1798 | height:319.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1799 | <v:imagedata src="Magnetic-IV_files/image045.png" o:title=""/> |
---|
1800 | </v:shape><![endif]--><![if !vml]><img border=0 width=480 height=426 |
---|
1801 | src="Magnetic-IV_files/image046.gif" v:shapes="Picture_x0020_20"><![endif]></span></p> |
---|
1802 | |
---|
1803 | <p class=MsoNormal>The <span class=SpellE>wR</span> ~26% with some intensity |
---|
1804 | for all the peaks in the pattern, but the magnetic moment is probably wrong. Go |
---|
1805 | to the magnetic phase Atoms tab and select refine <b style='mso-bidi-font-weight: |
---|
1806 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1807 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>M</span></b> |
---|
1808 | for the <span class=SpellE>Mn</span> atom. Do <b style='mso-bidi-font-weight: |
---|
1809 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1810 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Calculate/Refine</span></b> |
---|
1811 | again; the residual drops a bit but now the errors seem to be mostly peak |
---|
1812 | position. Go to the General tab for both phases and check the <b |
---|
1813 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1814 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1815 | minor-latin'>Refine unit cell</span></b> box for each. Then go to <b |
---|
1816 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1817 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1818 | minor-latin'>Sample parameters</span></b> for the PWDR data set, set goniometer |
---|
1819 | radius to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1820 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1821 | minor-latin'>1000</span></b> and check both <b style='mso-bidi-font-weight: |
---|
1822 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1823 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Sample |
---|
1824 | X & Y <span class=SpellE>displ</span></span></b> parameters. Do <b |
---|
1825 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1826 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1827 | minor-latin'>Calculate/Refine</span></b> again; <span class=SpellE>wR</span> ~ 7% |
---|
1828 | now. To finish the refinement, include Instrument parameters <b |
---|
1829 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1830 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1831 | minor-latin'>U, V, W, X, Y and SH/L</span></b>; use <b style='mso-bidi-font-weight: |
---|
1832 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1833 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>6</span></b> |
---|
1834 | Background term and refine <b style='mso-bidi-font-weight:normal'><span |
---|
1835 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1836 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>XU</span></b> |
---|
1837 | for all atoms in the chemical phase and <b style='mso-bidi-font-weight:normal'><span |
---|
1838 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1839 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>UM</span></b> |
---|
1840 | in the magnetic phase. After 2-3 sets of <b style='mso-bidi-font-weight:normal'><span |
---|
1841 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1842 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Calculate/Refine</span></b> |
---|
1843 | my residual was <span class=SpellE>wR</span>=6.15% and the magnetic <span |
---|
1844 | class=SpellE>Mn</span> atom moment <span class=SpellE>Mz</span> = 3.41. The fit |
---|
1845 | shown on the plot is quite good.</p> |
---|
1846 | |
---|
1847 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1848 | id="Picture_x0020_21" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:356.25pt; |
---|
1849 | height:316.5pt;visibility:visible;mso-wrap-style:square'> |
---|
1850 | <v:imagedata src="Magnetic-IV_files/image047.png" o:title=""/> |
---|
1851 | </v:shape><![endif]--><![if !vml]><img border=0 width=475 height=422 |
---|
1852 | src="Magnetic-IV_files/image048.gif" v:shapes="Picture_x0020_21"><![endif]></span></p> |
---|
1853 | |
---|
1854 | <p class=MsoNormal>I show the plot with <span class=SpellE><span class=GramE>sqrt</span></span><span |
---|
1855 | class=GramE>(</span>intensity) & weighted difference curves; the latter is |
---|
1856 | clearly all within 2-3 <span style='font-family:Symbol'>s</span> of the |
---|
1857 | observed data. Now lets try the other solution.</p> |
---|
1858 | |
---|
1859 | <h3>Step 6. Select 2nd magnetic structure<o:p></o:p></h3> |
---|
1860 | |
---|
1861 | <p class=MsoNormal>To continue the selection process, we need to use the saved |
---|
1862 | project used for the first selection because it contains the table of possible |
---|
1863 | magnetic space groups generated by k-SUBGROUPSMAG. Do <b style='mso-bidi-font-weight: |
---|
1864 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1865 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Open |
---|
1866 | project</span></b> from the main menu and select <b style='mso-bidi-font-weight: |
---|
1867 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
---|
1868 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>PrSrMnO3.gpx</span></b>; |
---|
1869 | youll see a reminder to save the old project (we just did this) and select the |
---|
1870 | <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
---|
1871 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
---|
1872 | minor-latin'>PrSrMnO3</span></b> phase (should be the only one); the General |
---|
1873 | tab will be shown</p> |
---|
1874 | |
---|
1875 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1876 | id="Picture_x0020_22" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:5in; |
---|
1877 | height:201pt;visibility:visible;mso-wrap-style:square'> |
---|
1878 | <v:imagedata src="Magnetic-IV_files/image049.png" o:title=""/> |
---|
1879 | </v:shape><![endif]--><![if !vml]><img border=0 width=480 height=268 |
---|
1880 | src="Magnetic-IV_files/image050.gif" v:shapes="Picture_x0020_22"><![endif]></span><o:p></o:p></p> |
---|
1881 | |
---|
1882 | <p class=MsoNormal>Do <b style='mso-bidi-font-weight:normal'><span |
---|
1883 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
---|
1884 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Compute/Select |
---|
1885 | magnetic phase</span></b> from the menu; the popup should look like<o:p></o:p></p> |
---|
1886 | |
---|
1887 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
---|
1888 | id="Picture_x0020_23" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:276.75pt; |
---|
1889 | height:222.75pt;visibility:visible;mso-wrap-style:square'> |
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1890 | <v:imagedata src="Magnetic-IV_files/image039.png" o:title=""/> |
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1891 | </v:shape><![endif]--><![if !vml]><img border=0 width=369 height=297 |
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1892 | src="Magnetic-IV_files/image040.gif" v:shapes="Picture_x0020_23"><![endif]></span></p> |
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1893 | |
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1894 | <p class=MsoNormal>We already tried the 1<sup>st</sup> one; now select the 2<sup>nd</sup> |
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1895 | and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
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1896 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
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1897 | minor-latin'>OK</span></b>; a popup will appear<o:p></o:p></p> |
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1898 | |
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1899 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
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1900 | id="Picture_x0020_24" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:281.25pt; |
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1901 | height:92.25pt;visibility:visible;mso-wrap-style:square'> |
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1902 | <v:imagedata src="Magnetic-IV_files/image051.png" o:title=""/> |
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1903 | </v:shape><![endif]--><![if !vml]><img border=0 width=375 height=123 |
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1904 | src="Magnetic-IV_files/image052.gif" v:shapes="Picture_x0020_24"><![endif]></span></p> |
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1905 | |
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1906 | <p class=MsoNormal>In this case, the <span class=SpellE>Mn</span> atom has |
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1907 | allowed <span class=SpellE>Mx</span> & <span class=SpellE>Mz</span> |
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1908 | components (the previous one had only <span class=GramE>My</span>). Press <span |
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1909 | class=GramE>Yes</span> to select it. The project will be saved and a new |
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1910 | project <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
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1911 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
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1912 | minor-latin'>PrSrMnO3 mag_8.gpx</span></b> will be created. The General tab for |
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1913 | this new phase will be shown</p> |
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1914 | |
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1915 | <p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape |
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1916 | id="Picture_x0020_25" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:355.5pt; |
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1917 | height:209.25pt;visibility:visible;mso-wrap-style:square'> |
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1918 | <v:imagedata src="Magnetic-IV_files/image053.png" o:title=""/> |
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1919 | </v:shape><![endif]--><![if !vml]><img border=0 width=474 height=279 |
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1920 | src="Magnetic-IV_files/image054.gif" v:shapes="Picture_x0020_25"><![endif]></span></p> |
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1921 | |
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1922 | <p class=MsoNormal>Select the Atoms tab & set <span class=SpellE>Mx</span> |
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1923 | & My for the <span class=SpellE>Mn</span> atom to <b style='mso-bidi-font-weight: |
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1924 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
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1925 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>1.0</span></b>. |
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1926 | Then do the refinement steps we outlined for the 1<sup>st</sup> magnetic structure. |
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1927 | Do <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
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1928 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
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1929 | minor-latin'>Calculate/Refine</span></b> first. Then set the <b |
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1930 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
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1931 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
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1932 | minor-latin'>M</span></b> refine flags for the magnetic atoms; do <b |
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1933 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
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1934 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
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1935 | minor-latin'>Calculate/Refine</span></b>. Add <b style='mso-bidi-font-weight: |
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1936 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
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1937 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>sample |
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1938 | X & Y displacements</span></b> (radius = <b style='mso-bidi-font-weight: |
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1939 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
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1940 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>1000</span></b>) |
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1941 | and both lattice parameters; do <b style='mso-bidi-font-weight:normal'><span |
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1942 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
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1943 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Calculate/Refine |
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1944 | </span></b>(<span class=GramE>wP~</span>11% - poorer than before). Then add |
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1945 | Instrument parameters <b style='mso-bidi-font-weight:normal'><span |
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1946 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
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1947 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>U, V, W, X, Y |
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1948 | & SH/L</span></b>; do <b style='mso-bidi-font-weight:normal'><span |
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1949 | style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin; |
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1950 | mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Calculate/Refine |
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1951 | </span></b>(<span class=SpellE>wR</span> ~10.75% - still poorer). Finally use <b |
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1952 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
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1953 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
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1954 | minor-latin'>6</span></b> background coefficients and refine <b |
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1955 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
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1956 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
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1957 | minor-latin'>XU</span></b> for the chemical phase atoms and <b |
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1958 | style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif; |
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1959 | mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font: |
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1960 | minor-latin'>XUM</span></b> for the magnetic atoms. Do <b style='mso-bidi-font-weight: |
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1961 | normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font: |
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1962 | minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Calculate/Refine</span></b> |
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1963 | a few times until it converges. I got <span class=SpellE>wR</span> = 10.2% |
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1964 | which is definitely poorer than the result for the first model. Therefore, the |
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1965 | model #7 is the correct one with magnetic space group A<sub>B</sub> <span |
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1966 | class=SpellE>mma</span> and a moment <span class=SpellE>m<sub>z</sub></span>=3.407(12) |
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1967 | on the <span class=SpellE>Mn</span> atom. Save the bad project if you wish. |
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1968 | This concludes the tutorial.<o:p></o:p></p> |
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1969 | |
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1970 | <p class=MsoNormal><o:p> </o:p></p> |
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1971 | |
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1972 | </div> |
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1973 | |
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1974 | </body> |
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1975 | |
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1976 | </html> |
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