source: Tutorials/2DCalibration/Calibration of an area detector in GSAS.htm @ 2349

Last change on this file since 2349 was 1732, checked in by vondreele, 8 years ago

update 2D calibration
  • Property svn:mime-type set to text/html
File size: 76.4 KB
Line 
1<html xmlns:v="urn:schemas-microsoft-com:vml"
2xmlns:o="urn:schemas-microsoft-com:office:office"
3xmlns:w="urn:schemas-microsoft-com:office:word"
4xmlns:m="http://schemas.microsoft.com/office/2004/12/omml"
5xmlns="http://www.w3.org/TR/REC-html40">
6
7<head>
8<meta http-equiv=Content-Type content="text/html; charset=windows-1252">
9<meta name=ProgId content=Word.Document>
10<meta name=Generator content="Microsoft Word 15">
11<meta name=Originator content="Microsoft Word 15">
12<link rel=File-List
13href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/filelist.xml">
14<link rel=Edit-Time-Data
15href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/editdata.mso">
16<!--[if !mso]>
17<style>
18v\:* {behavior:url(#default#VML);}
19o\:* {behavior:url(#default#VML);}
20w\:* {behavior:url(#default#VML);}
21.shape {behavior:url(#default#VML);}
22</style>
23<![endif]--><!--[if gte mso 9]><xml>
24 <o:DocumentProperties>
25  <o:Author>Von Dreele</o:Author>
26  <o:LastAuthor>Von Dreele</o:LastAuthor>
27  <o:Revision>4</o:Revision>
28  <o:TotalTime>250</o:TotalTime>
29  <o:Created>2014-07-21T14:30:00Z</o:Created>
30  <o:LastSaved>2015-03-17T21:04:00Z</o:LastSaved>
31  <o:Pages>1</o:Pages>
32  <o:Words>1117</o:Words>
33  <o:Characters>6373</o:Characters>
34  <o:Company>Argonne National Laboratory</o:Company>
35  <o:Lines>53</o:Lines>
36  <o:Paragraphs>14</o:Paragraphs>
37  <o:CharactersWithSpaces>7476</o:CharactersWithSpaces>
38  <o:Version>15.00</o:Version>
39 </o:DocumentProperties>
40 <o:OfficeDocumentSettings>
41  <o:AllowPNG/>
42 </o:OfficeDocumentSettings>
43</xml><![endif]-->
44<link rel=themeData
45href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/themedata.thmx">
46<link rel=colorSchemeMapping
47href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/colorschememapping.xml">
48<!--[if gte mso 9]><xml>
49 <w:WordDocument>
50  <w:SpellingState>Clean</w:SpellingState>
51  <w:GrammarState>Clean</w:GrammarState>
52  <w:TrackMoves>false</w:TrackMoves>
53  <w:TrackFormatting/>
54  <w:PunctuationKerning/>
55  <w:ValidateAgainstSchemas/>
56  <w:SaveIfXMLInvalid>false</w:SaveIfXMLInvalid>
57  <w:IgnoreMixedContent>false</w:IgnoreMixedContent>
58  <w:AlwaysShowPlaceholderText>false</w:AlwaysShowPlaceholderText>
59  <w:DoNotPromoteQF/>
60  <w:LidThemeOther>EN-US</w:LidThemeOther>
61  <w:LidThemeAsian>X-NONE</w:LidThemeAsian>
62  <w:LidThemeComplexScript>X-NONE</w:LidThemeComplexScript>
63  <w:Compatibility>
64   <w:BreakWrappedTables/>
65   <w:SnapToGridInCell/>
66   <w:WrapTextWithPunct/>
67   <w:UseAsianBreakRules/>
68   <w:DontGrowAutofit/>
69   <w:SplitPgBreakAndParaMark/>
70   <w:EnableOpenTypeKerning/>
71   <w:DontFlipMirrorIndents/>
72   <w:OverrideTableStyleHps/>
73  </w:Compatibility>
74  <w:BrowserLevel>MicrosoftInternetExplorer4</w:BrowserLevel>
75  <m:mathPr>
76   <m:mathFont m:val="Cambria Math"/>
77   <m:brkBin m:val="before"/>
78   <m:brkBinSub m:val="&#45;-"/>
79   <m:smallFrac m:val="off"/>
80   <m:dispDef/>
81   <m:lMargin m:val="0"/>
82   <m:rMargin m:val="0"/>
83   <m:defJc m:val="centerGroup"/>
84   <m:wrapIndent m:val="1440"/>
85   <m:intLim m:val="subSup"/>
86   <m:naryLim m:val="undOvr"/>
87  </m:mathPr></w:WordDocument>
88</xml><![endif]--><!--[if gte mso 9]><xml>
89 <w:LatentStyles DefLockedState="false" DefUnhideWhenUsed="false"
90  DefSemiHidden="false" DefQFormat="false" DefPriority="99"
91  LatentStyleCount="371">
92  <w:LsdException Locked="false" Priority="0" QFormat="true" Name="Normal"/>
93  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 1"/>
94  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
95   UnhideWhenUsed="true" QFormat="true" Name="heading 2"/>
96  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
97   UnhideWhenUsed="true" QFormat="true" Name="heading 3"/>
98  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
99   UnhideWhenUsed="true" QFormat="true" Name="heading 4"/>
100  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
101   UnhideWhenUsed="true" QFormat="true" Name="heading 5"/>
102  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
103   UnhideWhenUsed="true" QFormat="true" Name="heading 6"/>
104  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
105   UnhideWhenUsed="true" QFormat="true" Name="heading 7"/>
106  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
107   UnhideWhenUsed="true" QFormat="true" Name="heading 8"/>
108  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
109   UnhideWhenUsed="true" QFormat="true" Name="heading 9"/>
110  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
111   Name="index 1"/>
112  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
113   Name="index 2"/>
114  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
115   Name="index 3"/>
116  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
117   Name="index 4"/>
118  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
119   Name="index 5"/>
120  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
121   Name="index 6"/>
122  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
123   Name="index 7"/>
124  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
125   Name="index 8"/>
126  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
127   Name="index 9"/>
128  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
129   UnhideWhenUsed="true" Name="toc 1"/>
130  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
131   UnhideWhenUsed="true" Name="toc 2"/>
132  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
133   UnhideWhenUsed="true" Name="toc 3"/>
134  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
135   UnhideWhenUsed="true" Name="toc 4"/>
136  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
137   UnhideWhenUsed="true" Name="toc 5"/>
138  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
139   UnhideWhenUsed="true" Name="toc 6"/>
140  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
141   UnhideWhenUsed="true" Name="toc 7"/>
142  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
143   UnhideWhenUsed="true" Name="toc 8"/>
144  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
145   UnhideWhenUsed="true" Name="toc 9"/>
146  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
147   Name="Normal Indent"/>
148  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
149   Name="footnote text"/>
150  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
151   Name="annotation text"/>
152  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
153   Name="header"/>
154  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
155   Name="footer"/>
156  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
157   Name="index heading"/>
158  <w:LsdException Locked="false" Priority="35" SemiHidden="true"
159   UnhideWhenUsed="true" QFormat="true" Name="caption"/>
160  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
161   Name="table of figures"/>
162  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
163   Name="envelope address"/>
164  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
165   Name="envelope return"/>
166  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
167   Name="footnote reference"/>
168  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
169   Name="annotation reference"/>
170  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
171   Name="line number"/>
172  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
173   Name="page number"/>
174  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
175   Name="endnote reference"/>
176  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
177   Name="endnote text"/>
178  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
179   Name="table of authorities"/>
180  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
181   Name="macro"/>
182  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
183   Name="toa heading"/>
184  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
185   Name="List"/>
186  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
187   Name="List Bullet"/>
188  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
189   Name="List Number"/>
190  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
191   Name="List 2"/>
192  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
193   Name="List 3"/>
194  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
195   Name="List 4"/>
196  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
197   Name="List 5"/>
198  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
199   Name="List Bullet 2"/>
200  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
201   Name="List Bullet 3"/>
202  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
203   Name="List Bullet 4"/>
204  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
205   Name="List Bullet 5"/>
206  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
207   Name="List Number 2"/>
208  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
209   Name="List Number 3"/>
210  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
211   Name="List Number 4"/>
212  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
213   Name="List Number 5"/>
214  <w:LsdException Locked="false" Priority="10" QFormat="true" Name="Title"/>
215  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
216   Name="Closing"/>
217  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
218   Name="Signature"/>
219  <w:LsdException Locked="false" Priority="1" SemiHidden="true"
220   UnhideWhenUsed="true" Name="Default Paragraph Font"/>
221  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
222   Name="Body Text"/>
223  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
224   Name="Body Text Indent"/>
225  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
226   Name="List Continue"/>
227  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
228   Name="List Continue 2"/>
229  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
230   Name="List Continue 3"/>
231  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
232   Name="List Continue 4"/>
233  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
234   Name="List Continue 5"/>
235  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
236   Name="Message Header"/>
237  <w:LsdException Locked="false" Priority="11" QFormat="true" Name="Subtitle"/>
238  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
239   Name="Salutation"/>
240  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
241   Name="Date"/>
242  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
243   Name="Body Text First Indent"/>
244  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
245   Name="Body Text First Indent 2"/>
246  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
247   Name="Note Heading"/>
248  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
249   Name="Body Text 2"/>
250  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
251   Name="Body Text 3"/>
252  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
253   Name="Body Text Indent 2"/>
254  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
255   Name="Body Text Indent 3"/>
256  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
257   Name="Block Text"/>
258  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
259   Name="Hyperlink"/>
260  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
261   Name="FollowedHyperlink"/>
262  <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/>
263  <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/>
264  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
265   Name="Document Map"/>
266  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
267   Name="Plain Text"/>
268  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
269   Name="E-mail Signature"/>
270  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
271   Name="HTML Top of Form"/>
272  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
273   Name="HTML Bottom of Form"/>
274  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
275   Name="Normal (Web)"/>
276  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
277   Name="HTML Acronym"/>
278  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
279   Name="HTML Address"/>
280  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
281   Name="HTML Cite"/>
282  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
283   Name="HTML Code"/>
284  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
285   Name="HTML Definition"/>
286  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
287   Name="HTML Keyboard"/>
288  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
289   Name="HTML Preformatted"/>
290  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
291   Name="HTML Sample"/>
292  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
293   Name="HTML Typewriter"/>
294  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
295   Name="HTML Variable"/>
296  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
297   Name="Normal Table"/>
298  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
299   Name="annotation subject"/>
300  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
301   Name="No List"/>
302  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
303   Name="Outline List 1"/>
304  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
305   Name="Outline List 2"/>
306  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
307   Name="Outline List 3"/>
308  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
309   Name="Table Simple 1"/>
310  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
311   Name="Table Simple 2"/>
312  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
313   Name="Table Simple 3"/>
314  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
315   Name="Table Classic 1"/>
316  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
317   Name="Table Classic 2"/>
318  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
319   Name="Table Classic 3"/>
320  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
321   Name="Table Classic 4"/>
322  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
323   Name="Table Colorful 1"/>
324  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
325   Name="Table Colorful 2"/>
326  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
327   Name="Table Colorful 3"/>
328  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
329   Name="Table Columns 1"/>
330  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
331   Name="Table Columns 2"/>
332  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
333   Name="Table Columns 3"/>
334  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
335   Name="Table Columns 4"/>
336  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
337   Name="Table Columns 5"/>
338  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
339   Name="Table Grid 1"/>
340  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
341   Name="Table Grid 2"/>
342  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
343   Name="Table Grid 3"/>
344  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
345   Name="Table Grid 4"/>
346  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
347   Name="Table Grid 5"/>
348  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
349   Name="Table Grid 6"/>
350  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
351   Name="Table Grid 7"/>
352  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
353   Name="Table Grid 8"/>
354  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
355   Name="Table List 1"/>
356  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
357   Name="Table List 2"/>
358  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
359   Name="Table List 3"/>
360  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
361   Name="Table List 4"/>
362  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
363   Name="Table List 5"/>
364  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
365   Name="Table List 6"/>
366  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
367   Name="Table List 7"/>
368  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
369   Name="Table List 8"/>
370  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
371   Name="Table 3D effects 1"/>
372  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
373   Name="Table 3D effects 2"/>
374  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
375   Name="Table 3D effects 3"/>
376  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
377   Name="Table Contemporary"/>
378  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
379   Name="Table Elegant"/>
380  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
381   Name="Table Professional"/>
382  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
383   Name="Table Subtle 1"/>
384  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
385   Name="Table Subtle 2"/>
386  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
387   Name="Table Web 1"/>
388  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
389   Name="Table Web 2"/>
390  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
391   Name="Table Web 3"/>
392  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
393   Name="Balloon Text"/>
394  <w:LsdException Locked="false" Priority="59" Name="Table Grid"/>
395  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
396   Name="Table Theme"/>
397  <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/>
398  <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/>
399  <w:LsdException Locked="false" Priority="60" Name="Light Shading"/>
400  <w:LsdException Locked="false" Priority="61" Name="Light List"/>
401  <w:LsdException Locked="false" Priority="62" Name="Light Grid"/>
402  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/>
403  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/>
404  <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/>
405  <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/>
406  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/>
407  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/>
408  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/>
409  <w:LsdException Locked="false" Priority="70" Name="Dark List"/>
410  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/>
411  <w:LsdException Locked="false" Priority="72" Name="Colorful List"/>
412  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
413  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
414  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
415  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
416  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
417  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
418  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
419  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
420  <w:LsdException Locked="false" Priority="34" QFormat="true"
421   Name="List Paragraph"/>
422  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
423  <w:LsdException Locked="false" Priority="30" QFormat="true"
424   Name="Intense Quote"/>
425  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
426  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
427  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
428  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
429  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
430  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
431  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
432  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
433  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
434  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
435  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
436  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
437  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
438  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
439  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
440  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
441  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
442  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
443  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
444  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
445  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
446  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
447  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
448  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
449  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
450  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
451  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
452  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
453  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
454  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
455  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
456  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
457  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
458  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
459  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
460  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
461  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
462  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
463  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
464  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
465  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
466  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
467  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
468  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
469  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
470  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
471  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
472  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
473  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
474  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
475  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
476  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
477  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
478  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
479  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
480  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
481  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
482  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
483  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
484  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
485  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
486  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
487  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
488  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
489  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
490  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
491  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
492  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
493  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
494  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
495  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
496  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
497  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
498  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
499  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
500  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
501  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
502  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
503  <w:LsdException Locked="false" Priority="19" QFormat="true"
504   Name="Subtle Emphasis"/>
505  <w:LsdException Locked="false" Priority="21" QFormat="true"
506   Name="Intense Emphasis"/>
507  <w:LsdException Locked="false" Priority="31" QFormat="true"
508   Name="Subtle Reference"/>
509  <w:LsdException Locked="false" Priority="32" QFormat="true"
510   Name="Intense Reference"/>
511  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
512  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
513   UnhideWhenUsed="true" Name="Bibliography"/>
514  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
515   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
516  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
517  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
518  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
519  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
520  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
521  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
522  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
523  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
524  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
525  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
526  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
527  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
528  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
529  <w:LsdException Locked="false" Priority="46"
530   Name="Grid Table 1 Light Accent 1"/>
531  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
532  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
533  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
534  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
535  <w:LsdException Locked="false" Priority="51"
536   Name="Grid Table 6 Colorful Accent 1"/>
537  <w:LsdException Locked="false" Priority="52"
538   Name="Grid Table 7 Colorful Accent 1"/>
539  <w:LsdException Locked="false" Priority="46"
540   Name="Grid Table 1 Light Accent 2"/>
541  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
542  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
543  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
544  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
545  <w:LsdException Locked="false" Priority="51"
546   Name="Grid Table 6 Colorful Accent 2"/>
547  <w:LsdException Locked="false" Priority="52"
548   Name="Grid Table 7 Colorful Accent 2"/>
549  <w:LsdException Locked="false" Priority="46"
550   Name="Grid Table 1 Light Accent 3"/>
551  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
552  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
553  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
554  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
555  <w:LsdException Locked="false" Priority="51"
556   Name="Grid Table 6 Colorful Accent 3"/>
557  <w:LsdException Locked="false" Priority="52"
558   Name="Grid Table 7 Colorful Accent 3"/>
559  <w:LsdException Locked="false" Priority="46"
560   Name="Grid Table 1 Light Accent 4"/>
561  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
562  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
563  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
564  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
565  <w:LsdException Locked="false" Priority="51"
566   Name="Grid Table 6 Colorful Accent 4"/>
567  <w:LsdException Locked="false" Priority="52"
568   Name="Grid Table 7 Colorful Accent 4"/>
569  <w:LsdException Locked="false" Priority="46"
570   Name="Grid Table 1 Light Accent 5"/>
571  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
572  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
573  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
574  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
575  <w:LsdException Locked="false" Priority="51"
576   Name="Grid Table 6 Colorful Accent 5"/>
577  <w:LsdException Locked="false" Priority="52"
578   Name="Grid Table 7 Colorful Accent 5"/>
579  <w:LsdException Locked="false" Priority="46"
580   Name="Grid Table 1 Light Accent 6"/>
581  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
582  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
583  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
584  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
585  <w:LsdException Locked="false" Priority="51"
586   Name="Grid Table 6 Colorful Accent 6"/>
587  <w:LsdException Locked="false" Priority="52"
588   Name="Grid Table 7 Colorful Accent 6"/>
589  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
590  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
591  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
592  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
593  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
594  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
595  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
596  <w:LsdException Locked="false" Priority="46"
597   Name="List Table 1 Light Accent 1"/>
598  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
599  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
600  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
601  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
602  <w:LsdException Locked="false" Priority="51"
603   Name="List Table 6 Colorful Accent 1"/>
604  <w:LsdException Locked="false" Priority="52"
605   Name="List Table 7 Colorful Accent 1"/>
606  <w:LsdException Locked="false" Priority="46"
607   Name="List Table 1 Light Accent 2"/>
608  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
609  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
610  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
611  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
612  <w:LsdException Locked="false" Priority="51"
613   Name="List Table 6 Colorful Accent 2"/>
614  <w:LsdException Locked="false" Priority="52"
615   Name="List Table 7 Colorful Accent 2"/>
616  <w:LsdException Locked="false" Priority="46"
617   Name="List Table 1 Light Accent 3"/>
618  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
619  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
620  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
621  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
622  <w:LsdException Locked="false" Priority="51"
623   Name="List Table 6 Colorful Accent 3"/>
624  <w:LsdException Locked="false" Priority="52"
625   Name="List Table 7 Colorful Accent 3"/>
626  <w:LsdException Locked="false" Priority="46"
627   Name="List Table 1 Light Accent 4"/>
628  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
629  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
630  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
631  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
632  <w:LsdException Locked="false" Priority="51"
633   Name="List Table 6 Colorful Accent 4"/>
634  <w:LsdException Locked="false" Priority="52"
635   Name="List Table 7 Colorful Accent 4"/>
636  <w:LsdException Locked="false" Priority="46"
637   Name="List Table 1 Light Accent 5"/>
638  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
639  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
640  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
641  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
642  <w:LsdException Locked="false" Priority="51"
643   Name="List Table 6 Colorful Accent 5"/>
644  <w:LsdException Locked="false" Priority="52"
645   Name="List Table 7 Colorful Accent 5"/>
646  <w:LsdException Locked="false" Priority="46"
647   Name="List Table 1 Light Accent 6"/>
648  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
649  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
650  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
651  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
652  <w:LsdException Locked="false" Priority="51"
653   Name="List Table 6 Colorful Accent 6"/>
654  <w:LsdException Locked="false" Priority="52"
655   Name="List Table 7 Colorful Accent 6"/>
656 </w:LatentStyles>
657</xml><![endif]-->
658<style>
659<!--
660 /* Font Definitions */
661 @font-face
662        {font-family:"Cambria Math";
663        panose-1:2 4 5 3 5 4 6 3 2 4;
664        mso-font-charset:0;
665        mso-generic-font-family:roman;
666        mso-font-pitch:variable;
667        mso-font-signature:-536870145 1107305727 0 0 415 0;}
668@font-face
669        {font-family:Calibri;
670        panose-1:2 15 5 2 2 2 4 3 2 4;
671        mso-font-charset:0;
672        mso-generic-font-family:swiss;
673        mso-font-pitch:variable;
674        mso-font-signature:-536870145 1073786111 1 0 415 0;}
675@font-face
676        {font-family:Tahoma;
677        panose-1:2 11 6 4 3 5 4 4 2 4;
678        mso-font-charset:0;
679        mso-generic-font-family:swiss;
680        mso-font-pitch:variable;
681        mso-font-signature:-520081665 -1073717157 41 0 66047 0;}
682 /* Style Definitions */
683 p.MsoNormal, li.MsoNormal, div.MsoNormal
684        {mso-style-unhide:no;
685        mso-style-qformat:yes;
686        mso-style-parent:"";
687        margin:0in;
688        margin-bottom:.0001pt;
689        mso-pagination:widow-orphan;
690        font-size:12.0pt;
691        font-family:"Times New Roman",serif;
692        mso-fareast-font-family:"Times New Roman";
693        mso-fareast-theme-font:minor-fareast;}
694h1
695        {mso-style-priority:9;
696        mso-style-unhide:no;
697        mso-style-qformat:yes;
698        mso-style-link:"Heading 1 Char";
699        mso-margin-top-alt:auto;
700        margin-right:0in;
701        mso-margin-bottom-alt:auto;
702        margin-left:0in;
703        mso-pagination:widow-orphan;
704        mso-outline-level:1;
705        font-size:24.0pt;
706        font-family:"Times New Roman",serif;
707        mso-fareast-font-family:"Times New Roman";
708        mso-fareast-theme-font:minor-fareast;
709        font-weight:bold;}
710h2
711        {mso-style-noshow:yes;
712        mso-style-priority:9;
713        mso-style-qformat:yes;
714        mso-style-link:"Heading 2 Char";
715        mso-margin-top-alt:auto;
716        margin-right:0in;
717        mso-margin-bottom-alt:auto;
718        margin-left:0in;
719        mso-pagination:widow-orphan;
720        mso-outline-level:2;
721        font-size:18.0pt;
722        font-family:"Times New Roman",serif;
723        mso-fareast-font-family:"Times New Roman";
724        mso-fareast-theme-font:minor-fareast;
725        font-weight:bold;}
726h3
727        {mso-style-noshow:yes;
728        mso-style-priority:9;
729        mso-style-qformat:yes;
730        mso-style-link:"Heading 3 Char";
731        mso-margin-top-alt:auto;
732        margin-right:0in;
733        mso-margin-bottom-alt:auto;
734        margin-left:0in;
735        mso-pagination:widow-orphan;
736        mso-outline-level:3;
737        font-size:13.5pt;
738        font-family:"Times New Roman",serif;
739        mso-fareast-font-family:"Times New Roman";
740        mso-fareast-theme-font:minor-fareast;
741        font-weight:bold;}
742h4
743        {mso-style-noshow:yes;
744        mso-style-priority:9;
745        mso-style-qformat:yes;
746        mso-style-link:"Heading 4 Char";
747        mso-style-next:Normal;
748        margin-top:10.0pt;
749        margin-right:0in;
750        margin-bottom:0in;
751        margin-left:0in;
752        margin-bottom:.0001pt;
753        mso-pagination:widow-orphan lines-together;
754        page-break-after:avoid;
755        mso-outline-level:4;
756        font-size:13.0pt;
757        font-family:"Cambria",serif;
758        mso-ascii-font-family:Cambria;
759        mso-ascii-theme-font:major-latin;
760        mso-fareast-font-family:"Times New Roman";
761        mso-fareast-theme-font:major-fareast;
762        mso-hansi-font-family:Cambria;
763        mso-hansi-theme-font:major-latin;
764        mso-bidi-font-family:"Times New Roman";
765        mso-bidi-theme-font:major-bidi;
766        color:#4F81BD;
767        mso-themecolor:accent1;
768        font-weight:bold;
769        font-style:italic;}
770h5
771        {mso-style-noshow:yes;
772        mso-style-priority:9;
773        mso-style-qformat:yes;
774        mso-style-link:"Heading 5 Char";
775        mso-margin-top-alt:auto;
776        margin-right:0in;
777        mso-margin-bottom-alt:auto;
778        margin-left:0in;
779        mso-pagination:widow-orphan;
780        mso-outline-level:5;
781        font-size:12.0pt;
782        font-family:"Times New Roman",serif;
783        mso-fareast-font-family:"Times New Roman";
784        mso-fareast-theme-font:minor-fareast;
785        color:#4F4FFF;
786        font-weight:bold;}
787a:visited, span.MsoHyperlinkFollowed
788        {mso-style-noshow:yes;
789        mso-style-priority:99;
790        color:purple;
791        text-decoration:underline;
792        text-underline:single;}
793p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap
794        {mso-style-noshow:yes;
795        mso-style-priority:99;
796        mso-style-link:"Document Map Char";
797        margin:0in;
798        margin-bottom:.0001pt;
799        mso-pagination:widow-orphan;
800        font-size:8.0pt;
801        font-family:"Tahoma",sans-serif;
802        mso-fareast-font-family:"Times New Roman";
803        mso-fareast-theme-font:minor-fareast;}
804p
805        {mso-style-noshow:yes;
806        mso-style-priority:99;
807        mso-margin-top-alt:auto;
808        margin-right:0in;
809        mso-margin-bottom-alt:auto;
810        margin-left:0in;
811        mso-pagination:widow-orphan;
812        font-size:12.0pt;
813        font-family:"Times New Roman",serif;
814        mso-fareast-font-family:"Times New Roman";
815        mso-fareast-theme-font:minor-fareast;}
816pre
817        {mso-style-noshow:yes;
818        mso-style-priority:99;
819        mso-style-link:"HTML Preformatted Char";
820        margin:0in;
821        margin-bottom:.0001pt;
822        mso-pagination:widow-orphan;
823        tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt;
824        font-size:10.0pt;
825        font-family:"Courier New";
826        mso-fareast-font-family:"Times New Roman";}
827p.MsoAcetate, li.MsoAcetate, div.MsoAcetate
828        {mso-style-noshow:yes;
829        mso-style-priority:99;
830        mso-style-link:"Balloon Text Char";
831        margin:0in;
832        margin-bottom:.0001pt;
833        mso-pagination:widow-orphan;
834        font-size:8.0pt;
835        font-family:"Tahoma",sans-serif;
836        mso-fareast-font-family:"Times New Roman";
837        mso-fareast-theme-font:minor-fareast;}
838span.MsoPlaceholderText
839        {mso-style-noshow:yes;
840        mso-style-priority:99;
841        mso-style-unhide:no;
842        color:gray;}
843p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing
844        {mso-style-noshow:yes;
845        mso-style-priority:1;
846        mso-style-unhide:no;
847        mso-style-qformat:yes;
848        mso-style-parent:"";
849        margin:0in;
850        margin-bottom:.0001pt;
851        mso-pagination:widow-orphan;
852        font-size:12.0pt;
853        font-family:"Times New Roman",serif;
854        mso-fareast-font-family:"Times New Roman";
855        mso-fareast-theme-font:minor-fareast;}
856p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph
857        {mso-style-noshow:yes;
858        mso-style-priority:34;
859        mso-style-unhide:no;
860        mso-style-qformat:yes;
861        margin-top:0in;
862        margin-right:0in;
863        margin-bottom:0in;
864        margin-left:.5in;
865        margin-bottom:.0001pt;
866        mso-add-space:auto;
867        mso-pagination:widow-orphan;
868        font-size:12.0pt;
869        font-family:"Times New Roman",serif;
870        mso-fareast-font-family:"Times New Roman";
871        mso-fareast-theme-font:minor-fareast;}
872p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst
873        {mso-style-noshow:yes;
874        mso-style-priority:34;
875        mso-style-unhide:no;
876        mso-style-qformat:yes;
877        mso-style-type:export-only;
878        margin-top:0in;
879        margin-right:0in;
880        margin-bottom:0in;
881        margin-left:.5in;
882        margin-bottom:.0001pt;
883        mso-add-space:auto;
884        mso-pagination:widow-orphan;
885        font-size:12.0pt;
886        font-family:"Times New Roman",serif;
887        mso-fareast-font-family:"Times New Roman";
888        mso-fareast-theme-font:minor-fareast;}
889p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle
890        {mso-style-noshow:yes;
891        mso-style-priority:34;
892        mso-style-unhide:no;
893        mso-style-qformat:yes;
894        mso-style-type:export-only;
895        margin-top:0in;
896        margin-right:0in;
897        margin-bottom:0in;
898        margin-left:.5in;
899        margin-bottom:.0001pt;
900        mso-add-space:auto;
901        mso-pagination:widow-orphan;
902        font-size:12.0pt;
903        font-family:"Times New Roman",serif;
904        mso-fareast-font-family:"Times New Roman";
905        mso-fareast-theme-font:minor-fareast;}
906p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast
907        {mso-style-noshow:yes;
908        mso-style-priority:34;
909        mso-style-unhide:no;
910        mso-style-qformat:yes;
911        mso-style-type:export-only;
912        margin-top:0in;
913        margin-right:0in;
914        margin-bottom:0in;
915        margin-left:.5in;
916        margin-bottom:.0001pt;
917        mso-add-space:auto;
918        mso-pagination:widow-orphan;
919        font-size:12.0pt;
920        font-family:"Times New Roman",serif;
921        mso-fareast-font-family:"Times New Roman";
922        mso-fareast-theme-font:minor-fareast;}
923span.MsoIntenseReference
924        {mso-style-priority:32;
925        mso-style-unhide:no;
926        mso-style-qformat:yes;
927        font-variant:small-caps;
928        color:#C0504D;
929        mso-themecolor:accent2;
930        letter-spacing:.25pt;
931        font-weight:bold;
932        text-decoration:underline;
933        text-underline:single;}
934span.Heading1Char
935        {mso-style-name:"Heading 1 Char";
936        mso-style-priority:9;
937        mso-style-unhide:no;
938        mso-style-locked:yes;
939        mso-style-link:"Heading 1";
940        mso-ansi-font-size:24.0pt;
941        mso-bidi-font-size:24.0pt;
942        font-family:"Times New Roman",serif;
943        mso-ascii-font-family:"Times New Roman";
944        mso-fareast-font-family:"Times New Roman";
945        mso-fareast-theme-font:minor-fareast;
946        mso-hansi-font-family:"Times New Roman";
947        mso-bidi-font-family:"Times New Roman";
948        mso-font-kerning:18.0pt;
949        font-weight:bold;}
950span.Heading2Char
951        {mso-style-name:"Heading 2 Char";
952        mso-style-noshow:yes;
953        mso-style-priority:9;
954        mso-style-unhide:no;
955        mso-style-locked:yes;
956        mso-style-link:"Heading 2";
957        mso-ansi-font-size:18.0pt;
958        mso-bidi-font-size:18.0pt;
959        font-family:"Times New Roman",serif;
960        mso-ascii-font-family:"Times New Roman";
961        mso-fareast-font-family:"Times New Roman";
962        mso-fareast-theme-font:minor-fareast;
963        mso-hansi-font-family:"Times New Roman";
964        mso-bidi-font-family:"Times New Roman";
965        font-weight:bold;}
966span.Heading3Char
967        {mso-style-name:"Heading 3 Char";
968        mso-style-noshow:yes;
969        mso-style-priority:9;
970        mso-style-unhide:no;
971        mso-style-locked:yes;
972        mso-style-link:"Heading 3";
973        mso-ansi-font-size:13.5pt;
974        mso-bidi-font-size:13.5pt;
975        font-family:"Times New Roman",serif;
976        mso-ascii-font-family:"Times New Roman";
977        mso-fareast-font-family:"Times New Roman";
978        mso-fareast-theme-font:minor-fareast;
979        mso-hansi-font-family:"Times New Roman";
980        mso-bidi-font-family:"Times New Roman";
981        font-weight:bold;}
982span.Heading4Char
983        {mso-style-name:"Heading 4 Char";
984        mso-style-noshow:yes;
985        mso-style-priority:9;
986        mso-style-unhide:no;
987        mso-style-locked:yes;
988        mso-style-link:"Heading 4";
989        mso-ansi-font-size:13.0pt;
990        mso-bidi-font-size:13.0pt;
991        font-family:"Cambria",serif;
992        mso-ascii-font-family:Cambria;
993        mso-ascii-theme-font:major-latin;
994        mso-fareast-font-family:"Times New Roman";
995        mso-fareast-theme-font:major-fareast;
996        mso-hansi-font-family:Cambria;
997        mso-hansi-theme-font:major-latin;
998        mso-bidi-font-family:"Times New Roman";
999        mso-bidi-theme-font:major-bidi;
1000        color:#4F81BD;
1001        mso-themecolor:accent1;
1002        font-weight:bold;
1003        font-style:italic;}
1004span.Heading5Char
1005        {mso-style-name:"Heading 5 Char";
1006        mso-style-noshow:yes;
1007        mso-style-priority:9;
1008        mso-style-unhide:no;
1009        mso-style-locked:yes;
1010        mso-style-link:"Heading 5";
1011        mso-ansi-font-size:12.0pt;
1012        mso-bidi-font-size:12.0pt;
1013        font-family:"Times New Roman",serif;
1014        mso-ascii-font-family:"Times New Roman";
1015        mso-fareast-font-family:"Times New Roman";
1016        mso-fareast-theme-font:minor-fareast;
1017        mso-hansi-font-family:"Times New Roman";
1018        mso-bidi-font-family:"Times New Roman";
1019        color:#4F4FFF;
1020        font-weight:bold;}
1021span.HTMLPreformattedChar
1022        {mso-style-name:"HTML Preformatted Char";
1023        mso-style-noshow:yes;
1024        mso-style-priority:99;
1025        mso-style-unhide:no;
1026        mso-style-locked:yes;
1027        mso-style-link:"HTML Preformatted";
1028        font-family:"Courier New";
1029        mso-ascii-font-family:"Courier New";
1030        mso-fareast-font-family:"Times New Roman";
1031        mso-hansi-font-family:"Courier New";
1032        mso-bidi-font-family:"Courier New";}
1033span.DocumentMapChar
1034        {mso-style-name:"Document Map Char";
1035        mso-style-noshow:yes;
1036        mso-style-priority:99;
1037        mso-style-unhide:no;
1038        mso-style-locked:yes;
1039        mso-style-link:"Document Map";
1040        mso-ansi-font-size:8.0pt;
1041        mso-bidi-font-size:8.0pt;
1042        font-family:"Tahoma",sans-serif;
1043        mso-ascii-font-family:Tahoma;
1044        mso-fareast-font-family:"Times New Roman";
1045        mso-fareast-theme-font:minor-fareast;
1046        mso-hansi-font-family:Tahoma;
1047        mso-bidi-font-family:Tahoma;}
1048span.BalloonTextChar
1049        {mso-style-name:"Balloon Text Char";
1050        mso-style-noshow:yes;
1051        mso-style-priority:99;
1052        mso-style-unhide:no;
1053        mso-style-locked:yes;
1054        mso-style-link:"Balloon Text";
1055        mso-ansi-font-size:8.0pt;
1056        mso-bidi-font-size:8.0pt;
1057        font-family:"Tahoma",sans-serif;
1058        mso-ascii-font-family:Tahoma;
1059        mso-fareast-font-family:"Times New Roman";
1060        mso-fareast-theme-font:minor-fareast;
1061        mso-hansi-font-family:Tahoma;
1062        mso-bidi-font-family:Tahoma;}
1063span.SpellE
1064        {mso-style-name:"";
1065        mso-spl-e:yes;}
1066span.GramE
1067        {mso-style-name:"";
1068        mso-gram-e:yes;}
1069.MsoChpDefault
1070        {mso-style-type:export-only;
1071        mso-default-props:yes;
1072        font-size:10.0pt;
1073        mso-ansi-font-size:10.0pt;
1074        mso-bidi-font-size:10.0pt;
1075        font-family:"Calibri",sans-serif;
1076        mso-ascii-font-family:Calibri;
1077        mso-ascii-theme-font:minor-latin;
1078        mso-fareast-font-family:Calibri;
1079        mso-fareast-theme-font:minor-latin;
1080        mso-hansi-font-family:Calibri;
1081        mso-hansi-theme-font:minor-latin;
1082        mso-bidi-font-family:"Times New Roman";
1083        mso-bidi-theme-font:minor-bidi;}
1084@page WordSection1
1085        {size:8.5in 11.0in;
1086        margin:1.0in 1.0in 1.0in 1.0in;
1087        mso-header-margin:.5in;
1088        mso-footer-margin:.5in;
1089        mso-paper-source:0;}
1090div.WordSection1
1091        {page:WordSection1;}
1092-->
1093</style>
1094<!--[if gte mso 10]>
1095<style>
1096 /* Style Definitions */
1097 table.MsoNormalTable
1098        {mso-style-name:"Table Normal";
1099        mso-tstyle-rowband-size:0;
1100        mso-tstyle-colband-size:0;
1101        mso-style-noshow:yes;
1102        mso-style-priority:99;
1103        mso-style-parent:"";
1104        mso-padding-alt:0in 5.4pt 0in 5.4pt;
1105        mso-para-margin:0in;
1106        mso-para-margin-bottom:.0001pt;
1107        mso-pagination:widow-orphan;
1108        font-size:10.0pt;
1109        font-family:"Calibri",sans-serif;
1110        mso-ascii-font-family:Calibri;
1111        mso-ascii-theme-font:minor-latin;
1112        mso-hansi-font-family:Calibri;
1113        mso-hansi-theme-font:minor-latin;}
1114</style>
1115<![endif]--><!--[if gte mso 9]><xml>
1116 <o:shapedefaults v:ext="edit" spidmax="1026"/>
1117</xml><![endif]--><!--[if gte mso 9]><xml>
1118 <o:shapelayout v:ext="edit">
1119  <o:idmap v:ext="edit" data="1"/>
1120 </o:shapelayout></xml><![endif]-->
1121</head>
1122
1123<body lang=EN-US link="#000000" vlink=purple style='tab-interval:.5in'>
1124
1125<div class=WordSection1>
1126
1127<p class=MsoNormal><span class=Heading1Char><span style='font-size:24.0pt'>Calibration
1128of an area detector in GSAS-II</span></span><b><span style='font-size:14.0pt;
1129color:#365F91;mso-themecolor:accent1;mso-themeshade:191'><o:p></o:p></span></b></p>
1130
1131<p class=MsoNormal>In this tutorial, data collected with a Perkin-Elmer area
1132detector at APS 11-ID-C with a wavelength 0.10798 A, where the detector was
1133intentionally tilted at 45 degrees, are used. Note that menu entries are listed
1134in bold face below as <b style='mso-bidi-font-weight:normal'><span
1135style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1136mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1137minor-latin'>Help/About GSAS-II</span></b>, which lists first the name of the
1138menu (here <b style='mso-bidi-font-weight:normal'><span style='font-family:
1139"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1140minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Help</span></b>)
1141and second the name of the entry in the menu (here <b style='mso-bidi-font-weight:
1142normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1143minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1144mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).</p>
1145
1146<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
1147href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
1148text-underline:none'>start GSAS-II</span></a></span></u>.</p>
1149
1150<h1>Step 1: read in the data file</h1>
1151
1152<p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the <b
1153style='mso-bidi-font-weight:normal'>Data/Read image data</b> menu item to read
1154the data file into the current GSAS-II project. </p>
1155
1156<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
1157
1158<p class=MsoNormal>A file selection dialog will be shown; its appearance will
1159depend on your OS. Change the search directory to <b style='mso-bidi-font-weight:
1160normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1161minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1162mso-bidi-theme-font:minor-latin'>/exercises/2DCalibration</span></b> and then
1163select the file </p>
1164
1165<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
1166style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1167mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1168minor-latin'>La_hex_+45deg-00015.tif</span></b> and press <b style='mso-bidi-font-weight:
1169normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1170minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1171mso-bidi-theme-font:minor-latin'>Open</span></b>.<span style='mso-no-proof:
1172yes'> <o:p></o:p></span></p>
1173
1174<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype
1175 id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t"
1176 path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f">
1177 <v:stroke joinstyle="miter"/>
1178 <v:formulas>
1179  <v:f eqn="if lineDrawn pixelLineWidth 0"/>
1180  <v:f eqn="sum @0 1 0"/>
1181  <v:f eqn="sum 0 0 @1"/>
1182  <v:f eqn="prod @2 1 2"/>
1183  <v:f eqn="prod @3 21600 pixelWidth"/>
1184  <v:f eqn="prod @3 21600 pixelHeight"/>
1185  <v:f eqn="sum @0 0 1"/>
1186  <v:f eqn="prod @6 1 2"/>
1187  <v:f eqn="prod @7 21600 pixelWidth"/>
1188  <v:f eqn="sum @8 21600 0"/>
1189  <v:f eqn="prod @7 21600 pixelHeight"/>
1190  <v:f eqn="sum @10 21600 0"/>
1191 </v:formulas>
1192 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
1193 <o:lock v:ext="edit" aspectratio="t"/>
1194</v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1038" type="#_x0000_t75"
1195 style='width:300pt;height:187.5pt;visibility:visible;mso-wrap-style:square'>
1196 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png"
1197  o:title=""/>
1198</v:shape><![endif]--><![if !vml]><img border=0 width=400 height=250
1199src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png"
1200v:shapes="Picture_x0020_1"><![endif]></span></p>
1201
1202<p class=MsoNormal>At this point the data tree window will have several
1203entries; the highlighted one specifies the contents of the data window as <b
1204style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1205mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1206Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span><o:p></o:p></b></p>
1207
1208<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1209 id="Picture_x0020_2" o:spid="_x0000_i1037" type="#_x0000_t75" style='width:472.5pt;
1210 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1211 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png"
1212  o:title=""/>
1213</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518
1214src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image002.png"
1215v:shapes="Picture_x0020_2"><![endif]></span></p>
1216
1217<p class=MsoNormal><span style='mso-spacerun:yes'> </span>The plot window shows
1218the image; notice the elliptical shape of the powder diffraction rings due to the
121945 degree detector tilt. The blue <b style='mso-bidi-font-weight:normal'><span
1220style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1221mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1222minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span></b> marks the beam
1223location (which defaults to the image center); the calibration you will perform
1224here will find the correct placement for it. Also note that as the mouse is
1225moved across the plot the plot window status bar (at bottom of plot window)
1226shows the cursor position, as computed from the default (incorrect) calibration
1227values. These constants will be correctly determined after you finish the
1228calibration.</p>
1229
1230<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
1231style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_15"
1232 o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt;height:450pt;
1233 visibility:visible;mso-wrap-style:square'>
1234 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
1235  o:title=""/>
1236</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1237src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
1238v:shapes="Picture_x0020_15"><![endif]></span></p>
1239
1240<h1><span style='mso-spacerun:yes'> </span>Step 2: Edit image parameters</h1>
1241
1242<p class=MsoNormal>Note that, alas, very few image formats contain all of the
1243important metadata about the image, so it needs to be added manually. In this
1244case set the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1245"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1246minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>wavelength</span></b>
1247to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1248mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1249Calibri;mso-bidi-theme-font:minor-latin'>0.10798</span></b>. We will be determining
1250the calibration values of all the checked items. In this case wavelength is
1251known (‘Penetration’ is a correction for x-ray penetration into the detector;
1252it is only needed when the detector is close to the sample). Under certain
1253circumstances it may be useful to restrict the calibration to fewer parameters
1254(i.e. if distance is presumed to be “known”) in which case you can uncheck some
1255of the calibration parameters and use their fixed values. It is also helpful to
1256change the display of the image so that it is easier to see the diffraction
1257rings. Lowering the maximum intensity to 10,000 to 20,000 counts will help
1258(note that this can be done by moving the slider, or by typing a value in the
1259box and then clicking on another control or pressing the <b style='mso-bidi-font-weight:
1260normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1261minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1262mso-bidi-theme-font:minor-latin'>Enter</span></b> or <b style='mso-bidi-font-weight:
1263normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1264minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1265mso-bidi-theme-font:minor-latin'>Tab</span></b> key). You may also wish to
1266select another color scheme using the <b style='mso-bidi-font-weight:normal'><span
1267style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1268mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1269minor-latin'>Color bar</span></b> selector. </p>
1270
1271<h1><span style='mso-spacerun:yes'> </span>Step 3: Calibrate</h1>
1272
1273<h3><span style='mso-spacerun:yes'> </span>First: </h3>
1274
1275<p class=MsoNormal><span style='mso-spacerun:yes'>   </span>Set the material
1276used as a sample in the box labeled <span class=SpellE><b style='mso-bidi-font-weight:
1277normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1278minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1279mso-bidi-theme-font:minor-latin'>Calibrant</span></b></span>; select <b
1280style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1281mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1282Calibri;mso-bidi-theme-font:minor-latin'>LaB6 SRM660a</span></b></p>
1283
1284<h3>Second: </h3>
1285
1286<p class=MsoNormal><span style='mso-spacerun:yes'>   </span>Use the <b
1287style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1288mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1289Calibri;mso-bidi-theme-font:minor-latin'>Operations/Calibrate</span></b> menu
1290item (note this menu is on the <b style='mso-bidi-font-weight:normal'><span
1291style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1292mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1293minor-latin'>Image Controls</span></b> window or for the Mac, the <b
1294style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1295mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1296Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window must
1297be active to place this into the system menu bar). At this point the status
1298line on the bottom of the <b style='mso-bidi-font-weight:normal'><span
1299style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1300mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1301minor-latin'>Image Controls</span></b> window changes with a prompt to select
1302points for calibration.</p>
1303
1304<h3>Third: </h3>
1305
1306<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>Use the left mouse
1307button to click on at least five locations on the innermost ring. As each point
1308is defined, a red &quot;<b style='mso-bidi-font-weight:normal'><span
1309style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1310mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1311minor-latin;color:red'>+</span></b>&quot; is added to the plot. You need not
1312hit the ring exactly as the code will search for the locally highest point in a
131340x40 pixel box. (On the Mac with a two or three button mouse, also use the
1314left mouse button, or with a standard Mac single-button mouse, use the regular
1315mouse button.)</p>
1316
1317<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1318 id="_x0000_i1035" type="#_x0000_t75" style='width:525pt;height:450pt;
1319 visibility:visible;mso-wrap-style:square'>
1320 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
1321  o:title=""/>
1322</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1323src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
1324v:shapes="_x0000_i1035"><![endif]></span></p>
1325
1326<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>To remove a point
1327added in error click on that point with the right mouse button (on the Mac, if
1328you have a single-button mouse, hold the control key down and click). NB: it is
1329slightly better to pick points just inside the inner ring as GSAS-II will then find
1330the best point on that ring.</p>
1331
1332<h3><span style='mso-spacerun:yes'> </span>Fourth:</h3>
1333
1334<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>When done, press the
1335right mouse button well away from any points that have been added (on the Mac,
1336if you have a single-button mouse, hold the control key down and click). </p>
1337
1338<p class=MsoNormal>The calibration is then performed. First the rings are
1339located and an ellipse is optimized for each ring. The indexed rings are first
1340shown briefly in red as the calibration proceeds and center of each ellipse is
1341noted with a blue &quot;<b style='mso-bidi-font-weight:normal'><span
1342style='color:#4F81BD;mso-themecolor:accent1'>+</span></b>&quot;; these will
1343track in the direction of the tilt. When all rings have been fitted, the entire
1344ensemble of rings is refitted to the detector parameters and the rings are then
1345shown in blue. The beam position (blue “<span style='font-family:"Calibri",sans-serif;
1346mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1347Calibri;mso-bidi-theme-font:minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span>”)
1348is now correctly positioned.</p>
1349
1350<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
1351style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="_x0000_i1034" type="#_x0000_t75"
1352 style='width:525pt;height:450pt;visibility:visible;mso-wrap-style:square'>
1353 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
1354  o:title=""/>
1355</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1356src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
1357v:shapes="_x0000_i1034"><![endif]></span><span
1358style='mso-spacerun:yes'> </span></p>
1359
1360<p class=MsoNormal>The derived calibration results are shown in the <b
1361style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1362mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1363Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window.</p>
1364
1365<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1366 id="Picture_x0020_16" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:472.5pt;
1367 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1368 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png"
1369  o:title=""/>
1370</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518
1371src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image006.png"
1372v:shapes="Picture_x0020_16"><![endif]></span><span
1373style='mso-spacerun:yes'> </span></p>
1374
1375<p class=MsoNormal><span class=GramE>and</span> the console window shows
1376details of the fit.</p>
1377
1378<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1379 id="Picture_x0020_11" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:447.75pt;
1380 height:107.25pt;visibility:visible;mso-wrap-style:square'>
1381 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
1382  o:title=""/>
1383</v:shape><![endif]--><![if !vml]><img border=0 width=597 height=143
1384src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
1385v:shapes="Picture_x0020_11"><![endif]></span></p>
1386
1387<p class=MsoNormal>The <b style='mso-bidi-font-weight:normal'><span
1388style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1389mso-hansi-theme-font:minor-latin'>distance</span></b> is from the sample to the
1390plane containing the detector, <span class=SpellE><b style='mso-bidi-font-weight:
1391normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1392minor-latin;mso-hansi-theme-font:minor-latin'>det</span></b></span><b
1393style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1394mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-x</span></b>
1395&amp; <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
1396style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1397mso-hansi-theme-font:minor-latin'>det</span></b></span><b style='mso-bidi-font-weight:
1398normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1399minor-latin;mso-hansi-theme-font:minor-latin'>-y</span></b> is the incident
1400beam location on the image, <b style='mso-bidi-font-weight:normal'><span
1401style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1402mso-hansi-theme-font:minor-latin'>tilt</span></b> is the angle of detector
1403rotation from being normal to the incident beam and <b style='mso-bidi-font-weight:
1404normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1405minor-latin;mso-hansi-theme-font:minor-latin'>phi</span></b> is the rotation of
1406the detector tilt axis from the x-axis.<span style='mso-spacerun:yes'> 
1407</span>To see the actual points selected by the program, click on the <b
1408style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1409mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1410Calibri;mso-bidi-theme-font:minor-latin'>show ring picks?</span></b> <span
1411class=GramE>check</span> box </p>
1412
1413<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1414 id="_x0000_i1031" type="#_x0000_t75" style='width:525pt;height:450pt;
1415 visibility:visible;mso-wrap-style:square'>
1416 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
1417  o:title=""/>
1418</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1419src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
1420v:shapes="_x0000_i1031"><![endif]></span><span
1421style='mso-spacerun:yes'> </span><span style='color:#1F497D;mso-themecolor:
1422text2'><o:p></o:p></span></p>
1423
1424<p class=MsoNormal>When this is done, it sometimes occurs that the points
1425selected for the outermost rings are scattered between that and the next ring.
1426This can be repaired by changing the pixel search range to <b style='mso-bidi-font-weight:
1427normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1428minor-latin;mso-hansi-theme-font:minor-latin'>10</span></b> and using the <b
1429style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1430mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1431Calibri;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b> menu
1432item. Also notice that the right edge of the image shows a ragged fit to the
1433rings because of an intensity falloff. This can be removed by placing a frame
1434mask about the “good” part of the pattern. Select the <b style='mso-bidi-font-weight:
1435normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1436minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> GSAS-II data
1437tree item.</p>
1438
1439<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1440 id="Picture_x0020_19" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:297.75pt;
1441 height:99.75pt;visibility:visible;mso-wrap-style:square'>
1442 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image009.png"
1443  o:title=""/>
1444</v:shape><![endif]--><![if !vml]><img border=0 width=397 height=133
1445src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image009.png"
1446v:shapes="Picture_x0020_19"><![endif]></span></p>
1447
1448<p class=MsoNormal>The instruction in the status bar of this frame tells you
1449how to enter a frame: first select the plot window, then press the ’<b
1450style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1451mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>F</span></b>’
1452key; that will “arm” the frame mask creator. Then select each corner of the
1453good part of the image in turn (I chose points with x=400 for the right edge)
1454with the left mouse button. After selecting the last point, close the frame
1455with a press of the right mouse button. As each point is selected a small green
1456‘+’ will be drawn on the plot connected with a green line to the previous
1457point. When you are done the image should look something like</p>
1458
1459<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1460 id="Picture_x0020_13" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt;
1461 height:450pt;visibility:visible;mso-wrap-style:square'>
1462 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image010.png"
1463  o:title=""/>
1464</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1465src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image010.png"
1466v:shapes="Picture_x0020_13"><![endif]></span><span
1467style='mso-spacerun:yes'> </span></p>
1468
1469<p class=MsoNormal>Mask points can be moved by carefully selecting and dragging
1470then with the left button down (you may need to zoom in to do this); the right
1471mouse button will delete it. The <b style='mso-bidi-font-weight:normal'><span
1472style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1473mso-hansi-theme-font:minor-latin'>Mask</span></b> data window will show the new
1474frame mask.</p>
1475
1476<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1477 id="Picture_x0020_14" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:337.5pt;
1478 height:135pt;visibility:visible;mso-wrap-style:square'>
1479 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image011.png"
1480  o:title=""/>
1481</v:shape><![endif]--><![if !vml]><img border=0 width=450 height=180
1482src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image011.png"
1483v:shapes="Picture_x0020_14"><![endif]></span></p>
1484
1485<p class=MsoNormal>Now go back to the <b style='mso-bidi-font-weight:normal'><span
1486style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1487mso-hansi-theme-font:minor-latin'>Image Controls</span></b> tree item and do <b
1488style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1489mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1490Calibri;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b>; a
1491better calibration will result.</p>
1492
1493<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1494 id="Picture_x0020_20" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:525pt;
1495 height:450pt;visibility:visible;mso-wrap-style:square'>
1496 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image012.png"
1497  o:title=""/>
1498</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1499src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image012.png"
1500v:shapes="Picture_x0020_20"><![endif]></span></p>
1501
1502<p class=MsoNormal>Notice that the frame defined the calibration region.</p>
1503
1504<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1505 id="Picture_x0020_17" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:472.5pt;
1506 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1507 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image013.png"
1508  o:title=""/>
1509</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518
1510src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image013.png"
1511v:shapes="Picture_x0020_17"><![endif]></span></p>
1512
1513<p class=MsoNormal>And notice the better fit obtained (smaller chi**2 and
1514smaller <span class=SpellE>esds</span>).</p>
1515
1516<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1517 id="Picture_x0020_18" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:447.75pt;
1518 height:98.25pt;visibility:visible;mso-wrap-style:square'>
1519 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image014.png"
1520  o:title=""/>
1521</v:shape><![endif]--><![if !vml]><img border=0 width=597 height=131
1522src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image014.png"
1523v:shapes="Picture_x0020_18"><![endif]></span></p>
1524
1525<p class=MsoNormal>In cases where particular types of detectors are placed
1526close to the sample (not the case here) and the diffraction pattern extends to
1527near the edges of the detector, the <b style='mso-bidi-font-weight:normal'><span
1528style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1529mso-hansi-theme-font:minor-latin'>Penetration</span></b> correction may need to
1530be refined. Just select the check box and do <b style='mso-bidi-font-weight:
1531normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1532minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1533mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b>, the result
1534should be &gt;0 for a reasonable correction. Close examination of the outer
1535rings will show a small shift in the calculated rings to better match the
1536observed ones. Assuming that these calibration results will be applied to other
1537images to be later read into the same GSAS-II project, click on <b
1538style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1539mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1540Calibri;mso-bidi-theme-font:minor-latin'>Use as default for all images</span></b>.
1541You may also save a copy of the calibration values to a file <span
1542style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1543mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1544minor-latin'>(<span class=SpellE><i style='mso-bidi-font-style:normal'>name</i><b
1545style='mso-bidi-font-weight:normal'>.imctrl</b></span></span>) with the <b
1546style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1547mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1548Calibri;mso-bidi-theme-font:minor-latin'>Operations/Save Controls</span></b>
1549menu item. To save the project, including the now-derived calibration
1550information, use the <b style='mso-bidi-font-weight:normal'><span
1551style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1552mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1553minor-latin'>File/Save</span> </b><b style='mso-bidi-font-weight:normal'><span
1554style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1555mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1556minor-latin'>Project</span></b><span style='font-family:"Calibri",sans-serif;
1557mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1558Calibri;mso-bidi-theme-font:minor-latin'> </span>menu item associated with the
1559data tree window; as this project has not been saved before the file save
1560dialog will need a file name. Don’t enter the extension; it will be set to “<b
1561style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1562mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1563Calibri;mso-bidi-theme-font:minor-latin'>.<span class=SpellE>gpx</span></span></b>”.</p>
1564
1565<h2>Next step: <span class=MsoHyperlink><span style='color:#0070C0'>Integrate
1566the Data</span></span></h2>
1567
1568</div>
1569
1570</body>
1571
1572</html>
Note: See TracBrowser for help on using the repository browser.