source: Tutorials/2DStrain/Strain fitting of 2D data in GSAS-II.htm @ 3040

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415  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/>
416  <w:LsdException Locked="false" Priority="70" Name="Dark List"/>
417  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/>
418  <w:LsdException Locked="false" Priority="72" Name="Colorful List"/>
419  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
420  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
421  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
422  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
423  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
424  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
425  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
426  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
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428   Name="List Paragraph"/>
429  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
430  <w:LsdException Locked="false" Priority="30" QFormat="true"
431   Name="Intense Quote"/>
432  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
433  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
434  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
435  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
436  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
437  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
438  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
439  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
440  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
441  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
442  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
443  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
444  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
445  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
446  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
447  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
448  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
449  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
450  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
451  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
452  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
453  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
454  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
455  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
456  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
457  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
458  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
459  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
460  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
461  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
462  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
463  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
464  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
465  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
466  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
467  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
468  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
469  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
470  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
471  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
472  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
473  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
474  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
475  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
476  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
477  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
478  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
479  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
480  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
481  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
482  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
483  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
484  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
485  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
486  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
487  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
488  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
489  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
490  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
491  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
492  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
493  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
494  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
495  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
496  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
497  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
498  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
499  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
500  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
501  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
502  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
503  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
504  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
505  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
506  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
507  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
508  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
509  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
510  <w:LsdException Locked="false" Priority="19" QFormat="true"
511   Name="Subtle Emphasis"/>
512  <w:LsdException Locked="false" Priority="21" QFormat="true"
513   Name="Intense Emphasis"/>
514  <w:LsdException Locked="false" Priority="31" QFormat="true"
515   Name="Subtle Reference"/>
516  <w:LsdException Locked="false" Priority="32" QFormat="true"
517   Name="Intense Reference"/>
518  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
519  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
520   UnhideWhenUsed="true" Name="Bibliography"/>
521  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
522   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
523  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
524  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
525  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
526  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
527  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
528  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
529  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
530  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
531  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
532  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
533  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
534  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
535  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
536  <w:LsdException Locked="false" Priority="46"
537   Name="Grid Table 1 Light Accent 1"/>
538  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
539  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
540  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
541  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
542  <w:LsdException Locked="false" Priority="51"
543   Name="Grid Table 6 Colorful Accent 1"/>
544  <w:LsdException Locked="false" Priority="52"
545   Name="Grid Table 7 Colorful Accent 1"/>
546  <w:LsdException Locked="false" Priority="46"
547   Name="Grid Table 1 Light Accent 2"/>
548  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
549  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
550  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
551  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
552  <w:LsdException Locked="false" Priority="51"
553   Name="Grid Table 6 Colorful Accent 2"/>
554  <w:LsdException Locked="false" Priority="52"
555   Name="Grid Table 7 Colorful Accent 2"/>
556  <w:LsdException Locked="false" Priority="46"
557   Name="Grid Table 1 Light Accent 3"/>
558  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
559  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
560  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
561  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
562  <w:LsdException Locked="false" Priority="51"
563   Name="Grid Table 6 Colorful Accent 3"/>
564  <w:LsdException Locked="false" Priority="52"
565   Name="Grid Table 7 Colorful Accent 3"/>
566  <w:LsdException Locked="false" Priority="46"
567   Name="Grid Table 1 Light Accent 4"/>
568  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
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570  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
571  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
572  <w:LsdException Locked="false" Priority="51"
573   Name="Grid Table 6 Colorful Accent 4"/>
574  <w:LsdException Locked="false" Priority="52"
575   Name="Grid Table 7 Colorful Accent 4"/>
576  <w:LsdException Locked="false" Priority="46"
577   Name="Grid Table 1 Light Accent 5"/>
578  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
579  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
580  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
581  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
582  <w:LsdException Locked="false" Priority="51"
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584  <w:LsdException Locked="false" Priority="52"
585   Name="Grid Table 7 Colorful Accent 5"/>
586  <w:LsdException Locked="false" Priority="46"
587   Name="Grid Table 1 Light Accent 6"/>
588  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
589  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
590  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
591  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
592  <w:LsdException Locked="false" Priority="51"
593   Name="Grid Table 6 Colorful Accent 6"/>
594  <w:LsdException Locked="false" Priority="52"
595   Name="Grid Table 7 Colorful Accent 6"/>
596  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
597  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
598  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
599  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
600  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
601  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
602  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
603  <w:LsdException Locked="false" Priority="46"
604   Name="List Table 1 Light Accent 1"/>
605  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
606  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
607  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
608  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
609  <w:LsdException Locked="false" Priority="51"
610   Name="List Table 6 Colorful Accent 1"/>
611  <w:LsdException Locked="false" Priority="52"
612   Name="List Table 7 Colorful Accent 1"/>
613  <w:LsdException Locked="false" Priority="46"
614   Name="List Table 1 Light Accent 2"/>
615  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
616  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
617  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
618  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
619  <w:LsdException Locked="false" Priority="51"
620   Name="List Table 6 Colorful Accent 2"/>
621  <w:LsdException Locked="false" Priority="52"
622   Name="List Table 7 Colorful Accent 2"/>
623  <w:LsdException Locked="false" Priority="46"
624   Name="List Table 1 Light Accent 3"/>
625  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
626  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
627  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
628  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
629  <w:LsdException Locked="false" Priority="51"
630   Name="List Table 6 Colorful Accent 3"/>
631  <w:LsdException Locked="false" Priority="52"
632   Name="List Table 7 Colorful Accent 3"/>
633  <w:LsdException Locked="false" Priority="46"
634   Name="List Table 1 Light Accent 4"/>
635  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
636  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
637  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
638  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
639  <w:LsdException Locked="false" Priority="51"
640   Name="List Table 6 Colorful Accent 4"/>
641  <w:LsdException Locked="false" Priority="52"
642   Name="List Table 7 Colorful Accent 4"/>
643  <w:LsdException Locked="false" Priority="46"
644   Name="List Table 1 Light Accent 5"/>
645  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
646  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
647  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
648  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
649  <w:LsdException Locked="false" Priority="51"
650   Name="List Table 6 Colorful Accent 5"/>
651  <w:LsdException Locked="false" Priority="52"
652   Name="List Table 7 Colorful Accent 5"/>
653  <w:LsdException Locked="false" Priority="46"
654   Name="List Table 1 Light Accent 6"/>
655  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
656  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
657  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
658  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
659  <w:LsdException Locked="false" Priority="51"
660   Name="List Table 6 Colorful Accent 6"/>
661  <w:LsdException Locked="false" Priority="52"
662   Name="List Table 7 Colorful Accent 6"/>
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784        mso-margin-bottom-alt:auto;
785        margin-left:0in;
786        mso-pagination:widow-orphan;
787        mso-outline-level:5;
788        font-size:12.0pt;
789        font-family:"Times New Roman",serif;
790        mso-fareast-font-family:"Times New Roman";
791        mso-fareast-theme-font:minor-fareast;
792        color:#4F4FFF;
793        font-weight:bold;}
794p.MsoTitle, li.MsoTitle, div.MsoTitle
795        {mso-style-noshow:yes;
796        mso-style-priority:10;
797        mso-style-unhide:no;
798        mso-style-qformat:yes;
799        mso-style-link:"Title Char";
800        mso-style-next:Normal;
801        margin-top:0in;
802        margin-right:0in;
803        margin-bottom:15.0pt;
804        margin-left:0in;
805        mso-add-space:auto;
806        mso-pagination:widow-orphan;
807        border:none;
808        mso-border-bottom-alt:solid #4F81BD 1.0pt;
809        mso-border-bottom-themecolor:accent1;
810        padding:0in;
811        mso-padding-alt:0in 0in 4.0pt 0in;
812        font-size:26.0pt;
813        font-family:"Cambria",serif;
814        mso-ascii-font-family:Cambria;
815        mso-ascii-theme-font:major-latin;
816        mso-fareast-font-family:"Times New Roman";
817        mso-fareast-theme-font:major-fareast;
818        mso-hansi-font-family:Cambria;
819        mso-hansi-theme-font:major-latin;
820        mso-bidi-font-family:"Times New Roman";
821        mso-bidi-theme-font:major-bidi;
822        color:#17365D;
823        mso-themecolor:text2;
824        mso-themeshade:191;
825        letter-spacing:.25pt;
826        mso-font-kerning:14.0pt;}
827p.MsoTitleCxSpFirst, li.MsoTitleCxSpFirst, div.MsoTitleCxSpFirst
828        {mso-style-noshow:yes;
829        mso-style-priority:10;
830        mso-style-unhide:no;
831        mso-style-qformat:yes;
832        mso-style-link:"Title Char";
833        mso-style-next:Normal;
834        mso-style-type:export-only;
835        margin:0in;
836        margin-bottom:.0001pt;
837        mso-add-space:auto;
838        mso-pagination:widow-orphan;
839        border:none;
840        mso-border-bottom-alt:solid #4F81BD 1.0pt;
841        mso-border-bottom-themecolor:accent1;
842        padding:0in;
843        mso-padding-alt:0in 0in 4.0pt 0in;
844        font-size:26.0pt;
845        font-family:"Cambria",serif;
846        mso-ascii-font-family:Cambria;
847        mso-ascii-theme-font:major-latin;
848        mso-fareast-font-family:"Times New Roman";
849        mso-fareast-theme-font:major-fareast;
850        mso-hansi-font-family:Cambria;
851        mso-hansi-theme-font:major-latin;
852        mso-bidi-font-family:"Times New Roman";
853        mso-bidi-theme-font:major-bidi;
854        color:#17365D;
855        mso-themecolor:text2;
856        mso-themeshade:191;
857        letter-spacing:.25pt;
858        mso-font-kerning:14.0pt;}
859p.MsoTitleCxSpMiddle, li.MsoTitleCxSpMiddle, div.MsoTitleCxSpMiddle
860        {mso-style-noshow:yes;
861        mso-style-priority:10;
862        mso-style-unhide:no;
863        mso-style-qformat:yes;
864        mso-style-link:"Title Char";
865        mso-style-next:Normal;
866        mso-style-type:export-only;
867        margin:0in;
868        margin-bottom:.0001pt;
869        mso-add-space:auto;
870        mso-pagination:widow-orphan;
871        border:none;
872        mso-border-bottom-alt:solid #4F81BD 1.0pt;
873        mso-border-bottom-themecolor:accent1;
874        padding:0in;
875        mso-padding-alt:0in 0in 4.0pt 0in;
876        font-size:26.0pt;
877        font-family:"Cambria",serif;
878        mso-ascii-font-family:Cambria;
879        mso-ascii-theme-font:major-latin;
880        mso-fareast-font-family:"Times New Roman";
881        mso-fareast-theme-font:major-fareast;
882        mso-hansi-font-family:Cambria;
883        mso-hansi-theme-font:major-latin;
884        mso-bidi-font-family:"Times New Roman";
885        mso-bidi-theme-font:major-bidi;
886        color:#17365D;
887        mso-themecolor:text2;
888        mso-themeshade:191;
889        letter-spacing:.25pt;
890        mso-font-kerning:14.0pt;}
891p.MsoTitleCxSpLast, li.MsoTitleCxSpLast, div.MsoTitleCxSpLast
892        {mso-style-noshow:yes;
893        mso-style-priority:10;
894        mso-style-unhide:no;
895        mso-style-qformat:yes;
896        mso-style-link:"Title Char";
897        mso-style-next:Normal;
898        mso-style-type:export-only;
899        margin-top:0in;
900        margin-right:0in;
901        margin-bottom:15.0pt;
902        margin-left:0in;
903        mso-add-space:auto;
904        mso-pagination:widow-orphan;
905        border:none;
906        mso-border-bottom-alt:solid #4F81BD 1.0pt;
907        mso-border-bottom-themecolor:accent1;
908        padding:0in;
909        mso-padding-alt:0in 0in 4.0pt 0in;
910        font-size:26.0pt;
911        font-family:"Cambria",serif;
912        mso-ascii-font-family:Cambria;
913        mso-ascii-theme-font:major-latin;
914        mso-fareast-font-family:"Times New Roman";
915        mso-fareast-theme-font:major-fareast;
916        mso-hansi-font-family:Cambria;
917        mso-hansi-theme-font:major-latin;
918        mso-bidi-font-family:"Times New Roman";
919        mso-bidi-theme-font:major-bidi;
920        color:#17365D;
921        mso-themecolor:text2;
922        mso-themeshade:191;
923        letter-spacing:.25pt;
924        mso-font-kerning:14.0pt;}
925a:link, span.MsoHyperlink
926        {mso-style-noshow:yes;
927        mso-style-priority:99;
928        color:blue;
929        text-decoration:underline;
930        text-underline:single;}
931a:visited, span.MsoHyperlinkFollowed
932        {mso-style-noshow:yes;
933        mso-style-priority:99;
934        color:purple;
935        text-decoration:underline;
936        text-underline:single;}
937p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap
938        {mso-style-noshow:yes;
939        mso-style-priority:99;
940        mso-style-link:"Document Map Char";
941        margin:0in;
942        margin-bottom:.0001pt;
943        mso-pagination:widow-orphan;
944        font-size:8.0pt;
945        font-family:"Tahoma",sans-serif;
946        mso-fareast-font-family:"Times New Roman";
947        mso-fareast-theme-font:minor-fareast;}
948p
949        {mso-style-noshow:yes;
950        mso-style-priority:99;
951        mso-margin-top-alt:auto;
952        margin-right:0in;
953        mso-margin-bottom-alt:auto;
954        margin-left:0in;
955        mso-pagination:widow-orphan;
956        font-size:12.0pt;
957        font-family:"Times New Roman",serif;
958        mso-fareast-font-family:"Times New Roman";
959        mso-fareast-theme-font:minor-fareast;}
960pre
961        {mso-style-noshow:yes;
962        mso-style-priority:99;
963        mso-style-link:"HTML Preformatted Char";
964        margin:0in;
965        margin-bottom:.0001pt;
966        mso-pagination:widow-orphan;
967        tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt;
968        font-size:10.0pt;
969        font-family:"Courier New";
970        mso-fareast-font-family:"Times New Roman";}
971p.MsoAcetate, li.MsoAcetate, div.MsoAcetate
972        {mso-style-noshow:yes;
973        mso-style-priority:99;
974        mso-style-link:"Balloon Text Char";
975        margin:0in;
976        margin-bottom:.0001pt;
977        mso-pagination:widow-orphan;
978        font-size:8.0pt;
979        font-family:"Tahoma",sans-serif;
980        mso-fareast-font-family:"Times New Roman";
981        mso-fareast-theme-font:minor-fareast;}
982span.MsoPlaceholderText
983        {mso-style-noshow:yes;
984        mso-style-priority:99;
985        mso-style-unhide:no;
986        color:gray;}
987p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing
988        {mso-style-noshow:yes;
989        mso-style-priority:1;
990        mso-style-unhide:no;
991        mso-style-qformat:yes;
992        mso-style-parent:"";
993        margin:0in;
994        margin-bottom:.0001pt;
995        mso-pagination:widow-orphan;
996        font-size:12.0pt;
997        font-family:"Times New Roman",serif;
998        mso-fareast-font-family:"Times New Roman";
999        mso-fareast-theme-font:minor-fareast;}
1000p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph
1001        {mso-style-noshow:yes;
1002        mso-style-priority:34;
1003        mso-style-unhide:no;
1004        mso-style-qformat:yes;
1005        margin-top:0in;
1006        margin-right:0in;
1007        margin-bottom:0in;
1008        margin-left:.5in;
1009        margin-bottom:.0001pt;
1010        mso-add-space:auto;
1011        mso-pagination:widow-orphan;
1012        font-size:12.0pt;
1013        font-family:"Times New Roman",serif;
1014        mso-fareast-font-family:"Times New Roman";
1015        mso-fareast-theme-font:minor-fareast;}
1016p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst
1017        {mso-style-noshow:yes;
1018        mso-style-priority:34;
1019        mso-style-unhide:no;
1020        mso-style-qformat:yes;
1021        mso-style-type:export-only;
1022        margin-top:0in;
1023        margin-right:0in;
1024        margin-bottom:0in;
1025        margin-left:.5in;
1026        margin-bottom:.0001pt;
1027        mso-add-space:auto;
1028        mso-pagination:widow-orphan;
1029        font-size:12.0pt;
1030        font-family:"Times New Roman",serif;
1031        mso-fareast-font-family:"Times New Roman";
1032        mso-fareast-theme-font:minor-fareast;}
1033p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle
1034        {mso-style-noshow:yes;
1035        mso-style-priority:34;
1036        mso-style-unhide:no;
1037        mso-style-qformat:yes;
1038        mso-style-type:export-only;
1039        margin-top:0in;
1040        margin-right:0in;
1041        margin-bottom:0in;
1042        margin-left:.5in;
1043        margin-bottom:.0001pt;
1044        mso-add-space:auto;
1045        mso-pagination:widow-orphan;
1046        font-size:12.0pt;
1047        font-family:"Times New Roman",serif;
1048        mso-fareast-font-family:"Times New Roman";
1049        mso-fareast-theme-font:minor-fareast;}
1050p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast
1051        {mso-style-noshow:yes;
1052        mso-style-priority:34;
1053        mso-style-unhide:no;
1054        mso-style-qformat:yes;
1055        mso-style-type:export-only;
1056        margin-top:0in;
1057        margin-right:0in;
1058        margin-bottom:0in;
1059        margin-left:.5in;
1060        margin-bottom:.0001pt;
1061        mso-add-space:auto;
1062        mso-pagination:widow-orphan;
1063        font-size:12.0pt;
1064        font-family:"Times New Roman",serif;
1065        mso-fareast-font-family:"Times New Roman";
1066        mso-fareast-theme-font:minor-fareast;}
1067span.MsoIntenseReference
1068        {mso-style-priority:32;
1069        mso-style-unhide:no;
1070        mso-style-qformat:yes;
1071        font-variant:small-caps;
1072        color:#C0504D;
1073        mso-themecolor:accent2;
1074        letter-spacing:.25pt;
1075        font-weight:bold;
1076        text-decoration:underline;
1077        text-underline:single;}
1078span.Heading1Char
1079        {mso-style-name:"Heading 1 Char";
1080        mso-style-priority:9;
1081        mso-style-unhide:no;
1082        mso-style-locked:yes;
1083        mso-style-link:"Heading 1";
1084        mso-ansi-font-size:24.0pt;
1085        mso-bidi-font-size:24.0pt;
1086        font-family:"Times New Roman",serif;
1087        mso-ascii-font-family:"Times New Roman";
1088        mso-fareast-font-family:"Times New Roman";
1089        mso-fareast-theme-font:minor-fareast;
1090        mso-hansi-font-family:"Times New Roman";
1091        mso-bidi-font-family:"Times New Roman";
1092        mso-font-kerning:18.0pt;
1093        font-weight:bold;}
1094span.Heading2Char
1095        {mso-style-name:"Heading 2 Char";
1096        mso-style-noshow:yes;
1097        mso-style-priority:9;
1098        mso-style-unhide:no;
1099        mso-style-locked:yes;
1100        mso-style-link:"Heading 2";
1101        mso-ansi-font-size:18.0pt;
1102        mso-bidi-font-size:18.0pt;
1103        font-family:"Times New Roman",serif;
1104        mso-ascii-font-family:"Times New Roman";
1105        mso-fareast-font-family:"Times New Roman";
1106        mso-fareast-theme-font:minor-fareast;
1107        mso-hansi-font-family:"Times New Roman";
1108        mso-bidi-font-family:"Times New Roman";
1109        font-weight:bold;}
1110span.Heading3Char
1111        {mso-style-name:"Heading 3 Char";
1112        mso-style-noshow:yes;
1113        mso-style-priority:9;
1114        mso-style-unhide:no;
1115        mso-style-locked:yes;
1116        mso-style-link:"Heading 3";
1117        mso-ansi-font-size:13.5pt;
1118        mso-bidi-font-size:13.5pt;
1119        font-family:"Times New Roman",serif;
1120        mso-ascii-font-family:"Times New Roman";
1121        mso-fareast-font-family:"Times New Roman";
1122        mso-fareast-theme-font:minor-fareast;
1123        mso-hansi-font-family:"Times New Roman";
1124        mso-bidi-font-family:"Times New Roman";
1125        font-weight:bold;}
1126span.Heading4Char
1127        {mso-style-name:"Heading 4 Char";
1128        mso-style-noshow:yes;
1129        mso-style-priority:9;
1130        mso-style-unhide:no;
1131        mso-style-locked:yes;
1132        mso-style-link:"Heading 4";
1133        mso-ansi-font-size:13.0pt;
1134        mso-bidi-font-size:13.0pt;
1135        font-family:"Cambria",serif;
1136        mso-ascii-font-family:Cambria;
1137        mso-ascii-theme-font:major-latin;
1138        mso-fareast-font-family:"Times New Roman";
1139        mso-fareast-theme-font:major-fareast;
1140        mso-hansi-font-family:Cambria;
1141        mso-hansi-theme-font:major-latin;
1142        mso-bidi-font-family:"Times New Roman";
1143        mso-bidi-theme-font:major-bidi;
1144        color:#4F81BD;
1145        mso-themecolor:accent1;
1146        font-weight:bold;
1147        font-style:italic;}
1148span.Heading5Char
1149        {mso-style-name:"Heading 5 Char";
1150        mso-style-noshow:yes;
1151        mso-style-priority:9;
1152        mso-style-unhide:no;
1153        mso-style-locked:yes;
1154        mso-style-link:"Heading 5";
1155        mso-ansi-font-size:12.0pt;
1156        mso-bidi-font-size:12.0pt;
1157        font-family:"Times New Roman",serif;
1158        mso-ascii-font-family:"Times New Roman";
1159        mso-fareast-font-family:"Times New Roman";
1160        mso-fareast-theme-font:minor-fareast;
1161        mso-hansi-font-family:"Times New Roman";
1162        mso-bidi-font-family:"Times New Roman";
1163        color:#4F4FFF;
1164        font-weight:bold;}
1165span.HTMLPreformattedChar
1166        {mso-style-name:"HTML Preformatted Char";
1167        mso-style-noshow:yes;
1168        mso-style-priority:99;
1169        mso-style-unhide:no;
1170        mso-style-locked:yes;
1171        mso-style-link:"HTML Preformatted";
1172        font-family:"Courier New";
1173        mso-ascii-font-family:"Courier New";
1174        mso-fareast-font-family:"Times New Roman";
1175        mso-hansi-font-family:"Courier New";
1176        mso-bidi-font-family:"Courier New";}
1177p.msonormal0, li.msonormal0, div.msonormal0
1178        {mso-style-name:msonormal;
1179        mso-style-noshow:yes;
1180        mso-style-priority:99;
1181        mso-style-unhide:no;
1182        mso-margin-top-alt:auto;
1183        margin-right:0in;
1184        mso-margin-bottom-alt:auto;
1185        margin-left:0in;
1186        mso-pagination:widow-orphan;
1187        font-size:12.0pt;
1188        font-family:"Times New Roman",serif;
1189        mso-fareast-font-family:"Times New Roman";
1190        mso-fareast-theme-font:minor-fareast;}
1191span.TitleChar
1192        {mso-style-name:"Title Char";
1193        mso-style-priority:10;
1194        mso-style-unhide:no;
1195        mso-style-locked:yes;
1196        mso-style-link:Title;
1197        mso-ansi-font-size:26.0pt;
1198        mso-bidi-font-size:26.0pt;
1199        font-family:"Cambria",serif;
1200        mso-ascii-font-family:Cambria;
1201        mso-ascii-theme-font:major-latin;
1202        mso-fareast-font-family:"Times New Roman";
1203        mso-fareast-theme-font:major-fareast;
1204        mso-hansi-font-family:Cambria;
1205        mso-hansi-theme-font:major-latin;
1206        mso-bidi-font-family:"Times New Roman";
1207        mso-bidi-theme-font:major-bidi;
1208        color:#17365D;
1209        mso-themecolor:text2;
1210        mso-themeshade:191;
1211        letter-spacing:.25pt;
1212        mso-font-kerning:14.0pt;}
1213span.DocumentMapChar
1214        {mso-style-name:"Document Map Char";
1215        mso-style-noshow:yes;
1216        mso-style-priority:99;
1217        mso-style-unhide:no;
1218        mso-style-locked:yes;
1219        mso-style-link:"Document Map";
1220        mso-ansi-font-size:8.0pt;
1221        mso-bidi-font-size:8.0pt;
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1303</head>
1304
1305<body lang=EN-US link=blue vlink=purple style='tab-interval:.5in'>
1306
1307<div class=WordSection1>
1308
1309<h1>Strain fitting of 2D data in GSAS-II</h1>
1310
1311<p class=MsoNormal>For this tutorial, data were collected with a MAR2300 area
1312detector at APS 1-ID-C with a wavelength 0.12398 Å (100<span style='font-family:
1313Symbol'>m</span>m diameter beam) from a 1.5mm square hot rolled steel test specimen;
1314the front surface has been dusted with some CeO<sub>2</sub> to aid in
1315calibration. Three images are used here; one is with no load on the sample and
1316the other two are with the sample under tension along the y-axis (vertical).
1317The loading will distort the steel (ferrite &amp; austenite) diffraction rings
1318and our purpose here is to characterize this distortion via a strain model by
1319B. B. He &amp; K. L. Smith (Adv. in X-ray Anal. 41, 501, 1997). Note that menu
1320entries are listed in <b style='mso-bidi-font-weight:normal'><span
1321style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1322mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>bold face</span></b>
1323below as <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1324mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1325minor-latin'>Help/About GSAS-II</span></b>, which lists first the name of the
1326menu (here <b style='mso-bidi-font-weight:normal'><span style='font-family:
1327"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1328minor-latin;mso-bidi-theme-font:minor-latin'>Help</span></b>) and second the
1329name of the entry in the menu (here <b style='mso-bidi-font-weight:normal'><span
1330style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1331mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).</p>
1332
1333<h2>Step 1: Start GSAS-II and read the images</h2>
1334
1335<p class=MsoNormal>Use the <b style='mso-bidi-font-weight:normal'><span
1336style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1337mso-hansi-theme-font:minor-latin'>Data/Read image data</span></b> menu item to
1338read the data file into a new GSAS-II project. A file selection dialog will be
1339shown; its appearance will depend on your OS. Change the search directory to <b
1340style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1341mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1342minor-latin'>2Dstrain/data</span></b> and then select the files <b
1343style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1344mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1345minor-latin'>nx09_strain_001.mar2300<span class=GramE>, <span style='font-family:
1346"Times New Roman",serif;font-weight:normal'><span
1347style='mso-spacerun:yes'> </span></span>nx09</span>_strain_006.mar2300 </span></b>and
1348<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1349mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>nx09_strain_011.mar2300</span></b>
1350and press <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1351mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1352minor-latin'>Open</span></b>.<span style='mso-no-proof:yes'> Select the 1<sup>st</sup>
1353image (001) from the GSAS-II data tree and select </span><b style='mso-bidi-font-weight:
1354normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1355minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Image Controls</span></b><span
1356style='mso-no-proof:yes'>; adjust the </span><b style='mso-bidi-font-weight:
1357normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1358minor-latin;mso-hansi-theme-font:minor-latin;mso-no-proof:yes'>Max intensity</span></b><span
1359style='mso-no-proof:yes'> so that the CeO2 rings are visible (~1500 will
1360suffice or 99%). You should see:<o:p></o:p></span></p>
1361
1362<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype
1363 id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t"
1364 path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f">
1365 <v:stroke joinstyle="miter"/>
1366 <v:formulas>
1367  <v:f eqn="if lineDrawn pixelLineWidth 0"/>
1368  <v:f eqn="sum @0 1 0"/>
1369  <v:f eqn="sum 0 0 @1"/>
1370  <v:f eqn="prod @2 1 2"/>
1371  <v:f eqn="prod @3 21600 pixelWidth"/>
1372  <v:f eqn="prod @3 21600 pixelHeight"/>
1373  <v:f eqn="sum @0 0 1"/>
1374  <v:f eqn="prod @6 1 2"/>
1375  <v:f eqn="prod @7 21600 pixelWidth"/>
1376  <v:f eqn="sum @8 21600 0"/>
1377  <v:f eqn="prod @7 21600 pixelHeight"/>
1378  <v:f eqn="sum @10 21600 0"/>
1379 </v:formulas>
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1382</v:shapetype><v:shape id="Picture_x0020_22" o:spid="_x0000_i1046" type="#_x0000_t75"
1383 style='width:468pt;height:401.25pt;visibility:visible;mso-wrap-style:square'>
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1385  o:title=""/>
1386</v:shape><![endif]--><![if !vml]><img width=624 height=535
1387src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image001.png"
1388v:shapes="Picture_x0020_22"><![endif]><o:p></o:p></span></p>
1389
1390<p class=MsoNormal><span style='mso-no-proof:yes'>For the image and <o:p></o:p></span></p>
1391
1392<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1393 id="Picture_x0020_23" o:spid="_x0000_i1045" type="#_x0000_t75" style='width:468pt;
1394 height:225.75pt;visibility:visible;mso-wrap-style:square'>
1395 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image005.png"
1396  o:title=""/>
1397</v:shape><![endif]--><![if !vml]><img width=624 height=301
1398src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image003.png"
1399v:shapes="Picture_x0020_23"><![endif]><o:p></o:p></span></p>
1400
1401<p class=MsoNormal><span style='mso-no-proof:yes'>for the controls.<o:p></o:p></span></p>
1402
1403<h2>Step 2: Calibration of the detector position</h2>
1404
1405<p class=MsoNormal>This image is a superposition of three diffraction patterns;
1406CeO<sub>2</sub> calibrant, ferrite (BCC iron) and austenite (FCC iron).
1407Consequently the calibration needs to be done with some care; the steps are as
1408follows:</p>
1409
1410<p class=MsoNormal>Set the wavelength to <b style='mso-bidi-font-weight:normal'><span
1411style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1412mso-hansi-theme-font:minor-latin'>0.12398</span></b></p>
1413
1414<p class=MsoNormal>Set the calibrant to <b style='mso-bidi-font-weight:normal'><span
1415style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1416mso-hansi-theme-font:minor-latin'>CeO2 SRM674b<o:p></o:p></span></b></p>
1417
1418<p class=MsoNormal>Set <b style='mso-bidi-font-weight:normal'><span
1419style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1420mso-hansi-theme-font:minor-latin'>Min <span class=SpellE>calib</span> d-spacing</span></b>
1421to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1422mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1.09</span></b>;
1423this avoids picking a CeO<sub>2</sub> ring that overlaps one of the steel ones.</p>
1424
1425<p class=MsoNormal>Pick <b style='mso-bidi-font-weight:normal'><span
1426style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1427mso-hansi-theme-font:minor-latin'>Show ring picks?</span></b> check box</p>
1428
1429<p class=MsoNormal>Set <b style='mso-bidi-font-weight:normal'><span
1430style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1431mso-hansi-theme-font:minor-latin'>Pixel search range</span></b> to <b
1432style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1433mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>5</span></b>;
1434the rings are fairly widely separated will little chance for overlap.</p>
1435
1436<p class=MsoNormal>Use <b style='mso-bidi-font-weight:normal'><span
1437style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1438mso-hansi-theme-font:minor-latin'>Calibration/Calibrate</span></b>, select 5
1439points on the inner CeO<sub>2</sub> ring with left mouse button and start
1440calibration with right mouse button. The result should be something like</p>
1441
1442<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1443 id="Picture_x0020_24" o:spid="_x0000_i1044" type="#_x0000_t75" style='width:468pt;
1444 height:401.25pt;visibility:visible;mso-wrap-style:square'>
1445 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image021.png"
1446  o:title=""/>
1447</v:shape><![endif]--><![if !vml]><img width=624 height=535
1448src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image006.png"
1449v:shapes="Picture_x0020_24"><![endif]></span></p>
1450
1451<p class=MsoNormal>I’ve zoomed in to show that the CeO2 rings are well fitted
1452and don’t overlap any of the more intense steel ones. The calibration results
1453show on the data window</p>
1454
1455<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
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1457 height:321pt;visibility:visible;mso-wrap-style:square'>
1458 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image028.png"
1459  o:title=""/>
1460</v:shape><![endif]--><![if !vml]><img width=624 height=428
1461src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image007.png"
1462v:shapes="Picture_x0020_25"><![endif]></span><span
1463style='mso-spacerun:yes'> </span></p>
1464
1465<p class=MsoNormal>and the console</p>
1466
1467<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1468 id="Picture_x0020_5" o:spid="_x0000_i1042" type="#_x0000_t75" style='width:461.25pt;
1469 height:122.25pt;visibility:visible;mso-wrap-style:square'>
1470 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image030.png"
1471  o:title=""/>
1472</v:shape><![endif]--><![if !vml]><img width=615 height=163
1473src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image030.png"
1474v:shapes="Picture_x0020_5"><![endif]></span></p>
1475
1476<p class=MsoNormal>You should now copy these results to the other images. Use <span
1477class=SpellE><b style='mso-bidi-font-weight:normal'><span style='font-family:
1478"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1479minor-latin'>Parms</span></b></span><b style='mso-bidi-font-weight:normal'><span
1480style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1481mso-hansi-theme-font:minor-latin'>/Copy controls</span></b>; a popup dialog
1482will appear; select <b style='mso-bidi-font-weight:normal'><span
1483style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1484mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Set </span></b><span
1485class=GramE><b style='mso-bidi-font-weight:normal'><span style='font-family:
1486"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1487minor-latin'>All</span></b></span> and <b style='mso-bidi-font-weight:normal'><span
1488style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1489mso-hansi-theme-font:minor-latin'>OK</span></b>.</p>
1490
1491<h2 style='tab-stops:2.3in'>Step 3: Fitting unstrained steel</h2>
1492
1493<p class=MsoNormal>In this step you will select the diffraction rings to be
1494analyzed for strain; it is best to pick a few CeO<sub>2</sub> ones as well to
1495confirm that the sample position does not shift during loading. Select the
1496first image (001) and the <b style='mso-bidi-font-weight:normal'><span
1497style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1498mso-hansi-theme-font:minor-latin'>Stress/Strain</span></b> tree item. An empty
1499plot (“Strain”) will appear and the initial Stress/Strain data window</p>
1500
1501<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1502 id="Picture_x0020_34" o:spid="_x0000_i1041" type="#_x0000_t75" style='width:468pt;
1503 height:237pt;visibility:visible;mso-wrap-style:square'>
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1505  o:title=""/>
1506</v:shape><![endif]--><![if !vml]><img width=624 height=316
1507src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image008.png"
1508v:shapes="Picture_x0020_34"><![endif]></span><span
1509style='mso-spacerun:yes'> </span></p>
1510
1511<p class=MsoNormal>Change <b style='mso-bidi-font-weight:normal'><span
1512style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1513mso-hansi-theme-font:minor-latin'>Sample delta-z</span></b> to <b
1514style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1515mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-0.75</span></b>
1516since center of the steel sample is that much closer to the detector than the
1517CeO<sub>2</sub> calibrant. Then select <b style='mso-bidi-font-weight:normal'><span
1518style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1519mso-hansi-theme-font:minor-latin'>2D Powder Image</span></b> and follow the
1520instruction to add a ring; press <span class=GramE><b style='mso-bidi-font-weight:
1521normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1522minor-latin;mso-hansi-theme-font:minor-latin'>a</span></b> and</span> use the
1523mouse left button to select a ring. Do as many as you like but be sure to
1524select some CeO<sub>2</sub> rings as well; it is useful to zoom in to help with
1525the selection, but make sure zoom buttons are off for the selection. You can
1526control the image display with the <b style='mso-bidi-font-weight:normal'><span
1527style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1528mso-hansi-theme-font:minor-latin'>Image Controls</span></b>. Each time you pick
1529a ring, GSAS-II show the <b style='mso-bidi-font-weight:normal'><span
1530style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1531mso-hansi-theme-font:minor-latin'>2D Powder Image</span></b> zoomed in where
1532you were looking before your selection. I chose 12 rings. Do <b
1533style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1534mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1535minor-latin'>Operations/Fit stress/strain;</span></b> the Strain plot is
1536updated to show</p>
1537
1538<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1539 id="Picture_x0020_35" o:spid="_x0000_i1040" type="#_x0000_t75" style='width:468pt;
1540 height:401.25pt;visibility:visible;mso-wrap-style:square'>
1541 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image034.png"
1542  o:title=""/>
1543</v:shape><![endif]--><![if !vml]><img width=624 height=535
1544src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image010.png"
1545v:shapes="Picture_x0020_35"><![endif]></span></p>
1546
1547<p class=MsoNormal>Notice that each ring is plotted in different colors (they
1548may be somewhat mixed for the two lines ~2Å! We will fix this next). The 2D
1549Powder Image shows the picks as well</p>
1550
1551<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1552 id="Picture_x0020_36" o:spid="_x0000_i1039" type="#_x0000_t75" style='width:468pt;
1553 height:401.25pt;visibility:visible;mso-wrap-style:square'>
1554 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image038.png"
1555  o:title=""/>
1556</v:shape><![endif]--><![if !vml]><img width=624 height=535
1557src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image011.png"
1558v:shapes="Picture_x0020_36"><![endif]></span></p>
1559
1560<p class=MsoNormal>And the rings are listed on the <b style='mso-bidi-font-weight:
1561normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1562minor-latin;mso-hansi-theme-font:minor-latin'>Stress/Strain</span></b> data window;
1563a scroll bar allows easy access to all the entries.</p>
1564
1565<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1566 id="Picture_x0020_37" o:spid="_x0000_i1038" type="#_x0000_t75" style='width:468pt;
1567 height:300.75pt;visibility:visible;mso-wrap-style:square'>
1568 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image042.png"
1569  o:title=""/>
1570</v:shape><![endif]--><![if !vml]><img width=624 height=401
1571src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image012.png"
1572v:shapes="Picture_x0020_37"><![endif]></span></p>
1573
1574<p class=MsoNormal>If necessary, we can now fix the mixing of the two 2Å lines;
1575change the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1576"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1577minor-latin'>Pixel search range</span></b> to <b style='mso-bidi-font-weight:
1578normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1579minor-latin;mso-hansi-theme-font:minor-latin'>5</span></b> for both. Do <b
1580style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1581mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1582minor-latin'>Operations/Fit Stress <span class=GramE>Strain.</span></span></b>
1583After you are done the <b style='mso-bidi-font-weight:normal'><span
1584style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1585mso-hansi-theme-font:minor-latin'>Strain</span></b> plot should look like</p>
1586
1587<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1588 id="Picture_x0020_38" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:468pt;
1589 height:401.25pt;visibility:visible;mso-wrap-style:square'>
1590 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image046.png"
1591  o:title=""/>
1592</v:shape><![endif]--><![if !vml]><img width=624 height=535
1593src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image013.png"
1594v:shapes="Picture_x0020_38"><![endif]></span></p>
1595
1596<p class=MsoNormal>We are now ready for the first strain fit; do <b
1597style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1598mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Fit
1599stress/strain</span></b>. Each ring will be fitted to the three strain tensor
1600elements (&#949;<sub>11</sub>, &#949;<sub>12</sub> &amp; &#949;<sub>22</sub>)
1601that can be determined from a single 2D diffraction ring. The resulting Strain
1602plot now shows curves calculated from the fitted tensor elements; these are
1603very nearly straight lines as expected from an unloaded sample.<span
1604style='mso-spacerun:yes'>  </span>In particular the austenite 111 line (~2.08Å)
1605is much flatter than the ferrite 200 line (~2.03Å); this reflects the sample
1606history (hot rolled steel). The tensor elements with <span class=SpellE>esds</span>
1607are shown on the console and in the data window</p>
1608
1609<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1610 id="Picture_x0020_39" o:spid="_x0000_i1036" type="#_x0000_t75" style='width:468pt;
1611 height:300.75pt;visibility:visible;mso-wrap-style:square'>
1612 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image048.png"
1613  o:title=""/>
1614</v:shape><![endif]--><![if !vml]><img width=624 height=401
1615src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image014.png"
1616v:shapes="Picture_x0020_39"><![endif]></span><span
1617style='mso-spacerun:yes'> </span></p>
1618
1619<p class=MsoNormal>The <b style='mso-bidi-font-weight:normal'><span
1620style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1621mso-hansi-theme-font:minor-latin'>d-zero <span class=SpellE>ave</span></span></b>
1622is the average d-spacing around each ring; this can be used as the reference
1623d-spacing. If <b style='mso-bidi-font-weight:normal'><span style='font-family:
1624"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1625minor-latin;mso-bidi-theme-font:minor-latin'>Poisson <span class=SpellE>ave</span></span></b>
1626is checked then <b style='mso-bidi-font-weight:normal'><span style='font-family:
1627"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1628minor-latin;mso-bidi-theme-font:minor-latin'>d-zero <span class=SpellE>ave</span></span></b>
1629is determined from <span style='mso-spacerun:yes'> </span></p>
1630
1631<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1632
1633<p class=MsoNormal>If <b style='mso-bidi-font-weight:normal'><span
1634style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1635mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>e<sub>11</sub></span></b>
1636&lt; <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1637mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1638minor-latin'>e<sub>22</sub></span></b>: <b style='mso-bidi-font-weight:normal'><span
1639style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1640mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>d-zero <span
1641class=SpellE>ave</span></span></b> <b style='mso-bidi-font-weight:normal'><span
1642style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1643mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>= <span
1644class=SpellE>d<sub>min</sub></span>-(<span class=SpellE>d<sub>max</sub>-d<sub>min</sub></span>)/4</span></b>;
1645else: <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1646mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1647minor-latin'>d-zero <span class=SpellE>ave</span> = dmin+3*(<span class=SpellE>dmax-dmin</span>)<o:p></o:p></span></b></p>
1648
1649<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
1650style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1651mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'><o:p>&nbsp;</o:p></span></b></p>
1652
1653<p class=MsoNormal>Where <span class=SpellE><b style='mso-bidi-font-weight:
1654normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1655minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>d<sub>min</sub><span
1656class=GramE>,d<sub>max</sub></span></span></b></span><b style='mso-bidi-font-weight:
1657normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1658minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'> </span></b>are
1659the minimum and maximum d-<span class=SpellE>spacings</span> for a given
1660diffraction ring, thus selecting the place where the diffraction ring under
1661load would give a strain free value.</p>
1662
1663<p class=MsoNormal>Each d-zero value for this no load sample can be set to this
1664value; this will suppress any residual stress offset. To update all the d-zero
1665values to the calculated ones do <b style='mso-bidi-font-weight:normal'><span
1666style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1667mso-hansi-theme-font:minor-latin'>Operations/Update d-zero</span></b> then
1668repeat <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1669mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Fit
1670stress/strain</span></b>. Repeat as needed to make <b style='mso-bidi-font-weight:
1671normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1672minor-latin;mso-hansi-theme-font:minor-latin'>d-zero</span></b> match <b
1673style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1674mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>d-zero <span
1675class=SpellE>ave</span></span></b> for all lines so that <b style='mso-bidi-font-weight:
1676normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1677minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>h-<span
1678class=SpellE>mustrain</span></span></b> (= <b style='mso-bidi-font-weight:normal'><span
1679style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1680mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>d-zero/d-zero
1681<span class=SpellE>ave</span></span></b> -1) is small (less than ~±250). I got
1682for the no load sample</p>
1683
1684<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1685 id="Picture_x0020_40" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:468pt;
1686 height:221.25pt;visibility:visible;mso-wrap-style:square'>
1687 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image050.png"
1688  o:title=""/>
1689</v:shape><![endif]--><![if !vml]><img width=624 height=295
1690src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image015.png"
1691v:shapes="Picture_x0020_40"><![endif]></span></p>
1692
1693<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
1694style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1695mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>Ivar</span></b>
1696is the variance in the normalized ring intensity; <span class=GramE>if <span
1697style='mso-spacerun:yes'> </span>&gt;</span>0 the sample is textured in some
1698way. Finally you want this set of d-zero values to be applied to the images
1699from the loaded sample; do <b style='mso-bidi-font-weight:normal'><span
1700style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1701mso-hansi-theme-font:minor-latin'>Operations/Copy stress/strain</span></b> to
1702apply them to the other images.</p>
1703
1704<h2 style='tab-stops:2.3in'>Step 4: Sequential fitting of steel under load</h2>
1705
1706<p class=MsoNormal>For the result of the sequential fitting to make sense, we
1707need to enter the applied load for each image. Unfortunately, this must be done
1708by hand here because the load value is not in the image header. The loads are:
1709001: - 2.17425, 006: 527.917 and 011: 1004.41 all in <span class=SpellE>newtons</span>
1710(N). Each needs to be divided by the cross section area (2.25mm<sup>2</sup>) of
1711the sample; GSAS-II will do this bit of math for you, and this gives the values
1712in MPa. For image <b style='mso-bidi-font-weight:normal'><span
1713style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1714mso-hansi-theme-font:minor-latin'>001</span></b> enter <b style='mso-bidi-font-weight:
1715normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1716minor-latin;mso-hansi-theme-font:minor-latin'>-2.17425/2.25</span></b> in the <b
1717style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1718mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sample load
1719(MPa)</span></b> box, <b style='mso-bidi-font-weight:normal'><span
1720style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1721mso-hansi-theme-font:minor-latin'>527.917/2.25</span></b> for image <b
1722style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1723mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>006</span></b>
1724and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1725mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>1004.41/2.25</span></b>
1726for image <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1727mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>011</span></b>.
1728When done the data window for image 011 should look like</p>
1729
1730<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1731 id="Picture_x0020_41" o:spid="_x0000_i1034" type="#_x0000_t75" style='width:468pt;
1732 height:221.25pt;visibility:visible;mso-wrap-style:square'>
1733 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image052.png"
1734  o:title=""/>
1735</v:shape><![endif]--><![if !vml]><img width=624 height=295
1736src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image016.png"
1737v:shapes="Picture_x0020_41"><![endif]></span></p>
1738
1739<p class=MsoNormal>Note that if the beam line software has prepared the
1740appropriate file containing this information, it could be loaded via the <b
1741style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1742mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/Load
1743sample data</span></b> menu item.</p>
1744
1745<p class=MsoNormal>Next, we do the sequential refinement. Do <b
1746style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1747mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Operations/All
1748image fit</span></b> from the <b style='mso-bidi-font-weight:normal'><span
1749style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1750mso-hansi-theme-font:minor-latin'>Stress/Strain</span></b> data window menu
1751from any of the images. A popup window will show the selection of images</p>
1752
1753<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1754 id="Picture_x0020_14" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:204.75pt;
1755 height:251.25pt;visibility:visible;mso-wrap-style:square'>
1756 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image024.png"
1757  o:title=""/>
1758</v:shape><![endif]--><![if !vml]><img width=273 height=335
1759src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image024.png"
1760v:shapes="Picture_x0020_14"><![endif]></span></p>
1761
1762<p class=MsoNormal>Press <b style='mso-bidi-font-weight:normal'><span
1763style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1764mso-hansi-theme-font:minor-latin'>Set <span class=GramE>All</span></span></b>, all
1765boxes will be checked showing selection of the data sets. This also allows you
1766to instruct the sequential refinement to start at the last data set and proceed
1767backwards through them (<b style='mso-bidi-font-weight:normal'><span
1768style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1769mso-hansi-theme-font:minor-latin'>Reverse order</span></b>). It also allows you
1770to instruct the sequential refinement to use the current parameters as starting
1771values for the next data set. This works in either direction and facilitates
1772the initial sequential refinements. Select just <b style='mso-bidi-font-weight:
1773normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1774minor-latin;mso-hansi-theme-font:minor-latin'>Copy to next</span></b> and press
1775<b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1776mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b>;
1777the sequential refinement will proceed very rapidly displaying results for each
1778data set on the console and finally ending by displaying the <b
1779style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1780mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sequential strain
1781fit result.<o:p></o:p></span></b></p>
1782
1783<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1784 id="Picture_x0020_42" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:371.25pt;
1785 height:442.5pt;visibility:visible;mso-wrap-style:square'>
1786 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image054.png"
1787  o:title=""/>
1788</v:shape><![endif]--><![if !vml]><img width=495 height=590
1789src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image054.png"
1790v:shapes="Picture_x0020_42"><![endif]></span></p>
1791
1792<p class=MsoNormal>I only show the bottom of the listing. The data window shows
1793the results of the sequential fit.</p>
1794
1795<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1796 id="Picture_x0020_43" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:468pt;
1797 height:206.25pt;visibility:visible;mso-wrap-style:square'>
1798 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image055.png"
1799  o:title=""/>
1800</v:shape><![endif]--><![if !vml]><img width=624 height=275
1801src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image017.png"
1802v:shapes="Picture_x0020_43"><![endif]></span></p>
1803
1804<p class=MsoNormal>This table is the results of the sequential fit to the three
1805images. There are columns for each parameter. If you double click on a column
1806heading (try a steel e11 or e22 – I selected <b style='mso-bidi-font-weight:
1807normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1808minor-latin;mso-hansi-theme-font:minor-latin'>1<span class=GramE>;e22</span></span></b>
1809from my list). The plot shows the variation of this parameter with image
1810sequence; <span class=GramE>press ‘<b style='mso-bidi-font-weight:normal'><span
1811style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1812mso-hansi-theme-font:minor-latin'>s</span></b>’</span> and select <b
1813style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1814mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Sample load</span></b>
1815and the plot will show (you’ll have to pick something else &amp; then back to <b
1816style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1817mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:
1818minor-latin'>1:e22</span></b>).</p>
1819
1820<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1821 id="Picture_x0020_44" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:468pt;
1822 height:401.25pt;visibility:visible;mso-wrap-style:square'>
1823 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image057.png"
1824  o:title=""/>
1825</v:shape><![endif]--><![if !vml]><img width=624 height=535
1826src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image018.png"
1827v:shapes="Picture_x0020_44"><![endif]></span></p>
1828
1829<p class=MsoNormal>We can next fit this to a straight line. Select <b
1830style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1831mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Parametric
1832fit/Add equation</span></b>, select a variable (<b style='mso-bidi-font-weight:
1833normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1834minor-latin;mso-hansi-theme-font:minor-latin'>Global</span></b>) in the 1<sup>st</sup>
1835pull down box (I chose <b style='mso-bidi-font-weight:normal'><span
1836style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1837mso-hansi-theme-font:minor-latin'>1<span class=GramE>;e22</span></span></b>)
1838and enter <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1839mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>m*<span
1840class=SpellE>x+b</span></span></b> in the equation box; the frame will change
1841to give selections for <b style='mso-bidi-font-weight:normal'><span
1842style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1843mso-hansi-theme-font:minor-latin'>m</span></b>, <b style='mso-bidi-font-weight:
1844normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1845minor-latin;mso-hansi-theme-font:minor-latin'>x</span></b> &amp; <b
1846style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1847mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>b</span></b>.
1848Use <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1849mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Free</span></b>
1850for <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1851mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>m</span></b>
1852&amp; <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1853mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>b</span></b>
1854and <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1855mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Global/Sample
1856load</span></b> (at the bottom of list) for <b style='mso-bidi-font-weight:
1857normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1858minor-latin;mso-hansi-theme-font:minor-latin'>x</span></b>. Then press <b
1859style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1860mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Fit</span></b>.
1861The <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1862mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Expression
1863Editor</span></b> window should look like; press <b style='mso-bidi-font-weight:
1864normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1865minor-latin;mso-hansi-theme-font:minor-latin'>OK</span></b> to exit this
1866window.</p>
1867
1868<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1869 id="Picture_x0020_45" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:465pt;
1870 height:255pt;visibility:visible;mso-wrap-style:square'>
1871 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image059.png"
1872  o:title=""/>
1873</v:shape><![endif]--><![if !vml]><img width=620 height=340
1874src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image059.png"
1875v:shapes="Picture_x0020_45"><![endif]></span></p>
1876
1877<p class=MsoNormal>And the console shows the parameters with <span
1878class=SpellE>esds</span></p>
1879
1880<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1881 id="Picture_x0020_46" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:450.75pt;
1882 height:128.25pt;visibility:visible;mso-wrap-style:square'>
1883 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image060.png"
1884  o:title=""/>
1885</v:shape><![endif]--><![if !vml]><img width=601 height=171
1886src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image060.png"
1887v:shapes="Picture_x0020_46"><![endif]></span></p>
1888
1889<p class=MsoNormal>The plot will show the best fit line</p>
1890
1891<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1892 id="Picture_x0020_27" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:468pt;
1893 height:401.25pt;visibility:visible;mso-wrap-style:square'>
1894 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image061.png"
1895  o:title=""/>
1896</v:shape><![endif]--><![if !vml]><img width=624 height=535
1897src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image019.png"
1898v:shapes="Picture_x0020_27"><![endif]></span></p>
1899
1900<p class=MsoNormal>You can explore other features of this facility; pick more
1901than one column (single click on the label) and the <span class=GramE><b
1902style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1903mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Selected</span></b></span><b
1904style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1905mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'> cols/Plot
1906selected</span></b> menu item to plot them together. </p>
1907
1908<p class=MsoNormal>To see the effect of stress on one diffraction line, select
1909the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1910mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>Strain</span></b>
1911plot and zoom in on one line (I zoomed in on just one line; ferrite 211) from
1912image 011.</p>
1913
1914<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1915 id="Picture_x0020_28" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:468pt;
1916 height:401.25pt;visibility:visible;mso-wrap-style:square'>
1917 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image063.png"
1918  o:title=""/>
1919</v:shape><![endif]--><![if !vml]><img width=624 height=535
1920src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image020.png"
1921v:shapes="Picture_x0020_28"><![endif]></span></p>
1922
1923<p class=MsoNormal>The dashed line gives the d-zero position. When you look at
1924the other lines, you should notice that the ones at ca. 3.13Å, 1.63Å, and 1.24Å
1925remain straight lines; these are from CeO<sub>2</sub> and should be unchanged
1926under load.</p>
1927
1928<p class=MsoNormal>Finally we can investigate the appearance of texture in the
1929ring intensities, do Operations/Plot intensity distribution. A new plot
1930appears; the ‘u’ key will change the curve offsets to get</p>
1931
1932<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1933 id="Picture_x0020_47" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:468pt;
1934 height:401.25pt;visibility:visible;mso-wrap-style:square'>
1935 <v:imagedata src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image022.png"
1936  o:title=""/>
1937</v:shape><![endif]--><![if !vml]><img width=624 height=535
1938src="Strain%20fitting%20of%202D%20data%20in%20GSAS-II_files/image023.png"
1939v:shapes="Picture_x0020_47"><![endif]></span></p>
1940
1941<p class=MsoNormal><o:p>&nbsp;</o:p></p>
1942
1943<p class=MsoNormal>The CeO<sub>2</sub> lines are straight (MRD=1.0) while lines
1944from the two steel phases show the effect of texture but little graininess.</p>
1945
1946<p class=MsoNormal>Again you could save the project with <b style='mso-bidi-font-weight:
1947normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1948minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>File/Save
1949project</span></b> on the main <b style='mso-bidi-font-weight:normal'><span
1950style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1951mso-hansi-theme-font:minor-latin;mso-bidi-theme-font:minor-latin'>GSAS-II data
1952tree</span></b> menu <span class=GramE>although</span> it is not needed for any
1953further tutorials. The strain results from each image can be exported as a
1954comma delimited set of values which can easily be read by Microsoft Excel and
1955other spread sheet programs; see <b style='mso-bidi-font-weight:normal'><span
1956style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1957mso-hansi-theme-font:minor-latin'>Export/Image data as/Strain CSV file</span></b>.</p>
1958
1959</div>
1960
1961</body>
1962
1963</html>
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