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413  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 1"/>
414  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 1"/>
415  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 1"/>
416  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 1"/>
417  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 1"/>
418  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 1"/>
419  <w:LsdException Locked="false" SemiHidden="true" Name="Revision"/>
420  <w:LsdException Locked="false" Priority="34" QFormat="true"
421   Name="List Paragraph"/>
422  <w:LsdException Locked="false" Priority="29" QFormat="true" Name="Quote"/>
423  <w:LsdException Locked="false" Priority="30" QFormat="true"
424   Name="Intense Quote"/>
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426  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 1"/>
427  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 1"/>
428  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 1"/>
429  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 1"/>
430  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 1"/>
431  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 1"/>
432  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 1"/>
433  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 2"/>
434  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 2"/>
435  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 2"/>
436  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 2"/>
437  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 2"/>
438  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 2"/>
439  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 2"/>
440  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 2"/>
441  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 2"/>
442  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 2"/>
443  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 2"/>
444  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 2"/>
445  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 2"/>
446  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 2"/>
447  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 3"/>
448  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 3"/>
449  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 3"/>
450  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 3"/>
451  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 3"/>
452  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 3"/>
453  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 3"/>
454  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 3"/>
455  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 3"/>
456  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 3"/>
457  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 3"/>
458  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 3"/>
459  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 3"/>
460  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 3"/>
461  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 4"/>
462  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 4"/>
463  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 4"/>
464  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 4"/>
465  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 4"/>
466  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 4"/>
467  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 4"/>
468  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 4"/>
469  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 4"/>
470  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 4"/>
471  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 4"/>
472  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 4"/>
473  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 4"/>
474  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 4"/>
475  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 5"/>
476  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 5"/>
477  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 5"/>
478  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 5"/>
479  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 5"/>
480  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 5"/>
481  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 5"/>
482  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 5"/>
483  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 5"/>
484  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 5"/>
485  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 5"/>
486  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 5"/>
487  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 5"/>
488  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 5"/>
489  <w:LsdException Locked="false" Priority="60" Name="Light Shading Accent 6"/>
490  <w:LsdException Locked="false" Priority="61" Name="Light List Accent 6"/>
491  <w:LsdException Locked="false" Priority="62" Name="Light Grid Accent 6"/>
492  <w:LsdException Locked="false" Priority="63" Name="Medium Shading 1 Accent 6"/>
493  <w:LsdException Locked="false" Priority="64" Name="Medium Shading 2 Accent 6"/>
494  <w:LsdException Locked="false" Priority="65" Name="Medium List 1 Accent 6"/>
495  <w:LsdException Locked="false" Priority="66" Name="Medium List 2 Accent 6"/>
496  <w:LsdException Locked="false" Priority="67" Name="Medium Grid 1 Accent 6"/>
497  <w:LsdException Locked="false" Priority="68" Name="Medium Grid 2 Accent 6"/>
498  <w:LsdException Locked="false" Priority="69" Name="Medium Grid 3 Accent 6"/>
499  <w:LsdException Locked="false" Priority="70" Name="Dark List Accent 6"/>
500  <w:LsdException Locked="false" Priority="71" Name="Colorful Shading Accent 6"/>
501  <w:LsdException Locked="false" Priority="72" Name="Colorful List Accent 6"/>
502  <w:LsdException Locked="false" Priority="73" Name="Colorful Grid Accent 6"/>
503  <w:LsdException Locked="false" Priority="19" QFormat="true"
504   Name="Subtle Emphasis"/>
505  <w:LsdException Locked="false" Priority="21" QFormat="true"
506   Name="Intense Emphasis"/>
507  <w:LsdException Locked="false" Priority="31" QFormat="true"
508   Name="Subtle Reference"/>
509  <w:LsdException Locked="false" Priority="32" QFormat="true"
510   Name="Intense Reference"/>
511  <w:LsdException Locked="false" Priority="33" QFormat="true" Name="Book Title"/>
512  <w:LsdException Locked="false" Priority="37" SemiHidden="true"
513   UnhideWhenUsed="true" Name="Bibliography"/>
514  <w:LsdException Locked="false" Priority="39" SemiHidden="true"
515   UnhideWhenUsed="true" QFormat="true" Name="TOC Heading"/>
516  <w:LsdException Locked="false" Priority="41" Name="Plain Table 1"/>
517  <w:LsdException Locked="false" Priority="42" Name="Plain Table 2"/>
518  <w:LsdException Locked="false" Priority="43" Name="Plain Table 3"/>
519  <w:LsdException Locked="false" Priority="44" Name="Plain Table 4"/>
520  <w:LsdException Locked="false" Priority="45" Name="Plain Table 5"/>
521  <w:LsdException Locked="false" Priority="40" Name="Grid Table Light"/>
522  <w:LsdException Locked="false" Priority="46" Name="Grid Table 1 Light"/>
523  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2"/>
524  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3"/>
525  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4"/>
526  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark"/>
527  <w:LsdException Locked="false" Priority="51" Name="Grid Table 6 Colorful"/>
528  <w:LsdException Locked="false" Priority="52" Name="Grid Table 7 Colorful"/>
529  <w:LsdException Locked="false" Priority="46"
530   Name="Grid Table 1 Light Accent 1"/>
531  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 1"/>
532  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 1"/>
533  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 1"/>
534  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 1"/>
535  <w:LsdException Locked="false" Priority="51"
536   Name="Grid Table 6 Colorful Accent 1"/>
537  <w:LsdException Locked="false" Priority="52"
538   Name="Grid Table 7 Colorful Accent 1"/>
539  <w:LsdException Locked="false" Priority="46"
540   Name="Grid Table 1 Light Accent 2"/>
541  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 2"/>
542  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 2"/>
543  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 2"/>
544  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 2"/>
545  <w:LsdException Locked="false" Priority="51"
546   Name="Grid Table 6 Colorful Accent 2"/>
547  <w:LsdException Locked="false" Priority="52"
548   Name="Grid Table 7 Colorful Accent 2"/>
549  <w:LsdException Locked="false" Priority="46"
550   Name="Grid Table 1 Light Accent 3"/>
551  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 3"/>
552  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 3"/>
553  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 3"/>
554  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 3"/>
555  <w:LsdException Locked="false" Priority="51"
556   Name="Grid Table 6 Colorful Accent 3"/>
557  <w:LsdException Locked="false" Priority="52"
558   Name="Grid Table 7 Colorful Accent 3"/>
559  <w:LsdException Locked="false" Priority="46"
560   Name="Grid Table 1 Light Accent 4"/>
561  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 4"/>
562  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 4"/>
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564  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 4"/>
565  <w:LsdException Locked="false" Priority="51"
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567  <w:LsdException Locked="false" Priority="52"
568   Name="Grid Table 7 Colorful Accent 4"/>
569  <w:LsdException Locked="false" Priority="46"
570   Name="Grid Table 1 Light Accent 5"/>
571  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 5"/>
572  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 5"/>
573  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 5"/>
574  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 5"/>
575  <w:LsdException Locked="false" Priority="51"
576   Name="Grid Table 6 Colorful Accent 5"/>
577  <w:LsdException Locked="false" Priority="52"
578   Name="Grid Table 7 Colorful Accent 5"/>
579  <w:LsdException Locked="false" Priority="46"
580   Name="Grid Table 1 Light Accent 6"/>
581  <w:LsdException Locked="false" Priority="47" Name="Grid Table 2 Accent 6"/>
582  <w:LsdException Locked="false" Priority="48" Name="Grid Table 3 Accent 6"/>
583  <w:LsdException Locked="false" Priority="49" Name="Grid Table 4 Accent 6"/>
584  <w:LsdException Locked="false" Priority="50" Name="Grid Table 5 Dark Accent 6"/>
585  <w:LsdException Locked="false" Priority="51"
586   Name="Grid Table 6 Colorful Accent 6"/>
587  <w:LsdException Locked="false" Priority="52"
588   Name="Grid Table 7 Colorful Accent 6"/>
589  <w:LsdException Locked="false" Priority="46" Name="List Table 1 Light"/>
590  <w:LsdException Locked="false" Priority="47" Name="List Table 2"/>
591  <w:LsdException Locked="false" Priority="48" Name="List Table 3"/>
592  <w:LsdException Locked="false" Priority="49" Name="List Table 4"/>
593  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark"/>
594  <w:LsdException Locked="false" Priority="51" Name="List Table 6 Colorful"/>
595  <w:LsdException Locked="false" Priority="52" Name="List Table 7 Colorful"/>
596  <w:LsdException Locked="false" Priority="46"
597   Name="List Table 1 Light Accent 1"/>
598  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 1"/>
599  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 1"/>
600  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 1"/>
601  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 1"/>
602  <w:LsdException Locked="false" Priority="51"
603   Name="List Table 6 Colorful Accent 1"/>
604  <w:LsdException Locked="false" Priority="52"
605   Name="List Table 7 Colorful Accent 1"/>
606  <w:LsdException Locked="false" Priority="46"
607   Name="List Table 1 Light Accent 2"/>
608  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 2"/>
609  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 2"/>
610  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 2"/>
611  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 2"/>
612  <w:LsdException Locked="false" Priority="51"
613   Name="List Table 6 Colorful Accent 2"/>
614  <w:LsdException Locked="false" Priority="52"
615   Name="List Table 7 Colorful Accent 2"/>
616  <w:LsdException Locked="false" Priority="46"
617   Name="List Table 1 Light Accent 3"/>
618  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 3"/>
619  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 3"/>
620  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 3"/>
621  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 3"/>
622  <w:LsdException Locked="false" Priority="51"
623   Name="List Table 6 Colorful Accent 3"/>
624  <w:LsdException Locked="false" Priority="52"
625   Name="List Table 7 Colorful Accent 3"/>
626  <w:LsdException Locked="false" Priority="46"
627   Name="List Table 1 Light Accent 4"/>
628  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 4"/>
629  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 4"/>
630  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 4"/>
631  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 4"/>
632  <w:LsdException Locked="false" Priority="51"
633   Name="List Table 6 Colorful Accent 4"/>
634  <w:LsdException Locked="false" Priority="52"
635   Name="List Table 7 Colorful Accent 4"/>
636  <w:LsdException Locked="false" Priority="46"
637   Name="List Table 1 Light Accent 5"/>
638  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 5"/>
639  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 5"/>
640  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 5"/>
641  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 5"/>
642  <w:LsdException Locked="false" Priority="51"
643   Name="List Table 6 Colorful Accent 5"/>
644  <w:LsdException Locked="false" Priority="52"
645   Name="List Table 7 Colorful Accent 5"/>
646  <w:LsdException Locked="false" Priority="46"
647   Name="List Table 1 Light Accent 6"/>
648  <w:LsdException Locked="false" Priority="47" Name="List Table 2 Accent 6"/>
649  <w:LsdException Locked="false" Priority="48" Name="List Table 3 Accent 6"/>
650  <w:LsdException Locked="false" Priority="49" Name="List Table 4 Accent 6"/>
651  <w:LsdException Locked="false" Priority="50" Name="List Table 5 Dark Accent 6"/>
652  <w:LsdException Locked="false" Priority="51"
653   Name="List Table 6 Colorful Accent 6"/>
654  <w:LsdException Locked="false" Priority="52"
655   Name="List Table 7 Colorful Accent 6"/>
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1126<div class=WordSection1>
1127
1128<p class=MsoNormal><span class=Heading1Char><span style='font-size:24.0pt'>Calibration
1129of an area detector in GSAS-II</span></span><b><span style='font-size:14.0pt;
1130color:#365F91;mso-themecolor:accent1;mso-themeshade:191'><o:p></o:p></span></b></p>
1131
1132<p class=MsoNormal>In this tutorial, data collected with a Perkin-Elmer area
1133detector at APS 11-ID-C with a wavelength 0.10798 A, where the detector was intentionally
1134tilted at 45 degrees, are used. Note that menu entries are listed in bold face
1135below as <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1136mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1137Calibri;mso-bidi-theme-font:minor-latin'>Help/About GSAS-II</span></b>, which
1138lists first the name of the menu (here <b style='mso-bidi-font-weight:normal'><span
1139style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1140mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1141minor-latin'>Help</span></b>) and second the name of the entry in the menu
1142(here <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
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1144Calibri;mso-bidi-theme-font:minor-latin'>About GSAS-II</span></b>).</p>
1145
1146<p class=MsoNormal>If you have not done so already, <u><span style='color:#0070C0'><a
1147href="Starting%20GSAS.htm"><span style='color:windowtext;text-decoration:none;
1148text-underline:none'>start GSAS-II</span></a></span></u>.</p>
1149
1150<h1>Step 1: read in the data file</h1>
1151
1152<p class=MsoNormal><span style='mso-spacerun:yes'> </span>Use the <b
1153style='mso-bidi-font-weight:normal'>Data/Read image data</b> menu item to read
1154the data file into the current GSAS-II project. </p>
1155
1156<p class=MsoNormal><span style='mso-spacerun:yes'> </span></p>
1157
1158<p class=MsoNormal>A file selection dialog will be shown; its appearance will depend
1159on your OS. Change the search directory to <b style='mso-bidi-font-weight:normal'><span
1160style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1161mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1162minor-latin'>/Exercises/images</span></b> and then select the file </p>
1163
1164<p class=MsoNormal><b style='mso-bidi-font-weight:normal'><span
1165style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1166mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1167minor-latin'>La_hex_+45deg-00015.tif</span></b> and press <b style='mso-bidi-font-weight:
1168normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1169minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1170mso-bidi-theme-font:minor-latin'>Open</span></b>.<span style='mso-no-proof:
1171yes'> <o:p></o:p></span></p>
1172
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1197</v:shape><![endif]--><![if !vml]><img border=0 width=400 height=250
1198src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image001.png"
1199v:shapes="Picture_x0020_1"><![endif]></span></p>
1200
1201<p class=MsoNormal>At this point the data tree window will have several
1202entries; the highlighted one specifies the contents of the data window as <b
1203style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1204mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1205Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span><o:p></o:p></b></p>
1206
1207<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1208 id="_x0000_i1037" type="#_x0000_t75" style='width:472.5pt;height:388.5pt;
1209 visibility:visible;mso-wrap-style:square'>
1210 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image015.png"
1211  o:title=""/>
1212</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518
1213src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image015.png"
1214v:shapes="_x0000_i1037"><![endif]></span></p>
1215
1216<p class=MsoNormal><span style='mso-spacerun:yes'> </span>The plot window shows
1217the image; notice the elliptical shape of the powder diffraction rings due to
1218the 45 degree detector tilt. The blue <b style='mso-bidi-font-weight:normal'><span
1219style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1220mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1221minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span></b> marks the beam
1222location (which defaults to the image center); the calibration you will perform
1223here will find the correct placement for it. Also note that as the mouse is
1224moved across the plot the plot window status bar (at bottom of plot window)
1225shows the cursor position, as computed from the default (incorrect) calibration
1226values. These constants will be correctly determined after you finish the
1227calibration.</p>
1228
1229<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
1230style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_3"
1231 o:spid="_x0000_i1036" type="#_x0000_t75" style='width:525pt;height:450pt;
1232 visibility:visible;mso-wrap-style:square'>
1233 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
1234  o:title=""/>
1235</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1236src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image003.png"
1237v:shapes="Picture_x0020_3"><![endif]></span></p>
1238
1239<h1><span style='mso-spacerun:yes'> </span>Step 2: Edit image parameters</h1>
1240
1241<p class=MsoNormal>Note that, alas, very few image formats contain all of the
1242important metadata about the image, so it needs to be added manually. In this
1243case set the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1244"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1245minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>wavelength</span></b>
1246to <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1247mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1248Calibri;mso-bidi-theme-font:minor-latin'>0.10798</span></b>. We will be
1249determining the calibration values of all the checked items. In this case
1250wavelength is known (‘<span class=SpellE>dep</span>’ is a correction for x-ray
1251penetration into the detector; it is only needed when the detector is close to
1252the sample). Under certain circumstances it may be useful to restrict the
1253calibration to fewer parameters (i.e. if distance is presumed to be “known”) in
1254which case you can uncheck some of the calibration parameters and use their
1255fixed values. It is also helpful to change the display of the image so that it
1256is easier to see the diffraction rings. Lowering the maximum intensity to
125710,000 to 20,000 counts will help (note that this can be done by moving the
1258slider, or by typing a value in the box and then clicking on another control or
1259pressing the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1260"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1261minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Enter</span></b>
1262or <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1263mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1264Calibri;mso-bidi-theme-font:minor-latin'>Tab</span></b> key). You may also wish
1265to select another color scheme using the <b style='mso-bidi-font-weight:normal'><span
1266style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1267mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1268minor-latin'>Color bar</span></b> selector. </p>
1269
1270<h1><span style='mso-spacerun:yes'> </span>Step 3: Calibrate</h1>
1271
1272<h3><span style='mso-spacerun:yes'> </span>First: </h3>
1273
1274<p class=MsoNormal><span style='mso-spacerun:yes'>   </span>Set the material
1275used as a sample in the box labeled <span class=SpellE><b style='mso-bidi-font-weight:
1276normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1277minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1278mso-bidi-theme-font:minor-latin'>Calibrant</span></b></span>; select <b
1279style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1280mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1281Calibri;mso-bidi-theme-font:minor-latin'>LaB6 SRM660a</span></b></p>
1282
1283<h3>Second: </h3>
1284
1285<p class=MsoNormal><span style='mso-spacerun:yes'>  </span><span
1286style='mso-spacerun:yes'> </span>Use the <b style='mso-bidi-font-weight:normal'><span
1287style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1288mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1289minor-latin'>Operations/Calibrate</span></b> menu item (note this menu is on
1290the <b style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1291mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1292Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window or
1293for the Mac, the <b style='mso-bidi-font-weight:normal'><span style='font-family:
1294"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:
1295minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:minor-latin'>Image
1296Controls</span></b> window must be active to place this into the system menu
1297bar). At this point the status line on the bottom of the <b style='mso-bidi-font-weight:
1298normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1299minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1300mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window changes with
1301a prompt to select points for calibration.</p>
1302
1303<h3>Third: </h3>
1304
1305<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>Use the left mouse
1306button to click on at least five locations on the innermost ring. As each point
1307is defined, a red &quot;<b style='mso-bidi-font-weight:normal'><span
1308style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1309mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1310minor-latin;color:red'>+</span></b>&quot; is added to the plot. You need not
1311hit the ring exactly as the code will search for the locally highest point in a
131240x40 pixel box. (On the Mac with a two or three button mouse, also use the
1313left mouse button, or with a standard Mac single-button mouse, use the regular
1314mouse button.)</p>
1315
1316<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1317 id="Picture_x0020_4" o:spid="_x0000_i1035" type="#_x0000_t75" style='width:525pt;
1318 height:450pt;visibility:visible;mso-wrap-style:square'>
1319 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
1320  o:title=""/>
1321</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1322src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image004.png"
1323v:shapes="Picture_x0020_4"><![endif]></span></p>
1324
1325<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>To remove a point
1326added in error click on that point with the right mouse button (on the Mac, if
1327you have a single-button mouse, hold the control key down and click). NB: it is
1328slightly better to pick points just inside the inner ring as GSAS-II will then
1329find the best point on that ring.</p>
1330
1331<h3><span style='mso-spacerun:yes'> </span>Fourth:</h3>
1332
1333<p class=MsoNormal><span style='mso-spacerun:yes'>  </span>When done, press the
1334right mouse button well away from any points that have been added (on the Mac,
1335if you have a single-button mouse, hold the control key down and click). </p>
1336
1337<p class=MsoNormal>The calibration is then performed. First the rings are
1338located and an ellipse is optimized for each ring. The indexed rings are first
1339shown briefly in red as the calibration proceeds and center of each ellipse is
1340noted with a blue &quot;<b style='mso-bidi-font-weight:normal'><span
1341style='color:#4F81BD;mso-themecolor:accent1'>+</span></b>&quot;; these will
1342track in the direction of the tilt. When all rings have been fitted, the entire
1343ensemble of rings is refitted to the detector parameters and the rings are then
1344shown in blue. The beam position (blue “<span style='font-family:"Calibri",sans-serif;
1345mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1346Calibri;mso-bidi-theme-font:minor-latin;color:#4F81BD;mso-themecolor:accent1'>X</span>”)
1347is now correctly positioned.</p>
1348
1349<p class=MsoNormal><span style='mso-spacerun:yes'> </span><span
1350style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape id="Picture_x0020_9"
1351 o:spid="_x0000_i1034" type="#_x0000_t75" style='width:525pt;height:450pt;
1352 visibility:visible;mso-wrap-style:square'>
1353 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
1354  o:title=""/>
1355</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1356src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image005.png"
1357v:shapes="Picture_x0020_9"><![endif]></span><span
1358style='mso-spacerun:yes'> </span></p>
1359
1360<p class=MsoNormal>The derived calibration results are shown in the <b
1361style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1362mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1363Calibri;mso-bidi-theme-font:minor-latin'>Image Controls</span></b> window.</p>
1364
1365<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1366 id="Picture_x0020_16" o:spid="_x0000_i1033" type="#_x0000_t75" style='width:472.5pt;
1367 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1368 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image016.png"
1369  o:title=""/>
1370</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518
1371src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image016.png"
1372v:shapes="Picture_x0020_16"><![endif]></span><span
1373style='mso-spacerun:yes'> </span></p>
1374
1375<p class=MsoNormal><span class=GramE>and</span> the console window shows
1376details of the fit.</p>
1377
1378<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1379 id="Picture_x0020_11" o:spid="_x0000_i1032" type="#_x0000_t75" style='width:447.75pt;
1380 height:107.25pt;visibility:visible;mso-wrap-style:square'>
1381 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
1382  o:title=""/>
1383</v:shape><![endif]--><![if !vml]><img border=0 width=597 height=143
1384src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image007.png"
1385v:shapes="Picture_x0020_11"><![endif]></span></p>
1386
1387<p class=MsoNormal>The <b style='mso-bidi-font-weight:normal'><span
1388style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1389mso-hansi-theme-font:minor-latin'>distance</span></b> is from the sample to the
1390plane containing the detector, <span class=SpellE><b style='mso-bidi-font-weight:
1391normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1392minor-latin;mso-hansi-theme-font:minor-latin'>det</span></b></span><b
1393style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1394mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>-x</span></b>
1395&amp; <span class=SpellE><b style='mso-bidi-font-weight:normal'><span
1396style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1397mso-hansi-theme-font:minor-latin'>det</span></b></span><b style='mso-bidi-font-weight:
1398normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1399minor-latin;mso-hansi-theme-font:minor-latin'>-y</span></b> is the incident
1400beam location on the image, <b style='mso-bidi-font-weight:normal'><span
1401style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1402mso-hansi-theme-font:minor-latin'>tilt</span></b> is the angle of detector
1403rotation from being normal to the incident beam and <b style='mso-bidi-font-weight:
1404normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1405minor-latin;mso-hansi-theme-font:minor-latin'>phi</span></b> is the rotation of
1406the detector tilt axis from the x-axis.<span style='mso-spacerun:yes'> 
1407</span>To see the actual points selected by the program, click on the <b
1408style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1409mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1410Calibri;mso-bidi-theme-font:minor-latin'>show ring picks?</span></b> <span
1411class=GramE>check</span> box </p>
1412
1413<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1414 id="Picture_x0020_8" o:spid="_x0000_i1031" type="#_x0000_t75" style='width:525pt;
1415 height:450pt;visibility:visible;mso-wrap-style:square'>
1416 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
1417  o:title=""/>
1418</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1419src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image008.png"
1420v:shapes="Picture_x0020_8"><![endif]></span><span
1421style='mso-spacerun:yes'> </span><span style='color:#1F497D;mso-themecolor:
1422text2'><o:p></o:p></span></p>
1423
1424<p class=MsoNormal>When this is done, it sometimes occurs that the points
1425selected for the outermost rings are scattered between that and the next ring.
1426This can be repaired by changing the pixel search range to 10 and using the <b
1427style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1428mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1429Calibri;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b> menu
1430item. Also notice that the right edge of the image shows a ragged fit to the
1431rings because of an intensity falloff. This can be removed by placing a frame
1432mask about the “good” part of the pattern. Select the <b style='mso-bidi-font-weight:
1433normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1434minor-latin;mso-hansi-theme-font:minor-latin'>Masks</span></b> GSAS-II data
1435tree item.</p>
1436
1437<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1438 id="Picture_x0020_12" o:spid="_x0000_i1030" type="#_x0000_t75" style='width:337.5pt;
1439 height:99.75pt;visibility:visible;mso-wrap-style:square'>
1440 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image009.png"
1441  o:title=""/>
1442</v:shape><![endif]--><![if !vml]><img border=0 width=450 height=133
1443src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image009.png"
1444v:shapes="Picture_x0020_12"><![endif]></span></p>
1445
1446<p class=MsoNormal>The instruction in the status bar of this frame tells you
1447how to enter a frame: first select the plot window, then press the ’<b
1448style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1449mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin'>F</span></b>’
1450key; that will “arm” the frame mask creator. Then select each corner of the
1451good part of the image in turn (I chose points with x=400 for the right edge)
1452with the left mouse button. After selecting the last point, close the frame
1453with a press of the right mouse button. As each point is selected a small green
1454‘+’ will be drawn on the plot connected with a green line to the previous
1455point. When you are done the image should look something like</p>
1456
1457<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1458 id="Picture_x0020_13" o:spid="_x0000_i1029" type="#_x0000_t75" style='width:525pt;
1459 height:450pt;visibility:visible;mso-wrap-style:square'>
1460 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image010.png"
1461  o:title=""/>
1462</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1463src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image010.png"
1464v:shapes="Picture_x0020_13"><![endif]></span><span
1465style='mso-spacerun:yes'> </span></p>
1466
1467<p class=MsoNormal>Mask points can be moved by carefully selecting and dragging
1468then with the left button down (you may need to zoom in to do this); the right
1469mouse button will delete it. The <b style='mso-bidi-font-weight:normal'><span
1470style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1471mso-hansi-theme-font:minor-latin'>Mask</span></b> data window will show the new
1472frame mask.</p>
1473
1474<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1475 id="Picture_x0020_14" o:spid="_x0000_i1028" type="#_x0000_t75" style='width:337.5pt;
1476 height:135pt;visibility:visible;mso-wrap-style:square'>
1477 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image011.png"
1478  o:title=""/>
1479</v:shape><![endif]--><![if !vml]><img border=0 width=450 height=180
1480src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image011.png"
1481v:shapes="Picture_x0020_14"><![endif]></span></p>
1482
1483<p class=MsoNormal>Now go back to the <b style='mso-bidi-font-weight:normal'><span
1484style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1485mso-hansi-theme-font:minor-latin'>Image Controls</span></b> tree item and do <b
1486style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1487mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1488Calibri;mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b>; a
1489better calibration will result.</p>
1490
1491<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1492 id="Picture_x0020_15" o:spid="_x0000_i1027" type="#_x0000_t75" style='width:525pt;
1493 height:450pt;visibility:visible;mso-wrap-style:square'>
1494 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image012.png"
1495  o:title=""/>
1496</v:shape><![endif]--><![if !vml]><img border=0 width=700 height=600
1497src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image012.png"
1498v:shapes="Picture_x0020_15"><![endif]></span></p>
1499
1500<p class=MsoNormal>Notice that the frame defined the calibration region.</p>
1501
1502<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1503 id="Picture_x0020_17" o:spid="_x0000_i1026" type="#_x0000_t75" style='width:472.5pt;
1504 height:388.5pt;visibility:visible;mso-wrap-style:square'>
1505 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image017.png"
1506  o:title=""/>
1507</v:shape><![endif]--><![if !vml]><img border=0 width=630 height=518
1508src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image017.png"
1509v:shapes="Picture_x0020_17"><![endif]></span></p>
1510
1511<p class=MsoNormal>And notice the better fit obtained (smaller chi**2 and
1512smaller <span class=SpellE>esds</span>).</p>
1513
1514<p class=MsoNormal><span style='mso-no-proof:yes'><!--[if gte vml 1]><v:shape
1515 id="Picture_x0020_18" o:spid="_x0000_i1025" type="#_x0000_t75" style='width:447.75pt;
1516 height:98.25pt;visibility:visible;mso-wrap-style:square'>
1517 <v:imagedata src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image018.png"
1518  o:title=""/>
1519</v:shape><![endif]--><![if !vml]><img border=0 width=597 height=131
1520src="Calibration%20of%20an%20area%20detector%20in%20GSAS_files/image018.png"
1521v:shapes="Picture_x0020_18"><![endif]></span></p>
1522
1523<p class=MsoNormal>In cases where particular types of detectors are placed
1524close to the sample (not the case here) and the diffraction pattern extends to
1525near the edges of the detector, the <b style='mso-bidi-font-weight:normal'><span
1526style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1527mso-hansi-theme-font:minor-latin'>Penetration</span></b> correction may need to
1528be refined. Just select the check box and do <b style='mso-bidi-font-weight:
1529normal'><span style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:
1530minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;
1531mso-bidi-theme-font:minor-latin'>Operations/Recalibrate</span></b>, the result
1532should be &gt;0 for a reasonable correction. Close examination of the outer
1533rings will show a small shift in the calculated rings to better match the
1534observed ones. Assuming that these calibration results will be applied to other
1535images to be later read into the same GSAS-II project, click on <b
1536style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1537mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1538Calibri;mso-bidi-theme-font:minor-latin'>Use as default for all images</span></b>.
1539You may also save a copy of the calibration values to a file <span
1540style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1541mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1542minor-latin'>(<span class=SpellE><i style='mso-bidi-font-style:normal'>name</i><b
1543style='mso-bidi-font-weight:normal'>.imctrl</b></span></span>) with the <b
1544style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1545mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1546Calibri;mso-bidi-theme-font:minor-latin'>Operations/Save Controls</span></b>
1547menu item. To save the project, including the now-derived calibration
1548information, use the <b style='mso-bidi-font-weight:normal'><span
1549style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1550mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1551minor-latin'>File/Save</span> </b><b style='mso-bidi-font-weight:normal'><span
1552style='font-family:"Calibri",sans-serif;mso-ascii-theme-font:minor-latin;
1553mso-hansi-theme-font:minor-latin;mso-bidi-font-family:Calibri;mso-bidi-theme-font:
1554minor-latin'>Project</span></b><span style='font-family:"Calibri",sans-serif;
1555mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1556Calibri;mso-bidi-theme-font:minor-latin'> </span>menu item associated with the
1557data tree window; as this project has not been saved before the file save
1558dialog will need a file name. Don’t enter the extension; it will be set to “<b
1559style='mso-bidi-font-weight:normal'><span style='font-family:"Calibri",sans-serif;
1560mso-ascii-theme-font:minor-latin;mso-hansi-theme-font:minor-latin;mso-bidi-font-family:
1561Calibri;mso-bidi-theme-font:minor-latin'>.<span class=SpellE>gpx</span></span></b>”.</p>
1562
1563<h2>Next step: <span class=MsoHyperlink><span style='color:#0070C0'><a
1564href="Integration%20of%20area%20detector%20data%20in%20GSAS.htm"><u><span
1565style='color:black'>Integrate the Data</span></u></a></span></span></h2>
1566
1567</div>
1568
1569</body>
1570
1571</html>
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