source: Tutorials/2DCalibration/Calibration of an area detector in GSAS.htm @ 1714

Last change on this file since 1714 was 1705, checked in by toby, 9 years ago

load the tutorial web pages
  • Property svn:mime-type set to text/html
File size: 76.4 KB
Line 
1<html xmlns:v="urn:schemas-microsoft-com:vml"
2xmlns:o="urn:schemas-microsoft-com:office:office"
3xmlns:w="urn:schemas-microsoft-com:office:word"
4xmlns:m="http://schemas.microsoft.com/office/2004/12/omml"
5xmlns="http://www.w3.org/TR/REC-html40">
6
7<head>
8<meta http-equiv=Content-Type content="text/html; charset=windows-1252">
9<meta name=ProgId content=Word.Document>
10<meta name=Generator content="Microsoft Word 15">
11<meta name=Originator content="Microsoft Word 15">
12<link rel=File-List
13href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/filelist.xml">
14<link rel=Edit-Time-Data
15href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/editdata.mso">
16<!--[if !mso]>
17<style>
18v\:* {behavior:url(#default#VML);}
19o\:* {behavior:url(#default#VML);}
20w\:* {behavior:url(#default#VML);}
21.shape {behavior:url(#default#VML);}
22</style>
23<![endif]--><!--[if gte mso 9]><xml>
24 <o:DocumentProperties>
25  <o:Author>Von Dreele</o:Author>
26  <o:LastAuthor>Von Dreele</o:LastAuthor>
27  <o:Revision>3</o:Revision>
28  <o:TotalTime>238</o:TotalTime>
29  <o:Created>2014-07-21T14:30:00Z</o:Created>
30  <o:LastSaved>2015-02-13T15:44:00Z</o:LastSaved>
31  <o:Pages>1</o:Pages>
32  <o:Words>1126</o:Words>
33  <o:Characters>6423</o:Characters>
34  <o:Company>Argonne National Laboratory</o:Company>
35  <o:Lines>53</o:Lines>
36  <o:Paragraphs>15</o:Paragraphs>
37  <o:CharactersWithSpaces>7534</o:CharactersWithSpaces>
38  <o:Version>15.00</o:Version>
39 </o:DocumentProperties>
40 <o:OfficeDocumentSettings>
41  <o:AllowPNG/>
42 </o:OfficeDocumentSettings>
43</xml><![endif]-->
44<link rel=themeData
45href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/themedata.thmx">
46<link rel=colorSchemeMapping
47href="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/colorschememapping.xml">
48<!--[if gte mso 9]><xml>
49 <w:WordDocument>
50  <w:SpellingState>Clean</w:SpellingState>
51  <w:GrammarState>Clean</w:GrammarState>
52  <w:TrackMoves>false</w:TrackMoves>
53  <w:TrackFormatting/>
54  <w:PunctuationKerning/>
55  <w:ValidateAgainstSchemas/>
56  <w:SaveIfXMLInvalid>false</w:SaveIfXMLInvalid>
57  <w:IgnoreMixedContent>false</w:IgnoreMixedContent>
58  <w:AlwaysShowPlaceholderText>false</w:AlwaysShowPlaceholderText>
59  <w:DoNotPromoteQF/>
60  <w:LidThemeOther>EN-US</w:LidThemeOther>
61  <w:LidThemeAsian>X-NONE</w:LidThemeAsian>
62  <w:LidThemeComplexScript>X-NONE</w:LidThemeComplexScript>
63  <w:Compatibility>
64   <w:BreakWrappedTables/>
65   <w:SnapToGridInCell/>
66   <w:WrapTextWithPunct/>
67   <w:UseAsianBreakRules/>
68   <w:DontGrowAutofit/>
69   <w:SplitPgBreakAndParaMark/>
70   <w:EnableOpenTypeKerning/>
71   <w:DontFlipMirrorIndents/>
72   <w:OverrideTableStyleHps/>
73  </w:Compatibility>
74  <w:BrowserLevel>MicrosoftInternetExplorer4</w:BrowserLevel>
75  <m:mathPr>
76   <m:mathFont m:val="Cambria Math"/>
77   <m:brkBin m:val="before"/>
78   <m:brkBinSub m:val="&#45;-"/>
79   <m:smallFrac m:val="off"/>
80   <m:dispDef/>
81   <m:lMargin m:val="0"/>
82   <m:rMargin m:val="0"/>
83   <m:defJc m:val="centerGroup"/>
84   <m:wrapIndent m:val="1440"/>
85   <m:intLim m:val="subSup"/>
86   <m:naryLim m:val="undOvr"/>
87  </m:mathPr></w:WordDocument>
88</xml><![endif]--><!--[if gte mso 9]><xml>
89 <w:LatentStyles DefLockedState="false" DefUnhideWhenUsed="false"
90  DefSemiHidden="false" DefQFormat="false" DefPriority="99"
91  LatentStyleCount="371">
92  <w:LsdException Locked="false" Priority="0" QFormat="true" Name="Normal"/>
93  <w:LsdException Locked="false" Priority="9" QFormat="true" Name="heading 1"/>
94  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
95   UnhideWhenUsed="true" QFormat="true" Name="heading 2"/>
96  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
97   UnhideWhenUsed="true" QFormat="true" Name="heading 3"/>
98  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
99   UnhideWhenUsed="true" QFormat="true" Name="heading 4"/>
100  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
101   UnhideWhenUsed="true" QFormat="true" Name="heading 5"/>
102  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
103   UnhideWhenUsed="true" QFormat="true" Name="heading 6"/>
104  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
105   UnhideWhenUsed="true" QFormat="true" Name="heading 7"/>
106  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
107   UnhideWhenUsed="true" QFormat="true" Name="heading 8"/>
108  <w:LsdException Locked="false" Priority="9" SemiHidden="true"
109   UnhideWhenUsed="true" QFormat="true" Name="heading 9"/>
110  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
111   Name="index 1"/>
112  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
113   Name="index 2"/>
114  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
115   Name="index 3"/>
116  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
117   Name="index 4"/>
118  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
119   Name="index 5"/>
120  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
121   Name="index 6"/>
122  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
123   Name="index 7"/>
124  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
125   Name="index 8"/>
126  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
127   Name="index 9"/>
128  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
129   UnhideWhenUsed="true" Name="toc 1"/>
130  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
131   UnhideWhenUsed="true" Name="toc 2"/>
132  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
133   UnhideWhenUsed="true" Name="toc 3"/>
134  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
135   UnhideWhenUsed="true" Name="toc 4"/>
136  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
137   UnhideWhenUsed="true" Name="toc 5"/>
138  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
139   UnhideWhenUsed="true" Name="toc 6"/>
140  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
141   UnhideWhenUsed="true" Name="toc 7"/>
142  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
143   UnhideWhenUsed="true" Name="toc 8"/>
144  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
145   UnhideWhenUsed="true" Name="toc 9"/>
146  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
147   Name="Normal Indent"/>
148  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
149   Name="footnote text"/>
150  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
151   Name="annotation text"/>
152  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
153   Name="header"/>
154  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
155   Name="footer"/>
156  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
157   Name="index heading"/>
158  <w:LsdException Locked="false" Priority="35" SemiHidden="true"
159   UnhideWhenUsed="true" QFormat="true" Name="caption"/>
160  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
161   Name="table of figures"/>
162  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
163   Name="envelope address"/>
164  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
165   Name="envelope return"/>
166  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
167   Name="footnote reference"/>
168  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
169   Name="annotation reference"/>
170  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
171   Name="line number"/>
172  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
173   Name="page number"/>
174  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
175   Name="endnote reference"/>
176  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
177   Name="endnote text"/>
178  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
179   Name="table of authorities"/>
180  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
181   Name="macro"/>
182  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
183   Name="toa heading"/>
184  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
185   Name="List"/>
186  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
187   Name="List Bullet"/>
188  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
189   Name="List Number"/>
190  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
191   Name="List 2"/>
192  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
193   Name="List 3"/>
194  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
195   Name="List 4"/>
196  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
197   Name="List 5"/>
198  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
199   Name="List Bullet 2"/>
200  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
201   Name="List Bullet 3"/>
202  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
203   Name="List Bullet 4"/>
204  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
205   Name="List Bullet 5"/>
206  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
207   Name="List Number 2"/>
208  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
209   Name="List Number 3"/>
210  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
211   Name="List Number 4"/>
212  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
213   Name="List Number 5"/>
214  <w:LsdException Locked="false" Priority="10" QFormat="true" Name="Title"/>
215  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
216   Name="Closing"/>
217  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
218   Name="Signature"/>
219  <w:LsdException Locked="false" Priority="1" SemiHidden="true"
220   UnhideWhenUsed="true" Name="Default Paragraph Font"/>
221  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
222   Name="Body Text"/>
223  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
224   Name="Body Text Indent"/>
225  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
226   Name="List Continue"/>
227  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
228   Name="List Continue 2"/>
229  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
230   Name="List Continue 3"/>
231  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
232   Name="List Continue 4"/>
233  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
234   Name="List Continue 5"/>
235  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
236   Name="Message Header"/>
237  <w:LsdException Locked="false" Priority="11" QFormat="true" Name="Subtitle"/>
238  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
239   Name="Salutation"/>
240  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
241   Name="Date"/>
242  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
243   Name="Body Text First Indent"/>
244  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
245   Name="Body Text First Indent 2"/>
246  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
247   Name="Note Heading"/>
248  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
249   Name="Body Text 2"/>
250  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
251   Name="Body Text 3"/>
252  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
253   Name="Body Text Indent 2"/>
254  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
255   Name="Body Text Indent 3"/>
256  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
257   Name="Block Text"/>
258  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
259   Name="Hyperlink"/>
260  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
261   Name="FollowedHyperlink"/>
262  <w:LsdException Locked="false" Priority="22" QFormat="true" Name="Strong"/>
263  <w:LsdException Locked="false" Priority="20" QFormat="true" Name="Emphasis"/>
264  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
265   Name="Document Map"/>
266  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
267   Name="Plain Text"/>
268  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
269   Name="E-mail Signature"/>
270  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
271   Name="HTML Top of Form"/>
272  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
273   Name="HTML Bottom of Form"/>
274  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
275   Name="Normal (Web)"/>
276  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
277   Name="HTML Acronym"/>
278  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
279   Name="HTML Address"/>
280  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
281   Name="HTML Cite"/>
282  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
283   Name="HTML Code"/>
284  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
285   Name="HTML Definition"/>
286  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
287   Name="HTML Keyboard"/>
288  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
289   Name="HTML Preformatted"/>
290  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
291   Name="HTML Sample"/>
292  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
293   Name="HTML Typewriter"/>
294  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
295   Name="HTML Variable"/>
296  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
297   Name="Normal Table"/>
298  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
299   Name="annotation subject"/>
300  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
301   Name="No List"/>
302  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
303   Name="Outline List 1"/>
304  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
305   Name="Outline List 2"/>
306  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
307   Name="Outline List 3"/>
308  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
309   Name="Table Simple 1"/>
310  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
311   Name="Table Simple 2"/>
312  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
313   Name="Table Simple 3"/>
314  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
315   Name="Table Classic 1"/>
316  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
317   Name="Table Classic 2"/>
318  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
319   Name="Table Classic 3"/>
320  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
321   Name="Table Classic 4"/>
322  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
323   Name="Table Colorful 1"/>
324  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
325   Name="Table Colorful 2"/>
326  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
327   Name="Table Colorful 3"/>
328  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
329   Name="Table Columns 1"/>
330  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
331   Name="Table Columns 2"/>
332  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
333   Name="Table Columns 3"/>
334  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
335   Name="Table Columns 4"/>
336  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
337   Name="Table Columns 5"/>
338  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
339   Name="Table Grid 1"/>
340  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
341   Name="Table Grid 2"/>
342  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
343   Name="Table Grid 3"/>
344  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
345   Name="Table Grid 4"/>
346  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
347   Name="Table Grid 5"/>
348  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
349   Name="Table Grid 6"/>
350  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
351   Name="Table Grid 7"/>
352  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
353   Name="Table Grid 8"/>
354  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
355   Name="Table List 1"/>
356  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
357   Name="Table List 2"/>
358  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
359   Name="Table List 3"/>
360  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
361   Name="Table List 4"/>
362  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
363   Name="Table List 5"/>
364  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
365   Name="Table List 6"/>
366  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
367   Name="Table List 7"/>
368  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
369   Name="Table List 8"/>
370  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
371   Name="Table 3D effects 1"/>
372  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
373   Name="Table 3D effects 2"/>
374  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
375   Name="Table 3D effects 3"/>
376  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
377   Name="Table Contemporary"/>
378  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
379   Name="Table Elegant"/>
380  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
381   Name="Table Professional"/>
382  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
383   Name="Table Subtle 1"/>
384  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
385   Name="Table Subtle 2"/>
386  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
387   Name="Table Web 1"/>
388  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
389   Name="Table Web 2"/>
390  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
391   Name="Table Web 3"/>
392  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
393   Name="Balloon Text"/>
394  <w:LsdException Locked="false" Priority="59" Name="Table Grid"/>
395  <w:LsdException Locked="false" SemiHidden="true" UnhideWhenUsed="true"
396   Name="Table Theme"/>
397  <w:LsdException Locked="false" SemiHidden="true" Name="Placeholder Text"/>
398  <w:LsdException Locked="false" Priority="1" QFormat="true" Name="No Spacing"/>
399  <w:LsdException Locked="false" Priority="60" Name="Light Shading"/>
400  <w:LsdException Locked="false" Priority="61" Name="Light List"/>
401  <w:LsdException Locked="false" Priority="62" Name="Light Grid"/>
402  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1"/>
403  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2"/>
404  <w:LsdException Locked="false" Priority="65" Name="Medium List 1"/>
405  <w:LsdException Locked="false" Priority="66" Name="Medium List 2"/>
406  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1"/>
407  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2"/>
408  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3"/>
409  <w:LsdException Locked="false" Priority="70" Name="Dark List"/>
410  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading"/>
411  <w:LsdException Locked="false" Priority="72" Name="Colorful List"/>
412  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid"/>
413  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
414  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
415  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
416  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
417  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
418  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
419  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
420  <w:LsdException Locked="false" Priority="34" QFormat="true"
421   Name="List Paragraph"/>
422  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
423  <w:LsdException Locked="false" Priority="30" QFormat="true"
424   Name="Intense Quote"/>
425  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 1"/>
426  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
427  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
428  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
429  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
430  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
431  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
432  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
433  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
434  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
435  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
436  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
437  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
438  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
439  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
440  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
441  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
442  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
443  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
444  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
445  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
446  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
447  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
448  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
449  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
450  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
451  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
452  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
453  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
454  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
455  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
456  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
457  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
458  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
459  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
460  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
461  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
462  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
463  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
464  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
465  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
466  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
467  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
468  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
469  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
470  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
471  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
472  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
473  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
474  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
475  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
476  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
477  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
478  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
479  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
480  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
481  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
482  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
483  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
484  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
485  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
486  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
487  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
488  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
489  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
490  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
491  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
492  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
493  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
494  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
495  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
496  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
497  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
498  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
499  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
500  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
501  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
502  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
503  <w:LsdException Locked="false" Priority="19" QFormat="true"
504   Name="Subtle Emphasis"/>
505  <w:LsdException Locked="false" Priority="21" QFormat="true"
506   Name="Intense Emphasis"/>
507  <w:LsdException Locked="false" Priority="31" QFormat="true"
508   Name="Subtle Reference"/>
509  <w:LsdException Locked="false" Priority="32" QFormat="true"
510   Name="Intense Reference"/>
511  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
512  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
513   UnhideWhenUsed="true" Name="Bibliography"/>
514  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
515   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
516  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
517  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
518  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
519  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
520  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
521  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
522  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
523  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
524  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
525  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
526  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
527  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
528  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
529  <w:LsdException Locked="false" Priority="46"
530   Name="Grid Table 1 Light Accent 1"/>
531  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
532  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
533  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
534  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
535  <w:LsdException Locked="false" Priority="51"
536   Name="Grid Table 6 Colorful Accent 1"/>
537  <w:LsdException Locked="false" Priority="52"
538   Name="Grid Table 7 Colorful Accent 1"/>
539  <w:LsdException Locked="false" Priority="46"
540   Name="Grid Table 1 Light Accent 2"/>
541  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
542  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
543  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
544  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
545  <w:LsdException Locked="false" Priority="51"
546   Name="Grid Table 6 Colorful Accent 2"/>
547  <w:LsdException Locked="false" Priority="52"
548   Name="Grid Table 7 Colorful Accent 2"/>
549  <w:LsdException Locked="false" Priority="46"
550   Name="Grid Table 1 Light Accent 3"/>
551  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
552  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
553  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
554  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
555  <w:LsdException Locked="false" Priority="51"
556   Name="Grid Table 6 Colorful Accent 3"/>
557  <w:LsdException Locked="false" Priority="52"
558   Name="Grid Table 7 Colorful Accent 3"/>
559  <w:LsdException Locked="false" Priority="46"
560   Name="Grid Table 1 Light Accent 4"/>
561  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
562  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
563  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 4"/>
564  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
565  <w:LsdException Locked="false" Priority="51"
566   Name="Grid Table 6 Colorful Accent 4"/>
567  <w:LsdException Locked="false" Priority="52"
568   Name="Grid Table 7 Colorful Accent 4"/>
569  <w:LsdException Locked="false" Priority="46"
570   Name="Grid Table 1 Light Accent 5"/>
571  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
572  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
573  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
574  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
575  <w:LsdException Locked="false" Priority="51"
576   Name="Grid Table 6 Colorful Accent 5"/>
577  <w:LsdException Locked="false" Priority="52"
578   Name="Grid Table 7 Colorful Accent 5"/>
579  <w:LsdException Locked="false" Priority="46"
580   Name="Grid Table 1 Light Accent 6"/>
581  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
582  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
583  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
584  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
585  <w:LsdException Locked="false" Priority="51"
586   Name="Grid Table 6 Colorful Accent 6"/>
587  <w:LsdException Locked="false" Priority="52"
588   Name="Grid Table 7 Colorful Accent 6"/>
589  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
590  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
591  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
592  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
593  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
594  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
595  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
596  <w:LsdException Locked="false" Priority="46"
597   Name="List Table 1 Light Accent 1"/>
598  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
599  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
600  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
601  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
602  <w:LsdException Locked="false" Priority="51"
603   Name="List Table 6 Colorful Accent 1"/>
604  <w:LsdException Locked="false" Priority="52"
605   Name="List Table 7 Colorful Accent 1"/>
606  <w:LsdException Locked="false" Priority="46"
607   Name="List Table 1 Light Accent 2"/>
608  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
609  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
610  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
611  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
612  <w:LsdException Locked="false" Priority="51"
613   Name="List Table 6 Colorful Accent 2"/>
614  <w:LsdException Locked="false" Priority="52"
615   Name="List Table 7 Colorful Accent 2"/>
616  <w:LsdException Locked="false" Priority="46"
617   Name="List Table 1 Light Accent 3"/>
618  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
619  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
620  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
621  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
622  <w:LsdException Locked="false" Priority="51"
623   Name="List Table 6 Colorful Accent 3"/>
624  <w:LsdException Locked="false" Priority="52"
625   Name="List Table 7 Colorful Accent 3"/>
626  <w:LsdException Locked="false" Priority="46"
627   Name="List Table 1 Light Accent 4"/>
628  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
629  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
630  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
631  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
632  <w:LsdException Locked="false" Priority="51"
633   Name="List Table 6 Colorful Accent 4"/>
634  <w:LsdException Locked="false" Priority="52"
635   Name="List Table 7 Colorful Accent 4"/>
636  <w:LsdException Locked="false" Priority="46"
637   Name="List Table 1 Light Accent 5"/>
638  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
639  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
640  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
641  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
642  <w:LsdException Locked="false" Priority="51"
643   Name="List Table 6 Colorful Accent 5"/>
644  <w:LsdException Locked="false" Priority="52"
645   Name="List Table 7 Colorful Accent 5"/>
646  <w:LsdException Locked="false" Priority="46"
647   Name="List Table 1 Light Accent 6"/>
648  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
649  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
650  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
651  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
652  <w:LsdException Locked="false" Priority="51"
653   Name="List Table 6 Colorful Accent 6"/>
654  <w:LsdException Locked="false" Priority="52"
655   Name="List Table 7 Colorful Accent 6"/>
656 </w:LatentStyles>
657</xml><![endif]-->
658<style>
659<!--
660 /* Font Definitions */
661 @font-face
662        {font-family:"Cambria Math";
663        panose-1:2 4 5 3 5 4 6 3 2 4;
664        mso-font-charset:1;
665        mso-generic-font-family:roman;
666        mso-font-format:other;
667        mso-font-pitch:variable;
668        mso-font-signature:0 0 0 0 0 0;}
669@font-face
670        {font-family:Calibri;
671        panose-1:2 15 5 2 2 2 4 3 2 4;
672        mso-font-charset:0;
673        mso-generic-font-family:swiss;
674        mso-font-pitch:variable;
675        mso-font-signature:-536870145 1073786111 1 0 415 0;}
676@font-face
677        {font-family:Tahoma;
678        panose-1:2 11 6 4 3 5 4 4 2 4;
679        mso-font-charset:0;
680        mso-generic-font-family:swiss;
681        mso-font-pitch:variable;
682        mso-font-signature:-520081665 -1073717157 41 0 66047 0;}
683 /* Style Definitions */
684 p.MsoNormal, li.MsoNormal, div.MsoNormal
685        {mso-style-unhide:no;
686        mso-style-qformat:yes;
687        mso-style-parent:"";
688        margin:0in;
689        margin-bottom:.0001pt;
690        mso-pagination:widow-orphan;
691        font-size:12.0pt;
692        font-family:"Times New Roman",serif;
693        mso-fareast-font-family:"Times New Roman";
694        mso-fareast-theme-font:minor-fareast;}
695h1
696        {mso-style-priority:9;
697        mso-style-unhide:no;
698        mso-style-qformat:yes;
699        mso-style-link:"Heading 1 Char";
700        mso-margin-top-alt:auto;
701        margin-right:0in;
702        mso-margin-bottom-alt:auto;
703        margin-left:0in;
704        mso-pagination:widow-orphan;
705        mso-outline-level:1;
706        font-size:24.0pt;
707        font-family:"Times New Roman",serif;
708        mso-fareast-font-family:"Times New Roman";
709        mso-fareast-theme-font:minor-fareast;
710        font-weight:bold;}
711h2
712        {mso-style-noshow:yes;
713        mso-style-priority:9;
714        mso-style-qformat:yes;
715        mso-style-link:"Heading 2 Char";
716        mso-margin-top-alt:auto;
717        margin-right:0in;
718        mso-margin-bottom-alt:auto;
719        margin-left:0in;
720        mso-pagination:widow-orphan;
721        mso-outline-level:2;
722        font-size:18.0pt;
723        font-family:"Times New Roman",serif;
724        mso-fareast-font-family:"Times New Roman";
725        mso-fareast-theme-font:minor-fareast;
726        font-weight:bold;}
727h3
728        {mso-style-noshow:yes;
729        mso-style-priority:9;
730        mso-style-qformat:yes;
731        mso-style-link:"Heading 3 Char";
732        mso-margin-top-alt:auto;
733        margin-right:0in;
734        mso-margin-bottom-alt:auto;
735        margin-left:0in;
736        mso-pagination:widow-orphan;
737        mso-outline-level:3;
738        font-size:13.5pt;
739        font-family:"Times New Roman",serif;
740        mso-fareast-font-family:"Times New Roman";
741        mso-fareast-theme-font:minor-fareast;
742        font-weight:bold;}
743h4
744        {mso-style-noshow:yes;
745        mso-style-priority:9;
746        mso-style-qformat:yes;
747        mso-style-link:"Heading 4 Char";
748        mso-style-next:Normal;
749        margin-top:10.0pt;
750        margin-right:0in;
751        margin-bottom:0in;
752        margin-left:0in;
753        margin-bottom:.0001pt;
754        mso-pagination:widow-orphan lines-together;
755        page-break-after:avoid;
756        mso-outline-level:4;
757        font-size:13.0pt;
758        font-family:"Cambria",serif;
759        mso-ascii-font-family:Cambria;
760        mso-ascii-theme-font:major-latin;
761        mso-fareast-font-family:"Times New Roman";
762        mso-fareast-theme-font:major-fareast;
763        mso-hansi-font-family:Cambria;
764        mso-hansi-theme-font:major-latin;
765        mso-bidi-font-family:"Times New Roman";
766        mso-bidi-theme-font:major-bidi;
767        color:#4F81BD;
768        mso-themecolor:accent1;
769        font-weight:bold;
770        font-style:italic;}
771h5
772        {mso-style-noshow:yes;
773        mso-style-priority:9;
774        mso-style-qformat:yes;
775        mso-style-link:"Heading 5 Char";
776        mso-margin-top-alt:auto;
777        margin-right:0in;
778        mso-margin-bottom-alt:auto;
779        margin-left:0in;
780        mso-pagination:widow-orphan;
781        mso-outline-level:5;
782        font-size:12.0pt;
783        font-family:"Times New Roman",serif;
784        mso-fareast-font-family:"Times New Roman";
785        mso-fareast-theme-font:minor-fareast;
786        color:#4F4FFF;
787        font-weight:bold;}
788a:visited, span.MsoHyperlinkFollowed
789        {mso-style-noshow:yes;
790        mso-style-priority:99;
791        color:purple;
792        text-decoration:underline;
793        text-underline:single;}
794p.MsoDocumentMap, li.MsoDocumentMap, div.MsoDocumentMap
795        {mso-style-noshow:yes;
796        mso-style-priority:99;
797        mso-style-link:"Document Map Char";
798        margin:0in;
799        margin-bottom:.0001pt;
800        mso-pagination:widow-orphan;
801        font-size:8.0pt;
802        font-family:"Tahoma",sans-serif;
803        mso-fareast-font-family:"Times New Roman";
804        mso-fareast-theme-font:minor-fareast;}
805p
806        {mso-style-noshow:yes;
807        mso-style-priority:99;
808        mso-margin-top-alt:auto;
809        margin-right:0in;
810        mso-margin-bottom-alt:auto;
811        margin-left:0in;
812        mso-pagination:widow-orphan;
813        font-size:12.0pt;
814        font-family:"Times New Roman",serif;
815        mso-fareast-font-family:"Times New Roman";
816        mso-fareast-theme-font:minor-fareast;}
817pre
818        {mso-style-noshow:yes;
819        mso-style-priority:99;
820        mso-style-link:"HTML Preformatted Char";
821        margin:0in;
822        margin-bottom:.0001pt;
823        mso-pagination:widow-orphan;
824        tab-stops:45.8pt 91.6pt 137.4pt 183.2pt 229.0pt 274.8pt 320.6pt 366.4pt 412.2pt 458.0pt 503.8pt 549.6pt 595.4pt 641.2pt 687.0pt 732.8pt;
825        font-size:10.0pt;
826        font-family:"Courier New";
827        mso-fareast-font-family:"Times New Roman";}
828p.MsoAcetate, li.MsoAcetate, div.MsoAcetate
829        {mso-style-noshow:yes;
830        mso-style-priority:99;
831        mso-style-link:"Balloon Text Char";
832        margin:0in;
833        margin-bottom:.0001pt;
834        mso-pagination:widow-orphan;
835        font-size:8.0pt;
836        font-family:"Tahoma",sans-serif;
837        mso-fareast-font-family:"Times New Roman";
838        mso-fareast-theme-font:minor-fareast;}
839span.MsoPlaceholderText
840        {mso-style-noshow:yes;
841        mso-style-priority:99;
842        mso-style-unhide:no;
843        color:gray;}
844p.MsoNoSpacing, li.MsoNoSpacing, div.MsoNoSpacing
845        {mso-style-noshow:yes;
846        mso-style-priority:1;
847        mso-style-unhide:no;
848        mso-style-qformat:yes;
849        mso-style-parent:"";
850        margin:0in;
851        margin-bottom:.0001pt;
852        mso-pagination:widow-orphan;
853        font-size:12.0pt;
854        font-family:"Times New Roman",serif;
855        mso-fareast-font-family:"Times New Roman";
856        mso-fareast-theme-font:minor-fareast;}
857p.MsoListParagraph, li.MsoListParagraph, div.MsoListParagraph
858        {mso-style-noshow:yes;
859        mso-style-priority:34;
860        mso-style-unhide:no;
861        mso-style-qformat:yes;
862        margin-top:0in;
863        margin-right:0in;
864        margin-bottom:0in;
865        margin-left:.5in;
866        margin-bottom:.0001pt;
867        mso-add-space:auto;
868        mso-pagination:widow-orphan;
869        font-size:12.0pt;
870        font-family:"Times New Roman",serif;
871        mso-fareast-font-family:"Times New Roman";
872        mso-fareast-theme-font:minor-fareast;}
873p.MsoListParagraphCxSpFirst, li.MsoListParagraphCxSpFirst, div.MsoListParagraphCxSpFirst
874        {mso-style-noshow:yes;
875        mso-style-priority:34;
876        mso-style-unhide:no;
877        mso-style-qformat:yes;
878        mso-style-type:export-only;
879        margin-top:0in;
880        margin-right:0in;
881        margin-bottom:0in;
882        margin-left:.5in;
883        margin-bottom:.0001pt;
884        mso-add-space:auto;
885        mso-pagination:widow-orphan;
886        font-size:12.0pt;
887        font-family:"Times New Roman",serif;
888        mso-fareast-font-family:"Times New Roman";
889        mso-fareast-theme-font:minor-fareast;}
890p.MsoListParagraphCxSpMiddle, li.MsoListParagraphCxSpMiddle, div.MsoListParagraphCxSpMiddle
891        {mso-style-noshow:yes;
892        mso-style-priority:34;
893        mso-style-unhide:no;
894        mso-style-qformat:yes;
895        mso-style-type:export-only;
896        margin-top:0in;
897        margin-right:0in;
898        margin-bottom:0in;
899        margin-left:.5in;
900        margin-bottom:.0001pt;
901        mso-add-space:auto;
902        mso-pagination:widow-orphan;
903        font-size:12.0pt;
904        font-family:"Times New Roman",serif;
905        mso-fareast-font-family:"Times New Roman";
906        mso-fareast-theme-font:minor-fareast;}
907p.MsoListParagraphCxSpLast, li.MsoListParagraphCxSpLast, div.MsoListParagraphCxSpLast
908        {mso-style-noshow:yes;
909        mso-style-priority:34;
910        mso-style-unhide:no;
911        mso-style-qformat:yes;
912        mso-style-type:export-only;
913        margin-top:0in;
914        margin-right:0in;
915        margin-bottom:0in;
916        margin-left:.5in;
917        margin-bottom:.0001pt;
918        mso-add-space:auto;
919        mso-pagination:widow-orphan;
920        font-size:12.0pt;
921        font-family:"Times New Roman",serif;
922        mso-fareast-font-family:"Times New Roman";
923        mso-fareast-theme-font:minor-fareast;}
924span.MsoIntenseReference
925        {mso-style-priority:32;
926        mso-style-unhide:no;
927        mso-style-qformat:yes;
928        font-variant:small-caps;
929        color:#C0504D;
930        mso-themecolor:accent2;
931        letter-spacing:.25pt;
932        font-weight:bold;
933        text-decoration:underline;
934        text-underline:single;}
935span.Heading1Char
936        {mso-style-name:"Heading 1 Char";
937        mso-style-priority:9;
938        mso-style-unhide:no;
939        mso-style-locked:yes;
940        mso-style-link:"Heading 1";
941        mso-ansi-font-size:24.0pt;
942        mso-bidi-font-size:24.0pt;
943        font-family:"Times New Roman",serif;
944        mso-ascii-font-family:"Times New Roman";
945        mso-fareast-font-family:"Times New Roman";
946        mso-fareast-theme-font:minor-fareast;
947        mso-hansi-font-family:"Times New Roman";
948        mso-bidi-font-family:"Times New Roman";
949        mso-font-kerning:18.0pt;
950        font-weight:bold;}
951span.Heading2Char
952        {mso-style-name:"Heading 2 Char";
953        mso-style-noshow:yes;
954        mso-style-priority:9;
955        mso-style-unhide:no;
956        mso-style-locked:yes;
957        mso-style-link:"Heading 2";
958        mso-ansi-font-size:18.0pt;
959        mso-bidi-font-size:18.0pt;
960        font-family:"Times New Roman",serif;
961        mso-ascii-font-family:"Times New Roman";
962        mso-fareast-font-family:"Times New Roman";
963        mso-fareast-theme-font:minor-fareast;
964        mso-hansi-font-family:"Times New Roman";
965        mso-bidi-font-family:"Times New Roman";
966        font-weight:bold;}
967span.Heading3Char
968        {mso-style-name:"Heading 3 Char";
969        mso-style-noshow:yes;
970        mso-style-priority:9;
971        mso-style-unhide:no;
972        mso-style-locked:yes;
973        mso-style-link:"Heading 3";
974        mso-ansi-font-size:13.5pt;
975        mso-bidi-font-size:13.5pt;
976        font-family:"Times New Roman",serif;
977        mso-ascii-font-family:"Times New Roman";
978        mso-fareast-font-family:"Times New Roman";
979        mso-fareast-theme-font:minor-fareast;
980        mso-hansi-font-family:"Times New Roman";
981        mso-bidi-font-family:"Times New Roman";
982        font-weight:bold;}
983span.Heading4Char
984        {mso-style-name:"Heading 4 Char";
985        mso-style-noshow:yes;
986        mso-style-priority:9;
987        mso-style-unhide:no;
988        mso-style-locked:yes;
989        mso-style-link:"Heading 4";
990        mso-ansi-font-size:13.0pt;
991        mso-bidi-font-size:13.0pt;
992        font-family:"Cambria",serif;
993        mso-ascii-font-family:Cambria;
994        mso-ascii-theme-font:major-latin;
995        mso-fareast-font-family:"Times New Roman";
996        mso-fareast-theme-font:major-fareast;
997        mso-hansi-font-family:Cambria;
998        mso-hansi-theme-font:major-latin;
999        mso-bidi-font-family:"Times New Roman";
1000        mso-bidi-theme-font:major-bidi;
1001        color:#4F81BD;
1002        mso-themecolor:accent1;
1003        font-weight:bold;
1004        font-style:italic;}
1005span.Heading5Char
1006        {mso-style-name:"Heading 5 Char";
1007        mso-style-noshow:yes;
1008        mso-style-priority:9;
1009        mso-style-unhide:no;
1010        mso-style-locked:yes;
1011        mso-style-link:"Heading 5";
1012        mso-ansi-font-size:12.0pt;
1013        mso-bidi-font-size:12.0pt;
1014        font-family:"Times New Roman",serif;
1015        mso-ascii-font-family:"Times New Roman";
1016        mso-fareast-font-family:"Times New Roman";
1017        mso-fareast-theme-font:minor-fareast;
1018        mso-hansi-font-family:"Times New Roman";
1019        mso-bidi-font-family:"Times New Roman";
1020        color:#4F4FFF;
1021        font-weight:bold;}
1022span.HTMLPreformattedChar
1023        {mso-style-name:"HTML Preformatted Char";
1024        mso-style-noshow:yes;
1025        mso-style-priority:99;
1026        mso-style-unhide:no;
1027        mso-style-locked:yes;
1028        mso-style-link:"HTML Preformatted";
1029        font-family:"Courier New";
1030        mso-ascii-font-family:"Courier New";
1031        mso-fareast-font-family:"Times New Roman";
1032        mso-hansi-font-family:"Courier New";
1033        mso-bidi-font-family:"Courier New";}
1034span.DocumentMapChar
1035        {mso-style-name:"Document Map Char";
1036        mso-style-noshow:yes;
1037        mso-style-priority:99;
1038        mso-style-unhide:no;
1039        mso-style-locked:yes;
1040        mso-style-link:"Document Map";
1041        mso-ansi-font-size:8.0pt;
1042        mso-bidi-font-size:8.0pt;
1043        font-family:"Tahoma",sans-serif;
1044        mso-ascii-font-family:Tahoma;
1045        mso-fareast-font-family:"Times New Roman";
1046        mso-fareast-theme-font:minor-fareast;
1047        mso-hansi-font-family:Tahoma;
1048        mso-bidi-font-family:Tahoma;}
1049span.BalloonTextChar
1050        {mso-style-name:"Balloon Text Char";
1051        mso-style-noshow:yes;
1052        mso-style-priority:99;
1053        mso-style-unhide:no;
1054        mso-style-locked:yes;
1055        mso-style-link:"Balloon Text";
1056        mso-ansi-font-size:8.0pt;
1057        mso-bidi-font-size:8.0pt;
1058        font-family:"Tahoma",sans-serif;
1059        mso-ascii-font-family:Tahoma;
1060        mso-fareast-font-family:"Times New Roman";
1061        mso-fareast-theme-font:minor-fareast;
1062        mso-hansi-font-family:Tahoma;
1063        mso-bidi-font-family:Tahoma;}
1064span.SpellE
1065        {mso-style-name:"";
1066        mso-spl-e:yes;}
1067span.GramE
1068        {mso-style-name:"";
1069        mso-gram-e:yes;}
1070.MsoChpDefault
1071        {mso-style-type:export-only;
1072        mso-default-props:yes;
1073        font-size:10.0pt;
1074        mso-ansi-font-size:10.0pt;
1075        mso-bidi-font-size:10.0pt;
1076        font-family:"Calibri",sans-serif;
1077        mso-ascii-font-family:Calibri;
1078        mso-ascii-theme-font:minor-latin;
1079        mso-fareast-font-family:Calibri;
1080        mso-fareast-theme-font:minor-latin;
1081        mso-hansi-font-family:Calibri;
1082        mso-hansi-theme-font:minor-latin;
1083        mso-bidi-font-family:"Times New Roman";
1084        mso-bidi-theme-font:minor-bidi;}
1085@page WordSection1
1086        {size:8.5in 11.0in;
1087        margin:1.0in 1.0in 1.0in 1.0in;
1088        mso-header-margin:.5in;
1089        mso-footer-margin:.5in;
1090        mso-paper-source:0;}
1091div.WordSection1
1092        {page:WordSection1;}
1093-->
1094</style>
1095<!--[if gte mso 10]>
1096<style>
1097 /* Style Definitions */
1098 table.MsoNormalTable
1099        {mso-style-name:"Table Normal";
1100        mso-tstyle-rowband-size:0;
1101        mso-tstyle-colband-size:0;
1102        mso-style-noshow:yes;
1103        mso-style-priority:99;
1104        mso-style-parent:"";
1105        mso-padding-alt:0in 5.4pt 0in 5.4pt;
1106        mso-para-margin:0in;
1107        mso-para-margin-bottom:.0001pt;
1108        mso-pagination:widow-orphan;
1109        font-size:10.0pt;
1110        font-family:"Calibri",sans-serif;
1111        mso-ascii-font-family:Calibri;
1112        mso-ascii-theme-font:minor-latin;
1113        mso-hansi-font-family:Calibri;
1114        mso-hansi-theme-font:minor-latin;}
1115</style>
1116<![endif]--><!--[if gte mso 9]><xml>
1117 <o:shapedefaults v:ext="edit" spidmax="1026"/>
1118</xml><![endif]--><!--[if gte mso 9]><xml>
1119 <o:shapelayout v:ext="edit">
1120  <o:idmap v:ext="edit" data="1"/>
1121 </o:shapelayout></xml><![endif]-->
1122</head>
1123
1124<body lang=EN-US link="#000000" vlink=purple style='tab-interval:.5in'>
1125
1126<div class=WordSection1>
1127
1128<p class=MsoNormal><span class=Heading1Char><span style='font-size:24.0pt'>Calibration
1129of an area detector in GSAS-II</span></span><b><span style='font-size:14.0pt;
1130color:#365F91;mso-themecolor:accent1;mso-themeshade:191'><o:p></o:p></span></b></p>
1131
1132<p class=MsoNormal>In this tutorial, data collected with a Perkin-Elmer area
1133detector at APS 11-ID-C with a wavelength 0.10798 A, where the detector was intentionally
1134tilted at 45 degrees, are used. Note that menu entries are listed in bold face
1135below as <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1136mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1137Calibri;mso-bidi-theme-font:minor-latin'>Help/About GSAS-II</span></b>, which
1138lists first the name of the menu (here <b style='mso-bidi-font-weight:normal'><span
1139style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1140mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1141minor-latin'>Help</span></b>) and second the name of the entry in the menu
1142(here <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1143mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1144Calibri;mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).</p>
1145
1146<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
1147href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
1148text-underline:none'>start GSAS-II</span></a></span></u>.</p>
1149
1150<h1>Step 1: read in the data file</h1>
1151
1152<p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the <b
1153style='mso-bidi-font-weight:normal'>Data/Read image data</b> menu item to read
1154the data file into the current GSAS-II project. </p>
1155
1156<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
1157
1158<p class=MsoNormal>A file selection dialog will be shown; its appearance will depend
1159on your OS. Change the search directory to <b style='mso-bidi-font-weight:normal'><span
1160style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1161mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1162minor-latin'>/Exercises/images</span></b> and then select the file </p>
1163
1164<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
1165style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1166mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1167minor-latin'>La_hex_+45deg-00015.tif</span></b> and press <b style='mso-bidi-font-weight:
1168normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1169minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1170mso-bidi-theme-font:minor-latin'>Open</span></b>.<span style='mso-no-proof:
1171yes'> <o:p></o:p></span></p>
1172
1173<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shapetype
1174 id="_x0000_t75" coordsize="21600,21600" o:spt="75" o:preferrelative="t"
1175 path="m@4@5l@4@11@9@11@9@5xe" filled="f" stroked="f">
1176 <v:stroke joinstyle="miter"/>
1177 <v:formulas>
1178  <v:f eqn="if lineDrawn pixelLineWidth 0"/>
1179  <v:f eqn="sum @0 1 0"/>
1180  <v:f eqn="sum 0 0 @1"/>
1181  <v:f eqn="prod @2 1 2"/>
1182  <v:f eqn="prod @3 21600 pixelWidth"/>
1183  <v:f eqn="prod @3 21600 pixelHeight"/>
1184  <v:f eqn="sum @0 0 1"/>
1185  <v:f eqn="prod @6 1 2"/>
1186  <v:f eqn="prod @7 21600 pixelWidth"/>
1187  <v:f eqn="sum @8 21600 0"/>
1188  <v:f eqn="prod @7 21600 pixelHeight"/>
1189  <v:f eqn="sum @10 21600 0"/>
1190 </v:formulas>
1191 <v:path o:extrusionok="f" gradientshapeok="t" o:connecttype="rect"/>
1192 <o:lock v:ext="edit" aspectratio="t"/>
1193</v:shapetype><v:shape id="Picture_x0020_1" o:spid="_x0000_i1038" type="#_x0000_t75"
1194 style='width:300pt;height:187.5pt;visibility:visible;mso-wrap-style:square'>
1195 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png"
1196  o:title=""/>
1197</v:shape><![endif]--><![if !vml]><img border=0 width=400 height=250
1198src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png"
1199v:shapes="Picture_x0020_1"><![endif]></span></p>
1200
1201<p class=MsoNormal>At this point the data tree window will have several
1202entries; the highlighted one specifies the contents of the data window as <b
1203style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1204mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1205Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span><o:p></o:p></b></p>
1206
1207<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1208 id="_x0000_i1037" type="#_x0000_t75" style='width:472.5pt;height:388.5pt;
1209 visibility:visible;mso-wrap-style:square'>
1210 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image015.png"
1211  o:title=""/>
1212</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518
1213src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image015.png"
1214v:shapes="_x0000_i1037"><![endif]></span></p>
1215
1216<p class=MsoNormal><span style='mso-spacerun:yes'> </span>The plot window shows
1217the image; notice the elliptical shape of the powder diffraction rings due to
1218the 45 degree detector tilt. The blue <b style='mso-bidi-font-weight:normal'><span
1219style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1220mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1221minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span></b> marks the beam
1222location (which defaults to the image center); the calibration you will perform
1223here will find the correct placement for it. Also note that as the mouse is
1224moved across the plot the plot window status bar (at bottom of plot window)
1225shows the cursor position, as computed from the default (incorrect) calibration
1226values. These constants will be correctly determined after you finish the
1227calibration.</p>
1228
1229<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
1230style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_3"
1231 o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt;height:450pt;
1232 visibility:visible;mso-wrap-style:square'>
1233 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
1234  o:title=""/>
1235</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1236src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
1237v:shapes="Picture_x0020_3"><![endif]></span></p>
1238
1239<h1><span style='mso-spacerun:yes'> </span>Step 2: Edit image parameters</h1>
1240
1241<p class=MsoNormal>Note that, alas, very few image formats contain all of the
1242important metadata about the image, so it needs to be added manually. In this
1243case set the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1244"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1245minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>wavelength</span></b>
1246to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1247mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1248Calibri;mso-bidi-theme-font:minor-latin'>0.10798</span></b>. We will be
1249determining the calibration values of all the checked items. In this case
1250wavelength is known (‘<span class=SpellE>dep</span>’ is a correction for x-ray
1251penetration into the detector; it is only needed when the detector is close to
1252the sample). Under certain circumstances it may be useful to restrict the
1253calibration to fewer parameters (i.e. if distance is presumed to be “known”) in
1254which case you can uncheck some of the calibration parameters and use their
1255fixed values. It is also helpful to change the display of the image so that it
1256is easier to see the diffraction rings. Lowering the maximum intensity to
125710,000 to 20,000 counts will help (note that this can be done by moving the
1258slider, or by typing a value in the box and then clicking on another control or
1259pressing the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1260"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1261minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Enter</span></b>
1262or <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1263mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1264Calibri;mso-bidi-theme-font:minor-latin'>Tab</span></b> key). You may also wish
1265to select another color scheme using the <b style='mso-bidi-font-weight:normal'><span
1266style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1267mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1268minor-latin'>Color bar</span></b> selector. </p>
1269
1270<h1><span style='mso-spacerun:yes'> </span>Step 3: Calibrate</h1>
1271
1272<h3><span style='mso-spacerun:yes'> </span>First: </h3>
1273
1274<p class=MsoNormal><span style='mso-spacerun:yes'>   </span>Set the material
1275used as a sample in the box labeled <span class=SpellE><b style='mso-bidi-font-weight:
1276normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1277minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1278mso-bidi-theme-font:minor-latin'>Calibrant</span></b></span>; select <b
1279style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1280mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1281Calibri;mso-bidi-theme-font:minor-latin'>LaB6 SRM660a</span></b></p>
1282
1283<h3>Second: </h3>
1284
1285<p class=MsoNormal><span style='mso-spacerun:yes'>  </span><span
1286style='mso-spacerun:yes'> </span>Use the <b style='mso-bidi-font-weight:normal'><span
1287style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1288mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1289minor-latin'>Operations/Calibrate</span></b> menu item (note this menu is on
1290the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1291mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1292Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window or
1293for the Mac, the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1294"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1295minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Image
1296Controls</span></b> window must be active to place this into the system menu
1297bar). At this point the status line on the bottom of the <b style='mso-bidi-font-weight:
1298normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1299minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1300mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window changes with
1301a prompt to select points for calibration.</p>
1302
1303<h3>Third: </h3>
1304
1305<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>Use the left mouse
1306button to click on at least five locations on the innermost ring. As each point
1307is defined, a red &quot;<b style='mso-bidi-font-weight:normal'><span
1308style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1309mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1310minor-latin;color:red'>+</span></b>&quot; is added to the plot. You need not
1311hit the ring exactly as the code will search for the locally highest point in a
131240x40 pixel box. (On the Mac with a two or three button mouse, also use the
1313left mouse button, or with a standard Mac single-button mouse, use the regular
1314mouse button.)</p>
1315
1316<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1317 id="Picture_x0020_4" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:525pt;
1318 height:450pt;visibility:visible;mso-wrap-style:square'>
1319 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
1320  o:title=""/>
1321</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1322src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
1323v:shapes="Picture_x0020_4"><![endif]></span></p>
1324
1325<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>To remove a point
1326added in error click on that point with the right mouse button (on the Mac, if
1327you have a single-button mouse, hold the control key down and click). NB: it is
1328slightly better to pick points just inside the inner ring as GSAS-II will then
1329find the best point on that ring.</p>
1330
1331<h3><span style='mso-spacerun:yes'> </span>Fourth:</h3>
1332
1333<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>When done, press the
1334right mouse button well away from any points that have been added (on the Mac,
1335if you have a single-button mouse, hold the control key down and click). </p>
1336
1337<p class=MsoNormal>The calibration is then performed. First the rings are
1338located and an ellipse is optimized for each ring. The indexed rings are first
1339shown briefly in red as the calibration proceeds and center of each ellipse is
1340noted with a blue &quot;<b style='mso-bidi-font-weight:normal'><span
1341style='color:#4F81BD;mso-themecolor:accent1'>+</span></b>&quot;; these will
1342track in the direction of the tilt. When all rings have been fitted, the entire
1343ensemble of rings is refitted to the detector parameters and the rings are then
1344shown in blue. The beam position (blue “<span style='font-family:"Calibri",sans-serif;
1345mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1346Calibri;mso-bidi-theme-font:minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span>”)
1347is now correctly positioned.</p>
1348
1349<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
1350style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_9"
1351 o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt;height:450pt;
1352 visibility:visible;mso-wrap-style:square'>
1353 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
1354  o:title=""/>
1355</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1356src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
1357v:shapes="Picture_x0020_9"><![endif]></span><span
1358style='mso-spacerun:yes'> </span></p>
1359
1360<p class=MsoNormal>The derived calibration results are shown in the <b
1361style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1362mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1363Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window.</p>
1364
1365<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1366 id="Picture_x0020_16" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:472.5pt;
1367 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1368 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image016.png"
1369  o:title=""/>
1370</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518
1371src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image016.png"
1372v:shapes="Picture_x0020_16"><![endif]></span><span
1373style='mso-spacerun:yes'> </span></p>
1374
1375<p class=MsoNormal><span class=GramE>and</span> the console window shows
1376details of the fit.</p>
1377
1378<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1379 id="Picture_x0020_11" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:447.75pt;
1380 height:107.25pt;visibility:visible;mso-wrap-style:square'>
1381 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
1382  o:title=""/>
1383</v:shape><![endif]--><![if !vml]><img border=0 width=597 height=143
1384src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
1385v:shapes="Picture_x0020_11"><![endif]></span></p>
1386
1387<p class=MsoNormal>The <b style='mso-bidi-font-weight:normal'><span
1388style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1389mso-hansi-theme-font:minor-latin'>distance</span></b> is from the sample to the
1390plane containing the detector, <span class=SpellE><b style='mso-bidi-font-weight:
1391normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1392minor-latin;mso-hansi-theme-font:minor-latin'>det</span></b></span><b
1393style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1394mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-x</span></b>
1395&amp; <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
1396style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1397mso-hansi-theme-font:minor-latin'>det</span></b></span><b style='mso-bidi-font-weight:
1398normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1399minor-latin;mso-hansi-theme-font:minor-latin'>-y</span></b> is the incident
1400beam location on the image, <b style='mso-bidi-font-weight:normal'><span
1401style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1402mso-hansi-theme-font:minor-latin'>tilt</span></b> is the angle of detector
1403rotation from being normal to the incident beam and <b style='mso-bidi-font-weight:
1404normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1405minor-latin;mso-hansi-theme-font:minor-latin'>phi</span></b> is the rotation of
1406the detector tilt axis from the x-axis.<span style='mso-spacerun:yes'> 
1407</span>To see the actual points selected by the program, click on the <b
1408style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1409mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1410Calibri;mso-bidi-theme-font:minor-latin'>show ring picks?</span></b> <span
1411class=GramE>check</span> box </p>
1412
1413<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1414 id="Picture_x0020_8" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt;
1415 height:450pt;visibility:visible;mso-wrap-style:square'>
1416 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
1417  o:title=""/>
1418</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1419src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
1420v:shapes="Picture_x0020_8"><![endif]></span><span
1421style='mso-spacerun:yes'> </span><span style='color:#1F497D;mso-themecolor:
1422text2'><o:p></o:p></span></p>
1423
1424<p class=MsoNormal>When this is done, it sometimes occurs that the points
1425selected for the outermost rings are scattered between that and the next ring.
1426This can be repaired by changing the pixel search range to 10 and using the <b
1427style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1428mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1429Calibri;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b> menu
1430item. Also notice that the right edge of the image shows a ragged fit to the
1431rings because of an intensity falloff. This can be removed by placing a frame
1432mask about the “good” part of the pattern. Select the <b style='mso-bidi-font-weight:
1433normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1434minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> GSAS-II data
1435tree item.</p>
1436
1437<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1438 id="Picture_x0020_12" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:337.5pt;
1439 height:99.75pt;visibility:visible;mso-wrap-style:square'>
1440 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image009.png"
1441  o:title=""/>
1442</v:shape><![endif]--><![if !vml]><img border=0 width=450 height=133
1443src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image009.png"
1444v:shapes="Picture_x0020_12"><![endif]></span></p>
1445
1446<p class=MsoNormal>The instruction in the status bar of this frame tells you
1447how to enter a frame: first select the plot window, then press the ’<b
1448style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1449mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>F</span></b>’
1450key; that will “arm” the frame mask creator. Then select each corner of the
1451good part of the image in turn (I chose points with x=400 for the right edge)
1452with the left mouse button. After selecting the last point, close the frame
1453with a press of the right mouse button. As each point is selected a small green
1454‘+’ will be drawn on the plot connected with a green line to the previous
1455point. When you are done the image should look something like</p>
1456
1457<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1458 id="Picture_x0020_13" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt;
1459 height:450pt;visibility:visible;mso-wrap-style:square'>
1460 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image010.png"
1461  o:title=""/>
1462</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1463src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image010.png"
1464v:shapes="Picture_x0020_13"><![endif]></span><span
1465style='mso-spacerun:yes'> </span></p>
1466
1467<p class=MsoNormal>Mask points can be moved by carefully selecting and dragging
1468then with the left button down (you may need to zoom in to do this); the right
1469mouse button will delete it. The <b style='mso-bidi-font-weight:normal'><span
1470style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1471mso-hansi-theme-font:minor-latin'>Mask</span></b> data window will show the new
1472frame mask.</p>
1473
1474<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1475 id="Picture_x0020_14" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:337.5pt;
1476 height:135pt;visibility:visible;mso-wrap-style:square'>
1477 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image011.png"
1478  o:title=""/>
1479</v:shape><![endif]--><![if !vml]><img border=0 width=450 height=180
1480src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image011.png"
1481v:shapes="Picture_x0020_14"><![endif]></span></p>
1482
1483<p class=MsoNormal>Now go back to the <b style='mso-bidi-font-weight:normal'><span
1484style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1485mso-hansi-theme-font:minor-latin'>Image Controls</span></b> tree item and do <b
1486style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1487mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1488Calibri;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b>; a
1489better calibration will result.</p>
1490
1491<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1492 id="Picture_x0020_15" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:525pt;
1493 height:450pt;visibility:visible;mso-wrap-style:square'>
1494 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image012.png"
1495  o:title=""/>
1496</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1497src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image012.png"
1498v:shapes="Picture_x0020_15"><![endif]></span></p>
1499
1500<p class=MsoNormal>Notice that the frame defined the calibration region.</p>
1501
1502<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1503 id="Picture_x0020_17" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:472.5pt;
1504 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1505 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image017.png"
1506  o:title=""/>
1507</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518
1508src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image017.png"
1509v:shapes="Picture_x0020_17"><![endif]></span></p>
1510
1511<p class=MsoNormal>And notice the better fit obtained (smaller chi**2 and
1512smaller <span class=SpellE>esds</span>).</p>
1513
1514<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1515 id="Picture_x0020_18" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:447.75pt;
1516 height:98.25pt;visibility:visible;mso-wrap-style:square'>
1517 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image018.png"
1518  o:title=""/>
1519</v:shape><![endif]--><![if !vml]><img border=0 width=597 height=131
1520src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image018.png"
1521v:shapes="Picture_x0020_18"><![endif]></span></p>
1522
1523<p class=MsoNormal>In cases where particular types of detectors are placed
1524close to the sample (not the case here) and the diffraction pattern extends to
1525near the edges of the detector, the <b style='mso-bidi-font-weight:normal'><span
1526style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1527mso-hansi-theme-font:minor-latin'>Penetration</span></b> correction may need to
1528be refined. Just select the check box and do <b style='mso-bidi-font-weight:
1529normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1530minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1531mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b>, the result
1532should be &gt;0 for a reasonable correction. Close examination of the outer
1533rings will show a small shift in the calculated rings to better match the
1534observed ones. Assuming that these calibration results will be applied to other
1535images to be later read into the same GSAS-II project, click on <b
1536style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1537mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1538Calibri;mso-bidi-theme-font:minor-latin'>Use as default for all images</span></b>.
1539You may also save a copy of the calibration values to a file <span
1540style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1541mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1542minor-latin'>(<span class=SpellE><i style='mso-bidi-font-style:normal'>name</i><b
1543style='mso-bidi-font-weight:normal'>.imctrl</b></span></span>) with the <b
1544style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1545mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1546Calibri;mso-bidi-theme-font:minor-latin'>Operations/Save Controls</span></b>
1547menu item. To save the project, including the now-derived calibration
1548information, use the <b style='mso-bidi-font-weight:normal'><span
1549style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1550mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1551minor-latin'>File/Save</span> </b><b style='mso-bidi-font-weight:normal'><span
1552style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1553mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1554minor-latin'>Project</span></b><span style='font-family:"Calibri",sans-serif;
1555mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1556Calibri;mso-bidi-theme-font:minor-latin'> </span>menu item associated with the
1557data tree window; as this project has not been saved before the file save
1558dialog will need a file name. Don’t enter the extension; it will be set to “<b
1559style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1560mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1561Calibri;mso-bidi-theme-font:minor-latin'>.<span class=SpellE>gpx</span></span></b>”.</p>
1562
1563<h2>Next step: <span class=MsoHyperlink><span style='color:#0070C0'><a
1564href="Integration%20of%20area%20detector%20data%20in%20GSAS.htm"><u><span
1565style='color:black'>Integrate the Data</span></u></a></span></span></h2>
1566
1567</div>
1568
1569</body>
1570
1571</html>
Note: See TracBrowser for help on using the repository browser.